9iPPR01/L d
2000 Main Street,
Huntington Beach, CA
92648
City of Huntington Beach
File #: 22- 481 MEETING DATE: 6/ 7/ 2022
REQUEST FOR HOUSING AUTHORITY ACTION
SUBMITTED TO: Honorable Chair and Board Members
SUBMITTED BY: Sean Joyce, Interim Executive Director VIA: Ursula Luna- Reynosa, Director of Community Development PREPARED BY: Ursula Luna- Reynosa, Director of Community Development Subject:
Authorize and direct the Executive Director to execute an Exclusive Negotiating Agreement with Jamboree Housing Corporation to establish an exclusive negotiating period to determine the feasibility of Developer' s acquisition of 17642 Beach Boulevard for a mixed- use project consisting of a homeless shelter, affordable housing and various ancillary uses IIC=1441.,vL Lc) li,Z!PZ)
Statement of Issue:
The Housing Authority Board is requested to authorize and direct the Executive Director to execute an Exclusive Negotiating Agreement ( the " Agreement") with Jamboree Housing Corporation ( the Developer") for the property located at 17642 Beach Boulevard ( the " Property"). The purpose of this Agreement is to establish a period during which the Developer may perform studies and investigations and other due diligence activities within the Property and other feasibility and financial analysis to determine the feasibility of Developer' s acquisition of the Property and the City and Developer shall exclusively negotiate with each other in an attempt to agree on the terms of an affordable housing agreement, including a ground lease, fee-simple acquisition, or other disposition an "Affordable Housing Agreement").
Financial Impact:
There is no financial impact associated with this request. If staff and the Developer agree to terms of an Affordable Housing Agreement, staff will return to the Housing Authority for consideration of such agreement and any fiscal impacts will be identified at that time.
Recommended Action:
Authorize and direct the City Manager to execute the "Exclusive Negotiating Agreement" with Jamboree Housing Corporation, in a form approved by the City Attorney.
Alternative Action( s):
Do not approve the recommended action.
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File #: 22- 481 MEETING DATE: 6/ 7/ 2022
Analysis:
Background
The Huntington Beach Housing Authority ( the " Housing Authority") was established in 2011 per Health & Safety Code Sections 34200 et. seq. for the purpose of addressing a shortage of safe and sanitary dwelling accommodations in the City available to persons of low income. In 2019 and 2020, the Housing Authority acquired two adjacent parcels for a total of 1.6 acres to facilitate an affordable housing project. Since acquisition, the Property has been improved with a temporary homeless shelter ( the " Navigation Center").
On March 22, 2022 a Request for Qualifications (" RFQ") ( attached as Exhibit B to the Agreement) was released soliciting qualification statements to identify qualified development partners to develop, finance, and manage a new mixed- use development consisting of a homeless shelter, a sobering center, support services ( physical and behavioral healthcare, housing navigation and employment), and transitional and low- income housing at various income levels.
The Property is located within the Neighborhood Boulevard segment of the Beach and Edinger Corridors Specific Plan (" BECSP"). This segment along Beach Boulevard ( Hwy 39) is characterized by a significant amount of ageing commercial strip development, including auto-oriented uses, such as car dealerships. Development types are dominated by one- story, single- loaded commercial buildings surrounded by surface parking lots with little landscaping or pedestrian amenities. The planning approach to this area is to facilitate long-term transition from strip retail to uses more focus on nearby populations, featuring development types that retain visibility to motorists on Beach Boulevard, while providing a more visually attractive and comfortable pedestrian environment.
Neighborhood- serving and hospital- serving retail and services, corner/ crossroads located retail, and office and office- medical are encouraged to take advantage of the proximity to the Huntington Beach Hospital and its related cluster of medical services. In-fill residential uses are also permitted throughout this segment.
Since acquiring the Site in 2020, the Housing Authority has worked with the City and County of Orange to facilitate the Navigation Center and implemented the Be Well Mobile Response program.
These accomplishments are a testament to the City Council's aspirations to address homelessness in a unique and meaningful way. The Housing Authority desires a development partner to facilitate in creating a distinct facility to support individuals from street to home. The goal of this facility is to provide space that allows the engagement of unhoused individuals and create a path from homelessness to housing; while addressing the underlying barriers that have prevented housing in the past. The desired continuum of services to be provided on site include a combination of shelter operations, a sobering center, behavioral and physical healthcare, housing navigation, and employment services.
Assessment of Qualifications
Respondents to the RFQ were asked to submit information in the following categories:
Organizational Structure
Firm' s Experience
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File #: 22- 481 MEETING DATE: 6/ 7/ 2022
Relevant Experience
Financial Capacity
Respondents were required to identify their development team and provide biographies for key development staff. In addition, they were required to provide a narrative about their development approach for this particular project.
The evaluation process was designed to select a respondent, not based on the least cost, rather the respondent with the best combination of attributes ( experience, financial capacity/ ability to secure funding, and successful partnerships with service providers). The Developer submitted a qualification statement ( attached as Exhibit C) that demonstrated strong partnerships, experience and financial capacity. The Developer has partnered with Mercy House and Be Well which already have successful partnerships with the City. Equally important, the Developer effectively communicated their desire to be a partner that is equally committed to assisting the City in making significant impacts toward the well- being of our most vulnerable community members.
Exclusive Negotiating Agreement
Staff is seeking Housing Authority authorization and direction for the Executive Director to execute the Agreement with the Developer for 360 days during which the Developer may perform studies and investigations and other due diligence activities within the Property and other feasibility and financial analysis to determine the feasibility of Developer' s acquisition of the Property and the City and Developer shall exclusively negotiate with each other in an attempt to agree on the terms of an affordable housing agreement, including a fee- simple acquisition, ground lease, or other disposition.
Approval of the Agreement does not obligate the Housing Authority to enter into an Affordable Housing Agreement or any other agreement with the Developer.
During the negotiating period the Developer will conduct due diligence to fully understand the condition of the Property and any constraints to development. Collaborative discussions between the City and Developer will occur related to design and cost of a potential development project, including long- term operating costs. The Developer will also explore funding sources and financing options.
Successful negotiations will conclude in agreed upon business terms to be incorporated into an Affordable Housing Agreement. Such agreement will be brought to the Housing Authority Board for consideration along with project details including concept design, operation plan, estimated total project cost for construction, projected costs for operation, sources of funds (include Housing Authority and City contributions), Developer' s responsibilities, etc.
Environmental Status:
Pursuant to CEQA Guidelines Section 15378( b)( 5), administrative activities of governments that will not result in direct or indirect physical changes in the environment do not constitute a project. If negotiations are successful an Affordable Housing Agreement will be brought forward for the Housing Authority's considerationandan environmentalassessmentwill beconductedat that time.
Strategic Plan Goal:
Economic Development & Housing
Homelessness Response
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File #: 22- 481 MEETING DATE: 6/ 7/ 2022
Attachment( s):
1. Exclusive Negotiating Agreement
2. Exclusive Negotiating Agreement Exhibits
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EXCLUSIVE NEGOTIATING AGREEMENT
THIS EXCLUSIVE NEGOTIATING AGREEMENT ( the " Agreement") is entered into as of June
1)'
U, 2022 ( the " Effective Date"), by and between the HUNTINGTON BEACH HOUSING AUTHORITY, a public body, corporate and politic (" Authority"), and JAMBOREE HOUSING CORPORATION, a California corporation (" Developer").
Authority and Developer may be individually referred to herein as a " Party" and collectively referred to herein as the " Parties".
RECITALS
The following recitals are a substantive part of this Agreement.
A. Authority is the owner of fee title to certain real property commonly described as 17642 Beach Boulevard, in the City of Huntington Beach (" City"), County of Orange, State of California, consisting of Assesor Parcel Numbers 167-472-08; and -09, shown on Exhibit A and incorporated by this reference ( the " Property"). The Property is approximately 1.6 acres located within the Beach and Edingers Corridor Specific Plan BECSP") — Affordable Housing Overlay and improved with a temporary homeless shelter.
B. Authority desires to explore the possibility of repurposing the Property and issued a Request for Qualifications for Real Estate Developers ( the " RFQ") on March 22, 2022, ( attached as Exhibit B) in order to identify a qualified development partner to develop, finance, and manage a new mixed-use development consisting of a permanent homeless shelter, a sobering center, support services ( physical and behavioral healthcare, housing navigation, and employment), and transitional and low- income housing at various income levels (a "Healing Center").
C. Developer is an experienced developer of affordable and supportive rental housing development. Developer submitted a response to the RFQ (attached as Exhibit C), including proposed service partners Mercy House, a homeless shelter, housing and supportive services provider and Be Well, a behavioral health treatment and services organization.
D. Authorityfoundthe Developerto be a qualifiedpartnerand communicated the Developer had been selected as the recommended developer in the RFQ process.
E. Developer is interested in negotiating with Authority for purposes of determining the feasibility, and potential terms, for Developer's acquisition of a leasehold or fee- simple interest in the Property.
F. The purpose of this Agreement is to establish a period during which the Developer may perform studies and investigations and other due diligence activities within the Property and other feasibility and financial analysis to determine the feasibility 882/ 020587- 0128
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of Developer's acquisition of the Property for a Healing Center and the Parties shall exclusively negotiate with each other in an attempt to agree on the terms of an affordable housing agreement, including a fee-simple acquisition, ground lease, or other disposition an " Affordable Housing Agreement").
NOW THEREFORE, the Parties mutually agree as follows:
1. Agreement to Negotiate in Good Faith. Authority and Developer agree that for the term of the " Negotiating Period" ( as defined in Section 2 hereof) each Party shall diligently and in good faith attempt to negotiate the terms of an Affordable Housing Agreement for consideration by the Authority. During the Negotiating Period, Authority agrees to negotiate exclusively with Developer, and not to negotiate with any other person or entity, with regard to the sale or other disposition of the Property.
2. Negotiating Period. The negotiating period ( the " Negotiating Period") shall be for a period of three hundred sixty (360) days, commencing on the Effective Date.
The Executive Director of Authority, or his or her designee, shall have the right, in his or her sole discretion, to extend the Negotiating Period for up to an additional one hundred eighty ( 180) days, resulting in a total potential Negotiating Period of up to Five Hundred Forty ( 540) days. Upon the expiration of the Negotiating Period, or upon the Parties' signing an Affordable Housing Agreement for the Property, this Agreement shall automatically terminate, without further written notice or action by either Party. Upon such automatic termination, the Parties acknowledge and agree that neither Party shall have any further rights or remedies as to the other, except as specifically set forth herein.
3. Due Diligence. During the Negotiating Period, Developer and its employees, contractors, agents, representatives, architects, engineers and consultants collectively, the " Developer Entities"), at Developer' s sole cost and expense, shall have the right to enter and inspect the Property, make surveys and conduct such soils, engineering, hazardous or toxic material, pollution, seismic or other tests, studies and investigation as Developer may require ( collectively, the " Inspections"), pursuant to the terms of this Section 3.
a) Developer shall cause the Inspections to be conducted during regular business hours ( 7: 00 a. m. to 6: 00 p. m., Monday through Friday) upon not less than twenty- four ( 48) hours' prior written notice to Authority. Authority may have a representative present at any Inspections of the Property. b) In conducting its Inspections at the Property, Developer and the Developer Entities shall: ( i) not damage any part of the Property ( other than invasive testing conducted in accordance with Sections 3( c) and ( d) below) or any personal property owned or held by any third party; ( ii) promptly repair any damage to the Property resulting from the entry by Developer or the Developer Entities or from any such Inspections; ( iii) comply with all applicable laws; and ( iv) not permit any liens to attach to the Property by reason of the exercise of Developer' s rights hereunder. c) Notwithstanding anything to the contrary in this Section 3, Developer 882/ 020587- 0128
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shall not undertake any invasive testing, including, without limitation, taking samples of any kind or type from the Property, without Authority' s prior written approval, which approval shall not be unreasonably withheld, conditioned, or delayed. d) Promptly upon completion of each Inspection, Developer shall cause the portion of the Property subject to such Inspection to be restored to the condition existing immediately prior to such Inspection, to the extent reasonably practicable.
Developer shall provide Authority, at no additional charge and without representation or warranty of any kind, with copies of non- proprietary reports prepared by third parties for Developer in connection with the Inspections within three ( 3) business days of Developer' s receipt of the same.
e) Developer hereby indemnifies, defends, and holds harmless Authority and City and Authority' s and City' s officers, officials, members, employees, directors, agents, representatives, contractors, and volunteers ( collectively, the "Authority and City and Authority and City Personnel"), and the Property, free and harmless from and against any and all claims, damages, liabilities, demands, injury, actions, liens, stop notices, losses, costs and expenses ( including without limitation reasonable attorneys' fees and court costs) to the extent arising from or as a result of the conducting of Inspections, except to the extent caused by an indemnified party' s active negligence, recklessness or intentional misconduct.
f) Developer' s obligations under this Section 3 shall survive the expiration or termination of this Agreement.
4. Insurance. Without limiting Developer' s indemnification obligations under this Agreement, Developer shall procure and maintain, at its sole cost and for the duration of this Agreement, insurance coverage as provided below, against all claims for injuries against personsor damagesto propertywhich mayarisefrom or in connectionwith the performance of the work hereunder by Developer and/ or the Developer Entities, including without limitation Developer' s conducting of the Inspections. In the event that Developer subcontracts any portion of the work, the contract between Developer and such subcontractor shall require the subcontractor to maintain the same types ( with the same endorsements) and amounts of insurance that Developer is required to maintain pursuant to this Section.
A. Commercial General Liability Insurance which affords coverage at least as broad as Insurance Services Office " occurrence" form CG 00 01 including completed operations and contractual liability, with limits of liability of not less than 1, 000, 000 per occurrence and $ 2,000, 000 annual aggregate for liability arising out of Developer' s performance of this Agreement, including without limitation Developer' s conducting of the Inspections. Such insurance shall be endorsed to:
1) Name the Authority/City and Authority/City Personnel as additional insureds for claims arising out of Developer' s performance of this Agreement, including without limitation Developer' s conducting of the Inspections.
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2) Provide that the insurance is primary and non- contributing with any other valid and collectible insurance or self- insurance available to Authority/ City.
B. Automobile Liability Insurance with a limit of liability of not less than $ 1, 000, 000 each occurrence and $ 1, 000, 000 annual aggregate. Such insurance shall include coverage for all " owned," " hired" and " non- owned" vehicles, or coverage for any auto." Such insurance shall be endorsed to:
1) Name the Authority/ City and City Personnel as additional insureds for claims arising out of Developer' s performance of this Agreement, including without limitation Developer' s conducting of the Inspections.
2) Provide that the insurance is primary and non- contributing with any other valid and collectible insurance or self- insurance available to Authority/ City.
C. Workers' Compensation Insurance in accordance with the Labor Code of California and covering all employees of Developer providing any service in the performance of this Agreement. Such insurance shall be endorsed to waive the insurer's right of subrogation against the Authority/ City Personnel.
D. Evidence of Insurance: Developer shall provide to Authority/ City a Certificate(s) of Insurance evidencing such coverage, together with copies of the required policyendorsements, no laterthanfive (5) businessdayspriorto commencementof any inspections and prior to the expiration of any policy. Statements on an insurance certificate will not be accepted in lieu of the actual endorsements required.
Coverage shall not be suspended, voided, cancelled, reduced in coverage or in limits, non-renewed, or materially changed for any reason, without thirty (30) days prior written notice thereof given by the insurer to Authority by U.S. mail, or by personal delivery, except for nonpayment of premiums, in which case ten ( 10) days prior notice shall be provided.
E. Acceptability of Insurers. Each policy shall be from a company with current A.M. Best's rating of A- VII or higher and authorized to do business in the State of California, or otherwise allowed to place insurance through surplus lines brokers under applicable provisions of the California Insurance Code or any federal law. Any other rating must be approved in writing by Authority.
5. No Predetermination of City Discretion. The Parties acknowledge and agreethat nothingin this Agreementin any respectdoes or shallbe construedto affect or prejudgethe exerciseof Authority/City's discretionconcerningthe considerationof an Affordable Housing Agreement. The Parties do not intend for this Agreement to be an Affordable HousingAgreement, developmentagreement, or other agreementfor the lease or other conveyance, or the development, of the Property. The Parties acknowledge and agree that they have not agreed uponthe essential terms of the subject 882/ 020587- 0128
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matter of a transaction, and that such essential terms will be the subject matter of further negotiations. The Parties acknowledge and agree that any final agreement, if an agreement is reached, would be in the form of an Affordable Housing Agreement, and any such Affordable Housing Agreement would not be effective until it has been considered and formally approved by the Huntington Beach Housing Authority Board of Directors and Developer, and thereafter has been executed by authorized representatives of each of the Parties. Notwithstanding anything in this Agreement to the contrary, Authority does not intend by this Agreement to commit to a definite course of action with respect to the Property, and Authority retains full discretion with respect to ( i) the Property, ii) an Affordable Housing Agreement, ( iii) any determination under the California Environmental Quality Act of 1970, Public Resources Code Section 21000, et seq.
CEQA") with respect to the consideration of an Affordable Housing Agreement and/ or any proposed development of the Property.
6. Costs and Expenses. Each Party shall be responsible for its own costs and expenses in connection with any activities and negotiations undertaken in connection with the performance of its obligations under this Agreement.
7. Lead Negotiators. The Executive Director, or his or her designee, shall be the lead negotiator for the Authority with respect to the subject matter of this Agreement.
The Chief Development Officer of Developer, or his or her designee, shall be the lead negotiator for Developer with respect to the subject matter of this Agreement.
8. Change in Developer. The qualifications of Developer are of particular interest to Authority. Consequently, with the exception of an " Affiliate" ( as defined below), no person or entity, whether a voluntary or involuntary successor of Developer, shall acquire any rights or powers under this Agreement, nor shall Developer assign all or any part of this Agreement, without the prior written approval of Authority. Any such approval by Authority may be granted, withheld or denied at Authority' s sole and absolute discretion. Any other purported transfer, voluntarily or by operation of law, shall be absolutely null and void and shall confer no rights whatsoever upon any purported assignee or transferee. As used in this Agreement, the term "Affiliate" means any person or entity directly or indirectly, through one or more intermediaries, controlling, controlled by or under common control with Developer. The term " control" as used in the immediately preceding sentence, means, with respect to a person or entity that is a corporation, the right to the exercise, directly or indirectly, of more than fifty percent ( 50%) of the voting rights attributable to the shares of the controlled corporation, and, with respect to a person or entity that is not a corporation, the possession, directly or indirectly, of the power to direct or cause the direction of the management or policies of the controlled person or entity.
9. Property Documents; Authority Cooperation. Within fifteen ( 15) days after the Effective Date, Authority shall provide or cause to be provided to Developer all documents relating to the physical or environmental condition of the Property (including, but not limited to, environmental, property physical condition, geological studies, engineering and structural analyses, and geotechnical reports and soil tests and analyses) to the extent reasonably known to be in the Authority' s or City' s possession. 882/ 020587- 0128
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10. Address for Notices. Any notices pursuant to this Agreement shall be in writing and delivered ( i) in person, ( ii) by reputable overnight delivery service that provides a receipt with the time and date of delivery, such as Federal Express, or ( iii) by United States Mail, certified or registered, postage prepaid, return receipt requested, to the following addresses:
To Authority: Huntington Beach Housing Authority
2000 Main Street
Huntington Beach, CA 92648
Attn.: Executive Director
With a copy to: City of Huntington Beach
2000 Main Street
Huntington Beach, CA 92648
Attn: City Attorney
To Developer: Jamboree Housing Corporation
17701 Cowan, Suite 200
Irvine, CA 92614
Attn: Laura Archuleta, CEO
With a copy to: Rutan & Tucker, LLP
18575 Jamboree Road
9th Floor
Irvine, CA 92612
Attn: Pat McCalla
Any Party may designate a different address for itself by notice similarly given.
Any notice, demand or document so given, delivered or made by United States mail, shall be deemed to have been given seventy-two (72) hours after the same is deposited in the United States mail as registered or certified mail, addressed as above provided, with postage thereon fully prepaid. Any notice, demand or document delivered by overnight delivery service shall be deemed complete upon actual delivery or attempted delivery, provided such attempted delivery is made on a business day. Any such notice, demand or document not given by registered or certified mail or by overnight delivery service as aforesaid shall be deemed to be given, delivered or made upon receipt of the same by the Party to whom the same is to be given or delivered.
11. Default. Failure by either Party to negotiate in good faith or to perform any other of its obligations as provided in this Agreement shall constitute an event of default under this Agreement. The non-defaulting Party shall give written notice of a default to the defaulting Party, specifying the nature of the default and the action required to cure the default. If the default remains uncured fifteen ( 15) days after the date of such notice, 882/ 020587- 0128
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the non-defaulting Party may exercise the remedies set forth in Section 12 of this Agreement.
12. Remedies for Breach of Agreement. In the event of an uncured default under this Agreement, the sole remedies of the non- defaulting Party shall be to ( a) terminate this Agreement, ( b) institute an action for specific performance of this Agreement, or ( c) institute legal action to recover actual damages for the default ( limited to actual, documented out-of- pocket costs incurred by the non-defaulting Party as a result of such default). Following the termination of this Agreement, neither Party shall have any further rights, remedies or obligations under this Agreement, except as specifically set forth herein. Neither Party shall have any liability to the other for monetary damages for failure to reach agreement on an Affordable Housing Agreement, and each Party hereby waives and releases any such rights or claims it may otherwise have at law or at equity. The Parties' rights and obligations under this Section 12 shall survive the expiration or termination of this Agreement.
13. Entire Agreement. This Agreement constitutes the entire understanding and agreement of the Parties, integrates all of the terms and conditions mentioned herein or incidental hereto, and supersedes all negotiations or previous agreements between the Parties or their predecessors in interest with respect to all or any part of the subject matter hereof.
14. Time of Essence. Time is of the essence of every portion of this Agreement in which time is a material part.
15. Agreement Does Not Constitute Development Approval. City and Authority reserve final discretion and approval as to any proposed development of the Property and any Affordable Housing Agreement and all proceedings and decisions in connection therewith. This Agreement shall not be construed as a grant of development rights or land use entitlements to construct a Healing Center or any other project on the Property. All design, architectural, and building plans for any proposed development shall be subject to the review and approval of City and any other Federal, State or local entity with jurisdiction over the Property and/ or proposed development. By its execution of this Agreement, Authority is not committing itself to or agreeing to undertake any disposition of the Property to Developer, or any other acts or activities requiring the subsequent independent exercise of discretion by City or any agency or department thereof.
16. Governing Law. This Agreement shall be construed in accordance with the internal laws of the State of California, without regard to conflict of law principles.
17. Amendments. This Agreement may not be altered, amended, changed, waived, terminated or modified in any respect or particular unless the same shall be in writing and signed by the Parties.
18. Implementation of Agreement. The Authority shall maintain authority to implement this Agreement through the Executive Director ( or his or her designee). The Executive Director shall have the authority to make approvals, waive provisions and/or 882/ 020587- 0128
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enter into certain amendments of or implementing agreements for this Agreement on behalf of Authority so long as such actions do not materially or substantially change the substantive business terms of this Agreement, or add to the costs incurred or to be incurred by Authority or City as specified herein. All other material and/ or substantive approvals, waivers, or amendments shall require the consideration, action and written consent of the Huntington Beach Housing Authority Board of Directors.
21. Real Estate Commissions. Each of the Parties represents and warrants to the other Party that no real estate commission, broker's fees, or finder's fees which may accrue by means of the acquisition of the Property is due to any person, firm or entity.
Authority shall indemnify, protect, defend and hold harmless Developer from any loss, liability, damage, cost, claim or expense (including reasonable attorneys' fees) incurred by reason of any broker fee, commission or finder's fee that is payable or alleged to be payable to any broker or finder which results from any act or agreement of Authority.
Developer shall indemnify, protect, defend and hold harmless Authority from any loss, liability, damage, cost, claim or expense (including reasonable attorneys' fees) incurred by reason of any broker fee, commission or finder's fee that is payable or alleged to be payable to any broker or finder which results from any act or agreement of Developer.
22. Conflict of Interest. No member, official or employee of Authority/ City having any conflict of interest, direct or indirect, related to this Agreement shall participate in any decision relating to this Agreement. The Parties represent and warrant that they do not have knowledge of any such conflict of interest.
23. Counterparts. This Agreement may be executed in counterparts, each of which shall be deemed an original, but which when taken together shall constitute one and the same instrument.
End of Agreement- Signature page follows]
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NOW THEREFORE, Authority and Developer have executed this Exclusive Negotiating Agreement as of the date first set forth above.
CITY:
HUNTINGTON BEACH HOUSING
AUTHORITY, a public body, corporate and
politic
By:
ATTEST:
Authority Secretary
APPROVED AS FORM:
ity Attorney ,/
DEVELOPER:
JAMBOREE HOUSING CORPORATION, a
California corporation
By:
Its:
By:
Its:
882/ 020587. 0128
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COtJNi ER' ART°
NOW THEREFORE, Authority and Developer have executed this Exclusive Negotiating Agreement as of the date first set forth above.
CITY:
HUNTINGTON BEACH HOUSING
AUTHORITY, a public body, corporate and
politic
By:
ATTEST:
Authority Secretary
APPROVED AS TO FORM:
City Attorney
DEVELOPER:
JAMBOREE HOUSING CORPORATION, a
California corporation
ByA-.I I
Its: Chief Development Officer
By. Georee5tam(May31,202215:42PDT1
Its: Chief Impact Officer
192/ 020587- 0128
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COUNTERPART 1040
EXHIBIT " A"
LEGAL DESCRIPTION OF PROPERTY
Real property located in the City of HuntingtonBeach, Countyof Orange, State of California, described as follows:
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EXHIBIT 1
LEGAL DESCRIPTION
PARCEL 1:
17642 BEACH BLVD
APN: 167- 472- 09
ALL THAT CERTAIN REAL PROPERTY SITUATED IN THE COUNTY OF ORANGE, STATE OF CALIFORNIA, DESCRIBED AS FOLLOWS:
LOT 7 OF TRACT 405, AS PER MAP RECORDED IN BOOK 16, PAGES 31 OF MISCELLANEOUS MAPS, IN THE OFFICE OF THE RECORDER OF SAID COUNTY.
