Burbank City Council
June 2, 2026

\ .

1. A
time,
total
and
of
boring
six ( 6) soil test borings are required at this locations are identified below. a) One (1) boring is to be completed adjacent cutting machine to steel of the workshop. station located in the north east portion b) One ( 1) boring is to be completed adjacent cutting machine to steel of the workshop. station located in the southern portion c) One (1) boring is to be completed adjacent cutting machine st~tion to steel lQc.ated of the workshop. .. in tbe western portion Two (2} are to be drilled outside of immediate the workshop but adjacent machine station to the cutting workshop. located in the western portion of the
d) one
area
boring ls to be completed at in-house mair1tenance located in the northern portion or the facility.

2. Soil
surface samples
at each
must be taken at 1, 5, and 10 feet below land
be analyzed after
test boring location. All soil samples must
all laboratory analysis
a protocol is to be developed and to specify
all soil samples are
to be completed. M1nimum analyses of
petroleum hydrocarbons to include EPA Method 418.1 for total volatile organics. and EPA Methods 8010/8020 or 8260 for

3. In-house
the workshop maintenance
must be
area located in the northern portion of retrofitted material from in order to prevent waste infiltrating through surface throughout the asphalt concrete this area • . .. 4-; ·Please
underground submit
storage
a .. copy of the final report for former
your workplan. tank removal and related soil testing with Four
identified copies
above
of the workplan containing all of the information
If you have any questions
are due to this Regional Board by August 17, 1990. concerning Mr. Yue Ronq at (213) ~66-7528. this matter, please contact
~tM~tg a.cAMt~4
DAVID A. BACHAROWSKI Environmental Specialist IV
ATTACHMENT 6 - 3126
4099
Mr. Celli
Paqe J.

Enclosure
cc:

Alisa
Bill Jones - Los Angeles County, DOHS Greene - USEPA, Region IX Insp. Joe Solares - city of Burbank Fire Dept. - Fire Prevention Bureau ATTACHMENT 6 - 3127
4100

APPENDIX B

SAMPLING LOCATIONS

BORRMANN/RPT
ATTACHMENT 6 - 3128
4101
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ATTACHMENT 6 - 3129
4102

APPENDIX C

CHAIN-OF-CUSTODY SHEET

BORRMANN/RPT
ATTACHMENT 6 - 3130
4103
Envu vuhzen.~ Jtan•.tt;••J &: .c~ ... .!
Custody Transfer Record/Lab Work Request
Refrigerator# I LAB USE ONLY
#/Type Container Samples Were: Client Volume 1 Shipped or HandWork Order Preservative Delivered Date Rec'ci Date Due NOTES:

ANALYSES ~ I I 2 Amoient or Chilled Client Contact/Phone REQUESTED NOTES:

Client ID/Oescription Matrix Date I I I I LabiD Collected 3 Received BroKen! I I Leaking (lmorooeny
Sealed)
y N )
NOTES:
4 Properly Preserved
y N
NOTES:
5 Received Wi:;,rn
Holding Times
y N
NOTES:

I
CCC Tape Was: I
1 Present on Outer
Package y N
2 Unbroken on Outer
Package y N
I 3 Present on Sample y N ) Matrix: W- Water OS - Drum Solids X· Other Special Instructions: 4 Unbroken on Sample S·Soil 0-011 DL • Drum Uquids • NOTES: y N SE • Sediment A- Air F ·Fish so- Solid WI·Wipe L - EPfTCLP Leeehate
I Time I Date COC Record Was: ltemiReason Relinauished bv Received bv Date ltemiReason Relinauished bv Received bv Time 1 Present Upon Receipt of Samples Y N I I Discrepancies Between
Sample Labels and COC
Record? y N
NOTES:
-·- ----- ------ 1- --
ATTACHMENT 6 - 3131
4104

STATE OF CALIFORNIA
CALIFORNIA REGIONAl WATER QUALITY CONTROl BOARDlOS ANGELES REGION 101 CENTRE PlAZA DRIVE
MONTEREY PARK, CAliFORNIA 91754-2156
(213) 266-7500
July 25, 1990
Mr. Mark Celli
Vice President
Borrmann Steel Company
110 W. Olive Street
Burbank, CA 91502
GEORGE DEUKMEJIAN, ~ Governor
SUBSURFACE INVESTIGATION - WELL INVESTIGATION PROGRAM (FILE NO. 104.0197)
We have received your letter dated July 24, 1990, requesting additional time to submit the required Subsurface Investigation Workplan for the subject site. The additional time is requested due to the tight schedule for your company's upcoming inventory activities onsite. You are hereby granted a time extension until September 17, 1990, to submit your workplan. No further time extension will be granted.

By your request, enclosed is a partial list of consultants available to perform the engineering or geologic subsurface investigation required of you by this Regional Board. This Regional Board in no way endorses or preapproved any consultants on the list. Each consultant requested inclusion on this list and appears to have at least one staff person who meets the registration requirements of our Subsurface Investigation Guidelines. This list is not exclusive, as there are many consultants who meet the registration requirements but did not request to be included. You are free to retain the consultant of your choosing, either from this list or elsewhere.

Please note that retaining a consultant from this list does not assure acceptance of that consultant's work by this Regional Board.

The Regional Board reserves the authority to review any consultant's work to assure compliance with all applicable statutes, regulations, guidelines, and orders. It is your responsibility to ascertain that the consultant is professionally qualified and that the required work is adequately performed.