PARCEL 2:
17631 CAMERON LANE
APN 167- 472- 08
ALL THAT CERTAIN REAL PROPERTY SITUATED IN THE CITY OF HUNTINGTON BEACH, COUNTY OF ORANGE, STATE OF CALIFORNIA, DESCRIBED AS FOLLOWS:
LOT 6 OF TRACT NO. 405, IN THE CITY OF HUNTINGTON BEACH, COUNTY OF ORANGE, STATE OF CALIFORNIA, AS PER MAP RECORDED IN BOOK 16, PAGE 31, OF MISCELLANEOUS MAPS, IN THE OFFICE OF THE COUNTY RECORDER OF SAID COUNTY.
PLOTTED EASEMENT
EXHIBIT " B"
REQUEST FOR QUALIFICATIONS
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T!NG
4- 1 y
GUNTVPi,
Heal * ing
Request for Qualifications
For Real Estate Developers
Release Date: March 22, 2022
About the City gof Huntington Beach
N
P Q
GTO,L Huntington Beach is located along the Southern California Coast of Orange County, 35 miles southi pRRAT 9F9 of LosAngelesand 90 milesnorth of SanDiego. Namedfor railroad magnateHenryHuntington U who orchestrated the City's development, the City is best known today for its 8.5 miles of uninterrupted beaches, excellent year-round weather, and a surf culture that draws 4 million v
cF FFegag \ oQz visitors annually. Beyond the shoreline, Huntington Beach is a full-service city with its own fire and COUNTyCPS. police departments, an extensive park and library system, robust investments in capital infrastructure, a diverse economic base, and an excellent education system.
About Huntington Beach Housing Authority
The Huntington Beach Housing Authority(" HBHA") was established in 2011 per Health & Safety Code Sections 34200 et. seq. for the purpose of addressing a shortage of safe and sanitary dwelling accommodations in the City available to persons of low income at rents they can afford. HBHA facilitates affordable housing by acquiring and disposing of real property and providing a source of funding to be leveragedwith other funding sources.TheCityof Huntington Beachcurrently hasa portfolio of approximately 3,000 deed restricted, affordable housing units.
In 2019 and 2020 HBHAacquired two adjacent parcels for a total site area of 1.6 acres to facilitate an affordable housing project. The property is located at 17642 Beach Boulevard (" Site"). Since acquisition, the Site has been improved with a temporary homeless shelter(" Navigation Center").
City of C Request for Qualificiations - Healing Center
Solicitation Purpose
HBHA is releasing a Request for Qualifications(" RFQ") to identify experienced developers interested in redeveloping Responsesto this RFQare due on April 21, 2022. Following receipt the Site. The purpose of this RFQ is to identify qualified of qualification statements, HBHAwill identify a shortlist of development partners to develop, finance, and manage a developers to interview. If an appropriate development partner is new mixed- use development consisting of a homeless identified after the interviews, HBHA will enter into an Exclusive shelter, a sobering center, support services( physical and Negotiation Agreement(" ENA")with the selected developer during behavioral healthcare, housing navigation, and which time specific terms and conditions of a multiple agreements employment), and transitional and low- income housing at including, but not limited to a disposition and affordable housing various income levels. The City currently has a shelter agreements. operator under contract for the Navigation Center and
presumes that they will operate the permanent shelter if it is completed during the term of their contract. Impoftant Through this RFQprocess, HBHAseeksto alert experienced
developers to the opportunity; assess developer Optional Sit- Tour March 28, 2022 at 2pm qualifications, capacity and interest in working with HBHA Virtual • Session April
and other service providers; and receive market feedback on the broader vision for the Site. Interested developers are RFQ Deadline A• ril 21, 2022 at • invited to participate in an optional site tour on March 28, 2022 at 2: 00pm and a virtual information session on April 8, 2022 at 10: 00am.
City of Beach -• Qualificiations - Healing Center
About the Navigation Center
TOTAL ' i YEAR TO DATE
The Navigation Center was developed as a temporary,
emergency shelter to support individuals experiencing 120 homelessness. It is comprised of a sprung tent
structure that can accommodate up to 174 beds as a
congregate facility. There are separate areas for men,
women, couples, and non- binary. Trailer facilities are 80 70
utilized for bathrooms/ showers, laundry, hot box
room, communal dining/ lounge, administrative office
space and private counseling rooms. The Navigation40 Total Housed:
Center also accommodates storage, a dog run, and December 2020 Gresent space for a mobile trailer for supportive service
providers to provide medical serviceson a weekly
basis. The Navigation Center opened its doors in Most People who experience homelessness are single adults
December of 2020. Due to the COVID- 19 pandemic,
National A[ liance to[ nd Homelessness
social distancing requirements have reduced full
capacity to allow for extra space in between beds.
Upon stabilization, the Navigation Center has
experienced an average of roughly 100 occupants
KK,
Meats Served:
daily, at the reduced capacity, and has placed 55 85, 082 individuals into housing or other options that have
EMS
kept them from returning to the streets.
1 Project Vision
The Site is located within the Neighborhood Boulevard segment of the Beach and Edinger Corridors Specific Plan (" BECSP"). This segment alongBeachBoulevard (Hwy39) ischaracterizedby a significantamount of agingcommercialstrip development, includingauto-oriented uses, such as car dealerships. Development types are dominated by one-story, single-loaded commercial buildings surrounded by surface parkinglotswith little landscapingor pedestrianamenities.Theplanningapproachto this areaisto facilitatelong-term transition from strip retail to uses more focused on nearby populations, featuring development types that retain visibility to motorists on Beach Boulevard, while providinga morevisuallyattractiveand comfortablepedestrianenvironment. Neighborhood-servingand hospital-servingretail and services, corner/crossroadslocatedretail, and officeand office-medicalare encouragedto takeadvantageof the proximityto the Huntington BeachHospitaland its relatedclusterof medicalservices. In fill residentialusesare alsopermitted throughout this segment.
Sinceacquiringthe Sitein 2020, HBHAhasworkedwith the Cityand Countyof Orangeto facilitatethe NavigationCenter. TheCityCouncil's aspiresto addresshomelessnessin aunique and meaningfulway.Throughthis RFQ, HBHAisseekinga developmentpartnerto facilitate creating a distinct facility to support individuals from street to home. The goal of this facility is to provide space that allows the engagement of unhousedindividualsandcreatea path from homelessnessto housing;while addressingthe underlyingbarriersthat haveprevented housingin the past.Thedesiredcontinuumof servicesto be providedon site includea combinationof shelteroperations, a sobering center, behavioral and physical healthcare, housing navigation, and employment services. A development partner that is equally committed to assisting the City in making significant impacts toward the well-being of our most vulnerable community members is desired.
TheCityiscurrentlyworkingwith anarchitecturalfirm to understandthe improvementsthat are necessaryto realizethe vision. Potential operating models for the non-residential space are being explored. HBHA could solicit an operator( s)for the non-residential space through a separate procurement; however, respondents are encouraged to partner with potential operators and urged to express that interest in their response and outline a strategy for tenanting the building. Preference will be conferred to respondents that have a demonstrated track record working with the desired types of service providers.
City of for
1 Additional Site Information
TheSiteis locatedat 17642BeachBoulevardand iscomprisedof two parcels, both controlled by HBHA, totaling 1.6 acresof land. Beach Boulevard is a State highway( Hwy 39) and is a High Quality Transit Corridor with the closest bus stop located within 800 feet of the Site.The Site is located within 2,000 feet of Huntington Beach Hospital and within 1,000 feet of a Federally Qualified Health Center( FQHC). It is also located just over a half a mile from afull service grocery store. The Site is bordered by a residential neighborhood ( to the east) and commercial uses to the north, south and west.
The Site is zoned Mixed- Use- Affordable Housing Overlay( SP14- Beach and Edinger Corridors Specific Plan). SP14 is a form- based code with prescriptive development standards and allows for a mix of commercial and residential uses.The Affordable Housing Overlay allows for by-right development( i. e. no discretionary public hearing) for projects that include at least 20% of the units affordable at no more than 60% Area Median Income(" AMI").
HBHA desires 100% of the units to be affordable at various income levels with all units at 60% AMI or less. It is HBHA' s desire that the housing units qualify as supportive housing, as defined in Section 65650 of the Government Code.
As part of due diligence for acquisition, various contaminants were found on site. A full site assessment for each parcel is included as Appendices A and B. The Orange County Health CareAgency served as the oversight agency for the Navigation Center project. Their site summary and recommendations are included as Appendix C.
For informational purposes only, a Site Density Test Fitwas conducted and is included as Appendix D.
AESCOhas been retained to prepare a soils report. This report is not available at the time of publication of this RFQ. A letter containing preliminary foundation recommendations is included as Appendix E.
City of
rM Scope of Work
HBHA, City, and Developer Roles
HBHA seeks to engage a vertical developer that would be responsible for entitlements and approvals, environmental assessments and testing, infrastructure, and community engagement related to the project. HBHA is open to that partner bringing on other developers for discrete components such as affordable housing, medical office, etc. HBHA encourages partnerships with service providers. The developer whether a singleentity or a team of individualdevelopersand serviceproviders)would alsobe responsiblefor projectdesign, securing financing, overseeing construction, leasing, and ongoing property and asset management related to the project.
HBHNs role will be the pro- rata contribution of the land for housing and securing additional, limited funding for the affordable housing. Any form of disposition of HBHA-owned land for non-residential use will be at fair- market value. HBHA is open to exploring multiple disposition and/ or partnership structures that suit the best development outcome, including but not limited to fee-simple, installment sale,joint venture or long-term ground lease.
The Citys role will be its pro-rata share of the capital and infrastructure costs associated with the shelter and will work to identify other public sources of funding for ongoing operations.
Respondents will be evaluated based on their experience leading complex mixed- use development( ideally in the space of affordable housing, homelessshelters, soberingcenters, and supportiveservices), securingentitlementsandfinancing, abilityto providea guarantee of completion, achievingdesignexcellencewhile promoting the objectivesof SP14, and demonstrated partnershipswith serviceproviders and community organizations.
City of for
rM RFQ Proposal Ev Iuat oi na
Project Timeline Information
RFQ Release Date March 22, 2022
HBHA intends to select a development
Q& A Period March 22- April 4, 2022
partner based on the most qualified entity
for this unique project. Statements of Optional Site Tour March 2$, 2022 Qualification will be evaluated and only the A & A Answers Posted April 6, 2022 most qualified entities will be invited for an Virtual Q & A Session April 8, 2022 interview. The most qualified respondents
will be gauged by their demonstrated RFQ Deadline April 21, 2022 technical and financial ability to carry out Shortlist Interviews April 29, 2022 similar development projects on time and Finalize ENA Term Sheet May 26, 2022 on budget, established relationships with
service providers, and understanding the
Approval of ENA by CC June 7, 2022
vision and objectives for the Site.
City of Request for Qualificiations
rM Submission Instructions
Respondents interested in serving as HBHA's development partner must submit the following information in the order prescribed below.
Eachsection should be separated by headings and clearly marked. Points will be deducted for failure to comply with submission instructions. Responsesshould be thorough and clearly organized using the structure below, yet be as brief as possible.
Section 1: Cover Letter and Contact Information
Include a cover letter that succinctly summarizes your team' s interest in the project. Identify the single point of contact with authority to make decisions( preferably executive level)for your organization with whom to communicate during the solicitation process, along with their contact information.
Section 2: Developer Qualifications& Experience
A. Organizational Structure: Indicate if the Respondent to this RFQwill be a single firm, joint venture or partnership. If ajoint venture or partnership, describe the organizational structure and legal framework by which the work would be carried out.
B. Firm's Expertise: Provide an overview of the Respondent's expertise and services provided and an overall description of its portfolio of projects. Discussyour team's experience developing mixed- use and mixed- income projects, including those done through public-private partnerships if applicable. Highlight any development experience in the Orange County/ LosAngeles region if applicable.
C. Relevant Experience: Provide up to 3 detailed examples of your experience developing and/ or operating mixed-use, mixed- income projects of similar size, scope, and character, with an emphasis on any projects that included affordable and mixed- income housing, homeless shelters, and social services.
City of C for
m i i n InstructionsrM Sub ss o Cont.
The following must be included for each project example:
Project name and location
Date of award of contract
Construction start and end dates( include phasing plan if applicable) Program description and uses, including residential, homeless shelter, medical, social services, etc.
Include gross square footage and unit counts. For residential, note market rate vs. affordable and identify AMI levels.
Other partners involved (other developers, non-profits, government partners, community orgs., etc.) D. Financing Structure:
Names of financing institutions, including lenders and equity provider and the true ownership of borrowing entities.
Anysubsidiesor tax-credit programsutilized, if applicable.
Any public financing utilized.
Project budget vs. final cost.
Include details of performance and completion guarantees, including parties at-risk.
E. Project References:
Include contact name, position, organization, phone number, and e-mail F. Financial Capacity Statement:
Provide evidence of your firm' s financial capacity to take on this project, including:
Information about recent closings.
Liquid capital or letter of credit, and letters of support from debt and/ or equity providers, etc.
City of for
rM Submission Instructions Cont.
Audited financials for the previous two years for the Respondent, if the identified developer and manager parties are related parties Related Team Members") with an operating history. In the case of a Respondent( a) with Related Team Members, but no operating history or( b) that is a joint venture of otherwise unrelated developer(s) and property manager(s), supply audited financials for the previoustwo yearsfor both the developerteam member(s)and the property managerteam member(s).The FinancialStatementsshould be emailedseparatelyand directlyto the City'stechnicaladvisor,Andria Martinezwith the NationalDevelopmentCouncil (NDC)at AMartinez@ndconline. org.
Note: Financial statements and related information will not be returned. After review and analysis, all financial statements will be shredded and destroyedprior to award of the subsequentcontract(s). NDCwill usethis information onlyto confirm that the entity isfinancially capable of completing the project and will advise HBHA on the strength of the financial capacity. This information will be used for no other purposesandwill remain confidentialto the extent permitted by law.
G. Past and Current Litigation Disclosure: Provide documentation of all litigation actions taken against your firm, or related parties, in the past5 years, includinganyongoingand/or pendingactionswhich mayimpactyour firm's capacityto successfullyperform the CivicCenter project if selected.
Section 3: Respondent Information
Identify the development team and provide an organization chart that includes all anticipated team members and their roles( architect, engineer, specialty consultants, etc.).
Provide the biographies for key development staff that would work directly with HBHA.
Include the qualifications of your anticipated partners outside your immediate company, including firm/ organization overview, relevant experience, and biographies for key staff.
Describeprojectswhere membersof the Respondentteam workedtogether.
City of S
rM Submission Instructions Cont.
Section 4: M/ WBE Inclusion Goal
HBHA seeks to work with a developer(s)that is committed to high minority and women- owned business( M/WBE) participation as well as participation from local and/ or disadvantaged businesses.
Section 5: Development Approach
Pleaseprepare responses to the following:
Describe your team's preferred development strategy for the site. Does your team have a preferred disposition strategy( buy, ground lease, etc.)?
Provide your team's feedback on HBHA's overall vision for the Site. What opportunities and challenges does the Site present? How would your team approach public outreach and engaging the community? Describe your team's experience developing contaminated property( ies).
City of QUalificiations
rM Evaluation Criteria
The evaluating process is designed to select a Respondent, not based on the least cost, but rather the Respondent(s) with the best combination of attributes, ( experience, financial capacity/ ability to secure funding, and successful partnerships with service providers). Respondent( s) must provide all information outlined in the evaluation factors ( defined below) for the Respondent' s Submission of Qualifications to be considered responsive. The quality of answers rather than length of responses to this RFQ is important. The maximum points that shall be awarded for each of the evaluation factors are detailed and described below.
HBHA' s basis of selection for final determination of shortlisted Respondents shall be within its sole discretion.
A. Has the Respondent provided a detailed inventory of the D. Has the Respondent provided evidence of on-time, on- budget development team' s relevant projects, roles, and outcomes while completion of similar past projects? ( 10 points) highlighting comparable factors between the team' s experience and the Civic Center site? ( 20 points) E. Has the Respondent demonstrated experience leading projects that showcase both time- tested and cutting- edge best practices in B. Has the Respondent provided evidence of successful design and sustainability? ( 10 points) outcomes related to similar large- scale land development projects, including working with government agencies and F. Has the Respondent previously partnered with not- for- profit community groups to secure entitlements? ( 20 points) and/ or community- based organizations? Did the Respondent describe its role and responsibilities, and how the partnership C. Has the Respondent identified key financial relationships and contributed to a symbiotic arrangement to the benefit of the demonstrated a track record of securing financing and strong, project? ( 20 points) sustainable financial performance on relevant projects? ( 20 points)
City of Huritinglon Beach - Request for
rM Contact Information
Respondents who wish to make inquiries requesting clarification of the RFQmust do so in writing. All questions must be received by April 4, 2022 at 4pm. HBHAwill make all submitted questions and answers available to all participating parties no later than April 6, 2022 at 4pm. Respondents who are interested in participating in the optional site tour should RSVPvia e-mail to JasonAustin, Deputy Director of Homeless and Behavior Health at [email protected] no later than one day prior to the event. No RSVPwill be required prior to the Virtual Q&A Session. RFQ responses are due no later than April 21, 2022 at 5:00pm and must be submitted as a PDFand emailed to [email protected].
City of for Qualificiations
Appendix A
Corporate Office
Tel: ( 714) 667- 2300
CE C
Fax: ( 714) 667- 2310
One City Boulevard West, Suite 1800
Orange. California 92868
ENVI R © N MENTAL www, eecenvironmental. com
Site Assessment Report
Cameron Ln. Property
17631 Cameron Lane
Huntington Beach, California
OCHCA Case# 201C002
June 25, 2020
Prepared for:
Mr. Carlos Marquez
City of Huntington Beach
200 Main Street
Huntington Beach, California 92648
Prepared by:
EEC Environmental
One City Boulevard West, Suite 1800
S\pNALG
Orange, California 92868
EEC S- 3506. 02T G?
4 DAVID BERNIER
0 No. 9425
01,
OFCAL\FO
Laura Holder David Bernier, PG
Project Manager Principal Geologist
ENVIRONMENTAL ENGINEERING ( COMPLIANCE ( SAFETY 1TECHNOLOq& 1 '` Site Assessment Report June 25, 2020
TABLE OF CONTENTS
1. 0 INTRODUCTION ...................................................................................................................................... 1
1. 1 SCOPE OF WORK.................................................................................................................................. 1
2. 0 BACKGROUND ........................................................................................................................................ 1
2. 1 SITE DESCRIPTION................................................................................................................................. 1
2. 2 PHYSIOGRAPHY.................................................................................................................................... 2
2. 3 GEOLOGY AND HYDROGEOLOGY ............................................................................................................. 2
3. 0 SITE INVESTIGATION ACTIVITIES ............................................................................................................ 2
3. 1 PRE- FIELD ACTIVITIES............................................................................................................................ 2
3. 1. 1 Health and Safety Plan........................................................................................................ 2
3. 1. 2 Utility Clearance.................................................................................................................. 2
3. 2 HAND- AUGER SOIL BORING ADVANCEMENT AND SOIL SAMPLING................................................................ 3
3. 2. 1 Summary of Phases of Hand- Auger Soil Sampling.............................................................. 3
3. 3 GEOPROBE DRILLING AND SOIL AND GROUNDWATER SAMPLING.................................................................. 4
3. 3. 1 Groundwater Sampling....................................................................................................... S
4. 0 SAMPLING RESULTS................................................................................................................................ 7
4. 1 SOIL................................................................................................................................................... 7
4. 2 GROUNDWATER................................................................................................................................... 8
5. 0 INVESTIGATION DERIVED WASTE AND EXCAVATED SOIL...................................................................... 8
6. 0 CONCLUSIONS AND RECOMMENDATIONS............................................................................................ 8
7. 0 REFERENCES ......................................................................................................................................... 10 Tables
In Text
Table3- 1 Sampling Matrix........................................................................................................ 6 Attached
Table 1 Summary of Soil Analytical Results— Metals
Table 2 Summary of Soil Analytical Results— Pesticides and Herbicides Table 3 Summary of Groundwater Analytical Results— Hexavalent Chromium Figures
Figure 1 Site Location Map
Figure 2 Boring Location Map
Appendices
Appendix A Laboratory Analytical Reports, Chain- of- Custody Record, and QA/ QC Data S- 3506. 02T, Huntington Beach, CA i 1@99
Site Assessment Report June 25, 2020
1. 0 INTRODUCTION
On behalf of the City of Huntington Beach, EEC Environmental ( EEC) has prepared this Site Assessment Report for the Cameron Ln. Property located at 17631 Cameron Lane, Huntington Beach, California subject property; Figure 1, Site Location Map). The purpose of the site assessment was to address findings of EEC' s Phase I Environmental Site Assessment ( ESA) dated March 18, 2020, which identified potential use of pesticides/ herbicides and lead- based paint in connection with former agricultural use and residential use as environmental concerns and recommended soil sampling. The Phase I ESAand the site assessment activities were completed in connection with proposed redevelopment of the subject property.
This report documents the methods, procedures, and results of the site assessment activities at the subject property. All work was completed in general accordance with EEC's April 2, 2020 proposal to the City of Huntington Beach ( EEC, 2020) and subsequent correspondence between the City of Huntington Beach and EEC. All work was performed under the supervision of a California licensed Professional Geologist ( PG) and the Orange County Health Care Agency ( OCHCA).
1. 1 Scope of Work
The completed site assessment activities included the following tasks:
Preparing a site- specific health and safety plan ( HASP) appropriate for the scope of work.
Contacting Underground Service Alert ( USA) 72 hours prior to initiation of fieldwork.
Advancing 35 borings for the collection of soil and groundwater samples from depths ranging from approximately 0.5 feet below ground surface ( bgs) to 24 feet bgs.
The collection and analysis of 86 soil samples for organochlorine pesticides ( OCPs), herbicides, lead, Title 22 Metals, and hexavalent chromium and 3 groundwater samples for hexavalent chromium.
Excavation of soil containing elevated concentrations of lead and OCPs at two locations.
2. 0 BACKGROUND
2. 1 Site Description
The approximately 0.79-acre subject property consists of a residential lot identified as Assessor Parcel Number ( APN) 167- 042- 08, 17631 Cameron Lane in Huntington Beach, Orange County, California. The east side of the subject property is currently developed with an unoccupied single- family residence that was developed in 1947. A Phase I ESAwas completed for the subject property on March 18, 2020 ( EEC, 2020). The Phase I ESA indicated that based on a review of historical aerial photographs, the subject property appeared to be used for agricultural purposes (row crops) from the 1930s to the 1950s and giventhis usage, it is possiblethat pesticidesand/or herbicideswere onceusedonsite. Additionally, due to the date of construction of the residence, lead- based paint may have been used on the subject property residence. Basedon this information, the PhaseI ESArecommended soil sampling to assessfor potential residualpesticidesand herbicidesfrom former agriculturaluseandto assessfor potential lead in the location of the current building exterior.
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Site Assessment Report June 25, 2020
2. 2 Physiography
The most recent topographic map coverage of the subject property is provided by the U.S. Geological Survey (USGS) 7.5-minute, Newport Beach, California quadrangle map, dated 2012 (Figure 1). According to the USGStopographic map, the subject property is located at an elevation of approximately 25 to 30 feet above mean sea level ( msl). The topography in the general subject property area slopes gently to the north- northeast.
2. 3 Geology and Hydrogeology
Onsite activities described in this report indicated that soil at the subject property consists primarily of silt at 1 foot bgs. At five feet bgs, soil consists primarily of clayey sand and sandy clay. At 8 feet bgs soil consists of silt, clayey silt, silty sand, sand, sandy clay, and clayey sand. At 20 feet bgs, soil consists of silt, clayey sand, and clayey silt. At 24 feet bgs, the maximum depth explored, soil consists of sand and silty sand.
According to a Quarterly Status Report, Second Quarter 2019 for a site located approximately 500 feet northwest of the subject property, the groundwater flow direction is southwest ( Atlas Environmental Engineering, Inc., 2019). During onsite activities, groundwater was encountered at 23 and 24 feet bgs.
3. 0 SITE INVESTIGATION ACTIVITIES
Between April 6 and May 11, 2020, a total of 35 soil borings were advanced to depths ranging from approximately 0.5 to 8 feet bgs for the collection of soil samples at the subject property. In addition, three groundwater samples were collected and two soil excavations were completed.
3. 1 Pre- Field Activities
Prior to beginning soil sampling activities, EECcompleted the following tasks necessary to initiate field activity.
3. 1. 1 Health and Safety Plan
To protect workers, EECprepared a HASP as appropriate for the scope of work. The HASP informed all site workers of potential risks during field sampling activities and provided engineering controls to avoid physical and chemical hazards. The HASP addressed potential physical and chemical hazards associated with field operations. The HASP outlined the steps to prevent exposures from all site activities. The HASP also described the safe use of equipment, evaluation of hazards, safe investigation procedures, personal protective equipment, emergency procedures and training required to conduct the site assessment under typical Hazardous Waste Operations and Emergency Response protocol.
3. 1. 2 Utility Clearance
EECcontacted USA and provided the specific property boundaries so that the proposed work area was provided to utility owners responding to the USAticket. USAis a regional notification center that notifies owners and operators of subsurface utilities ( water, gas, electric, sewer, oil lines, etc.) and informs them S3506. 02T, Huntington Beach, CA 2 94
Site Assessment Report June 25, 2020
of a contractor' s intent to perform subsurface work. EEC notified USA of the intent to perform subsurface work a minimum of 72 hours prior to the beginning of the on-site activities.
3. 2 Hand- Auger Soil Boring Advancement and Soil Sampling Between April 6 and April 28, 2020, EECadvanced a total of 27 soil borings at the subject property ( B1 through B18, B4-A, B6-A, and B26- B32; Figure 2, Boring Location Map) to total depths of 3 feet bgs. The borings were advanced using a hand auger. Once each sampling depth was reached, the hand auger was removed from the borehole and an undisturbed soil sample was collected using a slide hammer sampler including a stainless steel sampling sleeve. Following sample retrieval, both ends of the sleeve were covered with a Teflon sheet and sealed with a plastic end cap. Soil samples were then labeled with an identification number, sealed in a plastic bag, and placed into a chilled cooler.
An unused portion of soil from each sampling interval was used for field screening using a photoionization detector ( PID) for evaluation of organic vapor content and for logging lithology. Field screening was conducted by placing a portion of the unpreserved soil in a sealable plastic bag for approximately 10 minutes. The organic vapor concentration in the headspace of the plastic bag was then measured using a PID. Soil descriptions and PID measurements were recorded and documented on field notes. All field activities were performed under the direct oversight of a California PG.
All soil samples were collected and transferred under proper chain- of- custody protocols to Eurofins Calscience ( Calscience) of Garden Grove, a California state- certified laboratory. Selected soil samples were analyzed for organochlorine pesticides ( OCPs) by United States Environmental Protection Agency USEPA) Method 8081A, herbicides by USEPA Method 8151A, California Title 22 metals by USEPA Method 6010B, mercury by USEPA Method 7471A, and hexavalent chromium by USEPAMethod 7199.
The specific soil sampling method for each sample location is provided in Table 3- 1, Soil Sampling Matrix, on Page 6 of this report. Because multiple phases of soil sampling and analysis were completed, Section 3.2.1 below provides a timeline summary to clarify the sequence of events that took place between April 6 and April 28, 2020. Specific details related to analytical results, screening levels, and soil excavations are provided in Sections 4. 1 and 5.1 of this report.
3. 2. 1 Summary of Phasesof Hand-Auger Soil Sampling
The initial sampling event took place at the subject property on April 6, 2020. The purpose of this initial sampling event was to determine if residual pesticides or lead were present in soil as a result of former agricultural use and potential use of lead- based paint on the residence as identified in EEC's Phase I ESA dated March 18, 2020. Six hand auger borings ( B1 through B6) were advanced and soil samples were collected from 0. 5 and 3 feet bgs. The soil samples were submitted to Calscience and analyzed for OCPs and lead by USEPA Methods 8081A and 6010B.
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Site Assessment Report June 25, 2020
Based on the results of the soil sampling, which identified elevated concentrations of lead and OCPs in B4 and B6, respectively, four additional hand- auger borings ( 67 through B10) were advanced on April 13, 2020 and soil samples were collected from 0. 5 and 3 feet bgs for additional site coverage. The soil samples were submitted to Calscience and analyzed for OCPs and lead by USEPA Methods 8081A and 6010B. Results of the April 13, 2020 soil sampling indicated that elevated concentrations of OCPs were found in B7, on the northwest portion of the subject property.
Due to the expeditious nature of the project, on April 13, 2020, soil at the location of borings B4 and B6 was excavated and soil samples were collected from confirmation borings at the sidewalls of the excavations ( 1315 through B18 around 134; B11 through B14 around 136) and submitted to Calscience for analysis of OCPs and lead by USEPA Methods 8081A and 60108. Elevated concentrations of OCPs and lead were not found in confirmation borings around B4 and B6, with the exception of boring 1311, which had elevated concentrations of OCPs. Approximately 1.39 cubic yards of material was removed from the location of boring B4 and approximately 1.39 cubic yards of material was removed from the location of boring B6.
Based on elevated concentrations of OCPs in B7 and 1311, step- out hand- auger borings were advanced adjacent to B7 ( 1329 through B32) and B11 ( B26 through B28) on April 16, 2020. Soil samples were collected from 0.5 and 3 feet bgs and submitted to Calscience for analysis of OCPs by USEPA Method 8081A. The only elevated concentrations of pesticides detected in the step- out borings were in B29 and B32, adjacent to boring location B7. The following additional tasks were planned to address the elevated concentrations of OCPs, but were not completed due to scope changes that occurred during the course of the project: excavation around B11 and excavation and confirmation soil sampling around B7, B29, and B32.
On April 27, 2020, the City of Huntington Beach entered into a Remedial Action Agreement with the OCHCA. The OCHCA indicated that select soil samples should also be analyzed for Title 22 Metals, mercury, hexavalent chromium, and herbicides. On April 29 and 30, 2020, soil samples from B4 and B6 through B10 were analyzed for California Title 22 metals by USEPA Method 6010B, mercury by USEPA Method 7471A, and hexavalent chromium by USEPA Method 7199 and soil samples from B7, B9, and B10 were analyzed for herbicides by USEPA Method 8151A. Because the laboratory hold time was exceeded, soil from B4 and B6 could not be analyzed for herbicides. Therefore, on April 28, 2020, hand- auger soil borings 134-A and 136-A were advanced near B4 and B6. Soil samples were collected from 0. 5 and 3 feet bgs and submitted to Calscience for analysis of herbicides by USEPA Method 8151A.
3. 3 Geoprobe Drilling and Soil and Groundwater Sampling Results of the additional soil analyses completed on April 29 and 30, 2020 indicated that elevated concentrations of hexavalent chromium were found in multiple soil samples at 0. 5 and 3 feet bgs. In order to better understand the lateral and vertical distribution of hexavalent chromium at the subject property, and to determine if groundwater was impacted, EECoversaw Strongarm Environmental Field Services, Inc. ( Strongarm) drill a total of 8 borings for the collection of soil and groundwater samples on May 11, 2020. The borings were placed in a grid pattern laterally over the subject property and close to previous boring locations; therefore, they were given similar nomenclature ( 131-A, 134-13, 135-A, 66- 13, 137- A, 138-A, 139-A, and B10- A; Figure 2).
The borings were advanced using Geoprobe direct- push drilling technology and hand-auger equipment.
Direct-push drilling rigs are hydraulically powered soil probing machines that use both static force and 53506. 02T, Huntington Beach, CA 4 1>CV59
Site Assessment Report June 25, 2020
percussion to drive steel boring rods into the subsurface. Before the initiation of drilling, Strongarm cleared the upper 5 feet of the borehole with a hand auger to verify the absence of underground utilities or other shallow obstructions.
A soil sample was collected from 4 feet bgs from each boring using the hand auger. The hand auger was removed from the borehole and an undisturbed soil sample was collected using a slide hammer sampler including a stainless steel sampling sleeve. Following sample retrieval, both ends of the sleeve were covered with a Teflon sheet and sealed with a plastic end cap. During direct- push drilling, continuous soil samples were collected using 5-foot long acetate sleeves. The direct- push rig hydraulically drove the sampling sleeve the entire 5-foot interval. Following sample retrieval the portion of the sleeve chosen for samples ( i. e., 5 feet bgs, 6 feet bgs, 7 feet bgs, and 8 feet bgs) was cut and the ends of each sample were covered with Teflon sheets and sealed with plastic end caps. Soil samples were then labeled with an identification number, sealed in a plastic bag, and placed into a chilled cooler.
An unused portion of soil from each sampling interval was used for field screening using a PID for evaluation of organic vapor content and for logging lithology. Field screening was conducted by placing a portion of the unpreserved soil in a sealable plastic bag for approximately 10 minutes. The organic vapor concentration in the headspace of the plastic bag was then measured using a PID. Soil descriptions and PID measurements were recorded and documented on field notes. All field activities were performed under the direct oversight of a California PG.
The collected soil samples were transferred under proper chain- of- custody protocols to Calscience and analyzed for hexavalent chromium by USEPA Method 7199, as shown on Table 3- 1 on Page 6 of this report.
3. 3. 1 Groundwater Sampling
Following soil sampling, groundwater samples were collected from three borings ( B4-B, B8-A, and B10- A). Groundwater samples were collected with a Hydropunch- type sampling device. The rod was withdrawn to expose the screen of the sampling device and a stainless steel bailer was then lowered into the borehole to collect a groundwater sample. Samples were labeled, sealed in a plastic bag, and placed into a chilled cooler. Collected groundwater samples were submitted to Calsciencefor analysis of hexavalent chromium by USEPA Method 218. 6.
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Site Assessment Report June 25, 2020
Table 3-1, Soil Sampling Matrix
Depth
Date
Soil Sampling
Location/ Rationale Boring IDs of Borings Sample
bgs)
Sampled p
Depth
Analytes
Residence exterior/ initial April 6, 0. 5 and 3
sampling
61 63 3 feet
2020 feet
Lead, OCPs
Residence exterior/ initial April 6, 0. 5 and 3
Lead, OCPs, Title 22
sampling
B4 3 feet
2020 feet Metals, Mercury,
Hexavalent Chromium
Undeveloped area/ initial April 6, 0. 5 and 3
sampling
B5 3 feet
2020 feet
Lead, OCPs
Undeveloped area/ initial April 6, 0. 5 and 3
Lead, OCPs, Title 22
sampling
B6 3 feet
2020 feet Metals, Mercury,
Hexavalent Chromium
Lead, OCPs, Herbicides,
Northwest corner/ additional
B7 3 feet
April 13, 0. 5 and 3 Title 22 Metals,
coverage 2020 feet Mercury, Hexavalent
Chromium
North center/ additional April 13, 0. 5 and 3
Lead, OCPs, Title 22
coverage
B8 3 feet
2020 feet Metals, Mercury,
Hexavalent Chromium
Lead, OCPs, Herbicides,
Northeast and southwest
Bg B10 3 feet
April 13, 0. 5 and 3 Title 22 Metals,
corners/ additional coverage 2020 feet Mercury, Hexavalent Chromium
Adjacent to B6/ confirmation April 13, 0. 5 and 3
borings
611 614 3 feet
2020 feet
Lead, OCPs
Adjacent to B4/ confirmation April 13, 0. 5 and 3
borings
B15 618 3 feet
2020 feet
Lead, OCPs
Adjacent to B11/ step- out
B26- B28 3 feet
April 16, 0. 5 and 3
OCPs
borings 2020 feet
Adjacent to B7/ step- out April 16, 0. 5 and 3
borings
B29 B32 3 feet
2020 feet
OCPs
Adjacent to B4/ herbicide
B4A 3 feet
April 28, 0. 5 and 3
Herbicides
sampling 2020 feet
Adjacent to B6/ herbicide
B6A 3 feet
April 28, 0. 5 and 3
Herbicides
sampling 2020 feet
Adjacent to B1 and
B1- A and B10- May 11,
B10/ hexavalent chromium
A
8 feet
2020
4 feet Hexavalent chromium
sampling
Adjacent to B4, B5, B6, B71 B8,
B4- B, B5- A,
B& B, B7- A, May 11, 4, 5, 6, 7,
and B9/ hexavalent chromium
B& A, and
8 feet
2020 and 8 feet
Hexavalent chromium
sampling
Bg A
Key:
bgs= below ground surface
OCPs= organochlorine pesticides
53506. 02T, Huntington Beach, CA 6
Site Assessment Report June 25, 2020
4. 0 SAMPLING RESULTS
4. 1 Soil
A total of 86 soil samples were collected and analyzed for OCPs, herbicides, California Title 22 metals, lead, mercury, and hexavalent chromium between April 6 and May 11, 2020 ( Table 3- 1). The soil laboratory results are summarized below and in Table 1, Summary of Soil Analytical Results— Metals and Table 2, Summary of Soil Analytical Results — Pesticides and Herbicides. Estimated values ( J), detected below the reporting limit and above the laboratory method detection limit are included in the summary.
Analytical results were compared to the USEPA Regional Screening Levels ( RSLs) for residential soil and DTSC Screening Levels ( SLs) for residential soil ( Cleanup Standards). If both RSLs and SLs were available for a particular analyte, then the more stringent value was used. Laboratory analytical results, chain- of- custody documentation, and quality control data are provided in Appendix A, Laboratory Analytical Reports, Chain- of- Custody Record, and QA/ QC Data.
4. 1. 1 Metals
With the exception of lead and hexavalent chromium, metals detected in soil samples were at concentrations below their respective Cleanup Standard, or established background levels.
Lead was detected at 101 milligrams per kilogram ( mg/ kg) in 134-0.5, exceeding the Cleanup Standards. The deeper sample ( 3 feet bgs) collected from the same boring contained lead at a concentration of 2.81 mg/ kg, below Cleanup Standards; therefore, vertical delineation was achieved. Lead was not detected above Cleanup Standards in confirmation samples collected after excavation of soil around 64 ( Section 5. 1).
Hexavalent chromium was detected throughout the subject property at depths ranging from 0.5 feet bgs to 8 feet bgs. Concentrations ranged from 200 to 980 micrograms per kilogram ( µg/ kg), some of which exceeded Cleanup Standards.
4. 1. 2 Pesticides and Herbicides
Several organochlorine pesticides were detected in shallow soil, including 4, 4'- Dichlorodiphenyldichloroethane ( 4, 4'- DDD), 4, 4'- Dichlorodiphenyldichloroethylene ( 4- 4'- DDE), 4- 4' Dichlorodiphenyltrichloroethane ( 4, 4'- DDT), alpha- chlordane, chlordane, dieldrin, and toxaphene. All concentrations were below Cleanup Standards for residential soil, with the exception of toxaphene and 4, 4'- DDE. No other pesticides were detected above Cleanup Standards.
Toxaphene was detected in three samples ( 86- 0. 5, 67- 0. 5, and 610- 0. 5) at concentrations ranging between 500 µg/ kg and 1,600 µg/ kg, which exceeded the USEPARSLof 490 µg/ kg and DTSCSL of 450 µg/ kg. 4,4'- DDE was detected in one sample ( 137-0.5) at 3,100 µg/ kg, which exceeded the USEPA RSLof 2,000 jig/ kg ( DTSCSL not established).
Herbicides were not detected above laboratory reporting limits in any of the samples that were analyzed ( 64- A, 136-A, 137, 69, and B10 at 0. 5 and 3 feet bgs).
S3506. 02T, Huntington Beach, CA 7 FO§
Site Assessment Report June 25, 2020
4. 2 Groundwater
On May 11, 2020, groundwater samples were collected from three of the geoprobe boring locations ( 138- A/ GW- 1, B4- B/ GW- 2, and B10- A/ GW- 3) in order to determine if hexavalent chromium in soil had impacted groundwater. Collected groundwater samples were transferred under proper chain- of- custody protocols to Calscience for analysis of hexavalent chromium by USEPA Method 218. 6.
Hexavalent chromium was not detected above the laboratory reporting limit of 0.038 micrograms per liter ( µg/ L) in any of the groundwater samples. It was detected at 0.086 J µg/ L in the equipment blank sample, which is laboratory- provided water used as a quality control sample.
5. 0 INVESTIGATION DERIVED WASTE AND EXCAVATED SOIL
Excavated soil, soil cuttings, and decontamination water generated during this assessment work were stored onsite in ten United States Department of Transportation ( DOT) approved 55- gallon drums. The drums were labeled documenting the accumulation start date, description of contents, and applicable contact information. Wastes will be profiled, manifested, and disposed of within 90 days of generation.
If available at the time of report preparation, the manifest( s) signed by the disposal facility will be included in the final report.
6. 0 CONCLUSIONS AND RECOMMENDATIONS
This site assessment and limited soil excavation was performed to address the findings of the Phase I ESA report. Based on the results of the site assessment and limited excavation activities, EEC has the following conclusions:
Soil impacted with lead, pesticides, and hexavalent chromium was found at the subject property.
Lead- impacted soil identified at the location of boring B4 was excavated and no additional investigation or excavation is warranted for lead impacts.
Pesticide- impacted soil at the location of boring B6 was partially excavated; however, multiple locations of elevated detections of pesticides remain at the subject property.
Hexavalent chromium was detected throughout the subject property at depths of up to 8 feet bgs; however, because hexavalent chromium was not detected in groundwater it appears to be a limited and isolated concern.
Based on the above conclusions, EEC recommends:
The ground surface at the subject property be covered with asphalt or concrete to eliminate the risk of dermal contact with soil at the subject property.
Any soil excavated from short- or long-term redevelopment be managed, handled, and disposed of in accordance with all regulatory requirements to minimize exposure to workers and the community.
S3506. 02T, Huntington Beach, CA 8
Site Assessment Report June 25, 2020
If a change to use of the subject property occurs, the soil contamination must be addressed and additional assessment may also be required.
The OCHCA must be notified if there are any changes in site use and/ or if there are any future findings of additional contamination at the site.
53506. 02T, Huntington Beach, CA 9 I W
Site Assessment Report June 25, 2020
7. 0 REFERENCES
Atlas Environmental Engineering, Inc. ( 2018, May 9). Quarterly Status Report, 2" d
Quarter 2019, OCHCA
Case # 93UT070, G& M Oil Company Station # 35, 17501 Beach Boulevard, Huntington Beach, California 92647,
EEC Environmental ( 2020, March 18). Phase 1 Environmental Site Assessment, 17631 Cameron Lane and 17642 Beach Boulevard, Huntington Beach, California.
United States Geological Survey ( USGS). 7.5- Minute Topographic Quadrangle Map, Newport Beach, California, 2012
S3506. 02T, Huntington Beach, CA 10 fdF§
Tables
1073
Table 1, Summary of Soil Analytical Results- Metals
17631 Cameron Lane
Huntington Beach, California
Antimatry Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thalllum Vanadium Zinc Mercury Hexavalent
Sample Depth mg/ Kg) ( m9/ Kg1 ( mg/ Kg) ( mg/ Kg) mg/ mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) Chromium..
Sample ID (
feet bgs)
Date pg/ Kg)
USEPA Method 60108 USEPA Method USEPA
7471A Method 7199
K
0. 5 04/ 6/ 2020 NA NA NA NA NA NA NA NA 44. 6 NA
3. 0 04/ 6/ 2020 NA NA NA NA NA NP NA NA 3. 23 NA NA NA NA NA NA NA NA NA
4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND< 200
0. 5 04/ 6/ 2020 NA NA NA NA NA NA NA NA 15. 6 NA NA NA NA NA NA NA NA NA
3. 0 04/ 6/ 2020 NA NA NA NA NA NA NA NA 3. 52 NA NA NA NA NA NA NA NA NA
0. 5 04/ 6/ 2020 NA NA NA NA NA NA NA NA 5. 29 NA NA NA NA NA NA NA NA NA
3. 0 04/ 6/ 2020 NA NA NA NA NA NA NA NA 2. 57 NA NA NA NA NA NA NA NA NA 64- 0. 5 0. 5 04/ 6/ 2020 4. 61 10. 3 150 0. 760 2. 11 21. 6 9. 81 38. 0 101 ND< 0. 260 17. 4 ND< 0. WU ND< 0. 260 ND< 0. 781 40. 1 240 0. 210 Soo B4- 3. 0 3. 0 04/ 6/ 2020 ND< 0. 735 2. 56 81. 1 0. 922 NIMA90 17. 3 7. 60 6. 29 2. 81 0. 696 12. 7 ND< 0. 735 ND< 0. 745 ND< 0. 735 35. 9 35. 1 ND< 0. 0794 2901 B413- 4. 0 4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 350J B413- 5. 0 5. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 300J B413- 6. 0 6. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 380J B413- 7. 0 7. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 330J B413- 8. 0 8. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 410J 65- 0. 5 0. 5 04/ 6/ 2020 NA NA NA NA NA NA NA NA 17. 9 NA NA NA NA NA NA NA NA NA 65- 3. 0 3. 0 04/ 6/ 2020 NA NA NA NA NA NA NA NA 2. 43 NA NA NA NA NA NA NA NA NA B5A- 4. 0 4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 300J B5A- 5. 0 5. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 540 B5A- 6. 0 6. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 330J B5A- 7. 0 7. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 580 B5A- 8. 0 8. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 200J UB
0. 5 04/ 6/ 2020 ND< 0. 785 8. 44 113 1. 12 1. 00 23. 1 10. 7 20. 3 7. 62 0. 617 16. 7 ND< OJ85 ND< 0. 262 ND< 0. 785 48. 7 75. 3 ND< 0. 0806 290J
3. 0 04/ 6/ 2020 ND< 0. 769 3. 27 81. 5 0. 858 ND< 0. 513 14. 0 6. 43 10. 3 12. 8 0. 712 12. 0 ND< 0J69 ND< 0. 2.56 ND< 0. 769 31. 1 45. 2 ND< 0. 0847 820
4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 570
5. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 430
6. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 620
7. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 350J
8. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA
NAMNA
NA NA NA NA NA NA NA ND< 400
B7- 0. 5 0. 5 04/ 13/ 2020 1. 0 3. 67 50. 9 NDd). 748 0. 748 9. 5 3. 44 17. 8 30. 0 6. 41 ND< 0. 741 0. 311 ND< 0. 743 13. 2 97. 1 0. 245 NA(1) B7- 3. 0 3. 0 04/ 13/ 2020 1. 37 ND< 0. 754 54. 1 0. 437 ND< 0. 503 7. 48 6. 71 6. 16 5. 16 6. 34 ND< 0. 754 ND< 0. 251 ND< 0. 754 19. 8 16. 0 0. 0817 380J B7A- 4. 0 4. 0- 05/ 11/ 2020 NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA ND< 1, 000 B7A- 5. 0 5. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA ND< 400 B7A- 6. 0 6. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA 420 67A- 7. 0 7. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA 270J 137A- 8. 0 8. 0 1 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 330J USEPA R5Ls for Soil- Residential k 31 0. 68 1 15 000 1 1, 600 1 71 1 120, 000 23 3100 82 390 1, 500 390 390 0. 78 390 23, 000 1 23 300 DTSC SL Lor Soil- Residential k 0. 11 1 16 910 1 -- 80 820 1. 0 300 EEC s- 3506. 02T I of 2
1074
Table 1, Summary of Soil Analytical Results- Metals
17631 Cameron Lane
Huntington Beach, California
Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead , Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc . Mercury Hexavalent
Sample Depth mg/ Kg) (-&/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg): ( rngft) ( mg/ Kg) :( mg/ Kg). ( mg/ Kg). ( m8/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) ( mg/ Kg) Chromium
Sample ID (
feet bgs) .
Date J1g/Kg)
USEPA Method 6010E
USEPA Method USEPA
7471A Method 7199
B8- 0. 5 0. 5 04/ 13/ 2020 0. 913 1. 83 54. 3 0. 372 ND< 0. 513 6. 62 4. 24 7. 55 25 ND< 0756 5. 86 ND< 0. 769 ND< 0. 256 ND< 0. 769 17. 3 26. 4 ND< 0. 0820 480 B8- 3. 0 3. 0 04/ 13/ 2020 1. 42 7. 30 109 ND< 0. 253 ND< 0. 505 3. 97 2. 40 8. 77 2. 45 1. 53 4. 27 ND< 0. 758 ND< OJ P ND< 0. 758 9. 2 14. 6 ND< 0. 0834 ND< 200 BSA- 4. 0 4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND<. 800 B8A- 5. 0 5. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND< 200 B8A- 6. 0 6. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 250J B8A- 7. 0 7. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 240J B8A- 8. 0 8. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 210J 39- 0. 5 0. 5 04/ 13/ 2020 ND< 0. 739 3. 15 57. 5 0. 282 ND< 0. 493 5. 45 3. 55 8. 26 9. 59 ND< 0. 7J6 5. 12 ND< 0. 739 ND< 0246 ND< 0. 739 14. 3 22. 3 ND< 0. 0847 ND< 200 B9- 3. 0 3. 0 04/ 13/ 2020 ND< 0. 743 2. 16 56. 5 ND< 0. 248 ND< 0. 495 4. 23 2. 66 4. 9 3. 33 ND< 0. 248 3. 85 ND< 0. 743 N0< 0. 248 ND< 0. 743 30. 9 12. 4 ND- 0. 0862 360J 139A- 4. 0 4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND< 800 69A- 5. 0 5. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 980 B9A- 6. 0 6. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 320J B9A- 7. 0 7. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND< 200 B9A- 8. 0 8. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NDDc200 B10- 0. 5 0. 5 04/ 13/ 2020 1. 15 5. 07 78. 3 0. 428 ND< 0. 488 9. 51 5. 03 18. 5 47. 3 0. 260 12. 5 ND< O 732 ND< 0. 244 ND< 0. 742 21. 0 51. 4 ND< 0. 0862 430 B10- 3. 0 3. 0 04/ 13/ 2020 ND< 0. 725 1. 55 40. 0 0. 378 ND< 0. 483 6. 28 2. 55 3. 52 2. 54 0. 654 5. 24 ND< 0. 725 ND< 0. 242 ND< 0. 725 22. 6 14. 2 ND< 0. 0877 310J B10A- 4. 0 4. 0 05/ 11/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 270 611- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 10. 2 NA NA NA NA NA NA NA NA NA B11- 3. 0 3. 0 04/ 13/ 2020 NA. NA NA NA NA NA NA NA 2. 44 NA NA NA NA NA NA NA NA NA B12- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 19. 6 NA NA NA NA NA NA NA NA NA B12- 3. 0 3. 0 04/ 13/ 2020 NA NA NA NA NA NA NA NA 4. 07 NA NA NA NA NA NA NA NA NA B13- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 18. 0 NA NA NA NA NA NA NA NA NA 813- 3. 0 3. 0 04/ 13/ 2020 NA PJA PJA NA NA NA NA NA 4. 02 NA NA NA NA NA NA NA NA NA 814- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 4. 64 NA NA NA NA NA NA NA NA NA B14- 3. 0 3. 0 04/ 13/ 2020 NA NA NA NA NA NA NA NA 3. 57 NA NA NA NA NA NA NA NA NA B15- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 11. 3 NA NA NA NA NA NA NA NA NA B15- 3. 0 3. 0 04/ 13/ 2020 NA NA NA NA NA NA NA NA 10. 9 NA NA NA NA NA NA NA NA NA B16- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 9. 86 NA NA NA NA NA NA NA NA NA 616- 3. 0 3. 0 04/ 13/ 2020 NA NA NA NA NA NA NA NA 5. 05 NA NA NA NA NA NA NA NA NA B17- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 4. 08 NA NA NA NA NA NA NA NA NA B17- 3. 0 3. 0 04/ 13/ 2020 NA NA NA NA NA NA NA NA 3. 06 NA NA NA NA NA NA PIA NA NA B18- 0. 5 0. 5 04/ 13/ 2020 NA NA NA NA NA NA NA NA 10. 5 NA NA NA NA NA NA NA NA NA 1318- 3. 0 3. 0 04/ 13/ 2020 NA NA NA NA NA NA NA NA 11 NA NA NA NA NA NA NA NA NA B31- 0. 5 0. 5 04/ 16/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND< 40O 631- 3. 0 3. 0 04/ 16/ 2020 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ND< 8O0 USEPA RSLs or Soil- Residential( pg/ kg). 31 0. 68* 15, 000 1, 600 71 120, 000 13 3, 100 81 390 1, 500 390 390 0. 78 390 13, 000 13 300141 DTSC 51 for Soil- Residential / kg)
l3j 0. 11* -- 1613J 910 - 80i31 820
i3j --
I. 0i3J 300t1i
Key:
NA- Not analyzed Notes:
a)= Enivronmental Protection Agency( EPA) Region IX Regional Screening Levels for Residential Soils ( 1) Sample was too small for analysis; B31 was selected as an alternate. bgs= below ground surface B31 was diluted due to the nature of the soil matrix.