ATTACHMENT 6 - 3132
4105
Mr. Celli

If you have any questions, please contact Yue Rong at (213) 266- 7528.
~~~~·
DAVID A. BACHAROWSKI
Environmental Specialist IV
Enclosures
cc: Bill Jones - Los Angeles County, DOHS
Alisa Greene - USEPA, Region IX
Insp. Joe Solares - City of Burbank Fire Dept. - Fire
Prevention Bureau
ATTACHMENT 6 - 3133
4106
-
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ATTACHMENT 6 - 3134
4107

STATE OF CALIFORNIA
CALIFORNIA REGIONAL WATER QUALITY CONTROL BOARDLOS ANGELES REGION 101 CENTRE PLAZA DRIVE
MONTEREY PARK, CALIFORNIA 917.54-2156
(213) 266-7500
July 16, 1990
Mr. Mark Celli (21lJ i~7 .. tl6c'(..l
Vice President
Borrmann Steel Company
110 w. Olive Street
Burbank, CA 91502
GEORGE DEUKMEJIAN, Gowtmor
SUBSURFACE INVESTIGATION - WELL INVESTIGATION PROGRAM (FILE NO. 104.0197)
On May 16, 1990, your facility was inspected by members of this Regional Board staff. The inspection focused mainly on past and present methods used for handling chemicals and wastes at your facility. During the site visit, the inspectors became aware of certain situations that may have resulted in soils and potential ground water pollution. Of primary concern are the areas listed below:

1. Cutting machine areas at your facility. There were obvious signs of waste discharge to the ground throughout these areas, and there were no control mechanisms in place to contain any spilled or leaked material.

2. Maintenance equipment area, where chemicaljwaste material discharges were observed.

3. Former underground fuel storage tank area previously located at the front of your facility.

The main objective of this Agency's Well Investigation Program (WIP) is to determine possible sources contributing to pollution in nearby drinking water wells. This program is comprehensive since even small discharges may have significant additive effects on the quality .of ground water in the area. You are hereby directed to submit a workplan for conducting a Subsurface Investigation to determine whether infiltration of contaminants into soils has occurred at the area of concern identified above.

Your workplan must address all items contained within the enclosed Workplan Requirements for Initial Subsurface Engineering/Geologic Soil Investigation and incorporate the site specific requirements listed below.

ATTACHMENT 6 - 3135
4108
Mr. Celli

1. A total of six { 6) soil test borings are required at this time, and boring locations are identified below.
a) One {1) boring is to be completed adjacent to steel
cutting machine station located in the north east portion of the workshop.
b) One {1) boring is to be completed adjacent to steel
cutting machine station located in the southern portion of the workshop.
c) One {1) boring is to be completed adjacent to steel
cutting machine station located in the western portion
of,the workshop. Two {2) are to be drilled immediate
outside of the workshop but adjacent to the cutting
machine station located in the western portion of the
workshop.
d) One boring is to be completed at in-house maintenance area located in the northern portion of the facility.

2. Soil samples must be taken at 1, 5, and 10 feet below land surface at each test boring location. All soil samples must be analyzed after a protocol is to be developed and to specify all laboratory analysis to be completed. Minimum analyses of all soil samples are to include EPA Method 418.1 for total petroleum hydrocarbons and EPA Methods 8010/8020 or 8260 for volatile organics.

3. In-house maintenance area located in the northern portion of the workshop must be retrofitted in order to prevent waste material from infiltrating through the asphalt concrete surface throughout this area.

4. Please submit a copy of the final report for former
underground storage tank removal and related soil testing with your workplan.

Four copies of the workplan containing all of the information identified above are due to this Regional Board by August 17, 1990.

If you have any questions concerning this matter, please contact Mr. Yue Rong at (213) 266-7528.
~a<"Va3 ack~· DAVID A. BACHAROWSKI
Environmental Specialist IV
ATTACHMENT 6 - 3136
4109
Mr. Celli

Enclosure
cc: Bill Jones - Los Angeles County, DOHS
Alisa Greene - USEPA, Region IX
Insp. Joe Solares - City of Burbank Fire Dept. - Fire
Prevention Bureau
ATTACHMENT 6 - 3137
.\
4110
-~
.·
Consulting Geologist
4520 E. Slauson Ave .. Maywood, California 90270 - ( 21 3) 771-3046 I (213) 596-0467 March 3, 1987
Project No. 128-037
Closure Permit No. 2372 B
L.A. County File No. 13289 3E
County of Los Angeles
Department of Public Works
Waste Management Division
1540 Alcazar St.

Los Angeles, CA 90033
Attn: Ms. Kelsey Schwartz
Subject: Geotechnical Evaluation and Review
Subsurface Tank Removal
Borrman Steel
110 W. Olive Ave., Burbank, CA
for Allied Environmental Management, Inc.

Dear Ms. Schwartz,
._c
c
C.!"
::)
..

This report presents the results of a geotechnical evaluation of the subsurface storage tank removal at the referenced slte and a review of the work performed, and summary data presented _by Allied Environmental Management, Inc. A total of one
1000-gallon, leaded gasoline tank was removed February 10, 1987, by Allied Environmental Management and transported by Allied for disposal. Local fire department personnel were present to insure proper removal and transportation procedures. A summary of the work performed is presented in the appendix. Vicinity and site maps are presented in Plates 1 & 2. Upon removal of the tank, selected soil samples were taken to determine the degree of contamination in the soils below the tanks. The results of laboratory testing are presented in Plate 4, whi e the Chain of Custody Record is presented in Plate 5. No subsurface logging was performed. ..

Registered Geologist Certified Engineering Geologist
ATTACHMENT 6 - 3138
4111
128-037/ Borrman Steel/ Burbank/ 3-3-87 Page 2

SITE LOCATION AND GEOLOGY
The subject site is located on the southeast side of Olive Ave. northeast of its junction with Lake St. in the City of Burbank, County of Los Angeles. The present elevation is approximately 560 feet above sea level. The site consists of predominantly alluvial basin fill deposits associated with ephemeral stream deposition within the L.A. basin. The present courses of the Burbank Western Channel and the Los Angeles River are located less than 0.2 mile to the east and 1.5 miles to the south, respectively. The alluvial materials are generally sandy and silty in nature, though some areas contain considerable clay or gravel.

Analysis of ground water contour data on file with the County of Los Angeles indicate the ground-water level in the vicinity of the site to be on the order of 75 feet below the ground surface.

No water was encountered in the excavation.

SOIL SAMPLING AND EVALUATION
Selected soil samples were obtained from the earth materials below the tanks. Sample locations were chosen in a manner so as to provide the most complete coverage of the subsurface materials and to provide for a more complete evaluation of potential soil contamination. Special attention was given to geol~gtcal conditions which may provide for accelerated downward movement of ground water. The sample locations are depleted in Plate 2.

The sample were taken in earth materials below the removed tank.

A total of two samples, one from the east end and one from the west end, were taken from below the tank bottom at a depth of 8 feet below surface <Plate.2>. The samples were placed in glass container, sealed with tape, placed in lee to chill, and transported to Curtis ~ Tompkins, Ltd. for laboratory analysis.

The samples were tested using EPA method 8015 and for lead. The laboratory test results and the Chain of Custody Record are presented in the appendix <Plates 4 ~ 5>.

CONCLUSIONS
Review of the summary data presented by Allied Environmental Management, Chain of Custody Record, and the laboratory test results indicate the amount of contamination in the earth materials below the tank to be within the guidel1nes of the County of Los Angeles. No additional removal or treatment of the earth material is ~eemed necessary. •
J
ATTACHMENT 6 - 3139
4112
128-037/ Borrman Steel/ Burbank/ 3-3-87 Page 3

REMARKS
This investigation was made in accordance with generally accepted geologic procedures and within the limits prescribed by the client. No other warranty, expressed or implied, is made as to the professional evaluation included in this report.

Although no significant variations in bedrock or soil conditions are anticipated, if conditions are encountered during future restoration work, and these conditions appear to be different from those disclosed by this preliminary report, this office shall be notified to consider the need for modification.

The backfill at the site was compacted using on-site equipment.

While a relative degree of compaction can be obtained in this manner, the fill was not tested and does not qualify as a certified fill. Should this area be used in the future to support structural loads, steps should be taken to test and insure the competence of the fill.

It should be realized that subsurface excavations are subject to caving and may present a hazard. In this regard, all shoring and bracing, if necessary, shall conform to current standards of the Industrial Accident Commission of the State of California and other public agencies having jurisdiction.

This report is subject to review by controlling pu~lic agencies having jurisdiction.

If you have any questions, please contac~ this office.

Respectfully subm~ ~
eorge DeVries
Registered Geologist 3721
GO:ga
Distr: Addressee <1>
Allied Environmental Management, Inc. <1>
Borrman·Steel <1>
Attachments: Appendix A - Plates 1 thru 5
i
ATTACHMENT 6 - 3140
4113
Appendix A
Vicinity Map
Site Map
Closure Summary
Laboratory Test Results
Chain of Custody Record
i
ATTACHMENT 6 - 3141
4114

VICINITY MAP
from USGS Burbank Quadrangle Map
Borrman Steel
110 W. Olive Ave.

Burbank, CA
George DeVries
...
<;:onsult:lng
SCALE 1:24,000
Proj. N2 128-037
Plate 1
Geologist
I
'
ATTACHMENT 6 - 3142
4115
Bldg.

SITE MAP
Olive Ave.
1000-gal gasoline tank
SP-B@ B'~SP -A@ 8'
Bldg. Bldg.

Borrman Steel
110 W. Olive Ave.

Burbank, CA
. ..

Bldg.
.. •.

Proj. Nt 12a-o37
Plate 2
George DeVries Consulting Geologist
ATTACHMENT 6 - 3143
4116
. ·
A L L I E D ENVIRONMENTAL MANAGEMENT, INC. 8316 FIRESTONE BLVD. DOWNEY, CA, 90241.

Borrman
following Steel, 110 West Olive Ave, Burbank, has maintained the underground tank(s):

They (1) - 1,000 gal. steel tank(s) for leaded gasoline.

The decision
have requested
was
a permanent closure for the present tank(s). based on the possibility of future tank leakage that would cause a contamination of the soil.

The
signed necessary permits were obtained by an agent of ALLIED and from the proper authorities needed:

Local
City I
Health
County Fire Department - Permit on file with Dept. Services Dept. - Permit #2372-B FEB.

The tank(s) had been rendered inert and removed from the site Allied 10,1987. Tank removal and soil sampling was performed by Industrial Services. of
PROCEDURES: After a backhoe had removed soil from the bottom the excavation floor, total soil sample(s) collected:

All (2) - sample(s) taken from the (8) foot level. soil samples were transported analysis, using to Curtis & Tompkins, Ltd, for sealed, E.P.A. method(s): 8015. The sample jars were labeled, and stored in ice, including Chain-of~Cu~tody record to insure tra~eability,(SEE ATTACHED).

LABORATORY RESULTS (ANALYSIS): Analysis ~f .the soil sampling taken from the tankbed(s) revealed the following:(SEE ATTACHED). mum
According to the County Department of Public Works, the maximillion allowable level of contam~nation in soil is 100 parts per (p.p.m.). Therefore, in conclusion, evidence there is not any of soil contamination Borrman Steel Company from the original tank bed(s) of in Burbank.

Respectfully submitted,
Todd
~~ Ellertson
Office Manager ALLIED ENVIRONMENTAL MANAGEMENT, INC •
Plate 3
ATTACHMENT 6 - 3144
4117
..

Curtis & Tompkins, Ltd., Analytical Laboratories, Since 1878 - Gooch Laboratories Division -
1250 S. Boyle Ave., Los Angeles. CA 90023, Ph. (213) 269-7421 LABORATORY NO.: 20738 DAlE REPORTED: 2/20/87
2/10/87
FOR:

REPORT ON:

MARl<:

DATE RECEIVED:

ALLIED ENVIRONMENTAL MANAGEMENT INC.

TWO SOIL SAMPLES

BORRMAN STEEL
1> SP1 8' East End
2> SP2 8' West End
See attached for resLlts.

D~o Rashmi Shah, ~'botio~ La ratory Dire or
San Francisco Wilmington
EPA 8015, Lead
EPA 8015, Lead
Plate 4a
Los Angeles
'
ATTACHMENT 6 - 3145
4118
. '
Curtis & Tompkins, Ltd., Analytical Laboratories, Since 1878 - Gooch Laboratories Division -
1250 S. Boyle Ave., Los Angeles, CA 90023. Ph. (213) 269-7421 LABORATORY NO.: 20738 DATE REPORTED: 2/20/87
DATE RECEIVED: 2/10/87
FOR: ALLIED ENVIFONMENTAL MANAGEMENT INC.

REPORT ON: TWO SOIL SAM~LES
MARK: BORRMAN STEEME~HOD REFERENCES
TPH, Total Petroleum Hydrocarbons, EPA 8015
C & T ID CLIENT ID TPH (mg/kg> LEAD (mglkg)
1 SPl 1. 9 <25.0
2 SP2 <1.0 <25.0
...

Plate 4b
Son Francisco Wilmington Los Angeles
ATTACHMENT 6 - 3146
4119

CHAIN OF CUSTODY RECORD
&UilVEY i1f 6m--~ .,;;;;/ SAM~i~~ S.MJAV.,A :
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NO;'QI· -k:~o SIAJIOM
HUMID Sf4fiOH lOCAJIOH OAfl fiMl Weter 5l0.

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.... 11. .. -~.:
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::JI by: ~~-.. rn .... r R~lved b· Mobile Laborqtory for Tleld Dclte/T-.;;;; ~·. . \' onolyala: flit-•,_, . · . . I - •· ., ..

G~~Potched lly: "'" 71111 DDte/rlme Received for Labo,rat~ry by:"· Dote/Time .. I ... . • ...._ • ofti!LI-- 'I _ .. _ .a. ·r .,,IJI_ . :

Plate 5 .. ,
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ATTACHMENT 6 - 3147
4120
---
.. , . ' .

WEIGHED AT
A.M.R. Dlv. of Nat'l. Metal & Corp.

CORNER OF MISSIO a ILIKEN, ONTARIO
Vehicle Uc. No.
16445
Name,4/?d;p£a.£ 1JZ ;f/ofv:tZ DrlveroffC j-._:I?P cJ'&M·W./l tiJ.tJ ; / /, c:?PJ . .. 4U I ·. /J7tJ Material
For Scrap Purpose!'
Only
__ lbs. Gross __ lbs.Tare
__ lbs.Net
@$
___ lbs. Gross
__ lbs.Tare
•. -lbs.Net
9$:1"@$

WEIGHMASTER CERTIFICATE
-'--·--
PerTon $
THIS IS TO CERTIFY that the following described commodity wea weighed, measured, or counted by a weighmaster, whoae signature Is on this certllicetlt, whO Is a recogniZed authOrity of accuracy, ea prescribed by Chapter 7 (commencing with Section 12700) of Division 5 of the California Business and Professions COde, administered by the Division of Measurement Standards of the CaiHornia Department of Food and Agricunure.

A.M.A. Dtw. o1 Nan. Metal a 11a11 Corp., Weighmaster
CHECK II----- TOTAL$ ;&It' C'tl'r

I HEREBY STATE THAT I AM OWNER OF THE ABOVE DESCRIBED

PROPERTY OR LEGALLY AUTHORIZED TO TRANSFER OWNERSHIP
AND HEREBY DO SO ..

INVOICE I STATEMENT

KING & KING
Drain Oil Service
635 Obispo • Long Beach, CA 90814
U.S. EPA ID #CAD 981423320
(213) 439-8500
zhoi-Klo f------,-- DATE
Waste Manifest
NAME

RUNNING TOTAL
OILP.U. GAL. OUT
BS&W P.U. 'lcfk .. GAL. /6-.S
TOTAL P.U. l (,5 GAL. CASH·AMT.
/ZS PER GAL. t .Z,olo:- PRICE 0 CHECK I TOTAL P.O./I 'I PAYABLE ON RECEIPT ;/
NOTICE: Pursuant to
·'··
..
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)
ATTACHMENT 6 - 3148
4121
.., . ..
2-87
MARSHALL LIClNU NO. 269241
CONSTRUCTION CO •• INC.
2111 WUT MAGNOLIA ILYD •• IUITK 107 D IURI~Nil. CALIFORNIA 11101 D (Zll) IU·4051/14t·llll

UNCONDITIONAL WAIVER AND RELEASE

UPON FINAL PAYMENT
The undersigned has been paid in full for all labor, services, eq~ipment or material furnished to _M_a_r_s_h_a_l_l_C"7"o:-::n_s_t_r_u':::::c_t_i-:-o_n_c_o:-.-'_r_n_~_. _______ on the job (Your Customer)
of Borrmann Steel Co.
(Owner) located at
110 W. Olive, Burbank, Ca 91502 and does ~----"7"(~J-o~b-=D-e_s_c_r~ip-t~~~·o_n_):----------------- hereby waive and release any right to a mechanic's lien, stop notice, or any right against a labor and material bond on the job, except for disputed claims for extra work in the amount of $ NONE ------~----------
Dated:
. NOTICE: THIS-DOCUMENT WAIVES RIGHTS UNCONDITIONALLY AND STATES THAT YOU HAVE BEEN PAID FOR GIVING UP THOSE RIGHTS. THIS DOCUMENT IS ENFORCEABLE AGAINST YOU IF YOU SIGN IT, EVEN IF YOU HAVE NOT BEEN PAID. IF YOU HAVE NOT BEEN PA~D, ·USE A CONDITIONAL RELEASE FORM.

Form No. 7350-45
Orig. 3/85

PLEASE SIGN AND RETURN THIS COPY
ATTACHMENT 6 - 3149
4122
MARSHALL LICEHK NO. 2692 ..

CONSTRUCTION CO •• INC.

Ull WElT MAGNOLIA ILVD •• IUITK 107 0 IUIII~NK. CALIFORNIA USOI 0 (Zll) 141·40Sl/14t·llll

UNCONDITIONAL WAIVER AND RELEASE

UPON FINAL PAYMENT
The undersigned has been paid in full for all labor,
services, eq~ipment or material furnished to
~B~O~R~R~M~A~N~N~ST~E~E~L~C~O~·~--~-------------------- on the job (Your Customer) of BORRMANN STEEL CO.
(Owner)
located at
110 West Olive Ave. Burbank ca. and does ----------(~J~o~b~D~e-s_c_r~i-p~t~io~n~)~~~~~------------- hereby waive and release any right to a mechanic's lien, stop notice, or any right against a labor and material bond on the job, except for disputed claims for extra work in the amount of $ -0- ------------------------ LEEFRAN, INC. DBA Oa ted: .S7 MAR 10 PHILLIPP ASPHALT PAVING

PRESIDENT
. NOTICE: THIS-DOCUMENT WAIVES RIGHTS UNCONDITIONALLY AND STATES THAT YOU HAVE BEEN PAID FOR GIVING UP THOSE RIGHTS. THIS DOCUMENT IS ENFORCEABLE AGAINST YOU IF YOU SIGN IT, EVEN IF YOU HAVE NOT BEEN PAID. IF YOU HAVE NOT BEEN PAlO, USE A CONDITIONAL RELEASE FORM.

Form No. 7350-45
Orig. 3/85
MARSHAL[ CONSTRY"T.'"''
" Iv,• CO., INc

PLEASE SIGN AND RETURN THIS COPY
'
ATTACHMENT 6 - 3150
4123
I
) I

INSPECTION CHECKLIST

SITE NAME

ADDRESS
(J 1.0 {I VVI th Vl 1--1 s-ipe ( (b--v 01.'2~_·] 1803 ID NO. 1 'J <]Z · O ( ~ 1 'J 0. Ol:ve S"t. ' V PSD <'.S~..s
f11,).d~ A...- k, C/'1 l j' 0 '? SIC CODE ---- CONTACT M r t<: (; TELEPHONE NO. P '8 8<.2. · ... > ') 1

GENERATOR

TREATMENT

STORAGE

DISPOSAL

TRANSPORTER

ACTIVITIES
yes no
X
_x
X
y
OWNERSHIP: FEDERAL __ STATE
SITE DESCRIPTION:
0 ~{r? I c -H
'""
0 W\t' I' (
'"r ,_T
t<..v ( · ~ . o · \~ cf. ~ f
we..,
0 f ~? · / ;; d r , bb I~ (
~'J y 0 o. ( of·~
/ PRIORITY 1' - '-
INSPECTOR 9 A ,. _...,!--=------
r
PERMITS PERMIT NOS.
yes no
LOCAL AGCY __ PRIVATE
I :? )
c -:tt j
r
-
1-. I I I I . .,
DATE---~----' IJ1f?
1/r(14
ATTACHMENT 6 - 3151
4124
. ·,
-·
" I
CHECKLIST (2)

QUESTIONNAIRES
Submitted
Returned Complete/Completed
Copy Left For Submittal

OVERALL FACILITY IMPRESSIONS
Clean
Good Housekeeping Practices
No Evidence of Discharge

STORAGE AREAS
YES NO
.J
yesjno
Underground Tanks: J
permits
tested for leaks
under monitoring program \\~
Above Ground Tanks:
good condition
no appearance of discharges
Other Storage:
covered
approved containment
All Materials listed in Questionnaire

PROCESS, HANDLING, DISPOSAL
Potential for Leaks, Spills, or Discharges
Clarifier(s)
Sumps(s)
Solvents
COMMENTS (Make sure questionnaires are
page if necessary for your comments):
l - '- ~ L,c.f, -v
complete,
~r C

INSPECTOR DATE
J
use another
J
ATTACHMENT 6 - 3152
4125
.
lf
~
~
\J
{j
lJ
[
~
fl
ATTACHMENT 6 - 3153
4126
~AY 10 '90 10:43 BORRMCNN P.2
ENTER FILE NO. , OM LETTER AB104.0l97
CALIFORNJ:A REG:IONAL WATER QUALI.TY CONTROL BOARD

LOS ANGELES REGION

CHEMICAL STORAGE AND USE QUESTIONNAIRE
I. COMPANY NAME: .. B.c;!:rrmann. Steel Company
II. FAOlLITY ADDRESS: _____ l~l~O~W~·~0~1~i~ve~S~t~,--~fl~~~r~~a~~~~44.~C~b~2~l~5~0~6.---·-··----~~~~ III. FACI LITY INFORMATION
A. STlNDARD INDUSTRIAL CLASSIFICATION COOE(SIC): _____ s~o~50~-------------- . ' B. GENERATOR NUMBER(EPA/STATE) :_---JnJ£u.~P---------------- C. B:R!EF DESCRIPTION OF OPERATIONS: .. S.:t!ie1 . g:j.stci,Pution D. SEWER SYSTEM: INDUSTRIAL. ____
SEPTIC TANK. ____
MUNICIPAL x
CESS POO·L. _ _ _
WAS A DIFFERENT SEWER SYSTEM USED IN THE PAST? ______ YES I ~ ... NO I F YES SPECIFY ~YPE ------- ------- DATE. ·coNVE:RTEO_ ......... ---- E. FACILITY OWNER~--~a~ca~Ewn~t~er~p~·~~~~~s~------------~--------------~-- F. HISTORY: DATE OPERATI ONS BEGAN: ____ ~2~~6---·-·--·~--------------------- PRIOR OWNERS : w BQnmsu:m steel Co:mpan:l
IV. CHEMICAL STORAGE AND USE AT THE SITE. Complete sections A-G(page 2} for all chemicals in current use or that have been used in the past, use additional sheets if necessary. l
ATTACHMENT 6 - 3154
4127
MRY 10 '90 i0:44 BORRMRNN P. 3 .. .

A. cijtMICAL NAME: __ ~JS~O~L~Q~Mlw·--·----·-· B. COMMON/TRACE. NAME: water SolphJe Oil C. Mi2Hoo OF STORAGE: UNDERGROUND 'l'ANR_ ABOVE GROUND TANI<_x_ · J¥.RRELS-L OTHER(specif;y) ________ __... _________ _ D. QUJNTI'l'Y STORED: __ ~s~S~G~a~l~·--------~------------------~-------- none - recycled th~ough t he saw E. W~~E DISPOSAL METHOD: SEWERED_ HAULE:D_ ONSITE DISPOSAL __ F. IS ... THE WASTE TREATEO . PRIOR TO DISPOSAL: YES_ NO_ If yes, method of .treatment: __________________ _ G. IS THE WASTE STORSO PRIOR TO DISPOSAL: . · . YEs~ . NO_ A. CHB:MICAL NAME: _________ _ B. COMMON/TRADE · NAME: _____ _ C. ME'biOD ~~---
OF STORAGE: OTHER(specify) UNDERGROUND TANK_ ABOVE GROUND TANK_ ____________________________________ _ D. QU~TIT¥ STORED: _____________________________________________ _ E. W,¥TE DISPOSAL METHOD: SEWEREO_ HAULED_ ONSITE DISPOSAL_ F. I$ ,THE WASTE TREATED PRIOR TO DISPOSAL: YES_ NO_
It.: yes, method of treatment:----.------~------------
G. IS .THE WASTE STORED PRIOR TO DISPOSAL: YES_ NO_
A. H~!CAL NAME: ________ _ B. COMMON/TRADEf NAME:_._' _··-·_· __ -_ ... _ .._ .. . ' . ' C. MstHOD . OF STORAGE: UNDERGROUND TANK,..._ A:SOVE GROUND TANK_ · :JAARELS_ OTHER( specify)-----------------------------

0. QUjNTITY STORED: ______________________________________________ _ E. WuTE DISPOSAL METHOD : · SEWEREO___;_ HAULED..__ ONSITE DISPOSAL_ F • IS :THE WAST!: TREATED PRIOR TO OISPOS:AL: YES_ NO_ It es, methQd of treatment: ________________ ______________ __ G. IS: THE WASTE S'l'OREO PRIOR TO DISPOSAL: YES_ NO_
2 ATTACHMENT 6 - 3155
4128
. . . . ~
tvlf=1Y 10 '90 10 : 45 BORRMANN
V. TH~· QUESTIONNAIRE SHALL· eE SI.GNED :BELOW A$ FOLLOWS:

P. 4
A . . ~n the case of corporations, by a principal executive officer at the ~evel of vice-president or his duly authorized representative if .. ~uch representative is resp9nsible ·for the overall operation of the facility, or . ·
B. ~n t .he ease of a pa.rtn•rship.; by· a qeneral partner, or c. · · :tn t he ca·se of · a sole proprietorship, · by the proprietor,· or o. J;n the case of a municipal, State, . or other public facility, by ·. e.ither a principal executive officer, ranking elected official, or ~ther duly authorized employee. ' This ql.ie¢tionnaire has been completed under penalty of perjury and, to the best of ;my knowledg·e, is true and correct.
~te: _____ M_a~-8~,_1_9_9_0 __________ _
.·.'
Printed .ame : ____ M_a_rk_R_._....c.;..eJ.;;..;l .. i _____ _ Title: __ ~ ____ _i_c_e_-P_r_e_s_id_e_n~~----------- Phone: < 21. 3 l 849 .... 6641 Contact lame: ___ s_a_rn_e_a_s __ a_b_ov_e __________ ~-- l'itle: ,' -- .,----------~~~------~-----
. '
3 ATTACHMENT 6 - 3156
4129
MAY 10 '90 10: 43 BORRMAI'lN
BORRtv~ NN STEEL COMPANY
Fax Tr ansmittal
Vo i ce I ines:. (818) 846- 7171 <2 13) 849-6641
Fa>< I i n e : ( 8 1 8 ) 84 6- 9 34 7
To :~~~~~~~~~~~~~~~~~~~~~~~~~~
Attn:~ /i~~Fax
From: £37~ R. t!a4.

Message:----------------~-------------------------------- '•
. ' Page 1 of _
P.1
ATTACHMENT 6 - 3157
4130
,.. STATE OF CALIFORNIA GEORGE OEUKMEJIAN, Governor
CALIFORNIA REGIONAL WATER QUALITY CONTROL BOARDLOS ANGELES REGION 101 CENTRE PLAZA DRIVE
MONTEREY PARK, CALIFORNIA 91754-2156
(213) 266-7500
April 20, 1990

BORRMAN STEEL COMPANY
110 w. Olive Ave.

Burbank, CA 91502
MANDATORY CHEMICAL USE QUESTIONNAIRE (FILE NO. AB104.0197) The California Regional Water Quality Control Board, Region 4, is the public agency with primary responsibility for the protection of ground and surface water quality for all beneficial uses within the region.

As part of the statewide monitoring program (AB1803) being conducted under the direction of the California Department of Health Services, ground water wells in your area have been sampled.

The results of the sampling indicate the presence of organic contaminants in the ground water.

Your facility is geographically within the area of concern and may be engaged in practices which might require the storage and use of chemicals such as solvents, oils, fuels, etc. Therefore, pursuant to Section 13267(b) of the California Water Code, you are requested to complete the attached questionnaire to provide information on past or present chemical storage or use at your facility. In addition to completing the questionnaire,' specify the type of sewer system (private, municipal, industrial) used at your site. Please return the completed questionnaire to the Regional Board by May 7, 1990. The return of this questionnaire, properly signed, is required even if no chemical is stored or used at your facility.

If you are new owners, complete the questionnaire to the best of your ability and provide available data concerning the past owners including contact and phone number.

If your facility is currently conducting or has in the past conducted an investigation associated with soil or ground water contamination, please include a copy of the findings or relevant information with the questionnaire.

If you have any questions, please call Mila Silvestre-Kleinbergs at (213) 266-7529.
4~·,.1. ' ~~DAVID A. BA~WSKI Environmental Specialist IV Enclosure
'.

ATTACHMENT 6 - 3158
4131
Environmental Managers
& Auditors, Inc.
2028 East Alosta Avenue, Suite 101
- Glendora. California 91740
Telephone: ( 818) 852-4261
Fax: (818) 852-4264
Khalid Mahmood, R.EA
Project Director
Environmental Managers
& Auditors, Inc.
2028 East Alosta Avenue, Suite 101
Glendora. California 91740
Telephone: (818) 852-4261
Fax: (818) 852-4264
J
Kllal iEI Mall"'eeel, R.E.A: R.o s s \\ra_ e \\
?n>[email protected]\ G--ee>\t€),.5.1-
Prsjest b'irseter

BORRMANN
,..-..,.S T E E L C 0 M P A N Y

STEEL DISTRIBUTORS

MARK CELLI
110 WEST OLIVE AVENUE • BURBANK,CA 91502
•Phone•
8181846-7171
2131849-6641 BORRMANN ~-.,S T E E L C 0 M P A N Y

STEEL DISTRIBUTORS
-- 110 WEST OLIVE AVENUE • BURBANK,CA 91502

MESA VERDE

ENVIRONMENTAL

CHARLES (RUS) PURCELL
Principal Geologist
P.O. Box 1225
Costa Mesa, CA 92628-1225
Telephone /714) 545-3174 • 957-()4()9
ATTACHMENT 6 - 3159
4132
ATTACHMENT 6 - 3160
4133
~TERIAL ENtERED INTO THE F~l
DATE CORRES. TO/FROM SUBJECT INITIALS
DATE
.

ATTACHMENT 6 - 3161
4134
~ • .. ..... .._. ...... '""> • .,._. 4 ..... ..-·.-;~ ....... .... - ....... 4111!* • .. ;, ...-...,.~-·.I ·. • . ' ~-~-· ~ '~ ;· . . . . . '*' MaM. --- . ..&...._ ,. ..... • ¥.41... ... ..

I, TO BE FILLED OUT BY PERSON BECEIVES THE FILE REVIEW REQUEST Request received by: _______ Date request made: 5' /"}-'S' t~\j Person(s) who wish
to review file(s) Phone number Representinq
0u-tl w~·l (A)< &/lr 1-. '>..deo o (fyou
"'·-.....

Purpose
Files desired to be reviewed (name, number): ___ \ 0;;...~...:.....--?~\""l-'--'1...._ __ ~vr'"~ '?~ ~ U -\1 <...- ~·-;-·
Appointed Requested For: Recommenced Staff
contact (proctor) Date ________ Time. ______ Assistant Execut":"iv-e~O~f~f~i-c_e_r Approval & Date: ______ _
II. TO BE FIIJ.ED OUT BY STAFF CONTACT AFTER FINAL APPOINTMENT Appointment Final
Date & Time: ___________ .staff contact Was _____ _
Staff Time Expended: _______ .Noted By Supervisor ____ _ III. TO BE FILLEQ OUT BY STAFF CONTACT WHENEVER IN-HOUSE CQPIES ABE BEQUESTEQ .
~ NO MORE THAN A TOTAL OF 10 COPIES WILL BE MADE WITHOUT -ADVA!ft!E APPROVAL BY MANAGEMENT. FURTHERMORE, NO FILES ARE TO LEAVE THE OFFICE WITHOUT EXECUTIVE OFFICER APPROVAL -- TO ~ IS ~ APPROVAL TO RBMOVB FILES!!