RSLs= Regional Screening Levels 2) DTSC Human and Ecological Risk Office( HERO) Human Health Risk J= Result is less than the reporting limit but greater than or equal to the method detection limit Assessment( HHRA) Note 3, April 2019. mg/ kg= milligrams per kilogram 3) Value is DTSC SL non- cancer endpoint ND< X= not detected above the reporting limit or method detection limit 4) RSL and SL were converted to pg/ kg SL= Screening level Note 3 SL not available or references USEPA RSLs USEPA= United States Environmental Protection Agency Yellow highlighed results exceed RSL and SL µg/ kg= micrograms per kilogram DTSCdocumentation indicates the background concentration for arsenic in Southern California is 12 mg/ kg EEC 5- 3506. 02T 2 of' 2
1075
Table 2, Summary of Soil Analytical Results- Pesticides and Herbicides 17631 Cameron Lane
Huntington Beach, California
4, 4'- DDD 4A'- DDE 4, 4'- DDT
I
alpha- Chlordane Dieldrin To" phene Other
pg/ Kg) ( µgJKg, l[tW ) Chlordane ( WjKg) ( pg/ Kg) ( pg/ Kg) Pesticides Herbicides Sample ID
Sample Depth
Date IWKg) li8/ KS) ( pdK8)
feet bgs),
Pesticides- USEPA Method 8081A
USEPA
Method 8151A
81- 0. 5 0. 5 04/ 6/ 2020 ND< 5. 0 10 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B1- 3. 0 3. 0 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B2- 0. 5 0. 5 04/ 6/ 2020 12 360 180 ND< 1D ND< 25 5. 0 ND< 25 ND NA 82- 3. 0 3. 0 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B3-. 05 0. 5 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 rJD< 1. 0 ND< 25 ND NA 83- 3. 0 3. 0 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA 134- 0. 5 1 0. 5 04/ 6/ 2020 ND< 5. 0 43 22 6. 7 33 2. 8 ND< 25 ND NA 64- 3. 0 3. 0 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B4A- 0. 5 0. 5 04/ 28/ 2020 NA NA NA NA NA NA NA NA ND
W- 3. 0 3. 0 04/ 28/ 2020 NA NA NA NA NA NA NA NA ND
95- 0. 5 0. 5 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 NDQ5 ND NA 85- 3. 0 3. 0 04/ 6/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA 86- 0. 5 0. 5 04/ 6/ 2020 ND< 25 1, 400 350 7. 2 54 ND< 1. 0 770 ND NA 136- 3. 0 3. 0 04/ 6/ 2020 ND< 5. 0 18 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B6A- 0. 5 0. 5 04/ 28/ 2020 NA NA NA NA NA NA NA NA ND
86A- 3. 0 3. 0 04/ 28/ 2020 NA NA NA NA NA NA NA NA ND
B7- 0. 5 0. 5 04/ 13/ 2020 32 3, 100 1, 300 ND< 1. 0 NID< 25 ND< 1. 0 1, 600 ND D 37- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 16 6. 6 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND ND 88- 0. 5 0. 5 04/ 13/ 2020 ND< 5. 0 270 63 ND< 1. 0 ND< 25 1. 5 110 ND NA B8- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 13 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B9- 0. 5 0. 5 04/ 13/ 2020 ND< 5. 0 17 9. 6 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND ND 89- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND ND B10- 0. 5 0. 5 04/ 13/ 2020 ND< 5. 0 770 410 2. 8 ND< 25 ND< 10 Soo ND ND B10- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND ND B11- 0. 5 0. 5 04/ 13/ 2020 13 1, 900 610 1. 5 ND< 25 ND< 1. 0 1, 200 ND NA 611- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< lA ND< 25 ND< 10 ND< 25 ND NA B12- 0. 5 0. 5 04/ 13/ 2020 5. 7 240 100 ND< 0. 99 ND< 25 1. 6 59 ND NA 812- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 0. 99 ND< 25 ND< 0. 99 ND< 25 ND NA 813- 0. 5 0. 5 04/ 13/ 2020 16 500 100 ND< 1. 0 ND< 25 2. 5 180 ND NA 813- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 7. 7 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA 814- 0. 5 0. 5 04/ 13/ 2020 8. 2 110 53 ND< 0. 99 ND< 25 ND< 0. 98 ND< 25 ND NA 814- 3. 0 3. 0 04/ 13/ 2020 ND< 4. 9 ND< 4. 9 ND< 4. 9 ND< 0. 98 ND< 25 ND< 0. 98 ND< 25 ND NA B15- 0. 5 0. 5 04/ 13/ 2020 ND< 4. 9 ND< 4. 9 ND< 4. 9 ND< 0. 99 ND< 25 NO< 0. 98 ND< 25 ND NA 815- 3. 0 3. 0 04/ 13/ 2020 ND< 5, 0 ND< 5. 0 ND< 5. 0 ND< 0. 99 ND< 25 ND< 0. 99 ND< 25 ND NA 816- 0. 5 0. 5 04/ 13/ 2020 ND< 5. 0 22 12 2. 2 ND< 25 ND< 1. 0 ND< 25 ND NA B16- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA 817- 0. 5 0. 5 04/ 13/ 2020 ND< 5. 0 6. 0 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 NDQ5 ND NA B17- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 ND< 1. 0 NDQ5 ND< 1. 0 ND< 25 ND NA B18- 0. 5 0. 5 04/ 13/ 2020 ND< 4. 9 20 8. 2 2. 1 ND< 25 ND< 0. 99 ND< 25 ND NA 818- 3. 0 3. 0 04/ 13/ 2020 ND< 5. 0 ND< 5. 0 ND< 5. 0 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA 826- 0. 5 0. 5 04/ 16/ 2020 ND< 5. 0 230 43 ND< 1. 0 ND< 25 1. 1 120 ND NA B26- 3. 0 3. 0 04/ 16/ 2020 1 ND< 5. 0 29 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA B27- 0. 5 0. 5 04/ 16/ 2020 ND< 5. 0 220 52 ND< 1. 0 ND< 25 ND< 1. 0 100 ND NA B27- 3. 0 3. 0 04/ 16/ 2020 ND< 5. 0 400 77 ND< 1. 0 ND< 25 ND< 1. 0 230 ND NA B28- 0. 5 0. 5 04/ 16/ 2020 ND< 5. 0 420 130 ND< 1. 0 ND< 25 2. 6 180 ND NA 828- 3. 0 3. 0 04 16 2020 ND< 5. 0 33 ND< 5. 0 ND< 1. 0 ND< 25 ND< 1. 0 ND< 25 ND NA 1329- 0. 5 0. 5 04/ 16/ 2020 95 1000 360 2. 5 ND< 25 ND< 1. 0 1 940 ND NA B29- 3. 0 3. 0 04/ 16/ 2020 ND< 5. 0 61 27 ND< 1. 0 ND< 25 ND< 1. 0 37 ND NA B30- 0. 5 0. 5 04/ 16/ 2020 38 460 120 2. 4 ND< 25 ND< 1. 0 410 1 ND NA B30- 3. 0 3. 0 1 04/ 16/ 2020 ND< 5. 0 20 8. 2 ND< 1. 0 ND< 25 ND< 1. 0 ND125 I ND NA B31- 0. 5 0. 5 04/ 16/ 2020 it 650 130 2. 1 ND< 25 ND< 1. 0 380 ND NA B31- 3. 0 3. 0 04 16 2020 ND< 5. 0 190 62 ND< 1. 0 ND< 25 ND< 1. 0 120 ND NA B32- 0. 5 0. 5 04/ 16/ 2020 93 16, 00 440 ND< 1. 0 ND< 25 ND< 1. 0 1200 ND NA 832- 3. 0 3. 0 04/ 16/ 2020 ND< 5. 0 85 33 ND< 1. 0 ND< 25 ND< 1. 0 50 ND NA USEPA RSds for Soil- Residential( pg/ kg) Ill 1, 900 2, 000 1, 900 -- 1, 700 34 490 Varies Varies OTSCSL for Soil- Residential( µg/ kg)
Iz)
2, 300 -- -- - - -- 450 Varies Varies Key: Notes:
NA- Not analyzed 1) RSLs. November 2019( Rev. 2) for soil. a)= Enivronmental Protection Agency( EPA) Region IX Regional Screening Levels for Residential Soils ( 2) DTSC Human and Ecological Risk Office( HERO) Human Health Risk bgs= below ground surface Assessment( HHRA) Note 3, April 2019, Cancer endpoint value DTSC= California State Department of Toxic Substances Control USEPA RSL Not Established; or Note 3 References USEPA RSLs ESLs= Environmental Screening Levels Yellow highlighed results exceed RSL and SL ND< X= not detected above the method detection limit
SL= Screening level
USEPA= United States Environmental Protection Agency
pg/ kg= micrograms per kilogram
EEC S- 3506. 02T I of 1
1076
Table 3, Summary of Groundwater Analytical Results - Hexavalent Chromium 17631 Cameron Lane
Huntington Beach, California
Hexavalent Chromium
Sample ID Date µg/ L)
USEPA Method 218. 6
GW- 1 05/ 11/ 2020 ND< 0. 038
GW- 2 05/ 11/ 2020 ND< 0. 038
GW- 3 05/ 11/ 2020 ND< 0. 038
WS- 1 05/ 11/ 2020 N D< 0. 038
WS- 2 05/ 11/ 2020 0. 086 J
Key:
J= Result is lessthan the reporting limit but greater than or equal to the method detection limit µg/ l-= micrograms per liter
ND<X= not detected above the reporting limit or method detection limit USEPA= United States Environmental Protection Agency
WS- 1= Duplicate
WS- 2= Equipment blank
EEC S- 3506. 02T 1 of 1 1077
Figures
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U. S. Geological Survey 7. 5 Minute SITE LOCATION MAP
Topographic Quadrangle Maps
CEEC Newport Beach and Seal Beach, CA- 2012 17631 Cameron Ln.
E N V t R 0 N M E N T A L Huntington Beach, California
Date Drafter
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APN: 167- 472- 08
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17642 Beach Blvd. L4
APN: 167- 472- 07
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LEGEND
Subject Property Boundary SOIL BORING
0 Soil Boring LOCATION MAP
T- -jEC
Soil Boring with Groundwater Sample 17631 Cameron Ln.
ENVIRONMENTAL Huntington Beach, California
Confirmation Soil Borings( B11- B18) and Step- out Soil Borings( B26- 1332)
Date Drafter Excavation( not to scale; actual size 3 x 3 x 31) PE/ P
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S- 3506. 02B
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02 Appendix
Laboratory Reports,
Chain- of- Custody Documentation,
and Quality Control Data
1081
eurofins
alIscience
ANALYTICAL REPORT
Eurofins Calscience LLC
7440 Lincoln Way
Garden Grove, CA 92841
Tel: ( 714) 895- 5494
Laboratory Job ID: 570- 25057- 1
Client Project/ Site: City of Huntington Beach / S- 3506. 02T For:
EEC Environmental
One City Blvd
Suite 1800
Orange, California 92868
Attn: Laura Holder
0XZ_
Authorized for release by.
41812020 7.-07. 32 AM
Stephen Nowak, Project Manager 1
714) 895- 5494
stephennowak@eurofinsus. com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e- mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample( s) as received by the laboratory. 1082 Client: EEC Environmental Laboratory Job ID: 570- 25057- 1 Project/ Site: City of Huntington Beach/ S-3506. 02T
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Definitions/ Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 Eurofins( science LLC
Definitions/ Glossary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
F1 MS and/ or MSD recovery exceeds control limits.
p The% RPD between the primary and confirmation column/ detector is> 40%. The lower value has been reported.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report. n
Listed under the" D" column to designate that the result is reported on a dry weight basis R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio( normalized absolute difference) Dil Fac Dilution Factor
DL Detection Limit( DoD/ DOE)
DL, RA, RE, IN Indicates a Dilution, Re- analysis, Re- extraction, or additional Initial metals/ anion analysis of the sample DLC Decision Level Concentration( Radiochemistry)
EDL Estimated Detection Limit( Dioxin)
LOD Limit of Detection( DoD/ DOE)
LOQ Limit of Quantitation( DoD/ DOE)
MDA Minimum Detectable Activity( Radiochemistry)
MDC Minimum Detectable Concentration( Radiochemistry)
MDL Method Detection Limit
ML Minimum Level( Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit( or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio( Radiochemistry)
RL Reporting Limit or Requested Limit( Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor( Dioxin)
TEQ Toxicity Equivalent Quotient( Dioxin)
Eurofins Calscience LLC
1084
Case Narrative
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Job ID: 570- 25057- 1
Laboratory: Eurofins Calscience LLC
I
Narrative
Job Narrative
570- 25057- 1
Comments
No additional comments.
Receipt
The samples were received on 4/6/2020 2: 05 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2. 70 C.
GC Semi VOA
Method 8081A: The matrix spike/ matrix spike duplicate( MS/ MSD) recoveries for the following sample associated with preparation batch 570- 61613 and analytical batch 570- 61652 were outside control limits: ( 570- 25057- A- 1- A MS) and ( 570- 25057- A- 1- B MSD). The associated laboratory control sample( LCS) recovery met acceptance criteria.
Method 8081A: The following samples has clear evidence of the presence of chlordane based on the presence of cis and trans chlordane; however, the chlordane peaks in the sample do not closely match the laboratory' s Technical Chlordane standard: 134-0.5( 570- 25057- 7) and 66- 0. 5( 570- 25057- 11). As a result, there is increased quantitative uncertainty associated with this result.
Method 8081A: The analyte 4, 4'- DDD was diluted due to the nature of the sample matrix: 136-0. 5( 570- 25057- 11) at 5X. Elevated reporting limits( RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/ Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/ Glossary page.
Eurofins CaW Sence LLC
Detection Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 131- 0. 5 Lab Sample ID: 570- 25057- 1 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 10 F1 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDT 5. 0 5. 0 ug/ Kg 1 8081A Total/ NA
I
Lead 44. 6 0. 503 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 131- 3. 0 Lab Sample ID: 570- 25057- 2 No Detections.
Client Sample ID: 132- 0. 5 Lab Sample ID: 570- 25057- 3 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDD 12 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDE 360 100 ug/ Kg 20 8081A Total/ NA
4, 4'- DDT 180 100 ug/ Kg 20 8081A Total/ NA
Dieldrin 5. 0 1. 0 ug/ Kg 1 8081A Total/ NA
Lead 15. 6 0. 493 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 132- 3. 0 Lab Sample ID: 570- 25057- 4 No Detections.
Client Sample ID: 133- 0. 5 Lab Sample ID: 570- 25057- 5 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 5. 29 0. 483 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 133- 3. 0 Lab Sample ID: 570- 25057- 6 No Detections.
Client Sample ID: 134- 0. 5 Lab Sample ID: 570- 25057- 7 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 43 25 ug/ Kg 5 8081A Total/ NA
4, 4'- DDT 22 5. 0 ug/ Kg 1 8081A Total/ NA
alpha- Chlordane 6. 7 p 1. 0 ug/ Kg 1 8081A Total/ NA
Chlordane 33 25 ug/ Kg 1 8081A Total/ NA
Dieldrin 2. 8 1. 0 ug/ Kg 1 8081A Total/ NA
Lead 101 0. 488 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 134- 3. 0 Lab Sample ID: 570- 25057- 8 No Detections.
Client Sample ID: 135- 0. 5 Lab Sample ID: 570- 25057- 9 No Detections.
Client Sample ID: 135- 3. 0 Lab Sample ID: 570- 25057- 10 No Detections.
Client Sample ID: 136- 0. 5 Lab Sample ID: 570- 25057- 11 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 1400 250 ug/ Kg 50 8081A Total/ NA
4, 4'- DDT 350 50 ug/ Kg 10 8081A Total/ NA
This Detection Summary does not include radiochemical test results.
Eurofins Calscience LLC
1086
Detection Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 136- 0. 5 ( Continued) Lab Sample ID: 570- 25057- 11 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type alpha- Chlordane 7. 2 1. 0 ug/ Kg 1 8081A Total/ NA
Chlordane 54 25 ug/ Kg 1 8081A Total/ NA
I
Toxaphene 770 25 ug/ Kg 1 8081A Total/ NA
Client Sample ID: 136- 3. 0 Lab Sample ID: 570- 25057- 12 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 18 5. 0 ug/ Kg 1 8081A Total/ NA
Client Sample ID: QA1 Lab Sample ID: 570- 25057- 13
No Detections.
This Detection Summary does not include radiochemical test results.
Eurofins Calscience LLC
1087
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC)
Client Sample ID: B1- 0. 5 Lab Sample ID: 570- 25057- 1 Date Collected: 04/ 06/ 20 08: 05 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 4, 4'- DDE 10 F1 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 I
4, 4'- DDT 5. 0 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 alpha- BHC ND 5. 0 ug/ Kg 04106/ 2015: 49 04/ 07/ 20 12: 04 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 04 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 62 23- 124 04/ 06/ 20 15: 49 04107120 12: 04 1 DC8 Decachlorobiphenyl( Surr) 55 20- 137 04106120 15: 49 04107120 12: 04 1 Client Sample ID: 1131-3. 0 Lab Sample ID: 570- 25057- 2 Date Collected: 04/ 06/ 20 08: 38 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 18 1 Eurofins Calscience LLC
1088
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B1- 3. 0 Lab Sample ID: 570- 25057- 2 Date Collected: 04/ 06/ 20 08: 38 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12. 18 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 2015: 49 04/ 07/ 2012: 18 1 IToxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2012: 18 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 69 23- 124 04106120 15: 49 04107120 12: 18 1 DCB Decachlorobiphenyl( Surr) 60 20- 137 04106120 15: 49 04107120 12: 18 1 Client Sample ID: 62- 0. 5 Lab Sample ID: 570- 25057- 3 Date Collected: 04/ 06/ 20 09: 00 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD 12 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 4, 4'- DDE 360 100 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 16: 47 20 4, 4'- DDT 180 100 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 16: 47 20 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 0612015: 49 04/ 07/ 20 12: 33 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Dieldrin 5. 0 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 33 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 68 23- 124 04106120 15: 49 04/ 07/ 20 12: 33 1 Tetrachloro- m- xylene 53 23- 124 04106120 15: 49 04107120 16: 47 20 DCB Decachlorobiphenyl( Surr) 71 20- 137 04106120 15: 49 04107120 12: 33 1 DCB Decachlorobiphenyl( Surr) 65 20- 137 04106120 15: 49 04107120 16: 47 20 Client Sample ID: B2- 3. 0 Lab Sample ID: 570- 25057- 4 Date Collected: 04/ 06/ 20 09: 26 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2012: 47 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2012: 47 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2012: 47 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2012: 47 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2012: 47 1 Eurofins Calscience LLC
1089
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: 132- 3. 0 Lab Sample ID: 570- 25057- 4 Date Collected: 04/ 06/ 20 09: 26 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04107/ 2012: 47 1 I
beta- BHC ND 5. 0 ug/ Kg 04/ 0612015: 49 04/ 07/ 20 12: 47 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 delta- BHC ND 5. 0 ug/ Kg 04106/ 2015: 49 04/ 07/ 20 12: 47 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 32 23- 124 04/ 06/ 20 15: 49 04/ 07/ 20 12: 47 1 DCB Decachlorobiphenyl( Surr) 22 p 20- 137 04106120 15: 49 04107120 12: 47 1 Client Sample ID: B3- 0. 5 Lab Sample ID: 570- 25057- 5 Date Collected: 04/ 06/ 20 09: 42 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 0612015: 49 04/ 07/ 20 13: 01 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 01 1 Eurofins Calscience LLC
1090
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 37 23- 124 04106120 15: 49 04107120 13: 01 1 DCB Decachlorobiphenyl( Surr) 36 20- 137 04/ 06/ 20 15: 49 04107120 13: 01 1 Client Sample ID: 63- 3. 0 Lab Sample ID: 570- 25057- 6 Date Collected: 04/ 06/ 20 10: 03 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 gamma- Chlordane ND 5. 0 ug/ Kg 04106/ 2015: 49 04/ 07/ 20 13: 15 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 15 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 48 23- 124 04106120 15: 49 04107120 13: 15 1 DCB Decachlorobiphenyl( Surr) 44 20- 137 04/ 06/ 20 15: 49 04107120 13: 15 1 Client Sample ID: 1134-0. 5 Lab Sample ID: 570- 25057- 7 Date Collected: 04/ 06/ 20 10: 25 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 4, 4'- DDE 43 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2017: 00 5 4, 4'- DDT 22 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 alpha- Chlordane 6. 7 p 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Chlordane 33 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Dieldrin 2. 8 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Eurofins Calscience LLC
1091
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B4- 0. 5 Lab Sample ID: 570- 25057- 7 Date Collected: 04/ 06/ 20 10: 25 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 ' gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Heptachlor ND 5. 0 ug/ Kg 04106/ 2015: 49 04/ 07/ 20 13: 29 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 29 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 58 23- 124 04106120 15: 49 04107120 13: 29 1 Tetrachloro- m- xylene 52 23- 124 04106120 15: 49 04107120 17: 00 5 DCB Decachlorobiphenyl( Surr) 59 20- 137 04106120 15: 49 04107120 13: 29 1 DCB Decachlorobiphenyl( Surr) 53 20- 137 04106120 15: 49 04107120 17: 00 5 Client Sample ID: 1134-3. 0 Lab Sample ID: 570- 25057- 8 Date Collected: 04/ 06/ 20 10: 40 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 64/ 06/ 2015: 49 04/ 07/ 20 13: 44 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Chlordane ND 25 ug/ Kg 04106/ 2015: 49 04/ 07/ 20 13: 44 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 44 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 79 23- 124 04/ 06/ 20 15: 49 04107120 13: 44 1 DCB Decachlorobiphenyl( Surr) 65 20- 137 04106120 15: 49 04107120 13: 44 1 Client Sample ID: 1135-0. 5 Lab Sample ID: 570- 25057- 9 Date Collected: 04/ 06/ 20 11: 15 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2013: 58 1 Eurofins Calscience LLC
1092
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: 65- 0. 5 Lab Sample ID: 570- 25057- 9 Date Collected: 04/ 06/ 20 11: 15 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 I
4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 13: 58 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 56 23- 124 04106120 15: 49 04107120 13: 58 1 DCB Decachlorobiphenyl( Surr) 53 20- 137 04106120 15: 49 04107120 13: 58 1 Client Sample ID: 135- 3. 0 Lab Sample ID: 570- 25057- 10 Date Collected: 04/ 06/ 20 11: 50 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 414'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 0712014: 12 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Eurofins Calscience LLC
1093
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B5- 3. 0 Lab Sample ID: 570- 25057- 10 Date Collected: 04/ 06/ 20 11: 50 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 I
Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 12 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 43 23- 124 04106120 15: 49 04107120 14: 12 1 DCB Decachlorobiphenyl( Surr) 40 20- 137 04106120 15: 49 04107120 14: 12 1 Client Sample ID: 136- 0. 5 Lab Sample ID: 570- 25057- 11 Date Collected: 04/ 06/ 20 11: 59 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2017: 14 5 4, 4'- DDE 1400 250 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 17: 10 50 4, 4'- DDT 350 50 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 16: 56 10 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 alpha- Chlordane 7. 2 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Chlordane 54 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Toxaphene 770 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 26 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 62 23- 124 04IM20 15: 49 04107120 14: 26 1 Tetrachloro- m- xylene 63 23- 124 04106120 15: 49 04107120 16: 56 10 Tetrachloro- m- xylene 72 23- 124 04106120 15: 49 04107120 17: 10 50 Tetrachloro- m- xylene 53 23- 124 04106120 15: 49 04107120 17: 14 5 DCB Decachlorobiphenyl( Surr) 55 20- 137 04106120 15: 49 04107120 14: 26 1 DCB Decachlorobiphenyl( Surr) 60 20- 137 04106120 15: 49 04107120 16: 56 10 DCB Decachlorobiphenyl( Surr) 65 20- 137 04106120 15: 49 04107120 17: 10 50 DCB Decachlorobiphenyl( Surr) 49 20- 137 04/ 06/ 20 15: 49 04107120 17. 14 5 Client Sample ID: B6- 3. 0 Lab Sample ID: 570- 25057- 12 Date Collected: 04/ 06/ 20 12: 20 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2014: 40 1 4, 4'- DDE 18 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 2014: 40 1 Eurofins Calscience LLC
1094
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: 1136-3. 0 Lab Sample ID: 570- 25057- 12 Date Collected: 04/ 06/ 20 12: 20 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 I
Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Chlordane ND 25 ug/ Kg 04106/ 2015: 49 04/ 07/ 20 14: 40 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 40 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 90 23- 124 04106120 15: 49 04107120 14: 40 1 DCB Decachlorobiphenyl( Surr) 81 20- 137 04106120 15: 49 04107120 14: 40 1 Client Sample ID: QA1 Lab Sample ID: 570- 25057- 13
Date Collected: 04/ 06/ 20 00: 00 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 Eurofins Calscience LLC
1095
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: QA1 Lab Sample ID: 570- 25057- 13
Date Collected: 04/ 06/ 20 00: 00 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 49 04/ 07/ 20 14: 55 1 ' Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 45 23- 124 04/ 06/ 20 15: 49 04107120 14: 55 1 DCB Decachlorobiphenyl( Surr) 44 20- 137 04106120 15: 49 04107120 14: 55 1 Eurofins Calscience LLC
1096
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 6010B - Metals ( ICP)
Client Sample ID: 1131-0. 5 Lab Sample ID: 570- 25057- 1 Date Collected: 04/ 06/ 20 08: 05 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 44. 6 0. 503 mg/ Kg 04/ 07/ 20 06: 55 04/ 07/ 20 12: 08 1 ' Client Sample ID: 132- 0. 5 Lab Sample ID: 570- 25057- 3 Date Collected: 04/ 06/ 20 09: 00 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 15. 6 0. 493 mg/ Kg 04/ 07/ 20 06: 55 04/ 07/ 20 12: 10 1 Client Sample ID: 133- 0. 5 Lab Sample ID: 570- 25057- 5 Date Collected: 04/ 06/ 20 09: 42 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 5. 29 0. 483 mg/ Kg 04/ 07/ 20 06: 55 04/ 07/ 20 12: 12 1 Client Sample ID: 134- 0. 5 Lab Sample ID: 570- 25057- 7 Date Collected: 04/ 06/ 20 10: 25 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 101 0. 488 mg/ Kg 04/ 07/ 20 06: 55 04/ 07/ 20 12: 14 1 Eurofins Calscience LLC
1097
Surrogate Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC)
Matrix: Solid Prep Type: Total/ NA
Percent Surrogate Recovery( Acceptance Limits)
TCX1 DCB1
Lab Sample ID Client Sample ID 23- 124) ( 20- 137)
570- 25057- 1 61- 0. 5 62 55
570- 25057- 1 MS B1- 0. 5 95 86
570- 25057- 1 MSD B1- 0. 5 80 72
570- 25057- 2 B1- 3. 0 69 60
I570- 25057- 3 B2- 0. 5 53 65
570- 25057- 3 B2- 0. 5 68 71
570- 25057- 4 B2- 3. 0 32 22 p
570- 25057- 5 B3- 0. 5 37 36
570- 25057- 6 B3- 3. 0 48 44
570- 25057- 7 B4- 0. 5 52 53
570- 25057- 7 B4- 0. 5 58 59
570- 25057- 8 B4- 3. 0 79 65
570- 25057- 9 B5- 0. 5 56 53
570- 25057- 10 B5- 3. 0 43 40
570- 25057- 11 B6- 0. 5 53 49
570- 25057- 11 B6- 0. 5 62 55
570- 25057- 11 B6- 0. 5 63 60
570- 25057- 11 66- 0. 5 72 65
570- 25057- 12 B6- 3. 0 90 81
570- 25057- 13 QA1 45 44
LCS 570- 61613/ 2- A Lab Control Sample 107 101
LCSD 570- 61613/ 3- A Lab Control Sample Dup 107 104
MB 570- 61613/ 1- A Method Blank 77 68
Surrogate Legend
TCX= Tetrachloro- m- xylene
DCB= DCB Decachlorobiphenyl( Surr)
Eurofins Calscience LLC
1098
QC Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach / S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC)
Lab Sample ID: MB 570- 6161311- A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
MB MB
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Aldrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 ' alpha- Chlordane ND 1. 0 ug/ Kg 04/ 06/ 20 15: 48 04107/ 2010: 53 1 beta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Chlordane ND 25 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 delta- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Dieldrin ND 1. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Endrin ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Heptachlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 Toxaphene ND 25 ug/ Kg 04/ 06/ 20 15: 48 04/ 07/ 20 10: 53 1 MB MB
Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 77 23- 124 04106120 15: 48 04107120 10: 53 1 DCB Decachlorobiphenyl( Surr) 68 20- 137 04106120 15: 48 04107120 10: 53 1 Lab Sample ID: LCS 570- 61613/ 2- A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
Spike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
4, 4'- DDD 12. 5 11. 43 ug/ Kg 91 50- 149
4, 4'- DDE 12. 5 11. 53 ug/ Kg 92 48- 144
4, 4'- DDT 12. 5 12. 43 ug/ Kg 99 37- 149
Aldrin 12. 5 11. 85 ug/ Kg 95 43- 139
alpha- BHC 12. 5 10. 98 ug/ Kg 88 51- 138
alpha- Chlordane 12. 5 10. 76 ug/ Kg 86 47- 136
beta- BHC 12. 5 12. 10 ug/ Kg 97 47- 135
delta- BHC 12. 5 9. 826 ug/ Kg 79 40- 146
Dieldrin 12. 5 11. 28 ug/ Kg 90 48- 141
Endosulfan 1 12. 5 10. 89 ug/ Kg 87 43- 139
Endosulfan II 12. 5 11. 22 ug/ Kg 90 48- 142
Endosulfan sulfate 12. 5 11. 54 ug/ Kg 92 47- 144
Endrin 12. 5 10. 90 ug/ Kg 87 35- 144
Endrin aldehyde 12. 5 10. 37 ug/ Kg 83 35- 138
gamma- Chlordane 12. 5 10. 32 p ug/ Kg 83 33- 155
gamma- BHC 12. 5 10. 79 ug/ Kg 86 51- 137
Eurofins Calscience LLC
1099
QC Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Lab Sample ID: LCS 570- 61613/ 2- A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
Spike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
Heptachlor 12. 5 10. 98 ug/ Kg 88 47- 137
Heptachlor epoxide 12. 5 11. 24 ug/ Kg 90 49- 135
Methoxychlor 12. 5 12. 32 ug/ Kg 99 39- 142
LCS LCS
I
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 107 23- 124
DCB Decachlorobiphenyl( Surr) 101 20- 137
Lab Sample ID: LCSD 570- 61613/ 3- A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
Spike LCSD LCSD Rec. RPD
Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit 4, 4'- DDD 12. 5 16. 75 ug/ Kg 86 50- 149 6 17
4, 4'- DDE 12. 5 10. 62 ug/ Kg 85 48- 144 8 18
4, 4'- DDT 12. 5 10. 98 ug/ Kg 88 37- 149 12 17
Aldrin 12. 5 10. 56 ug/ Kg 84 43- 139 12 15
alpha- BHC 12. 5 10. 56 ug/ Kg 84 51- 138 4 17
alpha- Chlordane 12. 5 10. 24 ug/ Kg 82 47- 136 5 16
beta- BHC 12. 5 10. 74 ug/ Kg 86 47- 135 12 17
delta- BHC 12. 5 9. 092 ug/ Kg 73 40- 146 8 20
Dieldrin 12. 5 10. 81 ug/ Kg 86 48- 141 4 16
Endosulfan 1 12. 5 10. 50 ug/ Kg 84 43- 139 4 16
Endosulfan 11 12. 5 11. 12 ug/ Kg 89 48- 142 1 16
Endosulfan sulfate 12. 5 11. 26 ug/ Kg 90 47- 144 2 16
Endrin 12. 5 10. 34 ug/ Kg 83 35- 144 5 18
Endrin aldehyde 12. 5 9. 860 ug/ Kg 79 35- 138 5 13
gamma- Chlordane 12. 5 10. 40 ug/ Kg 83 33- 155 1 59
gamma- BHC 12. 5 10. 32 ug/ Kg 83 51- 137 4 17
Heptachlor 12. 5 10. 88 ug/ Kg 87 47- 137 1 17
Heptachlor epoxide 12. 5 10. 32 ug/ Kg 83 49- 135 9 17
Methoxychlor 12. 5 11. 94 ug/ Kg 96 39- 142 3 17
LCSD LCSD
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 107 23- 124
DCB Decachlorobiphenyl( Surr) 104 20- 137
Lab Sample ID: 570- 25057- 1 MS Client Sample ID: B1- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits 4, 4'- DDD ND 12. 3 9. 024 ug/ Kg 73 12- 180
4, 4'- DDE 10 F1 12. 3 8. 778 F1 ug/ Kg 10 8- 184
4, 4'- DDT 5. 0 12. 3 8. 652 ug/ Kg 29 2- 187
Aldrin ND 12. 3 8. 804 ug/ Kg 71 9- 153
alpha- BHC ND 12. 3 8. 778 ug/ Kg 71 10- 149
alpha- Chlordane ND 12. 3 8. 433 ug/ Kg 68 9- 161
Eurofins Calscience LLC
1100
QC Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Lab Sample ID: 570- 25057- 1 MS Client Sample ID: B1- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits beta- BHC ND 12. 3 9. 012 ug/ Kg 73 9- 156
delta- BHC ND 12. 3 7. 817 ug/ Kg 63 6- 162
Dieldrin ND 12. 3 8. 988 ug/ Kg 73 11- 164
Endosulfan I ND 12. 3 8. 718 ug/ Kg 71 4- 156
Endosulfan II ND 12. 3 9. 233 ug/ Kg 75 12- 161
IEndosulfan sulfate ND 12. 3 9. 381 ug/ Kg 76 10- 165
Endrin ND 12. 3 7. 993 ug/ Kg 65 6- 166
Endrin aldehyde ND 12. 3 8. 611 ug/ Kg 70 1- 156
gamma- Chlordane ND F2 F1 ** 1 12. 3 8. 599 ug/ Kg 70 7- 177 gamma- BHC ND 12. 3 8. 601 ug/ Kg 70 9- 154
Heptachlor ND 12. 3 9. 100 ug/ Kg 74 3- 150
Heptachlor epoxide ND 12. 3 8. 658 ug/ Kg 70 7- 169
Methoxychlor ND 12. 3 9. 168 ug/ Kg 74 8- 163
MS MS
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 95 23- 124
DCB Decachlorobiphenyl( Surr) 86 20- 137
Lab Sample ID: 570- 25057- 1 MSD Client Sample ID: B1- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61652 Prep Batch: 61613
Sample Sample Spike MSD MSD Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit 4, 4'- DDD ND 12. 5 8. 932 ug/ Kg 72 12- 180 1 79
4, 4'- DDE 10 F1 12. 5 8. 819 F1 ug/ Kg 10 8- 184 0 76
4, 4'- DDT 5. 0 12. 5 9. 389 ug/ Kg 35 2- 187 8 78
Aldrin ND 12. 5 8. 620 ug/ Kg 69 9- 153 2 77
alpha- BHC ND 12. 5 8. 685 ug/ Kg 70 10- 149 1 85
alpha- Chlordane ND 12. 5 8. 281 ug/ Kg 66 9- 161 2 79
beta- BHC ND 12. 5 8. 752 p ug/ Kg 70 9- 156 3 78
delta- BHC ND 12. 5 7. 613 ug/ Kg 61 6- 162 3 85
Dieldrin ND 12. 5 8. 774 ug/ Kg 70 11- 164 2 77
Endosulfan I ND 12. 5 8. 501 ug/ Kg 68 4- 156 3 77
Endosulfan II ND 12. 5 8. 913 ug/ Kg 71 12- 161 4 77
Endosulfan sulfate ND 12. 5 9. 305 ug/ Kg 75 10- 165 1 73 Endrin ND 12. 5 8. 524 ug/ Kg 68 6- 166 6 82
Endrin aldehyde ND 12. 5 8. 550 ug/ Kg 69 1- 156 1 83
gamma- Chlordane ND 12. 5 8. 427 p ug/ Kg 68 7- 177 7 84 gamma- BHC ND 12. 5 8. 549 ug/ Kg 69 9- 154 1 79
Heptachlor ND 12. 5 8. 387 ug/ Kg 67 3- 150 8 85
Heptachlor epoxide ND 12. 5 8. 636 ug/ Kg 69 7- 169 0 79 Methoxychlor ND 12. 5 9. 931 ug/ Kg 80 8- 163 8 78
MSD MSD
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 80 23- 124
DCB Decachlorobiphenyl( Surr) 72 20- 137
Eurofins Calscience LLC
1101
QC Sample Results
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 6010B - Metals ( ICP)
Lab Sample ID: MB 570- 61674/ 1- A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61755 Prep Batch: 61674
MB MB
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead ND 0. 488 mg/ Kg 04/ 07/ 20 06: 55 04/ 07/ 20 11: 42 1 Lab Sample ID: LCS 570- 6167412- A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61755 Prep Batch: 61674
Spike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
Lead 24. 6 24. 13 mg/ Kg 98 80. 120
Lab Sample ID: LCSD 570- 61674/ 3- A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61755 Prep Batch: 61674
Spike LCSD LCSD Rec. RPD
Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit Lead 24. 5 24. 13 mg/ Kg 98 80- 120 0 20
Lab Sample ID: 570- 25008- A- 1- E MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61755 Prep Batch: 61674
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits Lead 6. 16 24. 6 30. 08 mg/ Kg 97 75- 125
Lab Sample ID: 570- 25008- A- 1- F MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 61755 Prep Batch: 61674
Sample Sample Spike MSD MSD Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Lead 6. 16 24. 8 30. 23 mg/ Kg 97 75- 125 1 20
Eurofins Calscience LLC
1102
QC Association Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
GC Semi VOA
Prep Batch: 61613
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25057- 1 B1- 0. 5 Total/ NA Solid 3545
570- 25057- 2 B1- 3. 0 Total/ NA Solid 3545
570- 25057- 3 B2- 0. 5 Total/ NA Solid 3545
570- 25057- 4 B2- 3. 0 Total/ NA Solid 3545
570- 25057- 5 B3- 0. 5 Total/ NA Solid 3545
570- 25057- 6 B3- 3. 0 Total/ NA Solid 3545
570- 25057- 7 B4- 0. 5 Total/ NA Solid 3545
570- 25057- 8 B4- 3. 0 Total/ NA Solid 3545
570- 25057- 9 B5- 0. 5 Total/ NA Solid 3545
570- 25057- 10 B5- 3. 0 Total/ NA Solid 3545
570- 25057- 11 B6- 0. 5 Total/ NA Solid 3545
570- 25057- 12 B6- 3. 0 Total/ NA Solid 3545
570- 25057- 13 QA1 Total/ NA Solid 3545
MB 570- 61613/ 1- A Method Blank Total/ NA Solid 3545
LCS 570- 61613/ 2- A Lab Control Sample Total/ NA Solid 3545 LCSD 570- 61613/ 3- A Lab Control Sample Dup Total/ NA Solid 3545 570- 25057- 1 MS B1- 0. 5 Total/ NA Solid 3545
570- 25057- 1 MSD B1- 0. 5 Total/ NA Solid 3545
Analysis Batch: 61648
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25057- 3 B2- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 7 B4- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 11 B6- 0. 5 Total/ NA Solid 8081A 61613
Analysis Batch: 61652
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25057- 1 B1- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 2 B1- 3. 0 Total/ NA Solid 8081A 61613
570- 25057- 3 B2- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 4 B2- 3. 0 Total/ NA Solid 8081A 61613
570- 25057- 5 B3- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 6 B3- 3. 0 Total/ NA Solid 8081A 61613
570- 25057- 7 B4- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 8 B4- 3. 0 Total/ NA Solid 8081A 61613
570- 25057- 9 B5- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 10 B5- 3. 0 Total/ NA Solid 8081A 61613
570- 25057- 11 B6- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 11 B6- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 11 B6- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 12 B6- 3. 0 Total/ NA Solid 8081A 61613
570- 25057- 13 QA1 Total/ NA Solid 8081A 61613
MB 570- 61613/ 1- A Method Blank Total/ NA Solid 8081A 61613 LCS 570- 61613/ 2- A Lab Control Sample Total/ NA Solid 8081A 61613 LCSD 570- 61613/ 3- A Lab Control Sample Dup Total/ NA Solid 8081A 61613 570- 25057- 1 MS B1- 0. 5 Total/ NA Solid 8081A 61613
570- 25057- 1 MSD B1- 0. 5 Total/ NA Solid 8081A 61613
Eurofins Calscience LLC
1103
QC Association Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Metals
Prep Batch: 61674
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25057- 1 B1- 0. 5 Total/ NA Solid 3050B
570- 25057- 3 B2- 0. 5 Total/ NA Solid 3050E
570- 25057- 5 B3- 0. 5 Total/ NA Solid 3050B
570- 25057- 7 B4- 0. 5 Total/ NA Solid 3050E
MB 570- 61674/ 1- A Method Blank Total/ NA Solid 3050B
LCS 570- 61674/ 2- A Lab Control Sample Total/ NA Solid 3050E LCSD 570- 61674/ 3- A Lab Control Sample Dup Total/ NA Solid 3050E 570- 25008- A- 1- E MS Matrix Spike Total/ NA Solid 3050B 570- 25008- A- 1- F MSD Matrix Spike Duplicate Total/ NA Solid 3050E Analysis Batch: 61755
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25057- 1 B1- 0. 5 Total/ NA Solid 6010E 61674
570- 25057- 3 B2- 0. 5 Total/ NA Solid 6010E 61674
570- 25057- 5 B3- 0. 5 Total/ NA Solid 6010B 61674
570- 25057- 7 B4- 0. 5 Total/ NA Solid 6010B 61674
MB 570- 61674/ 1- A Method Blank Total/ NA Solid 6010B 61674 LCS 570- 61674/ 2- A Lab Control Sample Total/ NA Solid 6010B 61674 LCSD 570- 61674/ 3- A Lab Control Sample Dup Total/ NA Solid 6010B 61674 570- 25008- A- 1- E MS Matrix Spike Total/ NA Solid 6010B 61674 570- 25008- A- 1- F MSD Matrix Spike Duplicate Total/ NA Solid 6010E 61674 Eurofins Calscience LLC
1104
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 131- 0. 5 Lab Sample ID: 570- 25057- 1 Date Collected: 04/ 06/ 20 08: 05 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 05 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 12: 04 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 1. 99 g 100 mL 61674 04/ 07/ 20 06: 55 WL8G ECL 1 Total/ NA Analysis 6010B 1 61755 04/ 07/ 20 12: 08 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 131- 3. 0 Lab Sample ID: 570- 25057- 2 Date Collected: 04/ 06/ 20 08: 38 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 06 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 12: 18 UHHN ECL 1 Instrument ID: GC44
Client Sample ID: 132- 0. 5 Lab Sample ID: 570- 25057- 3 Date Collected: 04/ 06/ 20 09: 00 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 07 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 12: 33 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 07 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 20 61648 04/ 07/ 20 16: 47 UHHN ECL 1 Instrument ID: GC51
Total/ NA Prep 3050B 2. 03 g 100 mL 61674 04/ 07/ 20 06: 55 WL8G ECL 1 Total/ NA Analysis 6010B 1 61755 04/ 07/ 20 12: 10 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 132- 3. 0 Lab Sample ID: 570- 25057- 4 Date Collected: 04/ 06/ 20 09: 26 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 19. 99 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 12: 47 UHHN ECL 1 Instrument ID: GC44
Eurofins Calscience LLC
1105
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 133- 0. 5 Lab Sample ID: 570- 25057- 5 Date Collected: 04/ 06/ 20 09: 42 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 01 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 13: 01 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050E 2. 07 g 100 mL 61674 04/ 07/ 20 06: 55 WL8G ECL 1 Total/ NA Analysis 6010E 1 61755 04/ 07/ 20 12: 12 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 133- 3. 0 Lab Sample ID: 570- 25057- 6 Date Collected: 04/ 06/ 20 10: 03 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 03 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 13: 15 UHHN ECL 1 Instrument ID: GC44
Client Sample ID: 134- 0. 5 Lab Sample ID: 570- 25057- 7 Date Collected: 04/ 06/ 20 10: 25 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 04 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 13: 29 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 04 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 5 61648 04/ 07/ 20 17: 00 UHHN ECL 1 Instrument ID: GC51
Total/ NA Prep 3050B 2. 05 g 100 mL 61674 04/ 07/ 20 06: 55 WL8G ECL 1 Total/ NA Analysis 6010B 1 61755 04/ 07/ 20 12: 14 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 134- 3. 0 Lab Sample ID: 570- 25057- 8 Date Collected: 04/ 06/ 20 10: 40 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 05 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 13: 44 UHHN ECL 1 Instrument ID: GC44
Eurofins Calscience LLC
1106
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 135- 0. 5 Lab Sample ID: 570- 25057- 9 Date Collected: 04/ 06/ 20 11: 15 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 06 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 13: 58 UHHN ECL 1 Instrument ID: GC44
Client Sample ID: 135- 3. 0 Lab Sample ID: 570- 25057- 10 Date Collected: 04/ 06/ 20 11: 50 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 00 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 14: 12 UHHN ECL 1 Instrument ID: GC44
Client Sample ID: 136- 0. 5 Lab Sample ID: 570- 25057- 11 Date Collected: 04/ 06/ 20 11: 59 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 03 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 14: 26 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 03 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 10 61652 04/ 07/ 20 16: 56 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 03 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 50 61652 04/ 07/ 20 17: 10 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 03 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 5 61648 04/ 07/ 20 17: 14 UHHN ECL 1 Instrument ID: GC51
Client Sample ID: 136- 3. 0 Lab Sample ID: 570- 25057- 12 Date Collected: 04/ 06/ 20 12: 20 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 00 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 14: 40 UHHN ECL 1 Instrument ID: GC44
Eurofins Calscience LLC
1107
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: QA1 Lab Sample ID: 570- 25057- 13
Date Collected: 04/ 06/ 20 00: 00 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 0 g 10 mL 61613 04/ 06/ 20 15: 49 USUL ECL 1 Total/ NA Analysis 8081A 1 61652 04/ 07/ 20 14: 55 UHHN ECL 1 Instrument ID: GC44
Laboratory References:
ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL( 714) 895- 5494 Eurofins Calscience LLC
1108
Accreditation/ Certification Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-35O6.02T
Laboratory: Eurofins Calscience LLC
All accreditations/ certifications held by this laboratory are listed. Not all accreditations/ certifications are applicable to this report.
Authority Program Identification Number Expiration Date California Los Angeles County Sanitation 10109 09- 29- 20 Districts
California SCAQMD LAP 17LA0919 11- 30- 20
California State 2944 09- 29- 20
Guam State 20- 003R 10- 31- 20
Nevada State CA00111 07- 31- 20
Oregon NELAP CA300001 01- 29- 21
USDA US Federal Programs P330- 20- 00034 02- 10- 23
Washington State C916- 18 10- 11- 20
Eurofins Calscience LLC
1109
Method Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method Method Description Protocol Laboratory
8081A Organochlorine Pesticides( GC) SW846 ECL 1
6010B Metals( ICP) SW846 ECL 1
3050B Preparation, Metals SW846 ECL 1
3545 Pressurized Fluid Extraction SW846 ECL 1
Protocol References:
SW846=" Test Methods For Evaluating Solid Waste, Physical/ Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL( 714) 895- 5494 Eurofins Calscience LLC
1110
Sample Summary
Client: EEC Environmental Job ID: 570- 25057- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID 570- 25057- 1 131- 0. 5 Solid 04/ 06/ 20 08: 05 04/ 06/ 20 14: 05 570- 25057- 2 61- 3. 0 Solid 04/ 06/ 20 08: 38 04/ 06/ 20 14: 05 570- 25057- 3 132- 0. 5 Solid 04/ 06/ 20 09: 00 04/ 06/ 20 14: 05 570- 25057- 4 132- 3. 0 Solid 04/ 06/ 20 09: 26 04/ 06/ 20 14: 05 570- 25057- 5 B3- 0. 5 Solid 04/ 06/ 20 09: 42 04/ 06/ 20 14: 05 570- 25057- 6 133- 3. 0 Solid 04/ 06/ 2010: 03 04/ 06/ 20 14: 05 570- 25057- 7 64- 0. 5 Solid 04/ 06/ 2010: 25 04/ 06/ 20 14: 05 570- 25057- 8 134- 3. 0 Solid 04/ 06/ 2010: 40 04/ 06/ 20 14: 05 570- 25057- 9 135- 0. 5 Solid 04/ 06/ 2011: 15 04/ 06/ 20 14: 05 570- 25057- 10 135- 3. 0 Solid 04/ 06/ 2011: 50 04/ 06/ 20 14: 05 570- 25057- 11 136- 0. 5 Solid 04/ 06/ 2011: 59 04/ 06/ 20 14: 05 570- 25057- 12 136- 3. 0 Solid 04/ 06/ 2012: 20 04/ 06/ 20 14: 05 570- 25057- 13 QA1 Solid 04/ 06/ 20 00: 00 04/ 06/ 20 14: 05 i
Eurofins Calscience LLC
1111
LQUQ!
7440 LINCOLN WAY CHAIN OF CUSTODY RECORD
euroflns
dlSt 32nC8
GARDEN GROVE, CA 92841- 1427 DATE: Aprll' 6, 2020
570-25057 Chain of CustodV—
TEL:( 714) 895. 5494. FAX:( 714) 894- 7501 PAGE: 1 OF 1 LABORATORY CLIENT:
EEC Environmental
CLIENT PROJECT NAME i NUMBER: P. O. NO.:
ADDRESS: City of Huntington Beach/ S-3506. 02T
One City Blvd. West# 1800 PROJECTCONTACT: LAB CONTACT OR QUOTE NO.:
CITY:
Orange CA 92868
STATE: LP:
Laura Holder/Allison Burnap
TEL:
SAMPLER( S):( SIGNATURE) tA, USE. O. LY.................................
FAX: MA
714) 667- 2300 714) 667- 2310 f f4£Ww LIJd t/
r ry
TURNAROUND TIME:
SAME DAY 24 HR 48 HR 72 HR 5 DAYS 10 DAYS REQUESTED ANALYSIS
SPECIAL REQUIREMENTS( ADDITIONAL COSTS MAY APPLY)
r RWQCB REPORTING ARCHIVE SAMPLES UNTIL _ I_!_
SPECIAL INSTRUCTIONS;
Email results to Iholder OQeecenvlronm ntal. com
ALSO: a6urA Q eece lllt rU Yl x~`
n a I.co! m
Z a aal w
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LOCATION/ a v
SE:• SAMPLE ID
SAMPLING
MATRIX OF ` UUyIp
Iv : ORGY.: DESCRIPTION DATE TIME CONT. J
CD B 1- 0. 5 North of residence
Gi 01+0S $ o 1 X X
w
B1- 3. 0 North of residence O 1
o
8v1
x
CA B2- 0. 5 East of residence 0 Cj'UD so 1 X X
132-3. 0 East of residence so 1
X
B3- 0. 5 South of residence
09fa so 1 X X
133- 3. 0 South of residence
100 so 1
X
84- 0. 5 West of residence so x x
64- 3. 0 west of residence
f' so 1 X
South central portion of
XB5- 0. 5 residential lot SO 1
135- 3. 0
South central portion of
so 1
residential lot X
B6- 0. 5 West portion Df residential lot
115 so 1
X
136-3. 0 West portion of residential lot s0 1
X
QA1 Duplicate a .
r"'^ $ o 1
X
Rdlinquished by:( Signature) RecaNed by:( a Date: Time:
06 lya5
Relinquished by:( SignatuW t V Received by:( Signature) Date: Time:
N Relinquished by:( Signature) Received by:( Signature) Date: Time:
OD f+
j 4' 6 7- 7 sGC 06101/ 10 Revision
O
IV
0 Login Sample Receipt Checklist
Client: EEC Environmental Job Number: 570- 25057- 1
Login Number: 25057 List Source: Eurofins Calscience
List Number: 1
Creator: Soriano, Precy
Question Answer Comment
Radioactivity wasn' t checked or is</= background as measured by a survey N/ A meter.