No. Of Copies Requested: ____ :"_~anaqement Approval: ___ _ In-house Copies $ 0.10 ........ -· . a) In-house copies: ____ _ Cost: $ ____ Paid: $ ___ _ If File(s) are to be taken from office
b) Copies By
Bonded
. Blueprinter~-----------
EXCEPT by blueprinter, Executive Officer or Assistant Executive Office
Approval __________________________ __
ATTACHMENT 6 - 3162
4135
CR~.J

LABORATORIES

INCORPORATED
. ,.

ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL • TESTING SERVICES 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • FAX 777-3926 March 18, 1991
California Regional Water Quality Control Board
Los Angeles Region
101 Centre Plaza Drive
Monterey Park, CA 91754-2156
ATTN:

RE:

Mr. David A. Bacharowski
Mr. Yue Rong
Well Investigation Program - Subsurface Investigation, Borrmann Steel Company, 110 W. Olive Street, Burbank (File No. 104.0197) - 18 soil samples submitted by Environmental Manager s & Auditors, Inc. for EPA8010/8020 testing.

Attached, please find all information identified in your letter dated March 6, 1991 regarding the above referenced matter.

If you have any questions, please feel free to contact me at (714)777-1425 or 1-800-3CROSBY.

Respectfully,
CROSBY LABORATORIES, INC.

Enclosure
cc: Cynthia Selassie, CL
Chan-Yu Chan, CL
Bill Jones - Los Angels County, DOHS
Ann Kaneshiro - Los Angeles County, DOHS
Mark Celli - Borrman Steel Company
Khalid Mohmood - Environmental Managers & Auditors
Richard Spinner- Dept. of Health Services, Water Laboratory Alisa Greene- U.S. EPA, Region IX
Approved by the State of California, Department of Health Services This report is submitted tor the exdusive use of the client to whom it is addressed. Any reproduction or use of the Laboratory's name tor advertising or publicity without authorization is prohibited.

ATTACHMENT 6 - 3163
4136
r B
I
L
L
r
T
0 SAMPLE(S)
62 1
CROSb l

LABORATORIES

INCORPORATED
(INVOICE)
ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL • TESTING SERVICES 5200 E. Hunter Street, Suite B Anaheim , Californ ia 92807 • 800/3CROSBY • FAX 777-3926 Invoice No: 9352
MARCH 20, 1991 WATER CeUJU,ITY CCWl'ROL BOARD
101 Center Plaza Drive
Monterey Park, CA 91754
-----·----------f
Account no:

ATIN: Mr. Y. Rong
P.O. No:

Project No:
""
LAB NO. ANALYlED FOR PRICE
AA14902-AA14919 Test Chromatograms @ $15 per Chromatogram $ 930.00 Analytical Data Coopilation Charge 50.00
t«> CHARGE - PROFESSICfiAL CXl1RTESY 'ID
OOVERfiltBNT AGENCY APPLIES
WE APPRECIATE YOUR BUSINESS TERMS : net 30 days INVOICE TOTAL • $ 980.00 " Past due accounts will be charged 1 112% per month ..) To assure proper credit, please return remittance copy with payment ATTACHMENT 6 - 3164
4137
THE FOLLOWING ITEMS ARE AITACHED IN THE ORDER SHOWN:

1. Analytical Data Request Form.

2. Laboratory Data File Sheet.

3. Revised Laboratory Reports for EPA-8010 and EPA-8020

4. Laboratory Report for EPA 418.1.

5. QAJQC data including laboratory control standard recoveries, matrix spike recoveries, duplicate recoveries and performance check recoveries.

6. Sample extraction sheets.

7. Method Detection Limit sheets.

8. Retention time sheets.

9. EPA 418.1 Calibration Curve.

10. Calibration standard log sheets

11. Sample chromatograms and calibration curves.

ATTACHMENT 6 - 3165
4138

ANALYTICAL DATA REQUEST FORM
ATTACHMENT 6 - 3166
4139
~
CRO~ f

LABORATORIES

INCORPORATED
ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL • TESTING SERVICES 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • FAX 777-3926

ANALYTICAL DATA REQUEST FORM
Date Requested:_0_3_/06_/_9_1 _______ _ 1 Copy 1: Mr. B. Jones - DOBS, L.A. County Requested by: Mr. D. A. Ba.charowski
Mr. Y Rong
2: Ms. A. Kaneshiro - DOBS, L.A. County
3: Mr. M. Celli - Borrmann Steel Co.
(Tel #) (213)266-7500 4: Mr. K. MohoDod - EJt&A
5: Mr. R. Spinner - DOBS, Water Lab.
6: Ms. A. Greene - U.S. EPA, Region IX
RE: Client Name: Environoental Managers & Auditors, Inc.

Project Name: 10m. STE
Project No: 0041-ol-ol
Lab ID #(s): AA14902-AA14919
Test(s) Requested: EPA-8010/EPA-8020, EPA-418.1
Release Approved by Client: Mr. Khalid Motuoood, Project Director Date: 03/12/91 TOTAL# OF PAGES ATTACHED:

1. Are copies of Laboratory Workbook for the specified samples attached? X Yes No

2. Are copies of the "Sample Queue/Sample set-up" information attached? x Yes No

3. Are copies of the "Component Table" information attached? X Yes No

4. Are copies of the "Peak Integration" information attached? x Yes No

5. Are copies of the "Data Acquisition" information attached? X Yes No

6. Is a copy of the calibration curve integration data used to quantify specified samples attached? X Yes No

7. Are the following QC chromatograms attached?
a. Reagent Blank X Yes
b. Matrix Spike X Yes
c. Duplicate Spike X Yes
d. Duplicate Run X Yes
e. QC Check Std X Yes

FOR OFFICE USE ONLY
Date Prepared: -=03=..1:....:1=8:L./=9l=--- Via: D
[!]
Certified Mail No:

Date Mailed: 03/20/91 Courier: Name:

Initials: l> 0 Fed ex: Tracking#:

CL-ADRF/Rev.91
Apptov8d by ltle State of Calltorn•a. Department of Health Serv.cas No
No
No
No
No
Pacific Delivery
Ttus report 1S subm•ned lor the exctus•ve use of the cl•ent to whom 11rs addressed Any reproduction or use ot the Laboralory·s name lor aelvt~rt•s•ng or publiCity withOut auttlouzat•on •s pronlb•led ATTACHMENT 6 - 3167
4140

LABORATORY DATA FILE SHEET
ATTACHMENT 6 - 3168
4141
CRO!. """' (

LABORATORIES

INCORPORATED
ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL • TESTING SERVICES 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • FAX 777-3926

LABORATORY DATA FILE SHEET
Client: Ell.-1 k --------~------------------- Project Manager:i/r: K· Uohrn.o~ e8 Project Name: 8 0 ~e. 5 TE # of Lab Reports:_Y=--1-+------ Report Period: From: ;!).J/7o
~I

1. Are all Report Copies made from the final report sent to the client, and are they auached?
)( Yes No

2. Are all calibration curve data along wirh blank data used for Sample results calculation au ached?
Yes No

3. Are all sample peak integration data complete and attached? Yes No

4. Are all Quality Control Data for each method used completed? Yes No

5. Are all SYSTEM AUDIT REFERENCE DATA (Data Access ID#; OC Std ID#, Sample Prep. Ref. #,·) attached?
Yes No

6. Is the QC & SYSTEM AUDIT DATA SHEET showing Accuracy & Precision Data complete and attached?
Yes No
If "YES", Data File is complete. Attach to final report and place in customer file. , OJ , , If "NO", STOP and complete before sending repon. w r NO REPORT SHALL GO OUT UNTIL ALL IS COMPLETE l
CL-LDFS-REV. 90 Approved by the State ot Cal•torn1a. Depanment of Health Serv•ces Thts report 1S subm•nad tor the exclus•ve use of the client to whom 11 •s addressed Any reproduction or use of the laboratory's name tor advert•stng or pubhc•ty without authonzaMn 1S prohibited ATTACHMENT 6 - 3169
4142
REVISED LABORATORY REPORTS FOR:

EPA-8010
EPA-8020
ATTACHMENT 6 - 3170
4143
---... ---... ---... ------ ------------~~~------------------------ --------------- ------ _j_~-~-·i_i_~~~-~-~-~5_o __________ A_n_a_)~ica1Re~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL •
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FH..ENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-050001
SOIL
AA14902
0041-01-01

BORR STE
EPA-5030 PURGE & TRAP
EMA14902
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1, 1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~ br ... - oleutomia, Dopanment of--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<lO
ND<5
ND<S
ND<20
ND<5
ND<S
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<S
ND<10
11/15/90 '
11/16/90
11119/90
11/20/90
11121190
Tl'oo ._-.,....,._lot t1o Olldusove UM oltlo dientto whom d ~~--·Any roproducllon or UN oltlo ~·,.,..lor --.g orpul)licil)o-.....,_,....,._, ..

ATTACHMENT 6 - 3171
4144
............ ............ ------- -------------~~------------------------- ~------------- ------ -~ __ fN_k~_-i_!P_x~_~_:T_·~-~ ___________ A_n_a_lyjical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-050005
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14903
0041-01-01

BORR STE
EPA-5030 PURGE & TRAP
EMA14903
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1 , 1 , 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
11/15/90~
11/16/90
11/19/90
11/20/90
11121190
Approved by ... s- ol Clilifomia, llopot1menl ol - - Thio-ia--forlheeKCIUaiveueeot"'dlontto-lla--. ,...,,.,.,_..,.,..ollhe~o-lor-.g ... p!JIIIdy--la..-.

ATTACHMENT 6 - 3172
4145
----..-.....
_______ .-..,.---____________ ..-....__,_ _______ ~---
_J_~_r_~_1_i_~-~-~-~g _________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-050010
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14904
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14904
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1, 4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1, 1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1 , 1 , 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
AjlpoYed by .. - of Celitomoa. Dopot1ment of - s.nnc..

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11115/90~
11116/90
11119/90
11120/90
11121190
Thoo ropatloa ll<ll>mll18d lor 1ho ••duo••• uM of IIMI dient to whom ft 1o --/vrt roproduc:tlon ot- oiiiMIIAborwloty'o...,. lot -..ng ot pulllidly-......,_ io ....-.

ATTACHMENT 6 - 3173
4146
___ --... ___________ .....,. ____________ ---.,._ _______ ~ __ _ _ A_A_~_·i_!_~-~-~-~-~-~--------~_A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-020001
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14905
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14905
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1, 4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1,1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1,1 , 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~ by ... Sllle ol Clolilomla, Dopor1rnenl .,_ s.r..-

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11/15/90 '
11116/90
11119/90
11/20/90
11121190
Thio '-' ,._,_ 1\:wllo exduatve -ollloc:MntiDwhom~io--. Any..-ar-olllo ~· -1\:w-.garpublic:ily --•praiii>Md.

ATTACHMENT 6 - 3174
4147
--.... ------ --------------~~------------------------ '--------------~----- =~6ft===--61=--f:_hi_!_!t_~_~A_R~-~s_D __________ A_n_a_lyjical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-020005
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14906
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14906
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1, 1 , 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~ bf ... - .. CUiomoa, Ooponment .. --

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
11/15/90'
11/16/90
11119/90
11/20/90
11121190
n.,...., • ......_ ....... ...,.._ ........ clleniiDwhomllo-.NJrropraducllanCW-GIIhe~-lor-.oinOCW~--·~· ATTACHMENT 6 - 3175
4148
------·~--------------~-------------------------- .---., ~------------- ------ =r&===o=----=-fN:_:_:Ag:..::g:..:::/:_:'to:...:..:T~:_:_:_:_:_:~~::..:::.~ __________ _:A:..__::_n_a_lyjical ReP-Qrt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-020010
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC Fll..ENAME:

AA14907
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14907
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
D ibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1, 1,1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11115/90 '
11/16/90
11119/90
11/20/90
11121190
~ 111 11e Sllle ol Calitomoa. Dopollrnent ol-s.- Thoo ropotl • ....,_lor lho ••'*'"""'- allho dienlto wham n II--· Ant roprodudlon or- ollho ~-lor -.g or pu011a1y-· ~· ATTACHMENT 6 - 3176
4149
~ --......, ~
------- -------------~~------------------------- --------------- ----- _A_il_~_i_h_7_~-~-~~_: __________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. K.HALID MAHMOOD
SAMPLE ID: BOR-040001
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14908
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14908
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene Chloride
1,1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
Approved ., .. - of California. llepol1mont of - Serviceo • TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
11/15/90 '
11/16/90
11/19/90
11/20/90
11121190
Thio repol110 l4bmCI8d"" lho OlldusNe UM oflho dlont 10 whom Mia--· /vrt repRiductian OIUM oflho ~·-far-.... otpul>licjly-· ...-.

ATTACHMENT 6 - 3177
4150
---""'---------\---------------.......
________ """"'---
_J_~_~_1_L_~-~-~_:_~~----------A __ n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-040005
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14909
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14909
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
1, 1, 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Vinyl Chloride
Apprvwd.., ... - ol Ceilfomoe. ~ ol--

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
11/15/90 ~
11/16/90
11119/90
11/20/90
11121190
Thior~ ·-lor.,. exc:l...,.. uaeol.,.cloentlllwham ••--· ,..,rwpradUclianorUMol.,.~o-lor-.oingor.,.-y-- • .,-.

ATTACHMENT 6 - 3178
4151
---~-------.-...:--------------..._~ _______ .:::::--. __ _ _ J_~-~-~-q-~_w_~-·~-~ __________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL •
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-040010
SOIL
AA14910
004-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14910
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
2-Chloroethyl vinyl ether
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-D ichloroethane
1 ,2-Dichloroethane
1,1-D ichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1, 1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1 , 1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Chloride
~~ .. -.,~~.,--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.5
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.5
ND<0.5
ND<0.5
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<2.0
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<0.2
ND<2.0
ND<2.0
11/15/90'
11116/90
11/19/90
11/20/90
11121190
Thio <-'•llbn-lorlhe exclusive- ollhedlen!I0-111-. Mr...,_ or-ollhe ~-lor-...nuorpubliclly-- • ..-.

ATTACHMENT 6 - 3179
4152
~ ~ ,..-., ------ --------------~.------------------------- L_______________ ~----- _j_~-~-·~_1_!_~-~-~-~_: __________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-030001
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14911
0041-01-01

BORR STE
EPA-5030 PURGE & TRAP
EMA14911
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
D ibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1 , 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1,1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
w- by ... - ol calilomia. Dlpollmont ol--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11/15/90 '
11116/90
11/19/90
11/20/90
11/21/90
Thil ,_. •-for h exduoNe ... olh client to whom Ill-· 1nt repnxluc:tlon or -olh ~~-lor --..ng or ..-,y--~~ prallllbd.

I
ATTACHMENT 6 - 3180
4153
-----......, ______ ___,."""' ____________ ~·-------- --...._ __ _ _ j_~-~-~-~-L-~-~-~~-~ __________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-030005
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14912
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14912
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
D ibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1, 1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1, 1 , 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~t., .. s-ol~~oi--

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11/15/90 '
11/16/90
11/19/90
11/20/90
11/21/90
Thilrwportll-lorlleudul ...... oi ....... ID-··--Ant..-OI_ol .. ~·-101--.gOtpullloclly ___ ....,__ ATTACHMENT 6 - 3181
4154
------~ ---~--------------~-------------------------- ~ ~-------------- ~ ------ _J_n_~_-i_L_~-~-~-:-~: __________ A __ n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATIN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-030010
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC Fll..ENAME:

AA14913
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14913
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1,1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~.., .. -of c.Jilamia. Depo11ment of-SeMceo

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11/15/90 '
11/16/90
11/19/90
11120/90
11/21190
Thio ._t ,.....,.._ lorlhe e..-uaeoflheclien!ID- ~~~-- lonf ropfOIM:Iion.OfUMoflhe~-IOf-.oingOfpublocllr--11~.

ATTACHMENT 6 - 3182
4155
-----"-------·.----....--------------~'-------- _...__ __ _ _ J_~-~-~-1-~-~-~-:~_~ _________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-060001
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC Fll..ENAME:

AA14914
0041-01-01

BORR STE
EPA-5030 PURGE & TRAP
EMA14914
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
1, 1,1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
11115/90 '
11/16/90
11/19/90
11120/90
11/21190
~ bJ ... - ol Clolilomle, Deponmont .. ._ Sonric»o
Thil<-'•....,_tor.,.udusiveuuol,.aoentto-hio-.An/..-oruuoi.,.Lolxnloty'o-tor-.;o;ngorpulllocilr--·~· ATTACHMENT 6 - 3183
4156
.-........ ~ .--. _...._, _...._, ------- -------------~,-------------------------- ----------- -~--~_5c_8g_~!_to_1~_:_~E_E~ ___________ A_n_a_-yjical ReP-Qrt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-060005
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14915
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14915
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1 , 1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
. '
~., ... - olc.lifomia, Depwlrnont oi--

TESTING SERVICES
COLLECTED: 11/15/90'
RECEIVED: 11/16/90
PREPARED: 11119/90
ANALYZED: 11120/90
REPORTED: 11/21190

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
TIIio,...,. .. - ........ lldusNa ... ollhecloeniiDwhom·lo-.,..,.,..-..... ol ... ~·---..r.gorpulllicily--·,..._· ATTACHMENT 6 - 3184
4157
An Ch..,ssv A ,,.. I R t -~--~:-~g_:_to_r~_:r_~~-~ ___________ n_a_I_,~ICa eP-Qr 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-060010
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14916
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14916
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1,1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1, 1 , 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
Ajlprowod by .. - al Califomio. Doponmenl al--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
11115/90 '
11116/90
11/19/90
11/20/90
11121190
Tlil._t • ....,.._ lor111eellduiNe-al111eclleni1Dwhoml•-· ,..,,.,._. .. _al111e~o-lor-.oirv .. publioily--•..-.

ATTACHMENT 6 - 3185
4158
---...., ------ ------------~~-------------------------- _Ai __ l1 __ ~_:c_88_s!_/o_r~_:_~~-~----------------------~--11 __ Ci __ l)[tic:Cll Fl~~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-010001
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14917
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14917
HALOGEN A TED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1, 4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1, 1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~byllos-ol~~oi--
. . TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<lO
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<10
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
11/15/90'
11116/90
11/19/90
11/20/90
11121190
Thiorwportia_,.,.,. • .-... ollhec:loonlll>whomlio--.,.,..-Ot ... ollho~•-lor-.olngOt~-......._.~.

ATTACHMENT 6 - 3186
4159
----,.-._---------.------------------.,.,....--------.--., ___ _ -~--~-~-~_1_!_w_:_~E_E: ___________ A_n_a_~rlica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-010005
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14918
0041-01-01

BORR STE
EPA-5030 PURGE & TRAP
EMA14918
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1 , 1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
~~.,.saw o1 Caldomia. Oepanment "'-s.rTESTING SERVICES COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg) ·
ND<S
ND<S
ND<S
ND<5
ND<S
ND<lO
ND<S
ND<S
ND<S
ND<lO
ND<5
ND<S
ND<lO
ND<5
ND<S
ND<20
ND<5
ND<S
ND<5
ND<5
ND<S
ND<S
ND<S
ND<5
ND<S
ND<lO
11/15/90 '
11116/90
11/19/90
11120/90
11121190
n. repclfl 10 ....,_lor lie exdusove uee ollie clieniiDwhom Mil-· lllty roproduclion or ueeollle '--~• ,..,.lor -.g or pu1111aty--~~ praiWbilad.

ATTACHMENT 6 - 3187
4160
---..._,--------..------------- ~-...-. _______ ,........,. ___ _ _Aft CkuSBY A ,,.. I R t -~----~-~_gR_Rt_~R_:_~-~~ ______________________ Il __ (l __ ~~~~(:(l ~~r 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-010010
MATRIX: SOIL
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

AA14919
0041-01-01

BORRSTE
EPA-5030 PURGE & TRAP
EMA14919
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromomethane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-D ichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-! ,3-Dichloropropene
Methylene Chloride
1, 1 ,2 ,2-Tetrachloroethane
Tetrachloroethene
1 , 1, 1-Trichloroethane
1 , 1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
w- by ... s... ol calitonia, Depot1ment ol-Servao

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(ug/kg)
ND<5
ND<5
ND<5
ND<5
ND<5
ND<10
ND<5
ND<5
ND<5
ND<IO
ND<5
ND<5
ND<IO
ND<5
ND<5
ND<20
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<5
ND<IO
11/15/90.
11116/90
11/19/90
11/20/90
11/21190
n..,_. .. ~tor.,.oxdusMI_ol.,.dioniiDwhomllo_.,..,,..,._.,_ol.,.~o-IIW-.gO<pullllclly--lo~.

ATTACHMENT 6 - 3188
4161
_j_~-~-~_1_!_~_:_~-·~_: ___________ A_n_a_~~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: REAGENT BLANK
MATRIX: LIQUID
LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:
004-01-01

BORRSTE
EPA-5030 PURGE & TRAP
RB112090
HALOGENATED VOLATILE ORGANICS, EPA-8010
Bromodichloromethane
Bromoform
Bromo methane
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
1, 1 , 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
Vinyl Chloride
,.,.,._.., ... -.. ~~ .. --
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED: 11/20/90
ANALYZED: 11120/90
REPORTED: 11121190

RESULTS
(ug/1)
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.2
ND<0.1
ND<0.1
ND<0.1
ND<0.2
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.3
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<0.1
ND<O.l
ND<0.1
ND<0.2
TNI report• -lor lhll exdusNe UN al lhll doenllll whom l le -· Anr reproducllon or uoaal.,. ~·-lor --.g or p&llllicily_......,_ • ..,.._.

ATTACHMENT 6 - 3189
4162
'------------~ ______ --... ___ _ An cRossv A . I R -~--~:_8o_:_t~_~A_R~-~~ _________ n_a_lyj1C3 eP-Qrt 5200 E. Hunter Street, Su1te B Anaheim, California 92807 • 714-777·1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-050001
MATRIX: SOIL
LAB#: AA14902
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC Fll..ENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14902
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit . .\p~'''-'•f'tl r . p,;· Stdlt- <1' ( i11 ,,,,. " Dt>''''''''·j·nt ('' Ht·.;ttr St"'. , ......

TESTING SERVICES
COLLECTED: 11/15/90
RECEIVED: 11/16/90
PREPARED: 11/19/90
ANALYZED: 11/20/90
REPORTED: 11/21/90

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
T~ s •e;J0'1 -~ o:,..;t;.r" lied •o· t• e ~-c·.r':>'\1:' ..t':>t- o•t••t- r_, c··t tu v.•-or·· t '"'col1ll'f'':>~t-c1 ~~.~ •e;;rod..JCI r~r o• >~'>t· u' t•·t· ~niJ•"dl'"'- · ·" t- • • .;d-t-·t ~ • ~ , ... ,,,,, 11 ••. !•·,,,, .. ,,.\ ,, :,.,•. -.. .' :• tec1 ATTACHMENT 6 - 3190
4163
~------------ ~. _______ _...._. ____ _
_ J_~-~-~_1_!_~_3_~-~~_g ___________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-050005
MATRIX: SOIL
LAB#: AA14903
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14903
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit . .\pp·o~<:-d lJ) !11;- Stiilt- t•' Cell fo•r,,c. Ot-prmn•£'''1 ot Ht•,1'rt•. ~t''''''f"~

TESTING SERVICES
COLLECTED: 11/15/90
11116/90
11/19/90
11/20/90
11121/90
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(l'g/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
Tr. ~ repo" "::-Jtor'1llf"C :or l''i;' e•.::IJS•V( .J:OE" o• l"t:." (i•f'''11U {,,,, .. ,( ,:::, d:Hlr(•':>Sf"il Ar•) 'l'PrOd.J(!.(J'l (J' u:.{· o! p-,p Liillll,fllH\ "'•.-·tlllt' !(l• cltht''l :--• f (l'' •. ,\ 1' u.rl ,,_,J'·,·· ;.tt , •. ~ ,l·,r• :· \t-',1 ATTACHMENT 6 - 3191
4164
~-----------------------~------------~--------
5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-050010
MATRIX: SOIL
LAB #: AA14904
PROJECT #: 0041-01-01
PROJECT NAME: BORR STE
SPL. PREP. METH.: EPA-5030/PURGE & TRAP
GC FILENAME: EMA14904
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1, 4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

A.pprO\~U t1, l''e State of C.ll·fort> a DeDar1me··t ~· H~'i1!1• S(·r, '"'=""

TESTING SERVICES
COLLECTED: 11/15/90
RECEIVED: 11/16/90
PREPARED: 11119/90
ANALYZED: 11/20/90
REPORTED: 11121/90

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
Tr, s "f:'P0'1 s. Sutlw.ttec 'G' 1"€' f'\CIUS•v€' .JSE.- of 1r.12 ·.1•€''"110 V~onon: I •S <1lld'i'"SSt:'iJ A!l} reprod.Jtl.u ur use of tne Lc'lbora\C/1 s. r'<'!11lt' ro rtlh€'·1 s ·~g 0 ,'_,L-,1.: t. 1\ tn.-.,,1 <1.•1''0' :at,~·- .,.. ~''•''' n 1r,1 ATTACHMENT 6 - 3192
4165
--------------------------~ -------------
_;_~-~-~_1_!_~_:_~-·~-~ ___________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street. Suite B Anaheim. California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-020001
MATRIX: SOIL
LAB#: AA14905
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14905
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit. .\,_,;1·v·t·U r)\ lilt" Stctk ,,, (c.l·hJ"1•o1 Dt";Jarlr'lt· 1 , •• Ht-diTI '-.t'"\ ,,.~ • TESTING SERVICES
COLLECTED: 11/15/90
11/16/90
11/19/90
11/20/90
11/21/90
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
T• S 't-;JV"! S S..Jbl)~ 1\e,: 'o· f 1
'E' t'>C.I.;S ~t.- ~St' 0 1 l"E' Cl·t-··tt( ~>.' ,,,-., 1 ·~ ih1flrf?'S">f'l1 Ar•, if:O•OChJ(IrOr· (H cl~t' l'' 1•, •. · ,;,•, -. •·.-'!•"• \> ,-h1lt''1., 1-, ,'A" !. ,, ! ,' ,r <'I,J!"<• ·~t ,,. ~ 1·, • ;, · ATTACHMENT 6 - 3193
4166
_...... ------ -------------- "-------------
_G_~-~-~-~-~_!_L_~_:_~~-~ ___________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-020005
MATRIX: SOIL
LAB#: AA14906
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14906
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1, 4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

ApOIO\.t'd b> trt- Stdlt: ol Cc~Liorn,eo Dt-11Z1flrl•t"'l o' Ht><1IP' ~,.,, ( t·:-

TESTING SERVICES
COLLECTED: 11115/90
11/16/90
11119/90
11120/90
11121190
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
~g/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
Tr s •e;:~ort s S.Jbn~.tted •or \11€' e(cluS·IE' use ot the cl ent to .... nom,\ •s adciTe!>Se.:l .l,n1 reprod.Kl•Or' o• u~f- of tne LatH)'f'lh"l s r·,1o"f' h.!' <>.11<-''1., "f ,,, l),d'l t 1, '' t ~.rl .'h-'I11P• ;.=;! o·· ., ,1.<'"! It•,' ATTACHMENT 6 - 3194
4167
--------------------------~ -------------
_G_~_l1 __ ~_:_;o_8:_8t_~_~A-~-~-~----------------------~--Il __ CI ___ I)[tic:CII fl~~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-020010
MATRIX: SOIL
LAB#: AA14907
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14907
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Appro~ed IJ~ lilt' State ol CallfOnlli't Departn,ent of Healtn Ser\•Ce~

TESTING SERVICES
COLLECTED: 11/15/90
11116/90
11119/90
11/20/90
11121190
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(J.Lg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