The cooler' s custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True Is the Field Sampler' s name present on COC? True
There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time( excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/ times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol. for all requested analyses, incl. any requested True MS/ MSDs
Containers requiring zero headspace have no headspace or bubble is True 6mm ( 1/ 4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/ A
Eurofins Calscience LLC 1113
ti . eurof ins
CalIscience
ANALYTICAL REPORT
Eurofins Calscience LLC
7440 Lincoln Way
Garden Grove, CA 92841
Tel: ( 714) 895- 5494
Laboratory Job ID: 570-25057- 2
Client Project/ Site: City of Huntington Beach / S- 3506. 02T For:
EEC Environmental
One City Blvd
Suite 1800
Orange, California 92868
Attn: Laura Holder
01(olle—
Authorized for release by:
411012020 9: 41: 04 AM
Stephen Nowak, Project Manager 1
714) 895- 5494
stephennowak@eurofinsus. com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e- mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample( s) as received by the laboratory. 1114 Client: EEC Environmental Laboratory Job ID: 570- 25057- 2 Project/ Site: City of Huntington Beach/ S-3506. 02T
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Definitions/ Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Eurofins 091science LLC
Definitions/ Glossary
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Qualifiers
Metals
Qualifier Qualifier Description
F1 MS and/ or MSD recovery exceeds control limits.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
II
Listed under the" D" column to designate that the result is reported on a dry weight basis R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio( normalized absolute difference) Dil Fac Dilution Factor
DL Detection Limit( DoD/ DOE)
DL, RA, RE, IN Indicates a Dilution, Re- analysis, Re- extraction, or additional Initial metals/ anion analysis of the sample DLC Decision Level Concentration( Radiochemistry)
EDL Estimated Detection Limit( Dioxin)
LOD Limit of Detection( DoD/ DOE)
LOQ Limit of Quantitation( DoD/ DOE)
MDA Minimum Detectable Activity( Radiochemistry)
MDC Minimum Detectable Concentration( Radiochemistry)
MDL Method Detection Limit
ML Minimum Level( Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit( or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio( Radiochemistry)
RL Reporting Limit or Requested Limit( Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor( Dioxin)
TEQ Toxicity Equivalent Quotient( Dioxin)
Eurofins Calscience LLC
1116
Case Narrative
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Job ID: 570- 25057- 2
Laboratory: Eurofins Calscience LLC
Narrative
Job Narrative
570- 25057- 2
Comments
No additional comments.
Receipt
The samples were received on 4/6/2020 2: 05 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2. 71 C.
Metals
Method 6010B: The matrix spike/ matrix spike duplicate( MS/ MSD) recoveries for preparation batch 570- 62199 and analytical batch 570- 62245 were outside control limits. Sample matrix interference and/ or non- homogeneity are suspected because the associated laboratory control sample( LCS) recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins CaWence LLC
Detection Summary
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 131- 3. 0 Lab Sample ID: 570- 25057- 2 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 3. 23 0. 498 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 132- 3. 0 Lab Sample ID: 570- 25057- 4 I
Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 3. 52 0. 518 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 133- 3. 0 Lab Sample ID: 570- 25057- 6 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 2. 57 0. 493 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 134- 3. 0 Lab Sample ID: 570- 25057- 8 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 2. 81 0. 513 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 135- 0. 5 Lab Sample ID: 570- 25057- 9 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 17. 9 0. 503 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 135- 3. 0 Lab Sample ID: 570- 25057- 10 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 2. 43 0. 483 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 136- 0. 5 Lab Sample ID: 570- 25057- 11 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 7. 62 0. 515 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 136- 3. 0 Lab Sample ID: 570- 25057- 12 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 12. 8 0. 483 mg/ Kg 1 6010E Total/ NA
This Detection Summary does not include radiochemical test results.
Eurofins Calscience LLC
1118
Client Sample Results
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S- 3506. 02T
Method: 6010B - Metals ( ICP)
Client Sample ID: B1- 3. 0 Lab Sample ID: 570- 25057- 2 Date Collected: 04/ 06/ 20 08: 38 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 3. 23 0. 498 mg/ Kg 04109/ 2010: 20 04/ 09/ 2019. 46 1 IClient Sample ID: B2- 3. 0 Lab Sample ID: 570- 25057- 4 Date Collected: 04/ 06/ 20 09: 26 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 3. 52 0. 518 mg/ Kg 04/ 09/ 2010: 20 04/ 09/ 2019: 48 1 Client Sample ID: B3- 3. 0 Lab Sample ID: 570- 25057- 6 Date Collected: 04/ 06/ 20 10: 03 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 2. 57 0. 493 mg/ Kg 04/ 09/ 2010: 20 04/ 09/ 2019: 50 1 Client Sample ID: 134- 3. 0 Lab Sample ID: 570- 25057- 8 Date Collected: 04/ 06/ 20 10: 40 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 2. 81 0. 513 mg/ Kg 04/ 09/ 2010: 20 04/ 09/ 2019: 52 1 Client Sample ID: B5- 0. 5 Lab Sample ID: 570- 25057- 9 Date Collected: 04/ 06/ 20 11: 15 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 17. 9 0. 503 mg/ Kg 04/ 09/ 2010: 20 04/ 09/ 2019: 54 1 Client Sample ID: 135- 3. 0 Lab Sample ID: 570- 25057- 10 Date Collected: 04/ 06/ 20 11: 50 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 2. 43 0. 483 mg/ K9 04/ 09/ 2010: 20 04/ 09/ 2019: 57 1 Client Sample ID: B6- 0. 5 Lab Sample ID: 570- 25057- 11 Date Collected: 04/ 06/ 20 11: 59 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 7. 62 0. 515 mg/ Kg 04/ 09/ 2010: 20 04/ 09/ 2019: 59 1 Client Sample ID: 136- 3. 0 Lab Sample ID: 570- 25057- 12 Date Collected: 04/ 06/ 20 12: 20 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 12. 8 0. 483 mg/ K9 04/ 09/ 20 10: 20 04/ 09/ 20 20: 00 1 Eurofins Calscience LLC
1119
QC Sample Results
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 6010B - Metals ( ICP)
Lab Sample ID: MB 570- 62199/ 1- A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62245 Prep Batch: 62199
MB MB
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead ND 0. 500 mg/ Kg 04/ 09/ 2010: 20 04/ 09/ 2018: 37 1 Lab Sample ID: LCS 570- 62199/ 2- A Client Sample ID: Lab Control Sample ' Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62245 Prep Batch: 62199
Spike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
Lead 25. 1 23. 79 mg/ Kg 95 80. 120
Lab Sample ID: LCSD 570- 62199/ 3- A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62245 Prep Batch: 62199
Spike LCSD LCSD Rec. RPD
Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit Lead 25. 3 24. 18 mg/ Kg 96 80. 120 2 20
Lab Sample ID: 570- 24627- A- 10- C MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62245 Prep Batch: 62199
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits Lead 55. 2 F1 25. 1 79. 00 mg/ Kg 95 75- 125
Lab Sample ID: 570- 24627- A- 10- D MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62245 Prep Batch: 62199
Sample Sample Spike MSD MSD Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Lead 55. 2 F1 25. 3 94. 55 F1 mg/ Kg 156 75- 125 18 20
Eurofins Calscience LLC
1120
QC Association Summary
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Metals
Prep Batch: 62199
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25057- 2 B1- 3. 0 Total/ NA Solid 3050B
570- 25057- 4 B2- 3. 0 Total/ NA Solid 3050E
570- 25057- 6 63- 3. 0 Total/ NA Solid 3050E
570- 25057- 8 B4- 3. 0 Total/ NA Solid 3050B
570- 25057- 9 B5- 0. 5 Total/ NA Solid 3050B
570- 25057- 10 B5- 3. 0 Total/ NA Solid 3050B
570- 25057- 11 B6- 0. 5 Total/ NA Solid 3050E
I
570- 25057- 12 B6- 3. 0 Total/ NA Solid 3050E
MB 570- 62199/ 1- A Method Blank Total/ NA Solid 3050B
LCS 570- 62199/ 2- A Lab Control Sample Total/ NA Solid 3050E LCSD 570- 62199/ 3- A Lab Control Sample Dup Total/ NA Solid 3050E 570- 24627- A- 10- C MS Matrix Spike Total/ NA Solid 3050E 570- 24627- A- 10- D MSD Matrix Spike Duplicate Total/ NA Solid 3050B Analysis Batch: 62245
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 57045057- 2 B1- 3. 0 Total/ NA Solid 6010B 62199
570- 25057- 4 B2- 3. 0 Total/ NA Solid 6010B 62199
570- 25057- 6 B3- 3. 0 Total/ NA Solid 6010B 62199
570- 25057- 8 B4- 3. 0 Total/ NA Solid 6010E 62199
570- 25057- 9 B5- 0. 5 Total/ NA Solid 6010E 62199
570- 25057- 10 B5- 3. 0 Total/ NA Solid 6010B 62199
570- 25057- 11 B6- 0. 5 Total/ NA Solid 6010B 62199
570- 25057- 12 B6- 3. 0 Total/ NA Solid 6010B 62199
MB 570- 62199/ 1- A Method Blank Total/ NA Solid 6010B 62199 LCS 570- 62199/ 2- A Lab Control Sample Total/ NA Solid 6010B 62199 LCSD 570- 62199/ 3- A Lab Control Sample Dup Total/ NA Solid 6010B 62199 570- 24627- A- 10- C MS Matrix Spike Total/ NA Solid 6010B 62199 570- 24627- A- 10- D MSD Matrix Spike Duplicate Total/ NA Solid 6010E 62199 Eurofins Calscience LLC
1121
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 131- 3. 0 Lab Sample ID: 570- 25057- 2 Date Collected: 04/ 06/ 20 08: 38 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050B 2. 01 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010E 1 62245 04/ 09/ 20 19: 46 OYW3 ECL 1 Instrument ID: ICP8
Client Sample ID: 132- 3. 0 Lab Sample ID: 570- 25057- 4 Date Collected: 04/ 06/ 20 09: 26 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
I
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050E 1. 93 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010B 1 62245 04/ 09/ 20 19: 48 OYW3 ECL 1 Instrument ID: ICP8
Client Sample ID: 133- 3. 0 Lab Sample ID: 570- 25057- 6 Date Collected: 04/ 06/ 20 10: 03 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050B 2. 03 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010E 1 62245 04/ 09/ 20 19: 50 OYW3 ECL 1 Instrument ID: ICP8
Client Sample ID: 134- 3. 0 Lab Sample ID: 570- 25057- 8 Date Collected: 04/ 06/ 20 10: 40 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050B 1. 95 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010B 1 62245 04/ 09/ 20 19: 52 OYW3 ECL 1 Instrument ID: ICP8
Client Sample ID: 135- 0. 5 Lab Sample ID: 570- 25057- 9 Date Collected: 04/ 06/ 20 11: 15 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 30506 1. 99 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010B 1 62245 04/ 09/ 20 19: 54 OYW3 ECL 1 Instrument ID: ICP8
Eurofins Calscience LLC
1122
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 135- 3. 0 Lab Sample ID: 570- 25057- 10 Date Collected: 04/ 06/ 20 11: 50 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050B 2. 07 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010E 1 62245 04/ 09/ 20 19: 57 OYW3 ECL 1 Instrument ID: ICP8
Client Sample ID: 136- 0. 5 Lab Sample ID: 570- 25057- 11 Date Collected: 04/ 06/ 20 11: 59 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
I
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050B 1. 94 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010E 1 62245 04/ 09/ 20 19: 59 OYW3 ECL 1 Instrument ID: ICP8
Client Sample ID: 136- 3. 0 Lab Sample ID: 570- 25057- 12 Date Collected: 04/ 06/ 20 12: 20 Matrix: Solid
Date Received: 04/ 06/ 20 14: 05
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050E 2. 07 g 100 mL 62199 04/ 09/ 20 10: 20 WL8G ECL 1 Total/ NA Analysis 6010B 1 62245 04/ 09/ 20 20: 00 OYW3 ECL 1 Instrument ID: ICP8
Laboratory References:
ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL( 714) 895- 5494 Eurofins Calscience LLC
1123
Accreditation/ Certification Summary
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Laboratory: Eurofins Calscience LLC
All accreditations/ certifications held by this laboratory are listed. Not all accreditations/ certifications are applicable to this report.
Authority Program Identification Number Expiration Date California Los Angeles County Sanitation 10109 09- 29- 20 Districts
California SCAQMD LAP 17LA0919 11- 30- 20
California State 2944 09- 29- 20
Guam State 20- 003R 10- 31- 20
Nevada State CA00111 07- 31- 20
Oregon N ELAP CA300001 01- 29- 21
USDA US Federal Programs P330- 20- 00034 02- 10- 23
Washington State C916- 18 10- 11- 20
Eurofins Calscience LLC
1124
Method Summary
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method Method Description Protocol Laboratory
6010B Metals( ICP) SW846 ECL 1
3050B Preparation, Metals SW846 ECL 1
Protocol References:
SW846=" Test Methods For Evaluating Solid Waste, Physical/ Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL( 714) 895- 5494 Eurofins Calscience LLC
1125
Sample Summary
Client: EEC Environmental Job ID: 570- 25057- 2
Project/ Site: City of Huntington Beach/ S-3506. 02T
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID 570- 25057- 2 131- 3. 0 Solid 04/ 06/ 20 08: 38 04/ 06/ 20 14: 05 570- 25057- 4 62- 3. 0 Solid 04/ 06/ 20 09: 26 04/ 06/ 20 14: 05 570- 25057- 6 133- 3. 0 Solid 04/ 06/ 2010: 03 04/ 06/ 20 14: 05 570- 25057- 8 64- 3. 0 Solid 04/ 06/ 2010: 40 04/ 06/ 20 14: 05 570- 25057- 9 65- 0. 5 Solid 04/ 06/ 2011: 15 04/ 06/ 20 14: 05 570- 25057- 10 135- 3. 0 Solid 04/ 06/ 2011: 50 04/ 06/ 20 14: 05 570- 25057- 11 136- 0. 5 Solid 04/ 06/ 2011: 59 04/ 06/ 20 14: 05 570- 25057- 12 136- 3. 0 Solid 04/ 06/ 2012: 20 04/ 06/ 20 14: 05 Eurofins Calscience LLC
1126
eurofins
7440LINCOLN WAY CHAIN OF CUSTODY RECORD
Colsc.jiertce
I GARDEN GROVE, CA 92841- 1427
Y — —---
DATE: April- 6, 2020
570- 25057 Chain of Custod
TEL:( 714) 895 5494. FAX:( 714) 894- 7501 PAGE: 1 OF 1
LABORATORY CLIENT: CLIENT PROJECT NAME I NUMBER: P. O. NO.:
EEC Environmental
ADDRESS: City of Huntington Beach/ S- 3506. 02T
One City Blvd. West# 1800 PROJECT CONTACT: LAB CONTACT OR QUOTE NO.:
CITY:
Orange CA
STATE: ZIP:
92868 Laura Holder/ Allison Burnap
SAMPLER($):( SIGNATURE) tAB. U$ E.O. LY.
TEL. (
714) 667- 2300
Pam` (
714) 667- 2310
MAIL.
TURNAROUN TIME:
SAME DAY 24 HR 48 HR 72 HR 5 DAYS 10 DAYS REQUESTED ANALYSIS
SPECIAL REQUIREMENTS( ADDITIONAL COSTS MAY APPLY)
J RWQCB REPORTING ARCHIVE SAMPLES UNTIL _/_/_
SPECIAL INSTRUCTIONS:
Email results to Iholder@eecenvironm ntal. com
Af- 50. a6L4rtiQ eecetivtrun.« n' tal.cor.
a aa
aw9'. LOCATION 1 SAMPLING NO. N a o
WSE' SAMPLE ID DESCRIPTION
MATRIX OF L
DATE TIME
w
TQIME col+ T. ti O
CD 61- 0. 5 North of residence
6 ZL1 V V o5 SO 1
X X
1 B1- 3. 0 North of residence
08o
O 1 X
B2- 0. 5 East of residence 0 C/t0 SO 1 X X
B2- 3. 0 East of residence SO 1
X
133- 0. 5 South of residence
OW01 SO 1
X X
B3- 3. 0 Soulhofresidence
100S SO 1
X
B4- 0. 5 West of residence
l rj SO 1 X x
84- 3. 0 West of residence Q a SO 1
X
South central portion of 1
XB5- 0. 5 residential lot SO
B 5- 3. 0
South central Portion of
Igo SO 1
residential lot J X
136- 0. 5 West portion of residential lot
5 SO 1
X
66- 3. 0 West portion of residential lot lagSO
1 X
QA1 Duplicate D -- SO 1
1ix 4 1
Rel inquished by:( Signature) Received by:( et Date: Time:
p y a5
Relinquished by:( Signatu Received by:( Signature) Date: Time:
N Relinquished by:( Signature) Received by:( Signature) Date: Time:
A 4
Ntc. 6 1 p 06101/ 10 Revision
ON
0 Stephen Nowak
From: Laura Holder < Iholder@eecenvironmental. com>
Sent: Thursday, April 09, 2020 2:40 PM
To: Stephen Nowak
Subject: RE: Preliminary Eurofins Calscience report files from 570- 25057- 1 City of Huntington Beach/ S- 3506. 02T
EXTERNAL EMAIL*
Hi Steve,
We would like to run all of the samples you have there for lead on a rush TAT. It would be samples 131-3.0, 62- 3.0, B3-
3.0, B4-3.0, B5-0.5, B5-3.0, 136-0.5, and B6-3.0. We need them as fast as possible.
Thank you!!
Laura Holder
Project Manager
EEC Environmental
IOne City Boulevard West I Suite 1800 1Orange, CA 92868 O ( 714) 667- 2304 1F (714) 667- 2310 1C (949) 274- 0224 IholderCcDeecenvironmental. com I www. eecenvironmental. com From: Stephen Nowak [ mailto: StephenNowak@eurofinsUS. com] Sent: Wednesday, April 08, 2020 2:33 PM
To: Laura Holder
Subject: Re: Preliminary Eurofins Calscience report files from 570- 25057- 1 City of Huntington Beach / S- 3506. 02T Yes- we' ll have them for another 60 days.
Stephen Nowak
Project Manager
Eurofins Calscience, LLC
Sentfrom my Whone
On Apr 8, 2020, at 2: 15 PM, Laura Holder< lholderkeecenvironmental. com> wrote:
EXTERNAL EMAIL*
Hi Steve,
Justa headsup that we may want to run some of the sampleswe collected Monday for lead analysis.
We will know in the next day or two for sure. I assumeyou guys still havethem and want you to know so you can still hold them for that. Can you confirm you still have them please? Thanks!
1 1128
Login Sample Receipt Checklist
Client: EEC Environmental Job Number: 570- 25057- 2
Login Number: 25057 List Source: Eurofins Calscience
List Number: 1
Creator: Soriano, Precy
Question Answer Comment
Radioactivity wasn' t checked or is</= background as measured by a survey N/ A meter.
The cooler' s custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True Is the Field Sampler' s name present on COC? True
There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time( excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/ times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol. for all requested analyses, incl. any requested True MS/ MSDs
Containers requiring zero headspace have no headspace or bubble is True 6mm ( 1/ 4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/ A
Eurofins Calscience LLC 1129
I
eurof ins
alscience
ANALYTICAL REPORT
Eurofins Calscience LLC
7440 Lincoln Way
Garden Grove, CA 92841
Tel: ( 714) 895- 5494
Laboratory Job ID: 570- 25623- 1
Laboratory Sample Delivery Group: 17631
Client Project/ Site: City of Huntington Beach / S- 3506. 02T For:
EEC Environmental
One City Blvd
Suite 1800
Orange, California 92868
Attn: Laura Holder
Authorized for release by.
411412020 4: 5127 PM
Stephen Nowak, Project Manager 1
714) 895- 5494
stephennowak@eurofinsus. com
The test results in this report meet all2003 NELAC and 2009 TNI requirements for accredited parameters, exceptionsarenotedin thisreport. Thisreportmaynotbereproducedexceptin full, and with written approval from the laboratory. For questions please contact the Project Manager at the e- mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample( s) as received by the laboratory. 1130 Client: EEC Environmental Laboratory Job ID: 570- 25623- 1 Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Definitions/ Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 Eurofins Old9cience LLC
Definitions/ Glossary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Qualifiers
GC Semi VOA
Qualifier Qualifier Description
p The% RPD between the pdmary and confirmation column/ detector is> 40%. The lower value has been reported.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report. n
Listed under the" D" column to designate that the result is reported on a dry weight basis R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio( normalized absolute difference) Dil Fac Dilution Factor
DL Detection Limit( DoD/ DOE)
DL, RA, RE, IN Indicates a Dilution, Re- analysis, Re- extraction, or additional Initial metals/ anion analysis of the sample DLC Decision Level Concentration( Radiochemistry)
EDL Estimated Detection Limit( Dioxin)
LOD Limit of Detection( DoD/ DOE)
LOQ Limit of Quantitation( DoD/ DOE)
MDA Minimum Detectable Activity( Radiochemistry)
MDC Minimum Detectable Concentration( Radiochemistry)
MDL Method Detection Limit
ML Minimum Level( Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit( or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio( Radiochemistry)
RL Reporting Limit or Requested Limit( Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor( Dioxin)
TEQ Toxicity Equivalent Quotient( Dioxin)
Eurofins Calscience LLC
1132
Case Narrative
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Job ID: 570- 25623- 1
Laboratory: Eurofins Calscience LLC
I
Narrative
Job Narrative
570- 25623- 1
Comments
No additional comments.
Receipt
The samples were received on 4/13/2020 11:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 3. 00 C.
GC Semi VOA
Method 8081A: The continuing calibration verification ( CCV) associated with 570- 62847 recovered high and outside the control limits for DCB Decachlorobiphenyl( Surr) on one column. Results are confirmed on both columns and reported from the passing column.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/ Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/ Glossary page.
Eurofins CaWence LLC
Detection Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: B11- 0. 5 Lab Sample ID: 570- 25623- 1 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDD 13 p 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDE 1900 500 ug/ Kg 100 8081A Total/ NA
I
4, 4'- DDT 610 500 ug/ Kg 100 8081A Total/ NA
alpha- Chlordane 1. 5 p 1. 0 ug/ Kg 1 8081A Total/ NA
Toxaphene 1200 25 ug/ Kg 1 8081A Total/ NA
Lead 10. 2 0. 495 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1311- 3. 0 Lab Sample ID: 570- 25623- 2 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 2. 44 0. 513 mg/ Kg 1 6010E Total/ NA
Client Sample ID: B12- 0. 5 Lab Sample ID: 570- 25623- 3 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 414'- DDD 5. 7 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDE 240 50 ug/ Kg 10 8081A Total/ NA
4, 4'- DDT 100 50 ug/ Kg 10 8081A Total/ NA
Dieldrin 1. 6 0. 99 ug/ Kg 1 8081A Total/ NA
Toxaphene 59 25 ug/ Kg 1 8081A Total/ NA
Lead 19. 6 0. 510 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1312- 3. 0 Lab Sample ID: 570- 25623- 4 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 4. 07 0. 493 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1313- 0. 5 Lab Sample ID: 570- 25623- 5 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDD 16 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDE 500 100 ug/ Kg 20 8081A Total/ NA
4, 4'- DDT 100 100 ug/ Kg 20 8081A Total/ NA
Dieldrin 2. 5 1. 0 ug/ Kg 1 8081A Total/ NA
Toxaphene 180 25 ug/ Kg 1 8081A Total/ NA
Lead 18. 0 0. 488 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1313- 3. 0 Lab Sample ID: 570- 25623- 6 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 7. 7 5. 0 ug/ Kg 1 8081A Total/ NA
Lead 4. 02 0. 495 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 11314-0. 5 Lab Sample ID: 570- 25623- 7 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDD 8. 2 4. 9 ug/ Kg 1 8081A Total/ NA
4, 4'- DDE 110 25 ug/ Kg 5 8081A Total/ NA
4, 4'- DDT 53 25 ug/ Kg 5 8081A Total/ NA
Lead 4. 64 0. 498 mg/ Kg 1 6010B Total/ NA
This Detection Summary does not include radiochemicaltest results.
Eurofins Calscience LLC
1134
Detection Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: 1314- 3. 0 Lab Sample ID: 570- 25623- 8 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 3. 57 0. 493 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1315- 0. 5 Lab Sample ID: 570- 25623- 9 I
Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 11. 3 0. 490 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1315- 3. 0 Lab Sample ID: 570- 25623- 10 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 10. 9 0. 505 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1316- 0. 5 Lab Sample ID: 570- 25623- 11 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 22 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDT 12 5. 0 ug/ Kg 1 8081A Total/ NA
alpha- Chlordane 2. 2 p 1. 0 ug/ Kg 1 8081A Total/ NA
Lead 9. 86 0. 503 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1316- 3. 0 Lab Sample ID: 570- 25623- 12 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 5. 05 0. 521 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1317- 0. 5 Lab Sample ID: 570- 25623- 13 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 6. 0 5. 0 ug/ Kg 1 8081A Total/ NA
Lead 4. 08 0. 493 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1317- 3. 0 Lab Sample ID: 570- 25623- 14 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 3. 06 0. 488 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1318- 0. 5 Lab Sample ID: 570- 25623- 15 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 20 4. 9 ug/ Kg 1 8081A Total/ NA
4, 4'- DDT 8. 2 4. 9 ug/ Kg 1 8081A Total/ NA
alpha- Chlordane 2. 1 p 0. 99 ug/ Kg 1 8081A Total/ NA
Lead 10. 5 0. 485 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1318- 3. 0 Lab Sample ID: 570- 25623- 16 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type alpha- Chlordane 1. 0 p 1. 0 ug/ Kg 1 8081A Total/ NA
Lead 11. 0 0. 505 mg/ Kg 1 60106 Total/ NA
This Detection Summary does not include radiochemical test results.
Eurofins Calscience LLC
1135
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC)
Client Sample ID: B11- 0. 5 Lab Sample ID: 570- 25623- 1 Date Collected: 04/ 13/ 20 09: 52 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD 13 p 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07. 38 1 I
4, 4'- DDE 1900 500 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 34 100 4, 4'- DDT 610 500 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 34 100 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 alpha- Chlordane 1. 5 p 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Toxaphene 1200 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 38 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 64 23- 124 04113120 13: 51 04114120 07: 38 1 Tetrachloro- m- xylene 42 23- 124 04113120 13: 51 04114120 12: 34 100 DCB Decachlorobiphenyl( Surr) 63 20- 137 04/ 13/ 20 13: 51 04114120 07: 38 1 DCB Decachlorobiphenyl( Surr) 70 20- 137 04113120 13: 51 04114120 12: 34 100 Client Sample ID: B11- 3. 0 Lab Sample ID: 570- 25623- 2 Date Collected: 04/ 13/ 20 10: 11 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Eurofins Calscience LLC
1136
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B11- 3. 0 Lab Sample ID: 570- 25623- 2 Date Collected: 04/ 13/ 20 10: 11 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 I
Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 45 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 66 23- 124 04113120 13: 51 04114120 09: 45 1 DCB Decachlorobiphenyl( Surr) 67 20- 137 04113120 13: 51 04114120 09: 45 1 Client Sample ID: B12- 0. 5 Lab Sample ID: 570- 25623- 3 Date Collected: 04/ 13/ 20 10: 20 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD 5. 7 5. 0 u9/ K9 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 4, 4'- DDE 240 50 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 48 10 4, 4'- DDT 100 50 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 48 10 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 alpha- Chlordane ND 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Dieldrin 1. 6 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Toxaphene 59 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 07: 52 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 69 23- 124 04/ 13/ 20 iY51 04114120 07: 52 1 Tetrachloro- m- xylene 68 23- 124 04113120 13: 51 04114120 12: 48 10 DCB Decachlorobiphenyl( Surr) 71 20- 137 04113120 13: 51 04114120 07: 52 1 DCB Decachlorobiphenyl( Surr) 70 20- 137 04113120 13: 51 04114120 12: 48 10 Client Sample ID: B12- 3. 0 Lab Sample ID: 570- 25623- 4 Date Collected: 04/ 13/ 20 10: 33 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Eurofins Calscience LLC
1137
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B12- 3. 0 Lab Sample ID: 570- 25623- 4 Date Collected: 04/ 13/ 20 10: 33 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 I
alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 alpha- Chlordane ND 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Dieldrin ND 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 06 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 62 23- 124 04113120 13: 51 04114120 08: 06 1 DCB Decachlorobiphenyl( Surr) 66 20- 137 04113120 13: 51 04114120 08: 06 1 Client Sample ID: B13- 0. 5 Lab Sample ID: 570- 25623- 5 Date Collected: 04/ 13/ 20 09: 32 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD 16 5. 0 ug/ Kg 04/ 13/ 2013. 51 04/ 14/ 20 10: 00 1 4, 4'- DDE 500 100 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 2013: 02 20 4, 4'- DDT 100 100 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 2013: 02 20 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Dieldrin 2. 5 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Toxaphene 180 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 00 1 Eurofins Calscience LLC
1138
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 68 23- 124 04113120 13: 51 04114120 10: 00 1 Tetrachloro- m- xylene 63 23- 124 04113120 13: 51 04114120 13: 02 20 DCB Decachlorobiphenyl( Surr) 68 20- 137 04113120 13: 51 04114120 10: 00 1 DCB Decachlorobiphenyl( Surr) 68 20- 137 04113120 13: 51 04114120 13: 02 20 I
Client Sample ID: 11313- 3. 0 Lab Sample ID: 570- 25623- 6 Date Collected: 04/ 13/ 20 09: 55 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 4, 4'- DDE 7. 7 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 20 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 57 23- 124 04113120 13: 51 04114120 08: 20 1 DCB Decachlorobiphenyl( Surr) 63 20- 137 04113120 13: 51 04114120 08: 20 1 Client Sample ID: B14- 0. 5 Lab Sample ID: 570- 25623- 7 Date Collected: 04/ 13/ 20 08: 45 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed oil Fac 4, 4'- DDD 8. 2 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 4, 4'- DDE 110 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 2013: 16 5 4, 4'- DDT 53 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 2013: 16 5 Aldrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 alpha- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 alpha- Chlordane ND 0. 98 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 beta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 delta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Dieldrin ND 0. 98 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Endosulfan I ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Endosulfan II ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Endosulfan sulfate ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Eurofins Calscience LLC
1139
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B14- 0. 5 Lab Sample ID: 570- 25623- 7 Date Collected: 04/ 13/ 20 08: 45 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Endrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 I
Endrin aldehyde ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Endrin ketone ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 gamma- Chlordane ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 gamma- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Heptachlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Heptachlor epoxide ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Methoxychlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 14 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 66 23- 124 04113120 13: 51 04114120 10: 14 1 Tetrachloro- m- xylene 63 23- 124 04113120 13: 51 04114120 13: 16 5 DCB Decachlorobiphenyl( Surr) 70 20- 137 04113120 13: 51 04114120 10: 14 1 DCB Decachlorobiphenyl( Surr) 66 20- 137 04113120 13: 51 04114120 13: 16 5 Client Sample ID: 1314- 3. 0 Lab Sample ID: 570- 25623- 8 Date Collected: 04/ 13/ 20 09: 10 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 4. 9 ug/ Kg 04/ 13/ ff 13. 51 04/ 14/ 20 08: 35 1 4, 4'- DDE ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 4, 4'- DDT ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Aldrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 alpha- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 alpha- Chlordane ND 0. 98 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 beta- BHC ND 4. 9 ug/ Kg 04/ 1 3120 13: 51 04/ 14/ 20 08: 35 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 delta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Dieldrin ND 0. 98 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Endosulfan I ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Endosulfan II ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Endosulfan sulfate ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Endrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Endrin aldehyde ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Endrin ketone ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 gamma- Chlordane ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 gamma- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Heptachlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Heptachlor epoxide ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Methoxychlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 35 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 46 23- 124 04113120 13: 51 04114120 08: 35 1 DCB Decachlorobiphenyl( Surr) 46 20- 137 04113120 13: 51 04114120 08: 35 1 Eurofins Calscience LLC
1140
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC)
Client Sample ID: B15- 0. 5 Lab Sample ID: 570- 25623- 9 Date Collected: 04/ 13/ 20 07: 42 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 I
4, 4'- DDE ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 4, 4'- DDT ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Aldrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04114/ 2010: 28 1 alpha- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 alpha- Chlordane ND 0. 98 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 beta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 delta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Dieldrin ND 0. 98 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Endosulfan I ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Endosulfan II ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Endosulfan sulfate ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Endrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Endrin aldehyde ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Endrin ketone ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 gamma- Chlordane ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 gamma- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Heptachlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Heptachlor epoxide ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Methoxychlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 28 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 60 23- 124 04113120 13: 51 04114120 10: 28 1 DCB Decachlorobiphenyl( Surr) 58 20- 137 04113120 13: 51 04114120 10: 28 1 Client Sample ID: 1315- 3. 0 Lab Sample ID: 570- 25623- 10 Date Collected: 04/ 13/ 20 07: 56 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 alpha- Chlordane ND 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Dieldrin ND 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Eurofins Calscience LLC
1141
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B15- 3. 0 Lab Sample ID: 570- 25623- 10 Date Collected: 04/ 13/ 20 07: 56 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 I
Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 08: 49 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 75 23- 124 04113120 13: 51 04114120 08: 49 1 DCB Decachlorobiphenyl( Surr) 75 20- 137 04113120 13: 51 04114120 08: 49 1 Client Sample ID: 1316- 0. 5 Lab Sample ID: 570- 25623- 11 Date Collected: 04/ 13/ 20 08: 06 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 4, 4'- DDE 22 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 4, 4'- DDT 12 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 alpha- Chlordane 2. 2 p 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 gamma- Chlordane ND 5. 0 ug/ Kg 04113/ 2013: 51 04/ 14/ 20 10: 46 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 10: 46 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 60 23- 124 04113120 13: 51 04114120 10: 46 1 DCB Decachlorobiphenyl( Surr) 58 20- 137 04113120 13: 51 04114120 10: 46 1 Client Sample ID: 1316- 3. 0 Lab Sample ID: 570- 25623- 12 Date Collected: 04/ 13/ 20 08: 22 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Eurofins Calscience LLC
1142
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: 11316- 3. 0 Lab Sample ID: 570- 25623- 12 Date Collected: 04/ 13/ 20 08: 22 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09. 03 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 IDieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 03 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 68 23- 124 04113120 13: 51 04114120 09: 03 1 DCB Decachlorobiphenyl( Surr) 69 20- 137 04113120 13: 51 04114120 09: 03 1 Client Sample ID: 11317- 0. 5 Lab Sample ID: 570- 25623- 13 Date Collected: 04/ 13/ 20 08: 36 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 4, 4'- DDE 6. 0 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 17 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 53 23- 124 04/ 13/ 20 13: 51 04114120 09: 17 1 DCB Decachlorobiphenyl( Surr) 51 20- 137 04113120 13: 51 04114120 09: 17 1 Eurofins Calscience LLC
1143
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC)
Client Sample ID: B17- 3. 0 Lab Sample ID: 570- 25623- 14 Date Collected: 04/ 13/ 20 08: 55 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 I
4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 09: 31 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 57 23- 124 04113120 13: 51 04114120 09: 31 1 DCB Decachlorobiphenyl( Surr) 60 20- 137 04113120 13: 51 04114120 09: 31 1 Client Sample ID: B18- 0. 5 Lab Sample ID: 570- 25623- 15 Date Collected: 04/ 13/ 20 08: 04 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 4, 4'- DDE 20 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 4, 4'- DDT 8. 2 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Aldrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 alpha- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 alpha- Chlordane 2. 1 p 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 beta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 delta- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Dieldrin ND 0. 99 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Endosulfan I ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Endosulfan 11 ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Endosulfan sulfate ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Endrin ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Endrin aldehyde ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Endrin ketone ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 gamma- Chlordane ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 gamma- BHC ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Heptachlor ND 4. 9 ug/ Kg 04/ 1312013: 51 04/ 14/ 20 11: 00 1 Eurofins Calscience LLC
1144
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Client Sample ID: B18- 0. 5 Lab Sample ID: 570- 25623- 15 Date Collected: 04/ 13/ 20 08: 04 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Heptachlor epoxide ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 ' Methoxychlor ND 4. 9 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 11: 00 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 63 23- 124 04113120 13: 51 04114120 11: 00 1 DCB Decachlorobiphenyl( Surr) 66 20- 137 04113120 13: 51 04114120 11: 00 1 Client Sample ID: B18- 3. 0 Lab Sample ID: 570- 25623- 16 Date Collected: 04/ 13/ 20 08: 14 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Aldrin ND 5. 0 ug/ Kg 04/ 1 3120 13: 51 04/ 14/ 20 12: 16 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 alpha- Chlordane 1. 0 p 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Methoxychlor ND 5. 0 ug/ Kg 04113/ 2013: 51 04/ 14/ 20 12: 16 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 12: 16 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 79 23- 124 64113126 13: 51 04114120 12: 16 1 DCB Decachlorobiphenyl( Surr) 77 20- 137 04113120 13: 51 04114120 12: 16 1 Eurofins Calscience LLC
1145
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 6010B - Metals ( ICP)
Client Sample ID: B11- 0. 5 Lab Sample ID: 570- 25623- 1 Date Collected: 04/ 13/ 20 09: 52 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 10. 2 0. 495 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2018. 24 1 IClient Sample ID: 11311- 3. 0 Lab Sample ID: 570- 25623- 2 Date Collected: 04/ 13/ 20 10: 11 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 2. 44 0. 513 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2018: 30 1 Client Sample ID: B12- 0. 5 Lab Sample ID: 570- 25623- 3 Date Collected: 04/ 13/ 20 10: 20 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 19. 6 0. 510 mg/ Kg 04/ 1312013: 30 04/ 13/ 2018: 32 1 Client Sample ID: B12- 3. 0 Lab Sample ID: 570- 25623- 4 Date Collected: 04/ 13/ 20 10: 33 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 4. 07 0. 493 mg/ Kg 04/ 1312013: 30 04/ 13/ 2018: 34 1 Client Sample ID: B13- 0. 5 Lab Sample ID: 570- 25623- 5 Date Collected: 04/ 13/ 20 09: 32 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 18. 0 0. 488 m9/ K9 04/ 13/ 2013: 30 04/ 13/ 2018: 36 1 Client Sample ID: B13- 3. 0 Lab Sample ID: 570- 25623- 6 Date Collected: 04/ 13/ 20 09: 55 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 4. 02 0. 495 m9/ K9 04/ 13/ 2013: 30 04/ 13/ 2018: 38 1 Client Sample ID: 1314- 0. 5 Lab Sample ID: 570- 25623- 7 Date Collected: 04/ 13/ 20 08: 45 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 4. 64 0. 498 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2018: 41 1 Client Sample ID: B14- 3. 0 Lab Sample ID: 570- 25623- 8 Date Collected: 04/ 13/ 20 09: 10 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 3. 57 0. 493 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2018: 55 1 Client Sample ID: B15- 0. 5 Lab Sample ID: 570- 25623- 9 Date Collected: 04/ 13/ 20 07: 42 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 11. 3 0. 490 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2018: 57 1 Eurofins Calscience LLC
1146
Client Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 6010B - Metals ( ICP)
Client Sample ID: B15- 3. 0 Lab Sample ID: 570- 25623- 10 Date Collected: 04/ 13/ 20 07: 56 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 10. 9 0. 505 mg/ Kg 04/ 13/ 20 13: 30 04/ 13/ 20 18: 59 1 ' Client Sample ID: B16- 0. 5 Lab Sample ID: 570- 25623- 11 Date Collected: 04/ 13/ 20 08: 06 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 9. 86 0. 503 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2019: 01 1 Client Sample ID: B16- 3. 0 Lab Sample ID: 570- 25623- 12 Date Collected: 04/ 13/ 20 08: 22 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 5. 05 0. 521 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2019: 04 1 Client Sample ID: 1317- 0. 5 Lab Sample ID: 570- 25623- 13 Date Collected: 04/ 13/ 20 08: 36 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 4. 08 0. 493 mg/ Kg 04/ 1312013: 30 04/ 13/ 2019: 06 1 Client Sample ID: B17- 3. 0 Lab Sample ID: 570- 25623- 14 Date Collected: 04/ 13/ 20 08: 55 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 3. 06 0. 488 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2019: 08 1 Client Sample ID: B18- 0. 5 Lab Sample ID: 570- 25623- 15 Date Collected: 04/ 13/ 20 08: 04 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 10. 5 0. 485 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2019: 10 1 Client Sample ID: B18- 3. 0 Lab Sample ID: 570- 25623- 16 Date Collected: 04/ 13/ 20 08: 14 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead 11. 0 0. 505 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2019: 12 1 Eurofins Calscience LLC
1147
Surrogate Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC)
Matrix: Solid Prep Type: Total/ NA
Percent Surrogate Recovery( Acceptance Limits)
TCX1 DCB1
Lab Sample ID Client Sample ID 23- 124) ( 20- 137)
67045623- 1 B11- 0. 5 64 63
570- 25623- 1 B11- 0. 5 42 70
570- 25623- 2 B11- 3. 0 66 67
570- 25623- 3 B12- 0. 5 69 71
I570- 25623- 3 B12- 0. 5 68 70
570- 25623- 4 B12- 3. 0 62 66
570- 25623- 5 B13- 0. 5 68 68
570- 25623- 5 B13- 0. 5 63 68
570- 25623- 6 B13- 3. 0 57 63
570- 25623- 7 B14- 0. 5 66 70
570- 25623- 7 B14- 0. 5 63 66
570- 25623- 8 B14- 3. 0 46 46
570- 25623- 9 B15- 0. 5 60 58
570- 25623- 10 B15- 3. 0 75 75
570- 25623- 11 B16- 0. 5 60 58
570- 25623- 12 B16- 3. 0 68 69
570- 25623- 13 B17- 0. 5 53 51
570- 25623- 13 MS B17- 0. 5 60 60
570- 25623- 13 MSD B17- 0. 5 69 70
570- 25623- 14 B17- 3. 0 57 60
570- 25623- 15 B18- 0. 5 63 66
570- 25623- 16 B18- 3. 0 79 77
LCS 570- 62818/ 2- A Lab Control Sample 86 86
LCSD 570- 62818/ 3- A Lab Control Sample Dup 86 89
MB 570- 62818/ 1- A Method Blank 86 87
Surrogate Legend
TCX= Tetrachloro- m- xylene
DCB= DCB Decachlorobiphenyl( Surr)
Eurofins Calscience LLC
1148
QC Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC)
Lab Sample ID: MB 570- 62818/ 1- A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
MB MB
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 4, 4'- DDE ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 4, 4'- DDT ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Aldrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Ialpha- Chlordane ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 beta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Chlordane ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 delta- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Dieldrin ND 1. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Endrin ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Heptachlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 Toxaphene ND 25 ug/ Kg 04/ 13/ 20 13: 51 04/ 14/ 20 06: 27 1 MB MB
Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 86 23- 124 04113120 13: 51 04114120 06: 27 1 DCB Decachlorobiphenyl( Surr) 87 20- 137 04113120 13: 51 04114120 06: 27 1 Lab Sample ID: LCS 570- 62818/ 2- A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
Spike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
4, 4'- DDD 25. 0 18. 61 ug/ Kg 74 50- 149
4, 4'- DDE 25. 0 19. 22 ug/ Kg 77 48- 144
4, 4'- DDT 25. 0 21. 30 ug/ Kg 85 37- 149
Aldrin 25. 0 19. 57 ug/ Kg 78 43- 139
alpha- BHC 25. 0 19. 75 ug/ Kg 79 51- 138
alpha- Chlordane 25. 0 19. 10 ug/ Kg 76 47- 136
beta- BHC 25. 0 19. 97 ug/ Kg 80 47- 135
delta- BHC 25. 0 16. 85 ug/ Kg 67 40- 146
Dieldrin 25. 0 20. 07 ug/ Kg 80 48- 141
Endosulfan 1 25. 0 19. 38 ug/ Kg 78 43- 139
Endosulfan II 25. 0 20. 08 ug/ Kg 80 48- 142
Endosulfan sulfate 25. 0 20. 51 ug/ Kg 82 47- 144
Endrin 25. 0 19. 74 ug/ Kg 79 35- 144
Endrin aldehyde 25. 0 18. 17 ug/ Kg 73 35- 138
gamma- Chlordane 25. 0 22. 12 ug/ Kg 88 33- 155
gamma- BHC 25. 0 19. 39 ug/ Kg 78 51- 137
Eurofins Calscience LLC
1149
QC Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Lab Sample ID: LCS 570- 6281812- A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
Spike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
Heptachlor 25. 0 19. 82 ug/ Kg 79 47- 137
Heptachlor epoxide 25. 0 19. 11 ug/ Kg 76 49- 135
Methoxychlor 25. 0 22. 15 ug/ Kg 89 39- 142
LCS LCS
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 86 23- 124
DCB Decachlorobiphenyl( Surr) 86 20- 137
Lab Sample ID: LCSD 570- 62818/ 3- A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
Spike LCSD LCSD Rec. RPD
Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit 4, 4'- DDD 25. 0 18. 86 ug/ Kg 75 50- 149 1 17
4, 4'- DDE 25. 0 19. 32 ug/ Kg 77 48- 144 1 18
4, 4'- DDT 25. 0 21. 55 ug/ Kg 86 37- 149 1 17
Aldrin 25. 0 19. 10 ug/ Kg 76 43- 139 2 15
alpha- BHC 25. 0 19. 32 ug/ Kg 77 51- 138 2 17
alpha- Chlordane 25. 0 18. 89 ug/ Kg 76 47- 136 1 16
beta- BHC 25. 0 18. 80 ug/ Kg 75 47- 135 6 17
delta- BHC 25. 0 16. 67 ug/ Kg 67 40- 146 1 20
Dieldrin 25. 0 19. 95 ug/ Kg 80 48- 141 1 16
Endosulfan 1 25. 0 19. 15 ug/ Kg 77 43- 139 1 16
Endosulfan 11 25. 0 19. 81 ug/ Kg 79 48- 142 1 16
Endosulfan sulfate 25. 0 20. 84 ug/ Kg 83 47- 144 2 16
Endrin 25. 0 19. 67 ug/ Kg 79 35- 144 0 18
Endrin aldehyde 25. 0 18. 32 ug/ Kg 73 35- 138 1 13
gamma- Chlordane 25. 0 21. 61 ug/ Kg 86 33- 155 2 59
gamma- BHC 25. 0 18. 89 ug/ Kg 76 51- 137 3 17
Heptachlor 25. 0 19. 42 ug/ Kg 78 47- 137 2 17
Heptachlor epoxide 25. 0 18. 81 ug/ Kg 75 49- 135 2 17
Methoxychlor 25. 0 22. 78 ug/ Kg 91 39- 142 3 17
LCSD LCSD
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 86 23- 124
DCB Decachlorobiphenyl( Surr) 89 20- 137
Lab Sample ID: 570- 25623- 13 MS Client Sample ID: B17- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits 4, 4'- DDD ND 24. 9 14. 27 ug/ Kg 55 12- 180
4, 4'- DDE 6. 0 24. 9 26. 20 ug/ Kg 81 8- 184
4, 4'- DDT ND 24. 9 26. 40 ug/ Kg 92 2- 187
Aldrin ND 24. 9 12. 22 ug/ Kg 49 9- 153
alpha- BHC ND 24. 9 12. 86 ug/ Kg 52 10- 149
alpha- Chlordane ND 24. 9 15. 08 ug/ Kg 61 9- 161
Eurofins Calscience LLC
1150
QC Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 8081A - Organochlorine Pesticides ( GC) ( Continued) Lab Sample ID: 570- 25623- 13 MS Client Sample ID: B17- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits beta- BHC ND 24. 9 13. 75 ug/ Kg 55 9- 156
delta- BHC ND 24. 9 11. 17 ug/ Kg 45 6- 162
Dieldrin ND 24. 9 14. 40 ug/ Kg 56 11- 164
Endosulfan I ND 24. 9 12. 50 ug/ Kg 50 4- 156
Endosulfan II ND 24. 9 13. 55 ug/ Kg 54 12- 161
Endosulfan sulfate ND 24. 9 13. 89 ug/ Kg 56 10- 165
Endrin ND 24. 9 13. 35 ug/ Kg 54 6- 166
Endrin aldehyde ND 24. 9 10. 57 ug/ Kg 43 1- 156
gamma- Chlordane ND 24. 9 12. 67 p ug/ Kg 51 7- 177
gamma- BHC ND 24. 9 13. 12 ug/ Kg 53 9- 154
Heptachlor ND 24. 9 12. 50 ug/ Kg 50 3- 150
Heptachlor epoxide ND 24. 9 12. 83 ug/ Kg 52 7- 169
Methoxychlor ND 24. 9 14. 63 ug/ Kg 59 8- 163
MS MS
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 60 23- 124
DCB Decachlorobiphenyl( Surr) 60 20- 137
Lab Sample ID: 570- 25623- 13 MSD Client Sample ID: B17- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62847 Prep Batch: 62818
Sample Sample Spike MSD MSD Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit 4, 4'- DDD ND 24. 8 17. 70 ug/ Kg 69 12- 180 21 79
4, 4'- DDE 6. 0 24. 8 34. 14 ug/ Kg 114 8- 184 26 76
4, 4'- DDT ND 24. 8 32. 50 ug/ Kg 117 2- 187 21 78
Aldrin ND 24. 8 14. 67 ug/ Kg 59 9- 153 18 77
alpha- BHC ND 24. 8 15. 35 ug/ Kg 62 10- 149 18 85
alpha- Chlordane ND 24. 8 18. 69 ug/ Kg 75 9- 161 21 79 beta- BHC ND 24. 8 15. 46 ug/ Kg 62 9- 156 12 78
delta- BHC ND 24. 8 13. 99 ug/ Kg 57 6- 162 22 85
Dieldrin ND 24. 8 18. 09 ug/ Kg 71 11- 164 23 77
Endosulfanl ND 24. 8 15. 68 ug/ Kg 63 4- 156 23 77
Endosulfanl) ND 24. 8 16. 12 ug/ Kg 65 12- 161 17 77
Endosulfan sulfate ND 24. 8 16. 20 ug/ Kg 65 10- 165 15 73 Endrin ND 24. 8 16. 79 ug/ Kg 68 6- 166 23 82
Endrin aldehyde ND 24. 8 12. 86 ug/ Kg 52 1- 156 19 83
gamma- Chlordane ND 24. 8 21. 03 ug/ Kg 85 7- 177 50 84 gamma- BHC ND 24. 8 15. 66 ug/ Kg 63 9- 154 18 79
Heptachlor ND 24. 8 15. 17 ug/ Kg 61 3- 150 19 85
Heptachlor epoxide ND 24. 8 15. 83 ug/ Kg 64 7- 169 21 79 Methoxychlor ND 24. 8 18. 03 ug/ Kg 73 8- 163 21 78
MSD MSD
Surrogate Recovery Qualifier Limits
Tetrachloro- m- xylene 69 23- 124
DCB Decachlorobiphenyl( Surr) 70 20- 137
Eurofins Calscience LLC
1151
QC Sample Results
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method: 6010B - Metals ( ICP)
Lab Sample ID: MB 570- 62809/ 1- A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62736 Prep Batch: 62809
MB MB
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac Lead ND 0. 503 mg/ Kg 04/ 13/ 2013: 30 04/ 13/ 2018: 05 1 Lab Sample ID: LCS 570- 62809/ 2- A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62736 Prep Batch: 62809
ISpike LCS LCS Rec.
Analyte Added Result Qualifier Unit D % Rec Limits
Lead 24. 6 21. 93 mg/ Kg 89 80. 120
Lab Sample ID: LCSD 570- 62809/ 3- A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62736 Prep Batch: 62809
Spike LCSD LCSD Rec. RPD
Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit Lead 24. 9 22. 13 mg/ Kg 89 80- 120 1 20
Lab Sample ID: 570- 25623- 1 MS Client Sample ID: B11- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62736 Prep Batch: 62809
Sample Sample Spike MS MS Rec.