Tr, s repo'1 s s.ubrn,lled lor tre fo'.o.tlus,vt use uf tne c11ent to who1r- 11 :s addresseo An1 reproduCitOn or ust- of tne Labordtor\ s n,w-.e lo· dd\f'f!,s,,ng o• ,:ubt .. -·h ~'>.tno.;t ihJ\'lor 1at o•' s IJ'QI:.n 1e,1 ATTACHMENT 6 - 3195
4168
----.........__--------------------------"-.,-------~---- _J_~-~-~-1-~-~-~-~~-~ _________ A_n_a_~~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL CHEMICAL MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-040001
MATRIX: SOIL
LAB#: AA14908
PROJECT#: 0041-01-01
PROJECT NAME: BORR STE
SPL. PREP. METH.: EPA-5030/PURGE & TRAP
GC FILENAME: EMA14908
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Ajlproved by ... - of California. Department of-SeMcos
• TESTING SERVICES
COLLECTED: 11/15/90
RECEIVED: 11/16/90
PREPARED: 11119/90
ANALYZED: 11120/90
REPORTED: 11121190

RESULTS
(Jlg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
This report is I<DniiiBd for the exclusive use oflhe client to whom k Is-· Any reproduction or use of 1118 ~·-lor -.g or publicity--io ~- ATTACHMENT 6 - 3196
4169
-----...... _________ ..,._ _____________ -........---------~---- _J\_l1_~$_i_8R_::_~R_:_~-~~----------A_n_a_lyjical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-040005
MATRIX: SOIL
LAB#: AA14909
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14909
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit. ~by ... - al c.lifornia, Deponment al-Sorviceo
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(#'g/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11/15/90
11116/90
11/19/90
11120/90
11121190
This ropottoa ....,.,_lor 1he exclusive uae allhe client to whom M is--Ant roproduction or uae allhe ~·-lor -.oing or publicily-- is~- ATTACHMENT 6 - 3197
4170
-~ __ f:_ki_!_!t_~_~A_R~-~_o __________ A_n_a_~yjical ReP-Qrt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL CHEMICAL MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-040010
MATRIX: SOIL
LAB#: AA14910
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14910
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit. ~by .. Slaleofc.lifomie. ~of--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11/15/90
11/16/90
11119/90
11/20/90
11121190
This'-' il....,_ Ia< lho oxdusMt uoe alt. dieniiOwhom ~ 11-. Any roproduclon or uoe alt.~~ -lor -.g or polllicity--il.,..._.

ATTACHMENT 6 - 3198
4171
----~--------,..._,--------------~..---------~·----
-~--~:_ht_iR_::_riR_0:_~-~~----------A_n_a_-yjical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-030001
MATRIX: SOIL
LAB#: AA14911
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14911
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approved by 111e s- of Celilomia, Department of-SeMoos
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11/15/90
11116/90
11119/90
11/20/90
11/21190
This report,. sullmiiiBd lor 1he exdusive uae of1he c11ant to whom n is-· /lny reproduction or use of1he ~·,_lor -.g or publicity- OUihorizalian is....-.

ATTACHMENT 6 - 3199
4172
--------~--------------~~--------------------------~~~------------~-------- -~--~-~_i_!_~-~-~-~-~ __________ A_n_a_~~icaiRe~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-030005
MATRIX: SOIL
LAB#: AA14912
PROJECT #: 0041-01-01
PROJECT NAME: BORR STE
SPL. PREP. METH.: EPA-5030/PURGE & TRAP
GC FILENAME: EMA14912
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approved by lho Slate of California. Dopartment of-Senlioos

TESTING SERVICES
COLLECTED: 11/15/90
RECEIVED: 11116/90
PREPARED: 11/19/90
ANALYZED: 11120/90
REPORTED: 11121/90

RESULTS
(~tglkg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
This,_ •• ~for lho oxduswe use ollho dient to whom His-· Any reproduction or uso ollho ~·""""'for~ CK publicity-lbJthoriulion is....-.

ATTACHMENT 6 - 3200
4173
----~---------~------------- -...._._,_, -------~----
=j~~~~-~-L-~-~-~_:_~g __________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-030010
MATRIX: SOIL
LAB#: AA14913
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14913
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approved by lhe s- of California. Depar1mont of-Services

TESTING SERVICES
COLLECTED: 11/15/90
RECEIVED: 11/16/90
PREPARED: 11/19/90
ANALYZED: 11/20/90
REPORTED: 11/21/90

RESULTS
(l'g/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
This report is auiJmilbld for 1ho axdusive use ollho diont to whom~ is-· Arrt reptOduclion or use of 1ho ~·,_for -.oing "'publicity -oulloriztllian ia ~- ATTACHMENT 6 - 3201
4174
........... ..-....,_ --... ------- ---------------~------------------------- ~,------------- ------- _il_l1_~:_hi_!R_::_~R_:_~-~~----------A_n_a_~y:tical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-060001
MATRIX: SOIL
LAB#: AA14914
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14914
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approved~ ... s-of c.Jitomia. Deportment of--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11115/90
11116/90
11119/90
11120/90
11121190
This ._n osiUbmiiiBdlor.,. oxclusMO uao of.,. client to whom~ Is--·,..,., ropiOI1uction or uao of.,.~,..,. fo< ~or publicity--Is prallibllod.

ATTACHMENT 6 - 3202
4175
-... ~ """"" ------- -------------~~~------------------------- ~------------ -------- -~------~N-~~-v/_!_/o_r~_:r_1 ~-~ _______________________________ A ___ n ___ a_~~ical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-060005
MATRIX: SOIL
LAB#: AA14915
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14915
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approved by lhe Slate of c.Jifomia. Dopar1mont of - SoMcoo • TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(l'g/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11/15/90
11/16/90
11119/90
11/20/90
11121190
This rwpott ia ..--lor lhe exdusove uae of lhe ctoont to whom lis-·""" reproduction at uee of lhe ~· _.., -.oing at pulllicjly--iO .....-.

ATTACHMENT 6 - 3203
4176
-------~----------------~--------------------------~~,-------------~-------- -~--~_i_L_~-~-~-:-~: __________ A_n_a_a~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL CHEMICAL MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-060010
MATRIX: SOIL
LAB#: AA14916
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14916
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approved by ... - ol C8litomia. Department ol - Senricos

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(l'g/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11115/90
11/16/90
11/19/90
11/20/90
11/21190
This report,. aubmill8d for lie exclusive uee ollie client to wllom H 1o -·Airy reproducllon 01 uee of lie~·-for --.;ng 01 publicity wilhoul.....,._ io prolibil8d.

ATTACHMENT 6 - 3204
4177
------...---------~------------- ""' ---------.... ___ _ -~ __ f5_i_iR_:t_riR_:_~-~~ __________ A_n_a_~yjical ReP-2rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-010001
MATRIX: SOIL
LAB#: AA14917
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14917
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1, 3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit. ~~ .. -oi~.Oopar1mentoi--

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11115/90
11116/90
11119/90
11/20/90
11121190
Thio '-'is -lor tho exclusive,_ of tho client 10 whom k io --·Any--or uae ollhe ~·-lor --.gorpublic:jty- outharizllian • .,..,_.

ATTACHMENT 6 - 3205
4178
-----------------~------------- ----.....-------~----
=J=-l1-~$_i_iR_:;_~R_:_~-~~ __________ A_n_a_~yjical ReP--Qrt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL MICROBIOLOGICAL
CLIENT: ENVIRONMENTAL MANAGERS & AUDITORS, INC.

ATTN: MR. KHALID MAHMOOD
SAMPLE ID: BOR-010005
MATRIX: SOIL
LAB#: AA14918
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORRSTE
EPA-5030/PURGE & TRAP
EMA14918
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Ch lorobenzene
1, 4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Approyed br ... - "'c.lifomia. Depattmont"'--
• TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11/15/90
11/16/90
11/19/90
11/20/90
11/21/90
This ._t 10 ~tor tie OXclusMI UOO ol tie doent IOwllom K is-. Nrf roproducllon 01 U08 ol tie~·- tor --.g 01 publlcily-lllllhariz80I1 is....-.

ATTACHMENT 6 - 3206
4179
-'-------
-~--~-~_1_L_~_:_~-~~-~ ___________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL CHEMICAL MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: BOR-010010
MATRIX: SOIL
LAB#: AA14919
PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
EMA14919
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethy I Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

A.pP•O•f'lil•) \Itt- Stdlt- 11' Cnltlorn.a Dt•~lrltltHt·"l ,,! ht rtlll St''> CP~

TESTING SERVICES
COLLECTED: 11115/90
RECEIVED: 11/16/90
PREPARED: 11/19/90
ANALYZED: 11/20/90
REPORTED: 11/21/90

RESULTS
(pg/kg)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
Tr. ':> 't:-Ov'1 ~ ';..Jbl'• lltJ 1
u' tnc t•CIJ!>•vt- u!:.t cd ttto:- Cl er:t tv .,..,,c•n· I ~ adfl·.-~~t-rJ A.r 1- reproduCI•o•·. p· ,,~t' o• l'•t· Li111,•'dhl•, ~ tli1t' f '·'' •Hht'tl "''f c ••• ~.,, •, ,., tr•,l .. t ., __ :· •• •· .-.... i' t.-d ATTACHMENT 6 - 3207
4180
'-------
_J_~-~-~_1_i_~_w_:_~~-~-----------A_n_a_l~ica1Re~rt 5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL • CHEMICAL MICROBIOLOGICAL
CLIENT:

ATTN:

ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
SAMPLE ID: REAGENT BLANK
MATRIX: LIQUID
LAB#:

PROJECT#: 0041-01-01
PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

BORR STE
EPA-5030/PURGE & TRAP
RB112090
AROMATIC VOLATILE ORGANICS, EPA-8020
Benzene
Chlorobenzene
1 ,4-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,2-Dichlorobenzene
Ethyl Benzene
Toluene
Total Xylenes
ND denotes Not Detected at the indicated detection limit.

Apu•O>h1 t•, Hrf- Stt1\t· tl 1 (.-ll •o••'•<> Ot-.;J. .. ·t•··t·' t ('~ 1-1.-,-.11' -; ... ,. "'' • TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(pg/1)
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<2
ND<4
11120/90
11/20/90
11121190
T"!:. ·e:J')r'l ~ S..JO....-lll?rl lor tr ~ t-•LI'-'':1 '"' ... ~c :.' lr•t- ~l·t-~1 1: .,..r l"l' I :- i10t1•t'!>!:>t'd ~·11 't'•1iOO .. ct r•r C" ,J~t' !Jl !l't ,,il•t''"W·, ~ <~'' t' •,., <>ll\e'l.., .=. ,. ,•.rt'l, t. ,, : ,• .• : •'·''"•' :c11 .~· ~ •"• • I• t....,l ATTACHMENT 6 - 3208
4181
LABORATORY REPORT FOR EPA 418.1
ATTACHMENT 6 - 3209
4182
__ _...-...... ---------~------------- ---\-------~--···--- =d~~~~-~-~-!-~_3_~-~~-~ ___________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-050001
SOIL
AA14902
0041-01-01

BORRSTE

EXTRACTION
EMA14902

PARAMETER

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)
11115/90
11/16/90
11/19/90
11/19/90
11/21/90
Total Recoverable Petroleum Hydrocarbons, EPA-418.1 12.7 Approved by lhe Slale of CaJrtorma, Depanmern of Hoi- Servoces Thrs report •s submitted for the exduslve use ot the dleniiO whom It is addressed. Any reproduction or use or the labofak>ry's name lot actvertts~ng or publte~ty wrthoul aulhOfiZabon IS ptotublted ATTACHMENT 6 - 3210
4183
~ ~-----------------------~ ~---------
-~--~-~_1_!_h_:_~_1~_g ___________ A_n_a ___ l~ica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-050005
SOIL
AA14903
0041-01-01

BORR STE

EXTRACTION
EMA14903

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by the Stale of Calrfo~n~a, Department of Heatlh ServiCeS

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

12.4 11115/90
11/16/90
11119/90
11/19/90
11/21190
TIK roportos submoll8dlorlhe oxdusrvo use of lhe dlont 10 whom rt is addt......S. Any ropr~ or use of lhrl Laboralor{s name lor advor1151ng or publoal)' wrllloul aulhonzabon os prollboted ATTACHMENT 6 - 3211
4184
-----~---------------~~--------------------------~·--------------~---------- =G~~~~-1_!_~-~-~-~-~_g __________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-050010
SOIL
AA14904
0041-01-01

BORR STE

EXTRACTION
EMA14904

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by lhe State of Califom•a. Department of Health ServiCeS

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

14.8 11/15/90
11/16/90
11/19/90
11/19/90
11/21190
Thts report•s submitted few the exdusiVtl use of the client to whOm It is addressed. Any reproduction or use of the Labofatory's name tor advertiSing 01 pubbcrty Wflhout authonzabon lS prohibited.

ATTACHMENT 6 - 3212
4185
~~-----------~----------
=Q§=~:_:_l1=---~-£c_~8_!_io_~_:_~~-~-----------A_n_a_l}1ical ReP-Qrt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-020001
SOIL
AA14905
0041-01-01

BORRSTE

EXTRACTION
EMA14905

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by lho Slate of Caldomoa. 0epartm8flt of Health SetviC<IS

TESTING SERVICES
COLLECTED: 11/15/90
11/16/90
11119/90
11119/90
11/21190
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

17.1 This report•s wbmllted lor the exdus•ve use ot the dlent to whom il is addressed. Any reproduction or use of the LaboraiOry's name lot advertising or publte~ty without aulhonzatlon 1s prohibited.

ATTACHMENT 6 - 3213
4186
~ -.-......, ~
----- -------------- '-------------------------- '------------- ---------- -~--~-~_1_!_!_~_:_~~-~ ___________ A_n_a_lrticaiRe~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714·777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-020005
SOIL
AA14906
0041-01-01

BORRSTE

EXTRACTION
EMA14906

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Appr011od by lho Slate ol Caldom ... Department ol Heahh Seni1C8S

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

18.1 11/15/90
11116/90
11119/90
11119/90
11121190
Ttvs repott1s submitted lor the exctusrve use of the cttent 10 whom il r1 addressed. Any reproduclion or use of the Laboratory's name tor advertising or publiCity wllhoul aulhonzallOn IS prohibited.

ATTACHMENT 6 - 3214
4187
'---------------~~--------------
_J_~-~-~-~-!-~_:_~-~~-~ ___________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. K.HALID MAHMOOD
BOR-020010
SOIL
AA14907
0041-01-01

BORRSTE

EXTRACTION
EMA14907

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by lhe State of Callfomoa, !lepattmeol of Heallll S.Noees

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

10.6 11/15/90
11/16/90
11/19/90
11/19/90
11/21/90
This report •s submltled lor the exdusrwe use ot the deent to whOm it IS addressed. Any repnxtucrton or use of the LaboraiOr'y's name tor actverosang or publiCity withOut aulhonzabon IS prOhibctad ATTACHMENT 6 - 3215
4188
_Q_~_f_~-~-~-r-~_:_~E_E~ ___________ A_n_a_lrticaiRe~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1·800·3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-040001
SOIL
AA14908
0041-01-01

BORRSTE

EXTRACTION
EMA14908

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by the State of Calltooua, Department ot Heatth Serv.ces

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

14.3 11115/90
11/16/90
11119/90
11/19/90
11/21190
Thas report 15 submitted tor rile exdus1ve usa ot the cbent to whom ll•s addressed. Any reprodudlOn Of use of the LaboraiOfy's name lor advertiSing or publicity without authonzabon IS prohibited ATTACHMENT 6 - 3216
4189
-'\
~--------------------------- '--------------
=G~~~~_q_§_!_~_~_\_~_: __________ A_n_a_t~ica1Re~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800·3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR -<>40005
SOIL
AA14909
0041-01-01

BORRSTE

EXTRACTION
EMA14909

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
AjlpiDYod by lhe State of Caltlom&a, Department ol Health Setvocas

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

17.8 11/15/90
11/16/90
11119/90
11119/90
11/21/90
Thts feport 15 submlhed lor thrlexdusiV8 use ot lhe dl8fll to whom t1 11 addresaed. Any reproducbon Of use of the L.abof~loty's name tor adYitfti$10Q or publiCity Wflhout au1honzab0n 15 prohlblled ATTACHMENT 6 - 3217
4190
_J_~-~-~-~_1_;_~-~-~-~_o ___________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-040010
SOIL
AA14910
0041-01-01

BORRSTE

EXTRACTION
EMA14910

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
ApprCllllld by the Stale of Calrtomoa. Depanmenl ol Healll1 Servoces

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

17.1 11115/90
11116/90
11119/90
11119/90
11/21190
Th•s repott•s subnuned torlhe exctuswe use ot the d1ent to whom ilta addresaect Any reproduction 01 uae of thel.aboratory·s name tor adv&rOs•ng or pubhoty wrthout authonzabOn IS ptohlbtled.

ATTACHMENT 6 - 3218
4191
_:_~_~_1_1_!_~-~-~-~-~ __________ A_n_a_~~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-030001
SOIL
AA14911
0041-01-01

BORRSTE

EXTRACTION
EMA14911

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418. 1
Apprcwad by 11w1 State of CalitDmla. Department of Health Son!..,.

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

13.7 11/15/90
11/16/90
11/19/90
11/19/90
11/21/90
This repot1•s IUbfrulled tor rhe eu:tusn~e use af the diem to whom d es addles&ed. Any teproduclion 01 use ol the LaborD»ry's name tor adv8f'laSWlg or publeQty Wl'lhout aullofazatton lS prohDied.

ATTACHMENT 6 - 3219
4192
------ ~ ~ ~ -----------------~~-------------------------- ~-------------- --------- _G __ ~-~-~-~ 1 __ __ ! __ k __ : __ ~ __ 1~_g ___________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1·800·3 CROSBY • FAX 714·777·3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-030005
SOIL
AA14912
0041-01-01

BORRSTE

EXTRACTION
EMA14912

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by lhe State of Calrfom•a. Department of Health ServtceS

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

17.3 11/15/90
11/16/90
11/19/90
11119/90
11/21190
Ttus report •s subnuned tor the exdusnftl use of the dlent to whom 11 is addfessed. Arty reproductton 01 use of the l.abofatory's name lor adverttsmg Of pubhcny Wffhout aulhorizallon IS prohtbrled.

ATTACHMENT 6 - 3220
4193
------~-----------------~.---------------------------~~,--------------~--------- -~-~-~-~-~_1_!_r_w_:_:~_: ___________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-030010
SOIL
AA14913
0041-01-01

BORR STE

EXTRACTION
EMA14913

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Appr<Ned by lhe Stale of Caltfom&a, Depanmonl of Heaflll Sennces

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

17.1 11/15/90
11/16/90
11119/90
11/19/90
11121190
Tht$ repon •s submeled for 1he exdu51Ve usa ot the c:1ten1 to whom II IS addressed. Anr reproducllon Of use ot the Labot'D'lf'ts name tor adver11Stng 01 pubbcrty WithOut aulhonzabon a& prohibited ATTACHMENT 6 - 3221
4194
~ --.., -..... ------ --------------~~-------------------------- ~------------- --------- _J_~-~-·t_i_~-~-~-~-~5_o __________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. K.HALID MAHMOOD
BOR-060001
SOIL
AA14914
0041-01-01

BORRSTE

EXTRACTION
EMA14914

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by lho Slahl of CaldOITlla. Dopanmenl of Heallll Sen,aiS

TESTING SERVICES
COLLECTED: 11/15/90
11116/90
11/19/90
11/19/90
11121190
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

14.7 This repot1•s SUbmftl8d tor the exdusNe uH of the ct.en110 whom il tS addfessed. Any reproductton or use of lhe Laboratory's name IOf advertiSUlQ or pubhe~ty wllhoul ~ulhoraziibon '' ptohOtled ATTACHMENT 6 - 3222
4195
-...., --- ---------
-~--~_1_i_~-~-~-~-~5_o __________ A_n_a_l~ica1Re~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714·777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-060005
SOIL
AA14915
0041-01-01

BORRSTE

EXTRACTION
EMA14915

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by llle Slate of Caldomoa. Oepanment ol Heallh S.rvoces

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

14.4 11/15/90
11116/90
11119/90
11119/90
11/21190
Tho$ ropon os sul>mrlled tor llle e.ldusrvo use of lhe client fD wflom rt is addtessed. fV>r reptoducllon or use of lhe UiboraiOry's name for' adveriiSrng or pul>locrly wrlhoulauthonzallOn rs protllbrled.

ATTACHMENT 6 - 3223
4196
.-......_ --... --.... ------ ----------------~--------------------------- ~------------- --------- _G_~_l1 __ ~_:~_~o_g:_8t_riR_~-~-~-~----------------------~--Il __ CI __ Il[tic:CII Fl~~r1: 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC Fll..ENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-060010
SOIL
AA14916
0041-01-01

BORRSTE

EXTRACTION
EMA14916

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by 1he State of Caldom1a, Department ol Haallh SetviC8S

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

12.2 11/15/90
11/16/90
11/19/90
11/19/90
11/21190
Tilts tepon: IS 5Ubmftled tor lhe exduSNe use of the dtent to whom il es addressed. Any reproducbon or use of the Labofatory's name lor adverbs.ng or pubbaty Wflhout au1honzabon •S protllbiled ATTACHMENT 6 - 3224
4197
~ -......., -.... ------ ---------------~~------------------------- ~------------- -------- -~--~:_hi_J_!t_~_~A_R~-~5_0 __________ A_n_a_lyjical ReRQrt 5200 E. Hunter Street. Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL •
CLIENT:

ATIN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-010001
SOIL
AA14917
0041-01-01

BORR STE

EXTRACTION
EMA14917

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Approved by lhe Stale of Califorma, Department of Heatth ServiCes

TESTING SERVICES
COLLECTED: 11/15/90
11/16/90
11/19/90
11/19/90
11121/90
RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

14.5 TNs report .:. ~utmlfted tor the eadUSJve use of lh8 client to whom dIS addressed. Any reproducbon Of use of lhe Labort~toty's name t01 adVerbsmg or pubPaty wtdlout aulhonzabon IS ptotwblled ATTACHMENT 6 - 3225
4198
--...... '-------------~ -... ___ _
. _G_~_(1 __ ~_$_lo_g:_t_~_~A-~-~-~----------------------~--Il __ CI __ Il[tiC:CII fl~~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC Fll...ENAME:

CHEMICAL • MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-010005
SOIL
AA14918
0041-01-01

BORRSTE

EXTRACTION
EMA14918

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
"'PPJr<>Ved by lie Slale of CaldO<Ylla. Depaltment of Heallh 5eMces

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

11.9 11/15/90
11/16/90
11119/90
11/19/90
11121190
This report •• SUbmllted lcwlhe exclusive use ot the client 10 whom d is addressed. Any reproduction or use of the LaboraiOI'y's name lot adver1tsang or pubhclty wtlhou1 auhltiH.tton IS prohii:Mied ATTACHMENT 6 - 3226
4199
-....._ --..._ .-...... ------ -------------- ~------------------------- ~------------- -------- _d_~-~-~-~-~-1-~_w_:_~~_: ___________ A_n_a_l~icaiRe~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL
CLIENT:

ATTN:

SAMPLE ID:

MATRIX:

LAB#:

PROJECT#:

PROJECT NAME:

SPL. PREP. METH.:

GC FILENAME:

CHEMICAL MICROBIOLOGICAL
ENVIRONMENTAL MANAGERS & AUDITORS, INC.

MR. KHALID MAHMOOD
BOR-010010
SOIL
AA14919
0041-01-01

BORRSTE

EXTRACTION
EMA14919

PARAMETER
Total Recoverable Petroleum Hydrocarbons, EPA-418.1
Appnwed by lho State ot Caldomta, Dopattmont of Heatll1 Ser<IC8s

TESTING SERVICES
COLLECTED:

RECEIVED:

PREPARED:

ANALYZED:

REPORTED:

RESULTS
(mg/Kg)

18.0 11/15/90
11/16/90
11119/90
11/19/90
11/21/90
nus repott 1S SUbmdted tor a.. •xduSNe use ol the dient 10 whom It is addressed. Any reproductton or use of the Labora&ory's name tor advet11r.tng 01 publiCity 'Mthout aulhonzatJon IS protwbned.

ATTACHMENT 6 - 3227
4200
---~------- '--------------~ -..., ___ _
_ G_~_£1 __ ~_5_io_g:_t_lR_~-~-~-~----------------------~--Il __ Cl __ l)[tiC:CII fl~~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL CHEMICAL MICROBIOLOGICAL
QUALITY CONTROL DATA -EPA 418.1

ACCURACY PRECISION
Percent Relative
Spike Control Percent
Recovery Limits Difference
105.3 80-120 2.2

SYSTEM AUDIT REFERENCE
Access 10# EMA14902-19
QC Std ID# P80VI
Sample Prep Ref.# : P66SPOVI
Approved by lhe State ol Cal~om1a. Depanmoot ol Health SetviC85 Control
Limits
0-15

TESTING SERVICES
QC &·$\'STEM AlJI)rr

DATASIIEET
TNa repon1s suDmlfted tor the exdus•ve use ot the dlent lo whom d tS addressed. Any reproducbon or use of the L..abc:H'alory's name fOf' adv8111SIOQ or pubhcrty without authofizabon •s prohOted.

ATTACHMENT 6 - 3228
4201
.,
QA/QC DATA INCLUDING:

Lab Control Standard Recoveries
Matrix Spike Recoveries
Duplicate Recoveries
Performance Check Recoveries
ATTACHMENT 6 - 3229
4202
~-
_.._, ---..,..----------------------
5200 E. Hunter Street, Su1te B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL
QUALITY CONTROL DATA - EPA8010

ACCURACY
Surrogate
Spike Percent Control
PARAMETER conc(ug/1) Recovery Limits
1, 1-Dichloroethene 4.0 70.1 60-120
Trichloroethene 4.0 86.1 60-120
Chlorobenzene 4.0 66.0 60-120

ACCURACY
Calibration
Check Percent Control
PARAMETER conc(ug/1) Recovery Limits
1, 1-Dichloroethene 4.0 100.9 90-110
Trichloroethene 4.0 99.1 90-110
Ch lorobenzene 4.0 95.5 90-110

PRECISION
Matrix Matrix Relative
Spike Spike Percent
PARAMETER conc(ug/1) conc(ug/1) Difference
1, 1-Dichloroethene 2.8 3.2 13.3
Trichloroethene 3.4 3.7 8.5
Chlorobenzene 2.6 2.9 10.9
~by ... s-GICelolomla.~ol-s--

TESTING SERVICES

QC & SYSTEM AUDIT

DATA SHEET
Lab control
Standard Percent Control
conc(ug/1) Recovery Limits

4.0 105.0 90-110

4.0 98.7 90-110

4.0 97.6 90-110
Control
Limits
0-40
0-40
0-40
TI'oor-'•-lor""'•llduiiNtiUMGI ... cHniiOwhamlll--l!lrr....-.arUMGI ... .__~I-Iar--.garpo-, ___ ..,__ ATTACHMENT 6 - 3230
4203
-~-~_l1 __ ~_:~_8g_!_Jo_r~_:_~-~~----------------------~--ll __ CI __ I){tic:CII Fl~~rt 5200 E. Hunter Street, Suite 8 Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL •
QUALITY CONTROL DATA- EPA-8020

ACCURACY
Surrogate
Spike Percent
PARAMETER conc(ug/1) Recovery
Benzene 4.0 92.3
Toluene 4.0 87.5
Ethyl Benzene 4.0 99.1

ACCURACY
Calibration
Check Percent
PARAMETER conc(ug/l) Recovery
Benzene 4.0 108.1
Toluene 4.0 92.0
Ethyl Benzene 4.0 96.0

PRECISION
Matrix Matrix
Spike Spike
PARAMETER conc(ug/l) conc(ug/1)
Benzene 3.7 3.8
Toluene 3.5 3.7
Ethyl Benzene 3.9 3.7

MICROBIOLOGICAL
Control
Limits
80-110
80-120
78-120
Control
Limits
90-110
90-110
90-110
Relative
Percent
Difference

2.7 5.6

5.3 • TESTING SERVICES
QC & SYST.EMi ~UDIT DATA SHEET .·. .

Lab control
Standard Percent Control
conc(ug/l) Recovery Limits

4.0 99.0 90-110

4.0 97.6 90-110

4.0 98.9 90-110
Control
Limits
0-28
0-25
0-27
Tloor-'oo-torlleoiiCiusnoeUMol11e.,.,.,.towhomllo-.lfty--or,_ol.,..___.,-a_lor-.g.,~--·..-. ~br .... SioleaiCalilomia. ~"'-­ ATTACHMENT 6 - 3231
4204
..-....., -, ,.....,., ------ ----------------~-------------------------- -------------- -------- =Jl==l1~~~:~_88_5!_Jo_r~_:_~~-~----------------------~--ll __ Cl __ l)[tic:Cll Fl~~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926

ENVIRONMENTAL CHEMICAL

SYSTEM AUDIT REFERENCE
Access ID#
QC Std ID#
Sample Prep Ref.# :

EMA14902-19
SP112090
P67SPOV1
ANALYTICAL QUALIFIERS:
• MICROBIOLOGICAL TESTING SERVICES

1. All solid and sludge samples are analyzed on an "as received" basis without correction for moisture content.

2. IF target analytes are found in the laboratory reagent blank at or above the indicated detection limit, the test result is corrected by the amount found before reporting.

No target analytes were found.

Senior~!; c~·~~
La~ratory Director
~by ... s- of California. Dopal1ment of--
Thio report,. a..bmOiod for lhe o•d\lsove UN of !he client to whom il ~~--·Ant roptOducbon or use oflhel..aiJcQIQry'a nome lot --.g orpubllcily-....,.,_ 11 ~· ATTACHMENT 6 - 3232
4205
-. rSAMPLE EXTRACTION SHEETS
ATTACHMENT 6 - 3233
4206
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ATTACHMENT 6 - 3234
4207
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ATTACHMENT 6 - 3235
4208
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1 ATTACHMENT 6 - 3236
4209

METHOD DETECTION LIMIT SHEETS
ATTACHMENT 6 - 3237
4210
(> ,,

METHOD DETECTION LIMIT
Method Reference: EPA 8010