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits Lead 10. 2 25. 6 37. 62 mg/ Kg 107 75- 125
Lab Sample ID: 570- 25623- 1 MSD Client Sample ID: B11- 0. 5 Matrix: Solid Prep Type: Total/ NA
Analysis Batch: 62736 Prep Batch: 62809
Sample Sample Spike MSD MSD Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Lead 10. 2 25. 3 37. 94 mg/ Kg 110 75- 125 1 20
Eurofins Calscience LLC
1152
QC Association Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 GC Semi VOA
Prep Batch: 62818
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25623- 1 B11- 0. 5 Total/ NA Solid 3545
570- 25623- 2 B11- 3. 0 Total/ NA Solid 3545
570- 25623- 3 B12- 0. 5 Total/ NA Solid 3545
570- 25623- 4 B12- 3. 0 Total/ NA Solid 3545
570- 25623- 5 B13- 0. 5 Total/ NA Solid 3545
570- 25623- 6 B13- 3. 0 Total/ NA Solid 3545
570- 25623- 7 B14- 0. 5 Total/ NA Solid 3545
570- 25623- 8 B14- 3. 0 Total/ NA Solid 3545
570- 25623- 9 B15- 0. 5 Total/ NA Solid 3545
570- 25623- 10 B15- 3. 0 Total/ NA Solid 3545
I570- 25623- 11 B16- 0. 5 Total/ NA Solid 3545
570- 25623- 12 B16- 3. 0 Total/ NA Solid 3545
570- 25623- 13 B17- 0. 5 Total/ NA Solid 3545
570- 25623- 14 B17- 3. 0 Total/ NA Solid 3545
570- 25623- 15 B18- 0. 5 Total/ NA Solid 3545
570- 25623- 16 B18- 3. 0 Total/ NA Solid 3545
MB 570- 62818/ 1- A Method Blank Total/ NA Solid 3545
LCS 570- 62818/ 2- A Lab Control Sample Total/ NA Solid 3545 LCSD 570- 62818/ 3- A Lab Control Sample Dup Total/ NA Solid 3545 570- 25623- 13 MS B17- 0. 5 Total/ NA Solid 3545
570- 25623- 13 MSD B17- 0. 5 Total/ NA Solid 3545
Analysis Batch: 62847
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25623- 1 B11- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 1 611- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 2 B11- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 3 B12- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 3 B12- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 4 B12- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 5 B13- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 5 B13- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 6 B13- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 7 B14- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 7 B14- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 8 B14- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 9 B15- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 10 B15- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 11 B16- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 12 B16- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 13 B17- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 14 B17- 3. 0 Total/ NA Solid 8081A 62818
570- 25623- 15 B18- 0. 5 Total/ NA Solid 8081A 62818
570- 25623- 16 B18- 3. 0 Total/ NA Solid 8081A 62818
MB 570- 62818/ 1- A Method Blank Total/ NA Solid 8081A 62818 LCS 570- 62818/ 2- A Lab Control Sample Total/ NA Solid 8081A 62818 LCSD 570- 62818/ 3- A Lab Control Sample Dup Total/ NA Solid 8081A 62818 570- 25623- 13 MS B17- 0. 5 Total/ NA Solid 8081A 62818 570- 25623- 13 MSD B17- 0. 5 Total/ NA Solid 8081A 62818 Eurofins Calscience LLC
1153
QC Association Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Metals
Analysis Batch: 62736
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25623- 1 B11- 0. 5 Total/ NA Solid 6010B 62809
570- 25623- 2 B11- 3. 0 Total/ NA Solid 6010E 62809
570- 25623- 3 B12- 0. 5 Total/ NA Solid 6010B 62809
570- 25623- 4 B12- 3. 0 Total/ NA Solid 6010B 62809
570- 25623- 5 B13- 0. 5 Total/ NA Solid 6010B 62809
570- 25623- 6 B13- 3. 0 Total/ NA Solid 6010E 62809
570- 25623- 7 B14- 0. 5 Total/ NA Solid 6010B 62809
570- 25623- 8 B14- 3. 0 Total/ NA Solid 6010B 62809
570- 25623- 9 B15- 0. 5 Total/ NA Solid 6010E 62809
570- 25623- 10 B15- 3. 0 Total/ NA Solid 6010E 62809
I570- 25623- 11 B16- 0. 5 Total/ NA Solid 6010E 62809
570- 25623- 12 B16- 3. 0 Total/ NA Solid 6010B 62809
570- 25623- 13 B17- 0. 5 Total/ NA Solid 6010E 62809
570- 25623- 14 B17- 3. 0 Total/ NA Solid 6010E 62809
570- 25623- 15 B18- 0. 5 Total/ NA Solid 6010B 62809
570- 25623- 16 B18- 3. 0 Total/ NA Solid 6010B 62809
MB 570- 62809/ 1- A Method Blank Total/ NA Solid 6010E 62809 LCS 570- 62809/ 2- A Lab Control Sample Total/ NA Solid 6010B 62809 LCSD 570- 62809/ 3- A Lab Control Sample Dup Total/ NA Solid 6010B 62809 570- 25623- 1 MS B11- 0. 5 Total/ NA Solid 6010E 62809
570- 25623- 1 MSD B11- 0. 5 Total/ NA Solid 6010E 62809 Prep Batch: 62809
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 570- 25623- 1 B11- 0. 5 Total/ NA Solid 3050B
570- 25623- 2 B11- 3. 0 Total/ NA Solid 3050E
570- 25623- 3 B12- 0. 5 Total/ NA Solid 3050E
570- 25623- 4 B12- 3. 0 Total/ NA Solid 3050B
570- 25623- 5 B13- 0. 5 Total/ NA Solid 3050E
570- 25623- 6 B13- 3. 0 Total/ NA Solid 3050B
570- 25623- 7 B14- 0. 5 Total/ NA Solid 3050E
570- 25623- 8 B14- 3. 0 Total/ NA Solid 3050E
570- 25623- 9 B15- 0. 5 Total/ NA Solid 3050B
570- 25623- 10 B15- 3. 0 Total/ NA Solid 3050B
570- 25623- 11 B16- 0. 5 Total/ NA Solid 3050B
570- 25623- 12 B16- 3. 0 Total/ NA Solid 3050E
570- 25623- 13 B17- 0. 5 Total/ NA Solid 3050B
570- 25623- 14 B17- 3. 0 Total/ NA Solid 3050B
570- 25623- 15 B18- 0. 5 Total/ NA Solid 3050E
570- 25623- 16 B18- 3. 0 Total/ NA Solid 3050B
MB 570- 62809/ 1- A Method Blank Total/ NA Solid 3050B
LCS 570- 62809/ 2- A Lab Control Sample Total/ NA Solid 3050B LCSD 570- 62809/ 3- A Lab Control Sample Dup Total/ NA Solid 3050B 570- 25623- 1 MS B11- 0. 5 Total/ NA Solid 3050B
570- 25623- 1 MSD B11- 0. 5 Total/ NA Solid 3050E
Eurofins Calscience LLC
1154
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: 1311- 0. 5 Lab Sample ID: 570- 25623- 1 Date Collected: 04/ 13/ 20 09: 52 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F71J1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 07: 38 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 100 62847 04/ 14/ 20 12: 34 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050E 2. 02 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 18: 24 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1311- 3. 0 Lab Sample ID: 570- 25623- 2 Date Collected: 04/ 13/ 20 10: 11 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 1 g 10 mL 62818 04/ 13/ 20 13: 51 F71J1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 09: 45 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050E 1. 95 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 18: 30 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1312- 0. 5 Lab Sample ID: 570- 25623- 3 Date Collected: 04/ 13/ 20 10: 20 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 2 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 07: 52 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 2 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 10 62847 04/ 14/ 20 12: 48 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 1. 96 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 32 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1312- 3. 0 Lab Sample ID: 570- 25623- 4 Date Collected: 04/ 13/ 20 10: 33 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 2 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 08: 06 UHHN ECL 1 Instrument ID: GC44
Eurofins Calscience LLC
1155
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: 1312- 3. 0 Lab Sample ID: 570- 25623- 4 Date Collected: 04/ 13/ 20 10: 33 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3050B 2. 03 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 34 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1313- 0. 5 Lab Sample ID: 570- 25623- 5 Date Collected: 04/ 13/ 20 09: 32 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 10: 00 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 20 62847 04/ 14/ 20 13: 02 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 05 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 36 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1313- 3. 0 Lab Sample ID: 570- 25623- 6 Date Collected: 04/ 13/ 20 09: 55 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total NA Prep 3545 20. 1 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 08: 20 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 02 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 38 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1314- 0. 5 Lab Sample ID: 570- 25623- 7 Date Collected: 04/ 13/ 20 08: 45 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch DII Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 4 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 10: 14 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3545 20. 4 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 5 62847 04/ 14/ 20 13: 16 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 01 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 41 ULPF ECL 1 Instrument ID: ICP8
Eurofins Calscience LLC
1156
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: 1314- 3. 0 Lab Sample ID: 570- 25623- 8 Date Collected: 04/ 13/ 20 09: 10 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 4 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 08: 35 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 03 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 55 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1315- 0. 5 Lab Sample ID: 570- 25623- 9 Date Collected: 04/ 13/ 20 07: 42 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 4 g 10 mL 62818 04/ 13/ 20 13: 51 F71- 11 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 10: 28 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050E 2. 04 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 18: 57 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1315- 3. 0 Lab Sample ID: 570- 25623- 10 Date Collected: 04/ 13/ 20 07: 56 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 2 g 10 mL 62818 04/ 13/ 20 13: 51 F71- 11 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 08: 49 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050E 1. 98 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 18: 59 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1316- 0. 5 Lab Sample ID: 570- 25623- 11 Date Collected: 04/ 13/ 20 08: 06 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 10: 46 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 1. 99 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 19: 01 ULPF ECL 1 Instrument ID: ICP8
Eurofins Calscience LLC
1157
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: 1316- 3. 0 Lab Sample ID: 570- 25623- 12 Date Collected: 04/ 13/ 20 08: 22 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 09: 03 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 1. 92 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 19: 04 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1317- 0. 5 Lab Sample ID: 570- 25623- 13 Date Collected: 04/ 13/ 20 08: 36 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 0 g 10 mL 62818 04/ 13/ 20 13: 51 F71- 11 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 09: 17 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 03 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 19: 06 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1317- 3. 0 Lab Sample ID: 570- 25623- 14 Date Collected: 04/ 13/ 20 08: 55 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 1 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 09: 31 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 05 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010B 1 62736 04/ 13/ 20 19: 08 ULPF ECL 1 Instrument ID: ICP8
Client Sample ID: 1318- 0. 5 Lab Sample ID: 570- 25623- 15 Date Collected: 04/ 13/ 20 08: 04 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 3 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 11: 00 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 2. 06 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 19: 10 ULPF ECL 1 Instrument ID: ICP8
Eurofins Calscience LLC
1158
Lab Chronicle
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Client Sample ID: 1318- 3. 0 Lab Sample ID: 570- 25623- 16 Date Collected: 04/ 13/ 20 08: 14 Matrix: Solid
Date Received: 04/ 13/ 20 11: 15
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/ NA Prep 3545 20. 1 g 10 mL 62818 04/ 13/ 20 13: 51 F7U1 ECL 1 Total/ NA Analysis 8081A 1 62847 04/ 14/ 20 12: 16 UHHN ECL 1 Instrument ID: GC44
Total/ NA Prep 3050B 1. 98 g 100 mL 62809 04/ 13/ 20 13: 30 WL8G ECL 1 Total/ NA Analysis 6010E 1 62736 04/ 13/ 20 19: 12 ULPF ECL 1 Instrument ID: ICP8
Laboratory References:
ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL( 714) 895- 5494 Eurofins Calscience LLC
1159
Accreditation/ Certification Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Laboratory: Eurofins Calscience LLC
All accreditations/ certifications held by this laboratory are listed. Not all accreditations/ certifications are applicable to this report.
Authority Program Identification Number Expiration Date California Los Angeles County Sanitation 10109 09- 29- 20 Districts
California SCAQMD LAP 17LA0919 11- 30- 20
California State 2944 09- 29- 20
Guam State 20- 003R 10- 31- 20
Nevada State CA00111 07- 31- 20
Oregon NELAP CA300001 01- 29- 21
USDA US Federal Programs P330- 20- 00034 02- 10- 23
Washington State C916- 18 10- 11- 20
Eurofins Calscience LLC
1160
Method Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Method Method Description Protocol Laboratory
8081A Organochlorine Pesticides( GC) SW846 ECL 1
6010E Metals( ICP) SW846 ECL 1
3050E Preparation, Metals SW846 ECL 1
3545 Pressurized Fluid Extraction SW846 ECL 1
Protocol References:
SW846=' Test Methods For Evaluating Solid Waste, Physical/ Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ECL 1 = Eurofins Calscience LLC Lincoln, 7440 Lincoln Way, Garden Grove, CA 92841, TEL( 714) 895- 5494 Eurofins Calscience LLC
1161
Sample Summary
Client: EEC Environmental Job ID: 570- 25623- 1
Project/ Site: City of Huntington Beach/ S- 3506. 02T SDG: 17631 Lab Sample ID Client Sample ID Matrix Collected Received Asset ID 570- 25623- 1 611- 0. 5 Solid 04/ 13/ 20 09: 52 04/ 13/ 20 11: 15 570- 25623- 2 1311- 3. 0 Solid 04/ 13/ 2010: 11 04/ 13/ 20 11: 15 570- 25623- 3 B12- 0. 5 Solid 04/ 13/ 2010: 20 04/ 13/ 20 11: 15 570- 25623- 4 B12- 3. 0 Solid 04/ 13/ 2010: 33 04/ 13/ 20 11: 15 570- 25623- 5 B13- 0. 5 Solid 04/ 13/ 20 09: 32 04/ 13/ 20 11: 15 570- 25623- 6 1313- 3. 0 Solid 04/ 13/ 20 09: 55 04/ 13/ 20 11: 15 570- 25623- 7 B14- 0. 5 Solid 04/ 13/ 20 08: 45 04/ 13/ 20 11: 15 570- 25623- 8 B14- 3. 0 Solid 04/ 13/ 20 09: 10 04/ 13/ 20 11: 15 570- 25623- 9 B15- 0. 5 Solid 04/ 13/ 20 07: 42 04/ 13/ 20 11: 15 570- 25623- 10 B15- 3. 0 Solid 04/ 13/ 20 07: 56 04/ 13/ 20 11: 15 570- 25623- 11 B16- 0. 5 Solid 04/ 13/ 20 08: 06 04/ 13/ 20 11: 15 570- 25623- 12 B16- 3. 0 Solid 04/ 13/ 20 08: 22 04/ 13/ 20 11: 15 570- 25623- 13 1317- 0. 5 Solid 04/ 13/ 20 08: 36 04/ 13/ 20 11: 15 570- 25623- 14 1317- 3. 0 Solid 04/ 13/ 20 08: 55 04/ 13/ 20 11: 15 570- 25623- 15 B18- 0. 5 Solid 04/ 13/ 20 08: 04 04/ 13/ 20 11: 15 570- 25623- 16 B18- 3. 0 Solid 04/ 13/ 20 08: 14 04/ 13/ 20 11: 15 i
Eurofins Calscience LLC
1162
25623
17440 LINCOLN WAY CHAIN OF CUSTODY RECORD
im"
y'
GARDEN GROVE, CA 92841- 1427 DATE: 4/ ZOZO
TEL:( 714) 8955
570- 25623 Chain of Custody
494. FAX:( 714) 894- T501 PAGE: 1 OF
LABORATORY CLIENT:
EEC Environmental
CLIENT PROJECT NAME/ NUMBER: P. O. NO.:
ADDRESS: City of Huntington Beach/ S- 3506. 02T OG3
One City Blvd. West
1 est# 1800 PROJECT CONTACT: LAB CONTACT OR QUOTE NO.:
CITY.
Orange
STATE
CA
ZIP:
92868 Laura Holder/Allison Bumap
SAMPLER( S):( SIGNATURE) LAB USE ONLY
TEL (
714) 667- 2300
FAX. (
714) 667- 2310
E- MAIL
Gt
TURNAROUND TIME:
SAME DAY 24 HR 48 HR 72 HR 5 DAYS 10 DAYS EQUESTED ANALYSIS
SPECIAL REQUIREMENTS( ADDITIONAL COSTS MAY APPLY)
RWQCB REPORTING ARCHIVE SAMPLES UNTIL _/
SPECIAL INSTRUCTIONS:
Email results to Ihoider@eecenvironmental. com & abumap@eecenvironmentai. com CDQ m
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06101/ 10 Rev' Ision
7440 LINCOLN WAY CHAIN OF CUSTODY RECORD
GARDEN GROVE, CA 92 841- 1 427 DATE: 4/1,12020
TEL:( 714) 895- 5494. FAX:( 714) 894- 7501 PAGE: OF LABORATORY CLIENT.,
EEC Environmental
CLIENT PROJECT NAME/ NUMBER:
I-
P. O. NO.:
ADDRESS: City of Huntington Beach/ S- 3506. 02T t' l
One City Blvd. West# 1800 PROJECT CONTACT: LAB CONTACT OR QUOTE NO.:
CITY:
Orange
STATE:
CA
ZIP:
92868 Laura Holder/ Allison Burnap I
SAMPLER( S):( SIGNATURE) LAB USE ONLY
T (
714) 667- 2300
FAX: (
714) 667- 231
IL:EL:
11:11:1 1-11:1
TURNAROUND TIME:
Ri& ESTED ANALYSIS
11 SAME DAY 0 24 HR 048HR 072HR 05DAYS 010DAYS
SPECIAL REQUIREMENTS( ADDITIONAL COSTS MAY APPLY)
0 RWQCB REPORTING 0 ARCHIVE SAMPLES UNTIL
SPECIAL INSTRUCTIONS:
Email results to[ holder@eecenvironmental. com & abumap@eecenvironmental. com 0 0co
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LAB LOCATION SAMPLING NO. 0) ( 0 '
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Login Sample Receipt Checklist
Client: EEC Environmental Job Number: 570- 25623- 1
SDG Number: 17631
Login Number: 25623 List Source: Eurofins Calscience
List Number: 1
Creator: Soriano, Precy
Question Answer Comment
Radioactivity wasn' t checked or is</= background as measured by a survey N/ A meter.
The cooler' s custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True Is the Field Sampler' s name present on COC? True
There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time( excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/ times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol. for all requested analyses, incl. any requested True MS/ MSDs
Containers requiring zero headspace have no headspace or bubble is True 6mm ( 1/ 4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/ A
Eurofins Calscience LLC 1165
0 I
e u rof i n s
Clsciene
ANALYTICAL REPORT
Eurofins Calscience LLC
7440 Lincoln Way
Garden Grove, CA 92841
Tel: ( 714) 895- 5494
Laboratory Job ID: 570- 25647- 1
Client Project/ Site: City of Huntington Beach / S- 3506. 02T For:
EEC Environmental
One City Blvd
Suite 1800
Orange, California 92868
Attn: Laura Holder
0 OW-
Authorized for release by:
411512020 8: 37. 11 AM
Stephen Nowak, Project Manager 1
714) 895- 5494
stephennowak@eurofinsus. com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample( s) as received by the laboratory. 1166 Client: EEC Environmental Laboratory Job ID: 570- 25647- 1 Project/ Site: City of Huntington Beach/ S-3506. 02T
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Definitions/ Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 Eurofins UWdence LLC
Definitions/ Glossary
Client: EEC Environmental Job ID: 570- 25647- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.
E Result exceeded calibration range.
F1 MS and/ or MSD recovery exceeds control limits.
p The% RPD between the primary and confirmation column/ detector is> 40%. The lower value has been reported.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report. u
Listed under the" D" column to designate that the result is reported on a dry weight basis R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio( normalized absolute difference) Dil Fac Dilution Factor
DL Detection Limit( DoD/ DOE)
DL, RA, RE, IN Indicates a Dilution, Re- analysis, Re- extraction, or additional Initial metals/ anion analysis of the sample DLC Decision Level Concentration( Radiochemistry)
EDL Estimated Detection Limit( Dioxin)
LOD Limit of Detection( DoD/ DOE)
LOQ Limit of Quantitation( DoD/ DOE)
MDA Minimum Detectable Activity( Radiochemistry)
MDC Minimum Detectable Concentration( Radiochemistry)
MDL Method Detection Limit
ML Minimum Level( Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit( or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio( Radiochemistry)
RL Reporting Limit or Requested Limit( Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor( Dioxin)
TEQ Toxicity Equivalent Quotient( Dioxin)
Eurofins Calscience LLC
1168
Case Narrative
Client: EEC Environmental Job ID: 570- 25647- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Job ID: 570- 25647- 1
Laboratory: Eurofins Calscience LLC
I
Narrative
Job Narrative
570- 25647- 1
Comments
No additional comments.
Receipt
The samples were received on 4/ 13/2020 2:07 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2. 11 C.
GC Semi VOA
Method 8081A: The matrix spike, and matrix spike duplicate( MS/ MSD) associated with preparation batch 570- 62993 and analytical batch 570- 62847 were out of control limit. Due to the additional level of 4,4'- DDE and 4,4'- DDT present in the spiked samples, the concentration of 4, 4'- DDE and 4, 4'- DDT in the MS/ MSD was above the instrument calibration range.
Method 8081A: The matrix spike/ matrix spike duplicate( MS/ MSD) recoveries for preparation batch 570- 62993 and analytical batch 570- 62847 were outside control limits. Sample matrix interference and/ or non- homogeneity are suspected because the associated laboratory control sample( LCS) recovery was within acceptance limits.
Method 8081A: The continuing calibration verification ( CCV) associated with batch 570- 63013 recovered above the upper control limit for alpha- BHC and gamma- BHC. The samples associated with this CCV were non- detects for the affected analytes; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/ Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/ Glossary page.
Eurofins Caft fl:ience LLC
Detection Summary
Client: EEC Environmental Job ID: 570- 25647- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Client Sample ID: 137- 0. 5 Lab Sample ID: 570- 25647- 1 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDD 32 p 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDE 3100 500 ug/ Kg 100 8081A Total/ NA
I
4, 4'- DDT 1300 500 ug/ Kg 100 8081A Total/ NA
Toxaphene 1600 p 25 ug/ Kg 1 8081A Total/ NA
Lead 30. 0 0. 495 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 137- 3. 0 Lab Sample ID: 570- 25647- 2 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 16 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDT 6. 6 5. 0 ug/ Kg 1 8081A Total/ NA
Lead 5. 16 0. 503 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 138- 0. 5 Lab Sample ID: 570- 25647- 3 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4114'- DDE 270 50 ug/ Kg 10 8081A Total/ NA
4, 4'- DDT 63 50 ug/ Kg 10 8081A Total/ NA
Dieldrin 1. 5 1. 0 ug/ Kg 1 8081A Total/ NA
Toxaphene 110 p 25 ug/ Kg 1 8081A Total/ NA
Lead 25. 0 0. 513 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 138- 3. 0 Lab Sample ID: 570- 25647- 4 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 13 5. 0 ug/ Kg 1 8081A Total/ NA
Lead 2. 45 0. 505 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 139- 0. 5 Lab Sample ID: 570- 25647- 5 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 17 5. 0 ug/ Kg 1 8081A Total/ NA
4, 4'- DDT 9. 6 5. 0 ug/ Kg 1 8081A Total/ NA
Lead 9. 59 0. 493 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 139- 3. 0 Lab Sample ID: 570- 25647- 6 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 3. 33 0. 495 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 11310-0. 5 Lab Sample ID: 570- 25647- 7 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type 4, 4'- DDE 770 500 ug/ Kg 100 8081A Total/ NA
4, 4'- DDT 410 100 ug/ Kg 20 8081A Total/ NA
alpha- Chlordane 1. 8 p 1. 0 ug/ Kg 1 8081A Total/ NA
Toxaphene 500 25 ug/ Kg 1 8081A Total/ NA
Lead 47. 3 0. 488 mg/ Kg 1 6010B Total/ NA
Client Sample ID: 1310- 3. 0 Lab Sample ID: 570- 25647- 8 Analyte Result Qualifier RL Unit Dil Fac D Method Prep Type Lead 2. 54 0. 483 mg/ Kg 1 6010B Total/ NA
This Detection Summary does not include radiochemical test results.
Eurofins Calscience LLC
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Client Sample Results
Client: EEC Environmental Job ID: 570- 25647- 1
Project/ Site: City of Huntington Beach/ S-3506. 02T
Method: 8081A - Organochlorine Pesticides ( GC)
Client Sample ID: B7- 0. 5 Lab Sample ID: 570- 25647- 1 Date Collected: 04/ 13/ 20 12: 25 Matrix: Solid
Date Received: 04/ 13/ 20 14: 07
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD 32 p 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16. 37 1 4, 4'- DDE 3100 500 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 47 100 I4, 4'- DDT 1300 500 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 47 100 Aldrin ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 beta- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Chlordane ND 25 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 delta- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Dieldrin ND 1. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Endosulfan II ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Endrin ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 gamma- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Heptachlor ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Heptachlor epoxide ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Methoxychlor ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Toxaphene 1600 p 25 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 37 1 Surrogate Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro- m- xylene 62 23- 124 04114120 09: 27 04114120 16: 37 1 Tetrachloro- m- xylene 65 23- 124 04114120 09: 27 04114120 16: 47 100 DC8 Decachlorobiphenyl( Surr) 75 p 20- 137 04114120 09: 27 04114120 16: 37 1 DCB Decachlorobiphenyl( Surr) 66 20- 137 04114120 09: 27 04114120 16: 47 100 Client Sample ID: 1137-3. 0 Lab Sample ID: 570- 25647- 2 Date Collected: 04/ 13/ 20 12: 43 Matrix: Solid
Date Received: 04/ 13/ 20 14: 07
Analyte Result Qualifier RL Unit D Prepared Analyzed Dil Fac 4, 4'- DDD ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 4, 4'- DDE 16 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 4, 4'- DDT 6. 6 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Aldrin ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 alpha- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 alpha- Chlordane ND 1. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 beta- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Chlordane ND 25 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 delta- BHC ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Dieldrin ND 1. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Endosulfan I ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Endosulfan 11 ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Endosulfan sulfate ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Endrin ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Endrin aldehyde ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Endrin ketone ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 gamma- Chlordane ND 5. 0 ug/ Kg 04/ 14/ 20 09: 27 04/ 14/ 20 16: 22 1 Eurofins Calscience LLC
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