Method Name: HALOGENATED VOLATILE ORGANICS
)
Date Started: 1/16 /q f Set-up by:

Estimated MDL: 3 to 4 times SD of Instrument Detection Limit Date _________ _
Reviewed by:

ANALYTE Concentration (ug/1) MDL
RUN# 1 2 3 4 5 6 7 (ug/1) (ug/1) (ug/1) (ug/1)
-
GCF# tD21>L( .$02 PL."2.. $t)2 $VlDLf/. &>"tDu- t c sl SD MDL UCL LCL )modichloromethane o.to9o ().tDS':f o.t•6o O.OfTr.S tJ. o'fl':/-' O.ot/":f?-4 D.Ot83l... O.o6 0.11 0.'* Bromoform o.o":fl/1 D. o'lll.s-t o.ofl(fo.> o.ohCfB' o.o6ca6 ., .. 0.03CIS"J 0. 0'2. 'Z.Sl> (),g1 0.1'!- o.osBromomethane ,. otb(' ,.;"'. J.16QK,o z. o.o'Z.Vc;g o.o-z..uo o.o?$fto o.on .. oz.o 0,0'2680 o.og 0,16 t;;.o6 Carbon Tetrachloride o,rz'6 D·/il-11- o.rz.6B O,fJIO o.ttl"l. o.o fz'lg O.tt9 I ..r. oz. J.s-x,.,-v O.otVOO e;,o6 0,/f Chlorobenzene O.llq> O,t:Jz.6 AO':/o?':f 0. lo6f o.oh-?3 0.100/ O,O'fZ.'l... o. 0 ':! (;).osChloroethane o.oi'Ho o.lil-10 (), 1:186 "l.o o.o"Tno o.•?-1.&> 0,09-ll.o (),fl 0.'2.( o.o7 Chloroform o.rz.#f o.o91WJ (),rz.f,f.J o.,'ZIG. 0./I'S{f o.O'J()oO 0.11 ':1-e, 2 )X,o-1 e;.o..s- 0.10 Chloromethane ?.'l&oxtal ,a" -· "..} f.tY/oXtO-. 6.,\.0XtO a.*x,(J I0,6HXto f.tJtoxlJ ?.go YIO·S" t.66o)(to -:1 o.os O.D"L...

Dibromochloromethane 0.131'2.. (),l{f':IS 1),(003 0,1338 O,fz.IJ Oo//36 o.of(,m ()./2.49- o.o 1'1Stt o.o6 O,ff J-Dichlorobenzene 0.1>2.6 o.tb'Jt o.oi33o o.tz "f1 O.af'f11 Q,O':Jol$ /. ":J Ot!/ o. "l./ o.o.! 1 , 3-Dichlorobenzene o.rz.3.,_ O.t'ZSI O.O';fOOO o./o'l6 0,/1,/ O.d(W o. o66?..'f o. O,.ofl o.ts o.o.> 1 ,4-Dichlorobenzene (),f":ft9 Dt/1. 3S" 0./S&f 0,!368 (), 1111 Q.<>'ZS?11 ().08 0./6 O·ob 1 , 1-Dichloroethane lo,1o":1Z (),1Sf16 O.tt68 o,,,, o.ogl'lo o.ofS?c o.o$757> a. Di 0.16 o.o6 1,2-Dichloroethane 0.1666 O,fCf/8 Ot!2g8 o.t616 Q,,,-r"l., O,IS"l-S 6.t:;o() 1o'f O.ou.so aog 0.16 0·06 • 1-Dichloroethene 0./lf/0 0,/tso 0 1 I "l,.QQ OJ0":/0 0,//bO O,IJS'Q o,rs6o 0,12.3o 6.'130)ao·'l 0 • 0 U3o C?.o8 17./b #:}.. ()6 II trans-1 ,2-Dichloroethene O,ftflio 0./"2.80 0./$50 o.t.S& o.t"Z.fo 0,1/30 (). OHir,o (). z..6 /;,f8 ----
CLMDI...8010/REV. 91
ATTACHMENT 6 - 3238
4211

ANALYTE
RUN#
) GCF#
,
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 , 3-Dichloropropene
Methylene Chloride
1,1 ,2,2-Tetrachloroethane
-
'
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
I
Trichloroethene
Vinyl Chloride
Notes: SD =
UCL =
LCL =
s:z =
c =
)
Reference
Concentration (ug/1) MDL
1 2 3 4 s 6 7 (ug/1) (ug/1, (ug/1) (ug/1)
-
Sf) '2.1> L.f '2. ..SOU>Ll Sf)'Z..I>LC(- SO't-IILS .rot-PLb c sz SD MDL UCL LCL Or136lf o.tC,glf O,fo/8 o,oob 0,//l(.l. o.C1fs6o o,rz.JJ o.ob o, rz o.o'f f).! I§!. 0. 06/tf/ J.Slll..t 10-'f o.oii'.J o.ob O.tf o.o(f o.o&m o.o:f6£6 ().o)'l-3./ o.o"f'I?S o.oilff-z. OJJ6f6"l, l. ) 1-oX&ci'f 0.ot136 o.o6 0.1( o,!ff?.-1 (),tS'fO o.tJIKJ o,ralfo o.ICftlo $-.OfOtto-«1 o o.o=! Orl<t o.o.> o.o'P;t-l o.o2.1•1. O.OS"31o 0.06861 o.o30<f1 o.otCI'U o,o5 O.df 11.03

0.1613 Ori=/-Z.O 01 I l-'Jf o. 1.$'f"'f O.l$11- ().llfb o.o-a..wg ().0-=f (),13 o.oS 0 f)}l.. fJ.t'#/z. o, to";fb o,l Jf8 (),IN O,llU (), Jt:7l,'f Orl'l-8<! -z.. rrtx '"-<,. 0.01 ':/00 o.os o.co 'o., rfl. Odt66 o.<>Jr3J1 0.1180 O'fl o. o '?' .Jlo o.to1o O.OZDJ& o,o6 0,/Z. '(),lsv-6 Orl:fJ6 o,rt./o o.to'8 0,!386 .f..sfoXJo.Jf O,o'2..16o f!l.o( 0.1 II- ().OS Ori?..Jl' tJ.ofJoo (),O'Ll#{;o ti.O)f+o o.OJSVO o.OI(.J6o o.o-stto o,,-z.. t},()g Standard Deviation [(S1) 1n] MDL = Method Detection (Factor)(SD) Upper Control Limit (1.92 MDL) where Factor is Students' t value at the 99% confidence level as follows:

Lower Control Limit (0.69 MDL)
Variance
Concentration (ug/1}
For 7 replicates use 3.143 as Students' t value.

For 8 replicates use 2.998 as Students' t value.

For 9 replicates use 2.896 as Students' t value.

For 10 replicates use 2.821 as Students' t value.

Glaser, J. A., Foerst., D.L., McKee, G. D., Quave, S.A., and Budde, W.L., "Trace Analysis for Wastewaters," Environmental Science and Technology, 15, 1426 1981).
__________________________________________________________________________ __ CLMDL8010/REV. 91
ATTACHMENT 6 - 3239
4212

METHOD DETECTION LIMIT
Method Reference: EPA 8020
Method Name: AROMATIC VOLATILE ORGANICS
Estimated MDL: 3 to 4 times SD of Instrument Detection Limit .Je Started:_l_.!__/_1 b_!_(....:...r'll __________ _ Date Completed: /·11·9! --~~~-------------------
" -
..,

ANALYTE
RUN#
GCF#
)zene
luene
Chlorobenzene
Ethyl Benzene
meta-Xylene
para-Xylene
ortho-Xylene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
) Dichlorobenzene
-
Notes: SD =
UCL =
LCL = sl =
c =
)
Reviewed bv:
- ~ Concentration (ugll) MDL
1 2 3 4 s 6 7 (ugll)
(ug/1) (ug/1) (ug/1)
-
502PLI 501. DL2. 502 /)L 3 .SOl IJL'f g;>a bL.S" ~a~"' $102/JLJ c sl SD MDL UCL LCL O.Ol!ZO'/ 0,/002 (). 0 ':/ 9'10 (),Olfl~ o.f181t~ o.o~!IL o.ol~! o.o,386 o.o1$n o.tJ~ ().tJ'fl88 o.tolf3 ().tJt081 r;.ot:~w:, (J.O'f/0/B o.otltl o.ofJ2.0 D.o688o O.Dtf.Jo o.oB':I~S' ......,
o.oUfo o.om~ o.o':Jol'f o.O~B (),Ofl6'f</ ~ o.o!"-'1 O.O'l':#l../ o.o6¥'S 11.dl•l1 0,4l'l-1o ().Ojt'flJ. o.o'i217 o.o6JJ':J- o.'1ffo8 o.ol(f,u- o.or~~3 o.Dqtlfl. o.o6No 0.081.19 O.OB$'11 o.o fl2.'ll ().~~ o.oiAII ().oS.t''U o.aa&t?
Standard Deviation [(S1) 111) MDL
Upper Control Limit (1.92 MDL)
Lower Control Limit (0.69 MDL)
Variance
Concentration (ug/1) ().(1~11- (J.Ai~2.f1 t%1ZJZ. g. 'ZO ~JUci S" (/.0$1 XIO·l o.oJ o.or (),0 z. o.o':fn$ ll,tJ,~S (1.0~ l~XIO-S' -J f.6'tt.Xro (>.03 0,0$' o.oz. o.08f?f' IU1":1':/z.J ~D9ZZCI --4' f,Ol.,)(IO (),0/tJIJ (1.03 o.o6 ().oz. tJoOBOfl7 o.o&'i-117 ().01/lfe. /,1(().,. )t' ;'I- (), 0/0S"Z. o.o~ o.o€ o.o~ o.012Jo o.~¥~H' o.t$~ t1.orf'Xto-> 'f.$2~)(10-.J o.o3 o.•' ~oz. ().07'13 o.D,ISC o.oi~~ /.Ogl '1t 10_,. o.otolf.o D.OJ 0.01 o.oz.. o.o':f-1'3 o.tN.I'i.J (). "''ll( -fir / . .,.fX•o o.0/2.1Z. o.o~ o.o'f o.OJ 0-0":H's<J t:~.o6z.tz. o.o~Zfi IJtfXto~ ().0/0SJ o.o~ o.o& o.o2_ o.OT'f~ o.o63t~ o.o81'f.o l.l#~.r,o·~ D·DIIJC/ D.O#- 0.111 o.o3 = Method Detection (Factor)(SD) where Factor is Students' t value at the 99% confidence level as follows: For 7 replicates use 3.143 as Students' t value. For 8 replicates use 2.998 as Students' t value.

For 9 replicates use 2.896 as Students' t value.

For 10 replicates use 2.821 as Students' t value.

Reference- Glaser, J. A., Foerst., D.L., McKee, G.D., Quave, S.A., and Budde, W.L., "Trace Analysis for Wastewaters," Environmental Science and Technology, 15, 1426 1981).

COMMENTS: ______________________________________________________________________________________ _ CLMDL8020/REV. 91
ATTACHMENT 6 - 3240
4213
HALOGENATED VOLATILE ORGANICS, EPA-8010

METHOD LABORATORY LABORATORY LABORATORY

DETECTION METHOD METHOD PRACTICAL
LIMIT* DETECTION DETECTION QUANTIFICATION

LIMIT LIMIT LIMIT
(ug/1) {ug/1) (ug/kg) (ug/kg)
Bromodichloromethane ND<0.10 0.06 3 ND<5
Bromoform ND<0.20 0.07 3.5 ND<5
Bromomethane 0.08 4 ND<5
Carbon Tetrachloride ND<0.12 0.06 3 ND<5
Chlorobenzene ND<0.25 0.05 2.5 ND<5
Chloroethane ND<0.52 0.11 5.5 ND<lO
Chloroform ND<0.05 0.05 2.5 ND<5
Chloromethane ND<0.08 0.03 1.5 ND<5
Dibromochloromethane ND<0.09 0.06 3 ND<5
1 ,2-Dichlorobenzene ND<0.15 0.11 5.5 ND<10
1 ,3-Dichlorobenzene ND<0.32 0.08 4 ND<5
1,4-Dichlorobenzene ND<0.24 0.08 4 ND<5
1, 1-Dichloroethane ND<0.07 0.16 8 ND<10
1 ,2-Dichloroethane ND<0.03 0.08 4 ND<5
1, 1-Dichloroethene ND<0.13 0.08 4 ND<5
trans-1 ,2-Dichloroethene ND<0.10 0.26 13 ND<20
1 ,2-Dichloropropane ND<0.04 0.06 3 ND<5
cis-1 ,3-Dichloropropene 0.06 3 ND<5
trans-1 ,3-Dichloropropene ND<0.34 0.06 3 ND<5
Methylene Chloride 0.07 3.5 ND<5
1,1 ,2,2-Tetrachloroethane ND<0.03 0.05 2.5 ND<5
Tetrachloroethene ND<0.03 0.07 3.5 ND<5
1, 1, 1-Trichloroethane ND<0.03 0.05 2.5 ND<5
1, 1 ,2-Trichloroethane ND<0.02 0.06 3 ND<5
Trichloroethene ND<0.12 0.07 3.5 ND<5
Vinyl Chloride ND<0.18 0.12 6 ND<lO
* "Test methods for evaluating solid waste; Volume IB: Laboratory Manual for Physical/Chemical Methods" U.S. EPA SW-846, 3rd Edition, November 1986.

ATTACHMENT 6 - 3241
4214
""'""·-- -~--~r_i_iR_:j_~R_:_~-~~ __________ A_n_a_lriical Re~rt 5200 E. Hunter Street, Suite B Anaheim, California 92807 • 714-777-1425 • 1-800-3 CROSBY • FAX 714-777-3926 ENVIRONMENTAL CHEMICAL • MICROBIOLOGICAL • TESTING SERVICES AROMATIC VOLATILE ORGANICS, EPA-8020

METHOD LABORATORY LABORATORY LABORATORY

DETECTION METHOD METHOD PRACTICAL

UMIT DETECTION DETECTION QUANTIFICATION

UMIT UMIT UMIT
(ug/1) (ug/1) (ug/kg) (ug/kg)
Benzene 0.2 0.03 1.5 ND<2
Chlorobenzene 0.2 0.03 1.5 ND<2
1,4-Dichlorobenzene 0.3 0.03 1.5 ND<2
1,3-Dichlorobenzene 0.4 0.04 2 ND<2
1,2-Dichlorobenzene 0.4 0.04 2 ND<2
Ethyl Benzene 0.2 0.03 1.5 ND<2
Toluene 0.2 0.03 1.5 ND<2
Total Xylenes 0.06 3 ND<4
Thio,_t•--....... ..,....,. _ .... - .. -··-·
~.., .. - ,., ..
............

CMfomoa. Dopottment - .... of-- ~_ .... --.,.,.._, ___ ...,.__ ATTACHMENT 6 - 3242
4215

RETENTION TIME SHEETS
ATTACHMENT 6 - 3243
4216
-· \ ...
,· I
,~H~I.CAL ' MI~.~O.fii't9~0G!CAL • ENVIRONf¥tENT~I. • TESTING SERVICES -.!:::::::r--- 625 w. Katella Aven~o~e, Unit4 • Oran~e. CA 92667 • 714(639-3821 • 800/3CROS6Y . '
/' [ RET:JiNTION TIME WINDOW SET-UP J
Method Ret: Eflj-80£0
Method Name: PfA/?,6EA6L£ ltAltlfJ€Hit1€/) VplA1l¢ o<t~lf#IGS '
Date Started: U· 2o·f..O Date Completed: 11·2.?:,·9o
Set-up by: eYe Reveiwed by: ~
Compound Retention Time (min) ( ± 3xSO)
Run# 1 2 3 4 - GCF# C5W!8 Csr~PP& CS'IOf/PIJj CSIJsPM s RT %RSD UCL LCL I t'HLollo~ET/fiiNE ~No ~.ss-3 l'.~?o 3.6oo O.O"z,f .3. S'U o.sa ~.&~~ 3.s~ VtAIYL CHLoll.tl>~ ~081- 4-.041 ~0.33 *-.os--:,. O,o'Z:.~ f',e>6o o.ss ~.12.6 .S.99</.

ERQ4t(o~c-. . .._wE ?-.9oo ~.'113 ,,($ ?.9/0 6./,XtO"~ _£!j_o'1_ o.rz .. c;.t,12-5 ~.88'1 C#i.~0£TIIME. 5.9W S: 91 =I ~9'1.~ S.9~3 C').0/..3 .5: 9-a.5 O,"Z:.'l.. 5:.96 z._ S:S~l!- 1,/-/>,' CHLflllo£THIAJE: 6.B03 6.RI"t- 6.B:Io 6.1lf-3 o,of?- 6-!l.J O."Z.-S 6.1f<f .6·7?-<- IM£7/IYIENE. Clll.o,ttl£ 8183 '·l'l'f 8. -z..o1 8.zJo O.QZ..O 3.20~ (), oz..S£ 3.~ 8.1W/ irMS ·I.Z-p,· Clltotoi!'TNM. i.'i6"1 r.qgo B.'ifl3 l(.ooo ().01'1- 6.,is- Otlb 9.ol.-"f 8.9~.3

1.1-P• 'clllOI.oE71iMIE /O,ofB to.ol=l /O.o</3 ,o.no (),Oil., /O.CJ13 o.,~ (0./l..<f IO. os-7- CHWI!DFOIIH II. 9'1? rz..OIO IZ.. OZ.O J"l.~t>t.1 0.0(.3 1 z., ollf- 0.1/ /Z.OS3 II. f/1-S'" /,/,I -1r,'CNttJbJETN4/oiE: IZ· 3(fo ,~.~ 12·~ /2.3~ IJ.<I/3 IZ.J.S"{. 0.1/ I 2. 3 'i'.s- IZ3t 1- I(' A68 cW ··••;-u -~· tlrt11.& IZ· =l-6o IZ·":/=1-0 IZ. ?-V IZ·'":fco o.o.J=I IZ.=I-$3 o.2.fl /2-~~ tz. 6~z /,2 ·j),"CHtoK~71fiiAE /~.oJo /l.o9o /~.O_,...l 1.5. 0,() 0.0/fF II.Q{'l. Oo/0 1~.oK8 /3,00~ TCE. lff,/6~ 1~1':1":1 l(f-,{83 l(f 1'13 11.01~ '~.t:r'l D·Of/ 1~. us- 1¥.1~~

1.2_ -f ... {;NI.oiJ;)pJtof~H.A; If/; St>.! 1~513 t9:n3 1~.$33 ().013 I~S78 o.o9 I<'!.SS:} ('!-;~ 19 isRD.44oD.f"..w, .L>. fi'TJI"-1. l/f.961 l'h 1~':1- llfr1J1' /¢.190 0.0/0 l~&flo 0.0=/ 1$".01~ 1~9S'O cis-l.s-1>1~" - -- 1~6JJ ($ 6q:s /S. ":ff;o IS. ~=I- o.oto /$.6?6 o.o6 I.J: '1~ IS.666 irlurs-/,l~'CIIlt~/(4ifP~~ /6.s-J =I- /6.$fB 16 . .>SO t6SS3 ~.Uro·.l /6.~' ().o.> l6.r?l 16 • .>2.1 I, I ,2. -Tn' CHLGRDeTHA/IJf 16-'=M1 /6.&0':1 /o. St.5 ll-'·'1<> 0-010 16.tD1 1)~~ 16.JJ9 16. ?r'i PeE 1':/.o::,.o 1':1.010 19-.o'to I ':J. 100 0.013 19.04> o.c1l I ':I./?. <I- /7..0~ [.A·~o'-toCHL~Hf.TitltaJE. FIA1o t=l. W.J 1::,.~ ll+.~lo g,u,o-1 I =i-.¥19 o.o.> 1':/. Will. I ?..39¥- CI1LO!roi..EIJ~NE. -18.314- /839-":1 l'r. J$·3 fS.J6o B.u.o-~ /ti.~(f9 o. olf. ltl.J":#~ 18.~'lllEllotvtoF,.RM ~~.S=13 l/9 .S£":[ 19. S"f_$ /9.~=1<> $-, ":f =I X to -:1 19.>3:-J o.o3 19.>1fK /tJ . ..s~~ f,t 2. 'l.·"'ft..h..CNI.~£7N~ ~~ 2.o,/ 't':f zo.-w3 'ZQ. uo 7.o. 7--l"f J.ZoK,o...s "ZO. 2-o':f (),ell~ w. ?...3-z.. ~.18l...

I ,J-P/CIIi.oi«J#EN~NE 2t.,5b ""'·65=1 '2./.U ':If 2/.6 ':/.3 0.0/o ~.66l... O.QS z,, 6 9Z. 2./.6~l... t,l.f.·P/ . A • • ·"' ii'EAJE "l./,=1~ 'l-1, =I~".:: J(.=f-8':1 'l.f, ':/i.3 J, Z-'XIO --3 ~. ':/~~ o.o~ 2.(. Jo,. 2(. ":/'$":/ /,2-f>.'I"U• •-•111:.. ,_.,, ?.. 2. 3 :&.lf "a-2. • .f~ ':I 2-L:f~3 Z."l..,~.J o.OIO U..J~ o.o~ '22-.J =to ~2..~10 Notes: 1. Must be established In a 72-hr period.

2. Must be established when GC System Is fully optimized . . . .

COMMENTS:
'I
I
""'
-_;
ATTACHMENT 6 - 3244
4217
Date Started:

Set-up by:

Compound
Run#
GCF#
Benzene
Chlorobenzene
1 A-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Ethyl Benzene
Toluene
ortho-Xylene
meta-Xylene
para-Xylene
r
"
"
CHEMICAL • MICROBIOLOGICAL • ENVIRONMENTAL • TESTING SERVICES 625 W. Katella Avenue, Unit 4 • Orange, CA 92667 • 714/639-3821 • 800/3CROSBY [ RETENTION TIME WINDOW SET·UP J
Method Ref: EPA- 8o2o
Method Name: PI.(R§EAJLE ARoHATIC VoLA7/LE O.(EiAtJICS
11-zo.qo Date Completed: tl· 2 2·'1o
cue Reveiwed by: (cJ;?_
Retention Time (min) ( ±. 3xSD)
1 2 3 4 -
CSiflfPB CS?3PPB CS/~1'18 CSI3S7/!8 s RT %RSD UCL LCL
f2. '17.1 (2. ~8=f /3.000 /.?. oO"':: o.ot.> /2.99~ o.o:. l~.t>~? /2, 9'1-'::! 18,'2g3 18.~~ 1'8.3o"t It/. 311 o.ot3 18.30/ D.O':/ /8.3~0 /fl. ~2. 2/.12.'1- 2/. 13"1 2-/.?lf':/ 21.Y.s1 o.ol 2 2/. '1~2.. o.o.s- 2./. ~1K 2../. ':/06 ~t.6oo 2/.6/o 2/.6JO "2./.IIJo ().0(3 ~.6ts- 0.06 .21. ~s~ 2/.S=/6 "2l.2IO 2-2-2.90 2.2.300 22.3/0 0.01_3 z_z.. "l.Cj> 0.06 2.2.33~ "22. 2S6 !rR.~s-o IR.~.3 I~ tf':/3 t8.t43 0.01.3 lf.6'1:# o.o":f /8.SD6 /3.~Z3 16,1 "::o t6.t!3 ,6,1'1=1 /6.~r 0,016 t6.11tj 0,(0 16.2.31 16.1'1-/ lrC?. "l.(l /'/.1.1,_3 tf/."Z-33 ,q. 2-S'o ().otz.. ,q. z;z..:t (),06 19.~6.3 19.1'11 tB.,2.3 18.631 IV.6'17 18.65"? o. 0/.3 /V.6~1 0,0":/- IZ.S06 te.C/2-t "
~
Notes: 1. Must be established In a 72-hr period.

2. Must be established when GC System Is fully optimized.

COMMENTS:
::L-RTW-88
"'
~
ATTACHMENT 6 - 3245
4218
EPA 418.1 CALIBRATION CURVE
ATTACHMENT 6 - 3246
4219
CROSBY LABORATORIES, INC.
625 W. KATELLA AVE, Unit #4
ORANGE, CALIFORNIA 92667
Page# go
LAB #: Mllf'foZ.- f'f Date Received: J t/t G/9o ----------------------------------------- CUSTOMER: fMA Date Started: 1 1j1q /::, 0
SAMPLE: ~ ~ Date Completed: 1 , ( 1q (
10 TEST: to.fat ~ ~J~.u ... J Hy~ii+H'b~ Ref: <f{g,J
lAGt/ -r.P/ r-tuv.d V~"lF~Vl A~~ fjJ,.,-. ~/;rJ
ifllfl.{qot. pc £. - 0 StX-bj /O.!>ztft /0~ - (_'?, I }:2,:j Mtc.r't"'..3 Sv R -o >l>OOS to.~su . ' - 12.'1 /2,Cf
ll11ttftioq. GcR~ os-oo1o /O.IIIB . '- JS,o 19,g
tflfl'f9o> B'vR-owaoj 10 ,z_g4.:J ., - /7.~ /.1, I
AtU(fqo{;. b\:.1<.- 02.000~ (O.fbb~ . . - i8. 'I- I 8.,/ /+lit¥fu=l- &;R.- 02.0<.'( 0 lo. ~St 1 . .... fl, I lO, b Mtlf'1oS b"\IR- O'foO~:JJ /0, I I l'f -~.. "" (4, s- 1Lf.3 Mt'+~? ~R- OlfiJoo) ta.~?v -. - /1;, '1 11, g
IWt4CftO i>u/Z- 04<Jolo 10,~~;) .... - /-=J-,g i 1./
lllltlf'Uf 6cR_ .. 03lX>of to. 1ttL .... - ~14-.t /3, 1 MtlftttD pu~, uJo ... cf ~'-'~') ,;.;, ~f - tie# 13.& /3, 'f .....

M1411L evR-o~s IV.)~ . ' - ~ i8.o i1,3
/Wtllflt /3 l>vf..' o30Q 1o fu.tfu53 _, - ( 9.4- 11. I
!Mt4414- B'*'- 06ooo1 1\J.Cftrf - I S.3 /4. r ~ ..

Sample Volume:

Titrant Normality: RESULT:

Titrant Volume:

Analysis Wavelength:

Storage/Disposal Code: (D, 2 3 4 5
Volume/Weight Remaining: ml
Tested by Lq(._. Date rl/11/~o
Verified by ~ Date 1l· I~ ·CfO
gm
ATTACHMENT 6 - 3247
4220
CROSBY LABORATORIES, INC.
625 W. KATELLA AVE, Unit #4
ORANGE, CALIFORNIA 92667
LAB#: lllltlf..9oz-t9
CUSTOMER: EM f)
SAMPLE: ~
1111J(f/J5 "'oR -ol:«cs /0.3t38
/fiJ 14'} ,, fJo/Z -o600t o iO, 2/SO
A111 ll11":1 Sc/Z ~ 01 ooo, 10, 3!l!'f
lfRilf71'& ~~P-.,, OIOC'C5 tO. Z-8(,1':}
Mt4111 BoR.~o1ooo I0.38.>o -·
---
Page# B I
Date Received: 11/16/7~
Date Started: 11 /t'l' (9o
Date Completed: 11( n(9o
METHOD Ref: 9-lo ,/
,o,.,~ ~ 14-,lf
,... lfC~ d .. - (2,<. If. f
'' - tQ..s ts.r:;
'' - ,, \? II.£ ~.
- /g,O t1.3
0~~~ <f<, I - 10$,3 ~ .tf.v
~ ~) f..ff) ~ 2.z.f'
~Ko /:R.CJ~l/.:'1,../._ - - - 0.2
(h[5frl I ere IOf'fM - - - IQ 2.
(tlsiJ z cce - - - .2.-{j,b 7offlt1
rat>~ 3 - -- .., ~
CC.f. 3opm - ~'C.~
~lsld4 4otrtr~ ocs - - %J.1 -
Sample Volume:

Cv, .,_ Cc.~:::: I 000
Titrant Normality: RESULT:

Titrant Volume:

Analysis Wavelength:

Storage/Disposal Code: @ 2 3 4 5
Volume/Weight Remaining: ____ ml ______ gm
Tested by __ ~..l..LJo!'l--+,--------------- Date n/ttho Verified by _ _,..~~~=---=---------------- Date ll' J"t ·Of6 ATTACHMENT 6 - 3248
4221
".~!' ~ ( "fd( ) I ~ ~
.... i ~ rl (J tf 3 <J , v .L I ~ -, (] ,_ ..
\ ~
,.
\~ ~ ~
" "I> Jp -~
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: \ ~ ~ ~ IC\ ~ ~ ,... - ~ ~ I~ I~ -......;.
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"'\ ~~ ~ lg ~ 0 1;::: .. I
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I
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.... I 1\ I~ -:::: ~ ,..
\ ~ ~ ~ .- N ~
N ~
1\ ·s ~ ~ ~ ~ ..
•
\ ~ ~ 1.3 ... .
~~ ~
' ~-
..
' 1-
ATTACHMENT 6 - 3249
4222

CALIBRATION STANDARD LOG SHEETS
ATTACHMENT 6 - 3250
4223
~--·- -·
r
~ LJo\ ~I-\ I V r< I c.;:,

INC 'PORATED
CHEMICAL • MICROBIOLOGICAL • ENVIRONMENTAL • TESTING SERVICES 625 W. Katella Avenue, Unit 4 • Orange, CA 92667 • 714/639-3821 • 800/3CROSBY .

CALIBRATION STANDARDS LOG SHEET
METHOD REFERENCE: EPA 8010

HALOGENATED VOLATILE ORGANICS
# OF COMPOUNDS: ___ 2 .... 8"----

SUPPLIER INFORMATION
Name: Uft;AA SGt·~
Lot#:

Catalog#
Matrix/solvent:

Concentration:

Expiration Date:

C -p2S8
He M.-6tP'

LIST OF COMPOUNDS
Benzyl chloride
Bis(2~hloroethoxy)methane
Bls (2~hloroisopropyl) ether
Bromobenzene c:s&.m<>¥ci11o-imethaiia:>
c~~m~ (_ ~romomethane ........ ·.
(CartioriT~trac'hforfde:

Ct11_oroacetaldehyde
c chrorob_enien-e---.
~~orQ~t'hclne~
(ChlOrO(~
1-Ch1orohexane
/~-£h~inyl ether
'-f_hlorom~th~f1V
Chforomethyl methyl ether
Chlorotoluen_e_
(Qibromochloromethane Dibrornomethane ______ _
~.2:olchrorobenzenv
t;..""'<' a ~·:;ll'hJl.. __ _
/1:3-olchlorobEmzen·e ~ '"" ·" 6-I'J"·"'"" · (l,~DJc_hlor_ob~_n_zen~ ,u..., v .A.I!J!m.f ~cchlorg_~i[T~eth~_ne-· :.o" '>- ~>' ~
(-:!Jj)Jct:ttor~~,~~e-· I CO, I /"}I-.e
loll.:._ '_,L<j/,~hlJ1IP_~thane--.. .~!;_I ,~Ay,.....J.. 1ov. 1,-":i/-.(d.l-DichloroetfiYieii~~, to a. 1 ,...~1~«-o..i. ,\J u." ""'~/,.~ctrans-!_r~~R!~_':I_!oro~brlefle~ • .;.;,. ' M)lno.f ,o.,.c ,4.<,, .. ....\'-P~_hl_grometharl'e-,. ~,_ u---, /()()_,_""''/~ ~c=nJ?~f:~o!!We~ ~&~.,.A.~)"~ '1.)"- 1 PYt'kJ.. (trans~l~_ oropropyleB,e' , ....... , '-'JI-.< , viJ. ~ .PJ/wJ2 (1 .. ,1,2,2-Tetrachloroethai:!.e-> '~"'-' -"'Jh.,.J. 1 c ~- o ,IA.9/M.l. 1,1,1,2 Te\raet:algrgett:aaRe
(T;iractiloroet~~~ ,0(1, I ..... ~~~
,_1:1,1-Trlc_hloroetha~ 1cc; ... .lA~/~~
1ov. 5 _pyn.Jt. <..1:l,2~Trlchloroethan·c:-· 1 o~. 1 ~·n .. ..;, <trichroroeth~ -- , u<J. I .A'!I/,~ (Ir!chlo-rofiuoromethane-. (o0<J. 1 ""''t,.,Jl
, o o. o .,1171...1<. TrlcnLo.ropropan_e_-
~lny'l chloride----· too..s: -"H...,,.(
NO· O,..!JI~J!.. ~-1 1 ~- p,·c~'!-"'-"I...,.~J ICv Cl ,.u;!Jt.Jl..

Comments: ________________________________________________________________ _ ~:l ~C #'f; : -ft? s-;~ ft.,_ afves 0 No
ruj Received by: Date received: MSDS·
~~· '~L<~~~~-~~~0~10~----------------------------------------------------------------·----------' ATTACHMENT 6 - 3251
4224
- •
/'
,
\..

I
\ LABO)il.QTORIES
INCO bRATED
CHEMICAL • MICROBIOLOGICAL • ENVIRONMENTAL • TESTING SERVICES 625 W. Katella Avenue, Unit 4 • Orange, CA 92667 • 714/639-3821 • 800/JCROSBY (CALIBRATION STANDARDS LOG SHEET J
-··--·- -- METHOD REFERENCE: EPA 8020 ...------ ..... i::J AROMATIC VOLATILE ORGANICS # OF COMPOUNDS: .6 E¥ Vet;_ 7
"--
--- ==="

SUPPLIER INFORMATION
Name: .'{(;ttt\ >c.,.~df,L
Lot#: D- r1>"1t cp
Catalog# 'i> r~ -, 0(1)
Matrix/solvent: ~z,~t-6 h.~ ~--(_
Concentration: ~ ~N
Expiration Date:
~

LIST OF COMPOUNDS
~ {DO. I ~j/n.Ji.

Chlorobenzene
1,4-D lchlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
dth'Yi Benzene fCJO. I,.~"~/~
CToluel'l~ roo. "/':JIJnk
crth~~le;) /00. o .MJI~>-J(.

Meta-xylenes JO(;. O,Pjl #~
Para-xylenes ( D:J I _l)j lwJ(
.. - ' (I
I
Comments: ,M.c; /):)
~ -~ &I-I M:;Ds. Ft&hri
7 I .. . II/) /_9~ 10"'ves 0No
0J'R~ceived by: Date received: MSDS:
\.. I CL-CSLS-Ie-IIOlO
""
~
ATTACHMENT 6 - 3252
4225

SAMPLE CHROMATOGRAMS AND CALIBRATION CURVES
ATTACHMENT 6 - 3253
4226
MAXIMA 820 METHOD REPORT
Printeo: 22-NOV-1990 03:39

HALOG&AROHATIC VOLATILE ORGANIC
:-----------------------------------~-----:
: Operating Conditions Gas Chromatography :
:-----------------------------------------:

Qperator' ID: CYC Injection Method: PURi3E~,: HW
Sample Size: 5 ml Sample Pressure: NA
Column Type: Cap i ll.::u~y
:-------------------------:
: Temperature Information :
:-------------------------:

Column Temperature: F't'CJ!jl·'c\m
InJector Temperature: 200
Detector Temperature: 250
ColU8Hl Temp!watyre Proaram
35 C FOR 8 MIN @10C/MIN TO 210 C AND HOLD FOR 3 MIN
TOTAL TIME = 28.5 MIN
,·
-f. I
ATTACHMENT 6 - 3254
4227
:--------------------:
: Column Information :
:--------------------:

Column 1
Column ID:

Material:

Length:

Internal Diameter:

Date Packed:

DB-·624 CAP.

SFEClALTf
75 m

0.53 mm
NA
Sol id Support: f'-IA
Percent Load: NA
Liquid Phase: NA
Mesh Size: 1\iA
Gas Seecification for Column 1
Cat't'ier Gas: HEL I Ut,·i Make-Up Gas: NA
Flow/Pressure: 1 0l"IL/t•1HJ <FLOW) Make-Up Flow: NA
Split Ratio: 1"-.lA
Comment: ULTRA HIGH PURITY.
:----------------------:
: Detector Information :
:----------------------:

No. ~ ~ Range Comment
1 ::·:::
t.KAH ELCD E. LCD (i TO lOv ATT=5;T£MP=SBO;PUMP=5RTN;t10DE=H bC>i:J:l PID PID 0 TO 1V ATT=l;TEMP=230;LJti1P INT. =/'liD .: ------------------:
: Genet'al Comments :
:------------------:

ELCD- Set Hydrogen flow at tha gauge to 40 psi. Set helium flow at the gauge to 80 psi. Total flow (Hydrogen + Carrier) snould be Le·c~let.m 105 to 110 ml/min). <Flow of Hydt~oge:~n should be appn::n:. 95 ml/min; carrier flow should be 10 ml/min).

Stripchat't CoMent
ATTACHMENT 6 - 3255
4228
MAXXMA 820 METHOD REPORT
Printed: 22-NOV-1990 03:40

HALOG&AROMATIC VOLATILE ORGANIC
:------------------:

I Data Acquisition I
;------------------:

Channels: 2
Trigger: External #1
Delay: U.O min
Duration: 30.00 min
Rate: 5.000 points/sec
Channel Parameters
Channel ID: GC#1 ELCD Ch#1 GL#1 PID Ch~2
Detect Peaks: v·es Y'E?S
AID Type: WD24 WD:?4
Slot •= 16 16
Channel •= 0 1
Range <volts>: 0--1. 00 0-1.00
Resolution: 22-bit 22-bit
x-Axis Units: minu·ces iTlinutes
x-Axis Start: 0.000 o.uoo
x-Axis End: :::;;o. 000 30.000
y-Axis Units: volts volts
y-Axi'S Min: 0.000 o. 0()0
y-Axis Max: 1 • 000 1.000
Expansion: 1. 00 1. 00
Off'Set: o. oo;-.; 0.00/..
,.3
ATTACHMENT 6 - 3256
4229
MAX:XMA 8:20 METHOD REPORT
Printed: 22-NOV-1990 03:41

HALOG&AROMATIC VOLATILE ORGANIC
:-----------------:

Component Table
:-----------------:
ll : Component Name Ret HftiE! Window Ref Det Group 1 Cal &as1s Curve Orig Wgting Y-axis Internal Std 1: lhClDiFI'lETHANE 0. 35 1 Yes Area 1 inear No none Cone 2: CHLORDI£THHNE 3.b0 0.35 1 Yes Area linear No none Cone :;,; VINYL CHLRD 4. 06 0.35 1 Yes Area linear r«J none Cone 4: BROMOMETHANE 4. 91 0. 35 1 Yes Area 1 inear He none Cone 5: CHUJROETHANE 5. 94 0.35 1 Yes Area linear No none Cone 6i i, 1-DiClETHYLEI'J-__..:....._..::6:.:.·~64.!.-...:..__..:0:;.:•.:::3~5__;:..__~--!,l_:...... __ ......:....:.:Ye::.:s::....:._H:.::··r:..:'e:::a:.._..:.....:l:..:l:.:.:n~e=ar~"--!Y.:.es=-_:.._.:.!no=n:.:.:e::..__..:.._.!Con='.:.c--''-------- 7' II l'lETHYLENE CHLRii 8.:3 0.35 1 Yes Area lineat' No none Cone B: tns-1,2-DIClENE 9,(K) 0.35 1 Yes Area linear No none 9: 1,1-DiClETHANE 10.11 0.35 'tes Area lineat' 1\io none 10: PWD1 11.40 0.35 Yes Area lineat' No none
lL CHLOROFOO.lil 12. 03 0. 35 Yes Area l ineat' ilia none 12: 1,1,1-Tt'iClETHA
13; CAABN TETRACHLR
14: 1,2-DiClEiHAf~
15: TCE
16: 1,2-DiClPROPANE
_+7: BrihCll'lETHi!NE
:_l~L cis-1,3-DiClPEN
19: tns-1,3-LilClPEN
20: 1, 1,2-TnClETHt'l
21; PCE
1 22: DiBrClMET~~
2~.: CHLORO§NZENE
25i 1,1,2,2-Cl4£THA
27: 1,4-DiClBENZENE
28i 1,2-DiClBENIEN£
l
·; 1"7 ..... -.~;

12.70 13.06

14.19 14.53

14.99 15. 7l
lo.55
1o.B2

17.10 17.43

18.36 19.57

20.22 21.b7
2i.79

22.35 0.35

0.35 1).35

0.35 0.35

0.35 0.35

0.35 0.35

0.35 0.35

0.35 0.35

0.35 i),35

0.35 0.35
Yes Area
Yes Area
Yes Area
Yes Area
Yes Area
Yes Area
Yes ikea
Yes lkea
Yes A1·ea
Yes Area
Yes Area
Yes Area
Yes At'ea
Yes Area
Yes Area
Yes Area
lineal' No
lineal' No
ltnear No
hnear No
l.ineat' No
linear No
linear· No
linear No
linear No
linear No
lmeal' No
linear' No
linear No
linear No
linear No
linear No
linear' : No
none
none
none
none
none
none
none
none
none
none
none
none
none
none
none
none
none
Cone
Cane
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
Cone
ATTACHMENT 6 - 3257
4230
MAXIMA 820 METHOD REPORT
Pt•inted: 22-NOV-1990 i)3:19
HALOG&AROMATIC VOLATILE ORGANlS
:-----------------------------:
: Peak Integration Parameters :
:-----------------------------:

Channel 1
Detection Pat'aaaeters
Baseline Points: 18
Filter Window <in Points>: 21
Integration Sensitivity <Coarse>: 64 .. 42
Integration Sensitivity <Fine>: c.;7. 39
Detect Negative Peaks: No
Skim Ratio: 16.00
m i c: ,.-~ovo 1 t /sec
,n i C n:JVD 1 t / SE"?.C: 2
Rejection Criteria
Minimum At'ea: 800 .. 0
Minimum Height: 57!5. ~3
Minimum Width: 6. '7'(H)
l1l i C I·"'Cl\/Cll t ·-·:;:;(?C
miC:t"'OVDl t
sec
f.S
ATTACHMENT 6 - 3258
4231
MAXIMA 820 METHOD REPORT
Printed: 22-NOV-1990 03:19

HALOG&AROMATIC VOLATILE ORGANIS
:-----------------------------:
: Peak Integration Parameters :
:-----------------------------:

Channel 2
Detectign Parameter's
Baseline Points: 18
Fi 1 ter"' Window <in Points): 21
Integration Sensitivity <Coarse>: 72.19
Integt"'ation Sensitivity <Fine>: 25.73
Detect Negative Peaks: No
Skim Ratio: 8.000
m i c: t~ovo l t /sec:
mict~ovol t/sec 2
Rejection Criteria
Minimum Area: 6524
Minimum Height: 2<Y2:·2
Minimum Width: 7.350
m i c r'rJvcll t -·sec
mict~ovol t
sec
ATTACHMENT 6 - 3259
4232
·· ..
·· ..
··.
'·. ·· ...
·· .•. ····· ... ···
•f-.
.•.
·· .•.. ··• ... ···. ···· .•...
··:t~············ .....
··· ... ··. ·· ..
··•·· ...
··· ...
• ..
···+ ·· .. ·· ....
t!~~'J
... c~
i 11!:1'1
1 1 .........

I
t··
I
r
,
•-.ur·
~··· <:;~
I r,'l')
L
.
i
r
i
I
L
I
I
~·
r.":(
·-· <;;;;•
I
I
,o;,:;
1 ,.-
i
r
!
!
i
I
I
L
·:::;:: i ....... r::;;!
I-I
l
·.. l.
······... r
·············.,·..

I
f
'
)-
9 .............. r .. -··--···-·-,-···· .. -···--···-; ..-............ --·-,·-------·-r·---·--···-·,·--·-·----r-.... - ... --... _,. .. --................. , .... -........ -·--·-r·---------,.---........... -r-···-·--·--· .. 1-- ~~ !'!S
.,:;.:;
~
Q.t
~···
~
0 ,:::;
1,11
~
II!:!" IJ.!
0 t ....

IJnnj . j;.;;l
::.::
<::~
~
·~;:
:t:"
;.~
r.oo~
::t;
·C::
4 ..,
,;_)
;l:;
....

ATTACHMENT 6 - 3260
4233
CHLOROMETHANE C~~ibr~ti~~
Quant Basis: ~tea
Curve Type: Llnear·
Y-axis Label: Concentratwn
Corr. Coef. <rl: C. 996!J918
Pr·inted: 22-NUV-1990 4:04:25
Rejection Tolerance: 204
Weightins: rJone
Coef. of Deterainatian <r2l: 0. 9961872
Equation: Conc*llnJ Vall = -3. 774462£+(J3 + 8.611590£-01 * R Internal Standard: t~one
Forced Throush Origin: No
Swle File Naill! ..YiliL Concentration Reseanse Calc'd Concentration l Deviation lf'H CS1IF'P8 y· l.OOOOOOE+OO 1. 0796501£+04 1.10460i3E+OO -9.47£+)0 lPPB CS21PPB y 1.000000£+00 1. (15.35552£ +04 1.059665£+00 -5.6.3£+0;) 2Pffi CS42PPB y 2.000000E+OO 1.5250828£+04 1. 871785£+00 6. 85£+i}) §-F'B CS73PPB y 3. OOiXiOOE+OO 2.1305326£+04 2. 914562£+0(: 2.93£-'-00 4PFB CS104Pi:'B y 4. Ol.)(l000E-t-Oi) 2.7312951£+04 3.949266£+00 i.28E+OO 3PPB CS135PFB '{ 5.000000£+00 3.3994918£+04 5. 100113£ +00 -1.96£+00 Reseqnse Factor

4. 631130£-{!:

4. 7458:~-{)1
t..557021E-o~

7.040493£-0l

7.322534£-Ul

7. 354040£-ijl
ATTACHMENT 6 - 3261
4234
<:
.....
:z
<
t'"'
0:::
:c
I:"'"
~
!:::;
~
l'tl
~
~
:::r.:t
I'D
Ill
lof:i
i~
:t
I,J~
1'1:1
);;
i-
.::iJ
::!''•
0 0
oo
Cone * In.,j
X .:to4
i-"
0 0
·-'---
Vol
~"1,)
0 0
' ~--·--.J.o
·· ..... ··· ... ·· ...•.
··•·• •... ·· ..•
················-· .. ,
·········-.. ~t.-. ..... .
·•·· ...
··· ...
'·· ... ·., ·· ..
··,· ..
··· ...
w
0 0
..L_
· .. · ..
····.,,
·· .. ·· ..
f>, 9
ATTACHMENT 6 - 3262
4235
Quant Basis: Area
Curve Type: Linear
Y-axis Label: Concentration
Carr. Coef. (r): 0.9914194
Printed: 22-NOV-1990 3:47:38
Rejection Tolerance: 154
Weighting: None
Coef. of Deteraination (r2): 0. 9829124
Internal Standard: None
Forced Through Origin: t.lo
Equation: Conc*(lnj Vol) = -2.119789£+03 + 1.310641£-02 * R Sitple File Hall Valid Cqncentration R!spq!se Cilc'd Cgncentratign l Deviation 1PPB CS11PPB y 1.000000£+00 5.3769075E+OS 9.B54817E-Q1 1.47£+00 1PPB CS21PPB y 1. 000000£+00 5.1525959E+OS 9.2bb833E-01 7.91£+00 2PPB CS42PPB y 2. 000000£+00 9. 6882862E+OS 2.11SblbE+OO -5.46£+00 3PPB CS73PPB y 3. OOOOOOE+t.'O 1.41741t)9E+Ob 3.291477E+Otj -8.86£+00 4PPB CS104PF'B y 4. 1)00(1(1(,'1£ +00 1.5539459E+Ob 3.649374E+OO 9.61£+00 SPPB CS135PPB y 5.000000£+(10 2. 0611669£+06 5.031369£+00 -6.23E-01 · Reseonse Factor

9.29902bE-03

9.7038%£-03

1.032174£-02

1. 05826SE -Q2

1.2B7046E-Q2

1.201249£-02
ATTACHMENT 6 - 3263
4236
0 0
oo
0 0
Cone ·=~· I.u·11._p !!Joll.
0 0
0 -t·-·--·_..,1,·-·----'· .. ---"·----·....l ... --·--'·------L--... -·---'-··--.. -...l__, __ _._ ............... ___ _,.,.,_., __ ,,_.,.,.,.L ...... _____ ,.J ............ .. c~ t··.
1 ',,'·-.. ,
0 (.1'1'-
0 1-"
0 0
~ .....•..
·-.•...
··•··· .•..
*· ····•·· ...•
··•·· •....
·•····•·· ...• _
··•· •..
·········-~··
·•·····•·· .. ,
····-. .. _
'······· ...
'··············· .•.
··•· ... ··· •...
······, ..•... -·~t;. + ··· ..• ···· ... ··., •·• :1" ·•• ••• _ -f~i~ ·· ... ··•· ... '··· .. ,
··., ·· ...•.
··· ...
··•· •..
\ .•.
..;f. ... ·.,
·· •...
'··.\· •...
·· ... '· .. · .. ·-.•..
fJ.''
ATTACHMENT 6 - 3264
4237
BRDMDMETHANE C~1ib~~ti~~
Quant Basis: At·ea
Curve Type: Lineat'
Y-axis Label: Concentt·ation
Cot·r. Caef. (rl: 0.9911957
Pt·inted: 22-NOV-1990 .):50:01
Rejection Tolerance: 15/.

Weighting: tJone
Coef. of Deter1ination (r2l: 0.9824689
Equation: Conc*(lnJ Voll = -9.657870£+02 + 8.474736£-03 * R Intemal Standard: None
Forced Through Origin: No
Sample File Nw Valid Concentration Respqtse Calc'd Concentration X Deviation 1PF'B CSliPPB "i l.OOOOOOE+OO 7.3158094£+05 1.046834£+00 -4.47E+OO lPPB CS21PPB y 1. OOOOOOE+OO 7.1608469£+05 1.020568E+i)i) -2.02E+OO 2fF'B C542F'PB '{ 1.000000E+OO 1.2284b36E+06 1.889023E+OO 5.87E+OO 3F'PB CS73PPB '{ 3.000000£+00 2. 0711704E+06 3.317367£+00 -9.57E+OO 4PPB CS104F'PB '{ 4.000000E+OO 2.2746995£+06 3.662338E+OO 9.22£+00 5PPB CS135PPB ¥ 5.000000£+1)0 3.1015880E+06 5.063870£+00 -1.26£+00 Response Factor

6.834514£-0.3

6.982414£-03

8.140249£-03

7.242282£-03

8.792370£-03

8.060387£-03
ATTACHMENT 6 - 3265
4238
"'• ...
ill
t'!;l
X
1-'*
0 0'~
Cone * InJ ~Jol
0 w
0 0
oo 0 0 r·---'------~---------'-----__L_ ____ _.___ ___ __._ __________ ._ ______ L ____ _._ ____ _, ________ _,_ _________ j ________ _ 0 ............. _
·· ..•
. ···,'···· ... '*
0 I'JI
I 0
I
--1
!
1-
0-----
0 1-
~l
~ I
!:'1.!1 I .
t."!!
0 --1
I
I
'·.,
·····• .. ,
···--·--...• _
·· ..•
···---•..•....
'··~ ..•...
·····, ·· •.. ~-.•...
+"····-.... __ '·· ...
'····· ...
............
'····-.•.
·· ..
·· ..•.
+"'·-.. ··-~·- ....• _
. ·· ..
···--......•.
····· .... -+·
'·· ....
··- ·· .•. _
·· ... ·-.
-f-13
• • f '
ATTACHMENT 6 - 3266
4239
Quant Basis: Area
Curve Type: Lineat·
Y-axis Label: Concentration
Corr. Coef. (rl: 0.9936101
Pt'inted: 22-NOV-1990 3:52:25
Rejection Tolerance: 15%
!*lighting: None
Coef. of Deteraination (r2): 0.9872611
Internal Standard: None
Forced Through Origin: rw
Equation: Conctilnj Voli = 1.133146£+03 + 1.310689£-02 t R Sa!ele File Nale Valid Concentration Response Calc'd Concentration X Deviation lf'PB CSllFPB y 1.000000£+00 2.5545759£+05 8.962801£-01 1.16£+01 iPPB CS21PPB y 1.000000E+OO 2.5195689£+05 8.871035E-Ol 1.27£+01 2PPB CS42PPB y 2.000000E+(i(l 7.6741931£+05 2.238325£+00 -1.06£+01 ~.PPB CS73PPB y 3.000000£+00 1.1478756£+06 3.235b45E+OO -7.28£+00 4FPB CS104PPB y 4.000000£+00 1.3822590£+06 3.850052£+00 3.89£+00 5PPB CS13SPPB y 5.000000£+00 1.7799669£+06 4.89259"".£+00 2.20E+OO Response Factor

1. 957272£-02

1. 984466£-02

1.303069£-02

1.306762£-02

1.446907£-02

1.404521£-02
ATTACHMENT 6 - 3267
4240
I-
...
.....

I
~
""''
r,;,
I-'
~
"""' :1.'::
t<. ::< !:""
IT!
~-- :-.;:
.... 0
lot:l ::r~
f't;
:u
·~

7.1 1'1:;
!.1']
i~
0 ::;:!
Ll'l
iT,I
0 0
0 0
~ .-1-.----.J-----'-.. -·--'-····-·-··-·L_··-·-'------··.1.·-·---- .. L·--"--... J.. ________ .•. .J... .... _. ____ ,_,_, ___ _... ________ _l __ , ... t.S J. 1
·····-.... '•.
··.
j '······ ... ··-...
;-j ~ .. ~,
i ··········,·-... 1 ··· ..... -~ ·········--~ t'•.J I -~:; • f ·-.•• _ 1:?-i ·· .... <..:• i ····· ...
1 ······--..... -1 ~ ···· ...

I ·····:,;:r,. -t ~
w f ' ;,:> --~ ·· .. ··-.
o_1 1
~
'··· .•. i
'1 ···· .. +
J ' ·· ..•.
~.- I ~ ··. ··•··· ...
8l ~ i ·· ... . I ... ··, - '
11 ~ '·. ·· .. _
:-1'! I
~--, - j
· .
... ·· ... ··· ...
i
j
ATTACHMENT 6 - 3268
4241
Quant Basis: Area
Curve Type: Line:at•
Y-axis Label: Concentt·auon
Corr. Coef. (r): 0. '1984634
Pt·inted: 23-NOV-1990 0:31:07
Rejection Tolerance: 207.

Weighting: None
Coef. of Deteraination (r2): 0.9969291
Internal Standard: None
Forced Through Origin: No
Equation: Conctilnj Voll = -5.208785£1{12 + 5.648343£-03 * R Sa!ele File Naale Valid Concentration Response Calc'd Concentration X Deviatioo 1PPB CS11P?B y l.OOOOOOE+OO 1.0118169£+06 1. 038842E+i)i) -3.74E+OO lPPB CS21PPB y 1. OOOOOOE+OO 1.1)31908SE+06 1. 061539£+00 -5.80E+OO 2FPB CS42PPB y 2.000000E+OO 1. 8139712£+06 1. 94501lE+OO 2.83E-t00 3PPB C573PPB y 3.000000E+OO 2.7199207£+06 2. 9b8433.E+OO 1.06£+00 4FPB CS104PPB y 4. 000000£ +(~) 3.5158080E+06 3.867522£+00 3.43E+OO 5PF'B CS1.35PFB y 5.000000£+00 4.623J285E+06 5.118b53E+OO -2.32£+00 Response Factor

4.941605E-03

4.845389£-03

5.512767£-03

5.51%67E-03

5.688593£-(3

5.407360£-03
ATTACHMENT 6 - 3269
4242
X
tfj
::t:: """'
""'"~ t"''
t.!f1
z
1?-1
!:")
:'.:1: X !::""
:::;:!
'""" I!:; 0
"'r.l 0"•
!'!:!
:'J.i
~
~
l'!:i
IJ'i
IT,::
rd
~
lfl
i'r,!
0 0
0 0
0 0
X .104.
0 0
r.,;;
0 -+-·-n--~·•--• .. -•--'--···--~·-•-'----·----~-••-·-----·~---·-•••••...L•--·---.J.,_,__L_,,_,, .. , .... , .... _._ ___ ,,_m .. ••••••-•••;•---·-•••••••••••••••• ,!.,, .. ,,., .. ,,,,., .. ,,,,, .. ..1,, .. ,,,,, .... , 0 ~
J
t·-.. '""".. . .. ,1 ··· .....
•······ ...•..
g-·J··· ··· ..... ···················4.:.
.t;l.t ···· ... ·· ... N I ·· .•...
8 ___ jj ··· .. , ··········· .... ···, .. ·· ...
d
C· I
0 i
~:~··············· ...
·i
Ul
• I
gl
d
•0 i
... ,
l
······•···· ....
·•······ ...•...
··· ...
'·· ··• ...
\ ..
+ ··· ... ···• ...
··. · ...
·· ..
4•. ··· ...
· ..
··.
··•·· ...

ATTACHMENT 6 - 3270
4243
Quant Basis: Area
Curve Type: L1near
Y-axis Label: Concentr·ahon
Corr. Coef. !rl: 0.9876849
Pt·inted: 22-NOV-1990 4:00:46
Rejection Tolerance: 15/.

Weighting: None
Coef. of Deter•ination !r2l: 0. 9755215
Internal Standard: None
Forced Through Origin: No
Equation: Conc*iinj Vall = -2. 737602£+03 + 5. i95989E-03 * R Sa!ple File Halle Valid Concentration Response Calc'd Concentration I Deviation lPFB CS11PPB y 1. (!1)0000£ +00 1.47o3352E+06 9.866839E-Ol 1.35£+00 lPf'B CS21PPB y 1. C~jOOOOE+OO 1.4089352£+06 9.166420£-01 9.09E+(l(, 2PPB CS42PPB y 2.000000E+OO 2.6307815£+06 2.186382E+OO -8.52£+00 3PPB CS73PPB y 3.000000E+OO 3.6994292£+06 3.296918£+00 -9.01E+OO 4PF'B CS104PPB y 4.000000E+OO 3. ~'526792£+06 3.560095£+00 1.24E+(ll 5PP& CSI35PPB y 5.000001)£+00 5.3895420£+06 5.053280E+OO -1.05£+00 Resegnse F!ftor

3. 3867b5E-03

3.548779£-03

3.801152£-03

4.054680£-03

5.059859E-03

4.638613£-03
ATTACHMENT 6 - 3271
4244
""""
:J
1,1~
I
..
"""'
N
I
!!;;.!
.....
f."':!
- X f:!!j
z i- rr.:! .C>
"T.:! ~,..,
!'!!I
~
"'
~
1'1::
lfl
t,..:
,;5
::t
lfl
1'1)
Cone ·:JoE- I n.,j Uo 1
x J .. o 4
0 0 0 0 00 ~:;::. 0 0
0 -·!-·••"' ......... -. ...I ........ _ .............. ..I ......... - .............. J ...... _,,_,. __ , .. L._ ............. -.I.. ....... ____ __,_, ... _._ ..... ..I .... - ............ - ••. f ............ - ........... 1 ............................ !.... . ............ , ..................................... i.. ........ ,.,. 0 ~
J'•
~ -~ ', '----,,
~~- ············•·· ....
•0' ····· ....
0 ········ ...

Jl ·, l ······ ....... .
w -, · ..4:.
0 ·-·1 '·
0 -i ················· ...
····• .. ,_
···· .. ,
"".
.0
.. ·~...J ················ ... ,
0 '
-1
I U'l ... 1
0~
() ·-1
I~ j I
·~
g ~
I
-j
I
~ l g--·1
-I
-1
..;:!::.. .. ·: · ••. ·· ... _
·· ..
+
··· ...
·· ....
·-.•.. ·.
··· .... ···· ... ·· ...
··· ...
+. . '·· ...
··· .. ,
···· ...
·· .. ,_
·· ...
··· ... ·· .•...

ATTACHMENT 6 - 3272
4245
Quant Basis: lkea
Curve Type: Linear'
Y-axis Label: Concentration
Corr. Coef. (r): 0.9954672
Pt·inted: 22-NOV-1990 4:05:02
Rejection Tolerance: 15/.

Weighting: None
Coef. of Detera~ination (r-2): 0.9909549
Internal Standard: None
Forced Through Origin: No
Equation: Conct\InJ Vol) = -2.60~32£+03 + 4.390265£-03 * R Salple File Naae Valid Conc:entration Reseonse Calc'd Concentration 7. Deviation 1PPB CS11PPB y 1. 000000£ +00 1.6697640£+06 9.450150£-01 5.82£+00 lPPB CS21PPB y i.OOOOOOE+OO 1.7095176£+06 9.799208£-01 2.05£+00 2PPE CS42PPB y 2.000000E+OO 2.9078692£+06 2.032137£+00 -1.58£+00 3PPB CS73PF'B y 3.000000£+00 4.3148510E+Ob 3.267542£+00 -8.19£+00 4F'PB CS104PPB y 4.000000£+00 4.9091455£+06 3.789364£+00 5. 56E+(i(l 5PPB CS135FPB 'i 5.000000E+OO 6.2719995£+06 4.986022£+00 2.00£-01 Response Factor

2.994435£-0Z

2.9248()2£-03
.3;.438944E-03

3.476366E-03

4.074029£-03

3. 9859/Ci -03
ATTACHMENT 6 - 3273
4246
...
, ......
0 .
0 0 0
~ ·-·-
0 '- 1
::.., -1 .....
¢
•1
~ j
J
: J 0 . ..... .... ·-·~ ..... ._. I
C• ~
(JI
o·····
¢
I
0 0
0 ¢
---.;:--L.. ........ ·--····-·'--··-·--·-.L··-·-·-·····---·-·j-··---·-··- .. -1-.......... - ....... ..L--·-···-.L-..... - ......... -l ............ -·····---L----··-···-···-··'--···--1·······-·····.L .......... ,,. __ ,,.,, ... i. ........... - ··-.. , __
'· ...
'···-.. ,_
····.,_
····~
~$t!··., __
··, ., ___ \
'·····-...
··-.. ,
···-.,
·······--.:a::t-:..
-...
.................
·· ..• _
·.,
··•··•··· •...
'·· .. '·-, ·-•.. ,_
·· .. + '· .. ,_ ··· .. ,
'··,_ ··,
·· ... + ···-...
···--....
'····-.,_
··-..• _
··-...
·-...
·····•··· ...•
···---•..
'··
*,, -....
··-.. ,
--•.. _
···-.. ... ··· ..• _
·-•... ··,_
fJ.21
ATTACHMENT 6 - 3274
4247
1,1-DiC1ETHANE C~1ib~~ti~~ R~p~~t
Quant Basis: At·ea
Curve Type: Linear
Y-axis Label: Concentt•ation
Carr. Coef. (r): 0.9924819
Printed: 22-NOV-1990 4:11:47
Rejection Tolerance: 1S7.

Weighting: None
Coef. of Deter~~ination !r2): 0. 9850204
Internal Standard: None
Forced Throush Origin: No
Equation: Conct(Inj Vol) = 1.396241£+03 + 5.157453£-03 * R Swle FileNw ...YiliL Concentration Reseooy Cilc'd Concentration X Qeviatioo lPPB CSllPPB y 1.000000£+00 6.8881312£+05 9.897525£-(ll 1.04£+00 1r'Pb CS21PF'B y 1.000000£+00 7.8654937£+05 1.090567£+00 -8.30ET00 2F'PB C542F'PB y 2. OOO(Ii)OE +00 1.574151)7£+06 1.902970£+00 5.10£+00 3PPB CS73PPB '{ 3.000000£+00 2.BB04707E+Ob 3.250427£+00 -7.70£+00 4f'PB i:5104PPB y 4.000000£+00 3.2859627£+06 3.668688£+00 9.03£+00 SF'PB CS135PPB y 5. 000001)£+00 4. 6712470£+06 5.097596£+00 -1.91£+00 Respqnse Factor

7.258863£-03

6.:.:.56880£-03

6.352632£-o::;

5.207482£-03

6. OB6496E -o:;.

5.351890£-03
ATTACHMENT 6 - 3275
4248
0 0
0 0
s ·-r~~---"---~-'-----~---~--~--'---~---"---------~--L. ___ _ I ·· •..
'·· ... . ··· •...
.. ··-..

J
J
,~·~
C> I
I
I
i
I
d
- I
o I
I
·· .. ·· .. · ..
··:;.."i;:..
'•'"'• ··.,_
··•· ... ·· ... ·· ...
'··········· ...
·· .. ··· .. ,
·· .. · ..• ··., ·· .•.
·········.,
··•···•··· •...
• ..
4~ .... '·· .•.
··· ... ·· ... · ..
·· .. · ..·· .. ·.,_
·· .. ·· ..
· ..•..

ATTACHMENT 6 - 3276
4249
Quant Basis: At·ea
Curve Type: Linear
Y-axis Label: Concentration
Corr. Coef. (rl: 0.9997041
Pnnted: 23-NOV-1990 0:30:45
Rejection Tolerance: 20%
Weighting: None
Coef. of Determination !r2l: 0. 9994083
Internal Standard: None
Forced Through Origin: No
Equation: C~nc-tHinj Vall = 1.573048£+02 + 1.44302.3£-02 * R Salple File Name ...wJL Concentration Reseonse Calc'd Concentration X Deviation H'B CS11PPB y l.OOOOOOE+OO 3.3276272£+05 9.918297£-01 8.24E-01 lPPB C521PPB y 1.000000£+00 3.3261637£+05 9.914073E-Ol 8.67£-(1 2PPB CS42PPB y 2.0000COE+OO 6.8554494£+05 2. 009976E+l)(l -4. 96£-(!1 :.PPB CS73PPB y 3. <)(H)OOOE +00 l. 0242374£+06 2.987458£+(10 4.20£-01 4F'PB CS1il4PPB y 4. OOO!X:OE +00 1.3993661£+06 4.070097£+00 -i. 7:2£ +00 5PPB CS135PPB y 5.00000!)£+(10 1.7039819£+06 4.949232£+00 1. 03E+O(i Response Factor

1. 502572E-(12

1. 5CC33E -02

1.458694E-02

1.464504£-02

1.429219£-02

1. 467152£-02
ATTACHMENT 6 - 3277
4250
j,..u
..
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i••dt
~-~
l=')
.....
~j -
~ X ,...,
~:r. ..- ::~~ 1;:>
'"i"1 o;:f';
i'~ ...
~l·
"""'
::0
o'f:;
!,1'!
1-rj
0 ~J
\ii
I'D
0 .:;::. c
~~ ···i········;::·:··--·--'··-······-···--'-··-·······---'··-·····-···---L------'-············--··-·'--··--···---·-'--····-·---·l-·-·-··· ··- -·-··-'····-····--··---'--·····-····-··-··•···-···············-·-·:·······--·· .,_.. i ·· ..... ··I
i
i
"1
I
I
-1
..,... I
0 --~ 0 i
1 -1
I
-j
N I
~·- ·-···1 o I
I
1 I
··-i
i
'
-·1
.:,..;t !
I 0 .... ,
.;:) j
j
I
-1
i
J
i
,.j;;o I
0 -i ~::> I
j
. J
I .. ,
·., ·· .. ·., ·· .. '·· ...... .
.. ·· ..
•····•···•··· •....
'·· ..
~ ··· ...
·· ...• ·· ... · .. ·· ...
·· .•..
· .. ·+ '· ..
·•·· ..
··-...
···· .•.
·•. ··., ·· .. ·-...
· ... ·· .. ·· ..•.
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4~·· .. ·.· ··· .•...
·· ..•. ·· •..
··· •... ··. ·· .. ·· .. '· .. ·· •... • .
·· .. · •..

ATTACHMENT 6 - 3278
4251
1,1,1-T~~C1ETHA C~1~b~~t~~~
Quant Basis: Area
Curve Type: Lineat·
Y-axis Label: Concentration
Printed: 22-t~GV-1990 23:3-4:4!:.

Rejection Tolerance: 20'!.

Weighting: None
Internal Standard: None
Forced Through Origin: No
Corr. Coef. (r): 0.9949805 Coef. of Deter•ination (r2): 0.9899862 Equation: Conc*<Inj !Joll ::: 7.331959£+02 + 6.245311£-03 '* R Sa!l!flle File Nalle Valid Concentration Response Calc'd Concentration 4 Deviation 1PPB CS11PPE y 1.000000£+00 6.4583281£+05 9.533245£-01 4.1:10£+00 lPPB CS21PPB y l.OOOOOOE+OO 6.8710562£+05 1.004877£+00 -4.85E-(•J 2PPB CS42PPB y 2. 00(i(li)OE +00 1.6414812[•06 2.196951£+00 -8.96E+OO .3PPB CS73PPB y 3.000000E+OO 2.2787032£+06 2.992881£+;)0 2.38£-;)1 4PPB CS104PPB y 4.000000E+OO 2. 864113:.£+!)6 3.724095£+00 7.41E+OO 5PPB CS135PPB y 5. OOOCij)OE+OO 3.9879772£+06 5.127871£+1)() -2.49E+OO Response Factor
7a7~1~42E-r3

7. 276'~"02E.-0.3

6.092059£-03
.~. :!826S'1E -03

6.982963£-(!}

6.268842£-03
ATTACHMENT 6 - 3279
4252
co n c * I n·11 .,j '·' ·c~ :n.
•.. -~~. o·4. :..-• .....
0 0
g --l;~::::~-~-------------•---·-····-··--.J---------------J·---------'---·----------·········-··-------'· . ··········-··----J _______ ,. ___________ , ___ ···-····-·····-'--·-···---------·······-·······-··-··· ... .J ............ . __ , ·,_ ·-.,
'·· i ···· ... 0 -1
-...... _
~ ... J ··.$-...... _ I -. __ -~ '··-, __
~ ,_ '·····~. _ _j
? I ' ~ --, ~~-- 0 I ·--...
l ···-·,,,
_i ··---._ '·····-.• ~:r~-
~l -;
I
0 i ~_j
<~ ~
i
-1
I
J
I- I
c· --1
0 J
I
-I
!=<• -j
I
"-l
t'>,:I .
~~ ~
\ ..•
··\· ...
··., ·· .•... ·· ..•.
······~
·· •.. ·-.
'--., ___ 4~--
·· ... ·· ... '· .. ,
· ..•..
·· .. ·· .•..
·-.

At·
· .•. ··= •. ATTACHMENT 6 - 3280
4253
Quant Basis: Area
Curve Type: L1near
Y-axis Label: Concentt·atlon
Corr. Coef. !ri: 0.9975601
Pnnted: 23-NOV-1990 0:.31:37
Rejection Tolerance: 20/.

Weighting: None
Coef. of Deten~ination !r2 l: 0.9951262
Internal Standard: None
Forced Through Origin: No
Equation: Conc•<lnj Voli = 3.3~)369E+02 + 2.460315£-02 * R Sample File Hale Valid Concentration Response Calc'd Concentration ~ Deviation lPFE CS11PPB y 1.00000C£+0C 1. 8593848£+05 9.819418E-01 1.84£+00 lF'PB CS21~'PB y i. OOOt)OOE+OO 2.0792486£+05 i. 090129£+00 -8.27E+OO ZPF'B CS42FPB y 2.000000£+01) 4.0304144£+05 2.050225E+OO -2.45£+00 3PF"B CS73PPE y 3. 000000£ +O;) 5.5127231£+05 2.779614£+00 7.93E+0(; 4FFB CSii.AF'Pb y 4. t)!)(j!)(n)£+00 8.1286137£+05 4. (;60797£+00 -l.o4E+OO 5PFB CSl35PPB y 5.000000£+(!0 i.0088720E+06 5.031293£+00 -b.22E-(;l Response Factor

2.689061£-02

2. 404715£ -!)2

2.481134£-02

2.720978£-02

2. ~60444£-(12

2.478015£-0:2
ATTACHMENT 6 - 3281
4254
i"'"'
j,'J,..
::;::J
.~
~ '·
il••l
i:'fl
i""'!
''!*
.......
~L· ~: .....
"""'
['~'] i<mf:

C• ~:i o'·•
•'tt
:!1.•
:;~;."'
:;2;;!
l't:
i/;
'ti
;:;
~
i,{j
, ....
•.
('~~
·~· ·~>
.>< . .il ()4.
:::::~ ··-+, .. ·;_·~·.··-··----··-·-·-·--- .... ---·-···--·---·--·-·-·-·--··,,, ____ l_, ___ ,, __ , __ ._,,,,.,.,.,,,.,_, __ ... , ________ ,, ___ _, __ , ............... J ....... ,_,,_,,_,,_, .. ,,,,.,_, __ , ___ ,,,J,.,, __ ,. ____ • __ ,,,,.,., _____ j_, .. ,,.,,. !;-=~ -j ·•·· ...
i '• .. ... f ··•··.

I '··.,,_
-1 ····· .., ·~ ....... =:·'"'l · .. \il;:• ..... +··.
l
:: .. -.j
:~:~ I
... 1
!
.J
!
!
-~ t:...:; I
:.....J
''m~~' t
o I
"'j
i
.. ~
I
-! ~~ i
~ .. ·--·1
C,; !
"i
l ... ,
... ,1
!~:j
" i :~· ---j
>;: I . ,,,. I
~ _,
;;:t'• I
~~ ..... ~ ...... I
C•
-·l
!
--i I
I ... ,
I
'· .. · .. '•,
··· ... '·.
·· ..•. ·.,_
• ..
·,_
··. · ..
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····•·· ...
·· •... ·· ...•.
···•·· ..
'·· ..
·····=+
'·· ..•. ·· ... ·.,
·· .. ,
·· .•.
··.,
·•···· •...
'·.
~--.•. \ ..
··. ·· ... '· ..
·· ..
·•··· ...

ATTACHMENT 6 - 3282
4255
Quant Basis: At·ea
Curve Type: Lin~ar
Y-axis Label: Concentration
Carr. Coef. ( r) : 0. 9980509
F't'iilted: 22-NQV-19'10 23:23:37
Rejection Tolerance: 20/.

Weighting: None
Coef. of Deter~~ination Cr-2): 0.9961057
Internal Standard: None
Forced Through Origin: tJo
Equation: Cone* (In .i Voli = 1.162986£+02 + 4. 629308£-03 * H Sallflle File Hille Valid Concentration Response Calc'd Concentration I Deviation lPPB C511PPB y 1. OO(li)l)i)£ -tOO 1.0104958E+06 q.588390E-01 4.29E+OC' lPFB C521PPB y 1. (iOOOOOE +i)(J 1.1809844E+06 1. 11668&E +('(• -1.04E•Ol 2PFB CS42PPB y 2.000000E+OO 2.1656117E+06 2. i)2E316E-t00 -1.40E+OO 3PPB CS73PPB y 3. OOOOOt.i£+00 3.0854237E+06 2.879935E+OO 4.17E+OO 4PFB CS104PPB y 4. OOOOOOE+C~j 4.1925682£+06 3. 9')4998E+OO 2.43E~YJ 5PF-B CS135PPB y 5.000000£+00 5.4953835£+06 5.111224£+00 -2.18E+OO Response Factor

4. 948066E-o::::

4. 22.375bE -;)3

4. 617633E-•:~.~

4.861569E-o:.

4. 77046E-o::

4.549273£-03
ATTACHMENT 6 - 3283
4256
~) """'
~
'"!:I
1'1:! v ~.1 :'"':
~ i-o•·
;,::! C•
!'r.i .~h
tfi
loja' •I
i~
~:;1
Ui
;j,;
..• .. 1 !["• ··J. ·'"· ... ..,
(:>
0 0 Q
0 -·+-·-·-·--··--·=-·------·'--·-·········-··· .. -·-·-··---·····-L-·--··-_;··---·····--········..l------·-·.....,·-·--·---L ......... _____ J .......... ----··········-'···-···--·--·······--'····--·-··-··-··-·····L···-······· C• I
.J• .. I ·· •..
',: '· ·· ... 1 ··,
· .. ~. ··•···· •.... - '·· ..•...
:.... ~ ······· .. :~!.,·
.c; I ~$· ....
1 ··., I ·· ...
··! ········· ..,
~ i ··· ... ··.
c. .... :· ... -~, ·· .... ... ·+·· ... - .. ' ·i ·· ... i ... 1
i
t;,.,) "1
;:) -1
.:-.:;:. i
i
·1
I
~ I
0 ..... ,
<:~ ~
I
·· ... ·· .. , __
· .. ·· .. ;· .•.
·•·· .•..
.a;• .. . -. ., .... , __ _
··. ·· .•.
'· ..
·· ... ·t· '•+ ..... ··.:,:·
·· ... · .. ·· ..
·· .. ·.,_
··· .. ,
··. ·-..,,f.o · .. ·· •.. ATTACHMENT 6 - 3284
4257
ICE
Quant Basis: Ar·e:~
Curve Type: L!nectr
Y-axis Label: Concentra~ioo
Carr. Coef. (t'): 0. 9S76125
Pr1nted: 22-NGV-1990 23:23;53
Rejection Tolerance: 20/.

Weighting: None
Coef. of Deter~~ination (,-2): t),9952307
Internal Standard: None
Forced Through Origin: No
Equation: Cone* \In J voli = -9. 633183£+02 + 5. 543515E-03 * R Sample File Name _llill!L Concentration Response Calc'd Concentration 4 Deviation lPf'f. CS11FF'B { 1. 0WOi)!JE -tOO 9.6209387£+05 8.740i27E-01 i. 44E-t(ll l~H CS21P;:B -{ 1. G00({J0E +(iO 1. 0770994£+06 1. (iO l520E -rOO -1.52E-01 2Ff'B CS42FF'B y 2. ljOiJOOOE +i)( 2.0989195£+06 2.1344:5E+(i) -6.)JE-t(;O 3PF'B CST!wPB y 3.000COOE+OJ 2.9982945£+06 3. 131554-E+(H) -4.20£+00 -iFP::. CS104F'PB y 4. 00(H)tJOt-t~:{J ).68o9857E+Oo 3.895109E+OC 2.t9E+OO 5PPb CSi35PPB y 5. i)(H)')i)OE +00 4.6505270E+Ob 4. 96)3;;;(,£+00 7.38£-0:

Response Factor

5. 19699BE-,J3

4. 64209?::-;)3

4.764356£-03

5. oo2i344E-o:J

5. 424485£-:C:
~. 2~75735E-(i3
ATTACHMENT 6 - 3285
4258
,,....,
,,
f.\)
F.:,l
.....
~:"':t
, .....
"":,
~:r,:!
('it
l•r1
:x: ;ri.
z I- !•.f'!
0 ~ cr·,
!'~!
~:u
~I
:::r.;
f~
ll!
"fj
4J
::;
~·· ~~·
!H!' ·a ·r·4: .I'· .... .•. 1
0 g -t::~:::::"-"""_ .. ._. _____ ... _ .. J,_, ___ ,.&..., _____________ I..., _________ ._ __________ , ... ~-···'--·····----·-·-----·--··-.!_ ....... _, ______ ..;_, ... ,., ___________ ,,,, _________ ,, .............. 1.._ ••.••. ,_,,,. ___ ,., ••••. ;. _______ ••..

I ·.,_
J ····· ... ·.
"'""
-~ .
-j t."'J 0
l
··.,
'·······t ·· •... •·· ... ·· ...
···•··· •...
·i
l
i
!:'•-' l . · .. _
<:!! -1
·~:~~
-' I
_J
I
I
!:...;. -·1
i . .. .. ~ 0
<:::. .J
I
_J
j
...1
~
--~ .
0 •0•
i
I
··I I
!
1~,1'1 l
" I
1!~~~1 ""i (:~
J
I
-1 !
I
1 i
·· ... _
..=:~···· ... ··· .. ,
··., ·. ~. •.
•., ·· ..
·•. ·•·. · ..
'······i· · .. ·-..
··•· ...
··. · ..
·· .•...
·-..
'·.

ATTACHMENT 6 - 3286
4259
Quant Basis: Area
Curve Type: Llnear
Y-axis Label: Con:::entt·atwn
Carr. Coef. <rl: ·~. 99?51312
Pt·inted: 22-NOV-1990 23:24:08
Rejection Tolerance: 20!.

Weishtins: None
Coef. of Deter•ination (r2 l: 0.99516&3
Intemal Standard: l~e
Forced Through Origin: No
Equation: Conc*\lnJ voli = 1.874608£+02 + 5.174059£-03 * R Sa!Ple File Naaae Valid Concentration Reseonse Calc'd Concentration X ll!viation ·iFh CS11:·p& y 1. OOOvOOE +00 6.0977012£+05 8.754519£-01 1.42E+Ol :F'PB CS21PFB y l.OOOOOOE+OO 9.0849o25E+05 9.776149E-Ol 2.29E+OO 2Ff-·B CS4ZPPB 2. 000ij90E+OO 2.0654760£+06 2.174871£+00 -8.04£+00 3FFB CS73PPB y 3. (li)OOOOE +00 2.9581802£+06 3. :)98652£+)0 -3.18£+0(• 4P;:.B CS104f'FB y 4.(100000£+00 3.7617900£+06 3.930237£+00 1. 78E+OO ::.PPi:; CSL\5Pfil 'f 5. (l(iOOt)i)£+00 4.7406500£+06 4. 1'43173£+0!) 1.15£-!-=)0 Reseonse Factor
u.1 · ·7pr~ ---~ ~ .::.:-u . .)

5.503600£-03

4.841499£-!j3

5.070o85E-03

5.316618£-(:3

5.2735-38£-(<)
ATTACHMENT 6 - 3287
4260
!:r,:t
~:t:l
.::;'
:::r
I~L~f
~
;.o.
!:"":!
......
:::1:
l:r.'i
, .... ~
>:: ·::~:;:
~'r.t· ~-.
2 ~::a
~~ 1.1'•
1'1::
•:J/
~
~~r,i
i'!:;
!,i'!
i~:
·:;:J
:~~
1,1~
!'1;;
0 0
0 ><. .1. o4
c.) --··t·----·····~::--····;····-·········-·-·····;-·····-····-·-··-····'-···-···-----·-·····1-··--·····---·····.t..... ·-···-·-·-··-··---1-·-·-·····-...1...---··-·--·--··-J··--·-·--····-·· .... ------·-·-··..f·--··--·-·-····-·-'-···---···-·······-j-··-········ o I ···· ..... I ..., __
~ ····· ....... ·+
·~ i $.
;.J'f ·---1 '·
·o I
I
I
-1
I
\.
'··
'·· .... · .. ·,
· ..'·.
'·. ·· ..
··· .•.
·•. ·,
,,f•······· ...
"'······ ..•
~>·· ..... ···•··•··•·· ....... _
·· ...
·-.•.. '·. •.
·•·· ..
·· .. ,
· .. ··· .. ,
'·.,
-.... ~
·· ....
········-...
·· ..•. · ..
·· ..• · .. · •..

ATTACHMENT 6 - 3288
4261
BROMODiC~METHAN C~~ibr~ti~~
Quant Basis: Area
Curve Type: Lineat·
Y-axis Label: Concentration
Corr. Coef. (rl: 0.9965433
Pt'inted: 23-NOV-1990 0:32:19
Rejection Tolerance: 20/.

Weighting: None
Coef. of Deter~~ination (r-2): o. 9930986
Ectuation: Conc*(lnj Voli = 1.335310£+03 + 9.924069£-03 * R Internal Standard: None
Forced Through Origin: No
Sa!ple File Hue Valid Concentration Response Calc'd Concentration I Deviation 1PPB CS11PPB v 1. i)QOOOOE +00 2.7850309£+05 8.198.38EE-01 2.20E+Ol lFPB CS21PPB '·' l l.OOOOOOE+OO 3.9293134£+05 1.04e958E+OO -4.49E+OO 2PPB C542FPB y 2. 00(!!)0!)£ +00 9.2136181£+05 2.095794£+00 -4.57E+OO 3PPB C573PPB y 3.000000E+OO 1.4694789£+06 3.183704E+OO -5.77£+00 4PPF. CSi04PPB y 4.000000E+OO 1.8656570£+06 3.970044£+00 7.55E-O! 5Ff9 CS135PPB v 5. OOOOOOE+•)O 2.3259612£+06 4.883662£+00 2.38£-'-0C Response Factor

1. '9:<5l::E-•);:

1.272487~-02

1. U95 35~)£-;)2
l. 0207J':!E->:J2

1. 0720(i81:-0:2

1. t74824E-Cl2
ATTACHMENT 6 - 3289
4262
I~J
.....

I,J'>
I
,_ ..
c...;.

I
~
Jml•
.--,
,_, ..... '"!::I :''"
~
'""" z 0
"or:! ~T·•
!'!)
!lJ
::J::"
~~
!1:1
Ill
''r.i
0 ~
i,l'!
1'1:1
0 n
0 oo
0 0
Cone: -31;f I n,J Vo 1
1:\,'J
0 0 0 --~~ __ ...._ __ _L___,___,_ _______ J. ____ ,..__ ______ J. .. _____ _. _______ __._ _______ .... __ .._ _____ .. , ... L.. ___ . 0 ~ '"·· .. I ····· .....
~ '·
~ · ...•.. '
=~·J' ······ .. : ......... ..__ '··· .. ,
1:1 ··· ...
'·* '· ..
l ~
·1
~ ~..:1 II
C• ... -
C•
~
·· .•..
···•·· .•...
·· •... '·. ·· ... ·· ...•.
··•· ...
<J;.'·· .•........ ,
·· .. ·· .•..
·· ... + .
··. · ..
·· .•.. ··•· .. ,
···•···•·· ..•.
·· ..
.,:.p.. · .. ·· ...
··· .•. ~ ..
··· .. ·· ... '·· ··. ·· .. ·· ... ·· ... '·· ... ·· ...

ATTACHMENT 6 - 3290
4263
Quant Basis: Area
Curve Type: Lineat·
Y-axis Label: Concentration
Carr. Coef. (rl: 0.9894167
Equation: Cone* iln J IJoll
Swle File Nale Valid
lPFB CSllPPB y
lF'Pl:l CS21PPB •j
2PPB CS42PPB y
3PPB CS73PPB y
4PFB CS104PFB y
SFPB CS135PPI:l y
Printed: 22-NOV-1990 4:36:57
Rejection· Tolerance: 15%
Weighting: None
Internal Standard: None
Forced Through Origin: No
Coef. of Deteraination (r2l: 0.9789453
= 6.876645£+02 + 7.624581£-03 * R
Concentration Besponse Calc'd Concentration 4 Deviation l.OOOOOOE+OO 5.7238037£+05 1. 0 10365E+OO -1.03E+OO
l.OOOOOOE+vO 6.1849225£+05 1.08i.J682E+OO -7.47£+00

2.000000E+OO 1.2194579E+06 1.997104E+OO 1.45E-Ol

3.000000£+00 2.0017261E+06 3.189998£+00 -5.96E+OO

4.000000E+OO 2.2346812£+06 3.545235£+00 1.28E+(il

5.000000£+00 3.3044987£+06 5.176617£+00 -3.41E+OO
Besponse F t= tor

8.735450£-03
B.08417bE-03

8.200365E-03

7.4935~3£-03

8.949822E-D3

7.5b5444£-(i3
ATTACHMENT 6 - 3291
4264
l.tJ
......
'· •'
-:;:::.
<:, 0
0 ···· 1' o 4 .r'-li. ..

C.'• ····-·i-'"-';'""'""""'' ...... I ........... , .. _ .. _,_,.,,.J,... ..• __ ...• ~ .. --. .L...., ... ______ ,., ...... l ....... _, ..... ,_,,,,,I----··•· .. --.. --J ........... ---......... 1 ...... _.,, ......... _! ___ ... _ ........ 1-------·---·-.. J. .......... - .. --.. -.L ......................... -l ............ . ~5 I ·· ...
· ....
, . ...,
~I . ··.
... !
I
.;,,• 1
J.;. -·1
·:::> !
-i
I
·'1
i
C• .. 1
..,
!
.::;;:. I
'~b, ~ 1
~- ; ..•. ....... !
5( I '...r' . ...f
I
-1
I
·· ..
··.
····~:;.
··. ·· ..
··. ···¢· ·· .. •• ••• !
·· .•... '· .•.
'···~ ..
• .. ·, __
·•. · ..
··,· ..
'··.
'+~ .. ··. · ... ...
·· ...
··· ..•
···-·•·· ...
·--~~-
·· ..•.
'··.
'· ..
·-... _
'· .. ,
··~--- ...
'·· ..
··•· ...
-~f.-.
···•·· ...
·.,
···· ...
··. '·· ... '·.

ATTACHMENT 6 - 3292
4265
Quant Basis: At'ea
Curve Type: Linear
Y-axis Label: Concentration
Carr. Coef. (rl: 0.9990953
Printed: 23-NOIJ-1990 0:33:04
Rejection Tolerance: 201.

Weisflting: None
Coef. of DeteNination lr2l: 0.9981915
Internal Standard: None
Forced Through Origin: No
Equation: Conc*<Inj Vall = 8.803937E+02 + 1.973323£-02 * R Sa!ple File Malle Valid Concentration Response Calc'd Concentration X Deviation 1F'PB CS11PPB y 1. 000000£ +00 1.9484680E+05 9.450701E-01 5.81E+OO l~='PB CS21PPB y l.OOOOOOE+OO 2.3711691E+05 1.111895E+OO -1.01E+01 2PPB CS42PPB y 2. C~)OOOOE+CO 4.450S197E+05 1.lf32660E+OO 3.48E+OO 3PPB CS73PPB v 3. rXJ00t)OE+OO 7.2135425£+05 3.023009£+00 -7.61E-01 4PPB CS104PPB y 4.00oOOOE+OO 9.5680675E+05 3.952256E+00 1.21E+OO SPPB CS135PPB v S.OOOOOOE+OO 1.2311799E+06 5. 035110E+OO -6.97E-01 Response Factor

2. 56bl1.;'E-()2

2. iUB664E-02

2. 246777E-02

2.079422E-02

2.090286E-02

2.030573£-02
ATTACHMENT 6 - 3293
4266
I-'•
..
"""'
!;=,,~
, ... :~
~
lm'•
()
""'''
~ '!t' Juail •·· ~ 1-~' ::r.:!• c~
'"i:;i ;:,'f·~
!'J:i
;:U
~
'::r.:!
"l:l
;,1'1
"'~ 1::)
:~j
!.f'1
l'l:l
Cone: ·:tor. J: n,J Vol
)·( .:il..()4
0 0 0
oo ;::> 0 .......
·····''
8 -r -~----·---------·-····-'-........... -.... _l..._ .. _ .. ____ ...... _________ .. ____ .... ____ ... __ .. __ L.. ....... - ... -... -.L--.... --..................... ________ .. ··--····-···· .. --.. -.i ............. .. ·-,····· ...•.

I ·., ··· ... . ,.t ·· •...
i '·
I
""i
: ·-1
<::. i
i
I
""1
!
...j
~ ___ j
·:::> I
.. J
I
l . .1
I r..,.] I
~~~ ..... ,
·6 I
-!
l
-1 ~ i
i
C• ·--1 ("~
m' I
1 I
-I
I
!
·· ...
·· .•..
·•·· .... '··.
~~-•.. ·· •...
···•· ...
··· ...
··. ·•· .•.
····•···• .. ,
·· .. ,
·· ...• ··., ·· ..
·· .
·· ...
····-.. +
·-.•..
·· ..
·.,_
·., ·· ...
4=---.
·· ..
·· ....
· ..

ATTACHMENT 6 - 3294
4267
lilant Basis: Hl'e3
Curve Type: Lineal'
Y-axis Label: Concentr·ation
Corr. Coef. (rl: 0.9983439
Pl'inted: 23-NOV-1990 0:33:33
Rejection Tolerance: 207.

Weighting: None
Coef. of Deter~~ination (r-2): 0. 9966905
Intemal Standard: None
Forced Through Origin: No
Equation: Conc*<InJ Voli = -1.421809£+03 + 7.193796£-03 * R Sa!ele File Halle Valid Concentration Reseonse Calt'd Concentration % Deviation lPPB CSllPFB '{ l.OOOOOOE+OO 9.1760562£+05 1. (;.35852£+00 -3.46£+00 !PPB CS21PPB y 1. 0(i0000E+•)0 8.b0Bl812£+05 9.541484£-01 4.81E+OO 2F'Pf CS42PF'B ~ 2.000000t+OO 1.6308276£+06 2.062007£+00 -3.01E+UU 3PP& CS73PPB I" 3.000000E+OO 2. 1062802£+06 3.03~~820C+OO -1.11E+OO 4FF'& CS!•AFf'B y 4. (li)(U}!)(l£+00 2.8599825£+06 3.8304b5E+0(i 4.43E+OO 5fPB CSi35PPB y 5. OOC!(JOOE +Oo 3.7310412£+06 5.083706£+00 -1. 65E+i)0 Reseonse Fador

5. 448964£-0.3

5.808428£-03

6.13Hi56E-03

6. 5C;398CE -03

6. 993(!50£-(:3

6.700542£-03
ATTACHMENT 6 - 3295
4268
··.-· ·H ,;"'1.4. .h. ..n .. _,,,..

0. 0
c, ~ ---l-·-....... -........ ,, __________ ,;,_ .. ,_ .. ,_ .......... , ... _, __ .......... _L ........ ____ ,,.J .. _. __ .,,. ___ , ____ , ........... - ......... ___ , .. _ .... ___ l. ___ , ........................ ___ .. __ J.. .......................... __ ..................... : ............ .. ~·- i .::~ J,
1'·, '·· ..... ···i ·· ••.

I ··· ...
-4
I
-,
0"• i • I
•0 ··-j 0 I
·· ... · ... · .. · ...
'-.• ·,_
'·· ..
'·· .. ,
·· ..•. ·· .•... ·· ..
·· .. ·.,_
·· .. +···· ...
·· •...
·· .. '· ..
·· .. ·· ..•. · ...
·· ... ··.,
ATTACHMENT 6 - 3296
4269
Quant Basis: Area
Curve Type: Linear
Y-axis Label: Concentration
Corr. Coef. (r): 0.9987313
Pt'inted: 23-NOV-1990 0:33:58
Rejection Tolerance: 20/.

Weighting: None
Coef. of Deteraination {r2l: 0.9974642
Internal Standard: None
Forced Through Origin: No
Equatioo: Conc•(lnj \loll = -9. 772779E+02 + 5.269503£-03 * R Sa!ele File Naae Valid Concentration Response Calc'd Concentratioo X Deviation !PFB CSliPPB y : • OOOO!))E +00 1.07124i1E+06 9.335261£-01 7.12£+00 lFH CS21PPB y 1. OOOOOOE +00 1.0933315£+06 9.568072£-01 4.51E+0•) 2f'PB CS42PF'B y 2. !)(li)i)(J'OE +00 2.2219372£+06 2.146240£+00 -6.81E+OO -~PPB CS73F'PB y 3.000000E+OO 3. 075797Cf.+06 3.046129E+OO -1.51£+00 4FPE ·:Sl04PPB y 4. OO({lfiOE +00 3.9253580£+06 3.941482£+00 1.48E+OO 5PPB CS13:f·PB y 5. OOi)OCK!E +00 4.9067870E+Ob 4. 975B10E+OO 4.86£-01 Response Factor

4.b674B3E-03
4S'.3178E-03

4.500577£-03

4.876785£-03

5.09507/E-03

5.094984£-03
ATTACHMENT 6 - 3297
4270
b:!
~
~"'J
:i
()
1:;::1
""'' ... ,: •' l-'
:X
M
;..., :_,.
~ •'''-
::1} ...... ::! I
<>
"'" ~j;
-.~
It
•i,J
~
:::.~
;'tf
Ill
~
!j
:I
Iii
l'l:i
0 0
Cone * In,J Vol
;_~ --j---·····--r:---..1..----····--:·--·"--·-·---L..---·--__ ,..L_. ___ ....__._ ___ .._ ___ , ______ --~..... _______ l _________ __J_, _____ .... _.-~..._ .... - ... -L_._ c~ ; ·-.. i ····.

I · ..
;
I
I
I
I
·· .•..
··.•. . ....
···...,~·-,
·•·· ...•..
···•·· ...•..
·· ..
'·· •.. '·.,
··· •..
·--~~--...
'·.
···• ..•
·.,
··,· .•...
·-... ·-.
',,~'-,,_ · ...
·· ... ·•. ····,· ...
·•·· ..
··--.... __ *-'
·· .•.•... _
... ·•· ...
'·· •..
'·., ·· ...
·•··•·· ....
· .. ·•·.
·· .. '· ...
··.

ATTACHMENT 6 - 3298
4271
BROMODiC1METHAN C~1ibr~ti~~ R~p~rt
Quant Basis: Area
Curve Type: L1near
Y-axis Label: Concentration
Carr. Caef. Crl: 0.9965433
Pt·inted~ 24-NOV-1990 1:27:32
Rejection Tolerance: 207.

Weighting: None
Coef. of Deter~~ination Cr2l: 0. 9930986
Internal Standard: None
Forced Through Origin: No
Equation: Concf(Inj Vall = 1.3.35310E+03 + 9.924069£-03 * R Sa!ple
1PPB
lP?B
2FPB
3f'PP
4PPB
5PPB
File Na~~e
CS11PPB
CS21PF'B
CS42PPB
CS73PPB
CS104PPB
CS135PPB
Valid Concentration
y 1.000000E+OO
y l.OOOOOOE+OO
'( 2.000000£+00
y 3.000000E+OO
y 4.0000COE+OO
v S.OOOOOOE+OO
Reseonse Calc'd Concentration 4 Deviation

2.7850309£+1)5 8.19838BE-01 2.2CE+01

3.92'13134£+05 1.04b958E+OO -4.49£+!)0

9.2136181E+05 2.095794E+OO -4.57E+ij0

1.4694789£+06 3.183704£+00 -5.77£+00

1.8656570E+06 3.970044E+OO 7.55E-01

2.3259612£+06 4. 883662E+01
) 2.38E+(l(l
Response Factor

1.79:3!2E-G2
!.272487E-02

1.085350E-02

1.020770E-02

1.072008E-02

1.074824E-02
ATTACHMENT 6 - 3299
4272
......
(,,'j0 '•.c' i .....
·-1 }-II
.;;:)
:oj .,., 0.
0 I
N
f.Ji
<:>
~j 0 j
~·~ I
+······ ... ········-•....
·-•... __
··--..
··· .. ,4h ... ,
---... _
N
0 0
···· ... '-....... .;t.:.-
·-... ---...
-.. -..

ATTACHMENT 6 - 3300
4273
CHLOROBENZENE C~1ibr~ti~~ R~p~rt
Quant Basis: Area
Curve Type: Lineat'
Y-axis Label: Concentratlon
Carr. Coef. (rl: 0.9885136
Printed: 22-NOV-1990 5:01:05
Rejection Tolerance: 15%
Weighting: None
Coef. of Deteraination <r2l: 0.9771591
Intemal Standard: None
Forced Through Origin: No
Equation: Concf(lnj Vall = -1.2b4631E+03 + 9.181994£-03 * R Sa!!lflle File Naae ..Y.!li.L Concentration Response Calc'd Concentration I Deviation lPPB CSilPHi y 1.000000£+00 6.4728431£+05 9.357460E-Ol b.87E+O!) lPF'£; CS21F'PB y l.OOOOOOE+OO 7.5403569£+05 1.131784E+OO -1.16£+01 2PPB C542PPB y 2.000000£+00 1.2721947£+06 2.083331£+00 -4.00£+00 3PPB CS73PPB y 3. 000000£+00 1.8411076£+06 3.128082£+00 -4.09£+00 4PPB CS104PPB y 4.000000E+OO 2.0590261£+06 3.528267£+00 1. 34£+01 5F'PB CS135PPB y 5.000000E+OO 2.9654320£+06 5.192790£+00 -3.71£+00 Response Factgr

7.724581£-03

6.630986£-03

7.860432E-03

8.14727oc-o:.

9.71333(1£-03

8.430475£-03
ATTACHMENT 6 - 3301
4274
~:r~i
~~"'
·~=~· :r.
r,;)
,,,~;
:j:
"'"'
:i X
lttt~~ ::tub ,,.) r,:;:. ;~.;
l~li ~~I
:::r,:l
•'!:!
I.!'!
llj~
;~~
ml
l.l't
iT.l
5 ... l ......... ---···'··· ............. --.. t .... ,_ •••••• - .... t .......... ,_ .............. L.. .... __ , __ , ...... - •. ·--·-··"-·---.............. J .•. _. __ ,, ___ .L,_, ................... t .......................... ..l.. ........... .. ........ 1 ........................ i.. .... .. f.,,
1 ·· .. I
I ··· ..•.
-· '•,_
(;;• ·., ,. I ·-._
l:'..:t """i ··· ... .:::~ I '·· ... .. , ·· .. 4:-:
.J ~
l ·· ...... •:';! -, . i
'~ ""i t!m~ I m• -~
1 l
f.:) -·i
. I
1!;1'1 -"i ......
.... _.. !
·--.
·· ... · .. __ _
·-....
~ ..
·· ...
·-... _
·-... ··--..
.,.~:········ ...
· .. _
'·. ·-.. ,_
·-.,
···--.
·-... __
-. __
··-,
··-.
·-... · .. __
..:F··. ··-.. ,
·-, __
f41
ATTACHMENT 6 - 3302
4275
BROMOFORM C~1ibr~ti~~
Quant Basis: Area
Curve Type: L::near
Y-axis Label: Cur.centt'ati;Jn
Corr·. Coef. (rl: <),9139354
~nnted: 22-NOV-119(1 4:29:22
Rejection Tolerance: 157.

Weighting: Nooe
Coef. of Deter1ination (r2l: 0. 987913o
Equation: Conc*\InJ voll = -2.002325£+03 + 2.t.2130t£-01 * R Internal Standard: Non2
Fot'Ced Through Origin: No
Sample tile Na8le Valid Concentration Response Calc'd Concentration X Deviation :Pf'B CS11PPB y 1. 000000£+00 2.6865785E+04 1. 008004E +00 -7.94E-01 lPFB CS21PPB y l.OO(IOOOE+OO 2.6633553E+04 9.958289E-01 4.19£-01 2PPt CS42PPB y 2.000000E+OO 4.6880562£+04 2.057301E+OO -2.79E+OO 3PFB CS73PPB y 3.000000E+OO 6.7B82570Et04 3.158355£+00 -5.01£+00 ;J·r·B CSW4PPB y 4.ooooooE+w 7.7397930£+04 3.657208£+00 9.37E+OO 5PPE CS135PPB y 5.000000£+00 l.053629iE+05 5.123.304£+0() -2.41E+OO Reseonse Factor

1. 861103£-01

1. B77331E -jl

2.133080£-01

2. 209698£-01

2.594048£-01

2.372751£-01
ATTACHMENT 6 - 3303
4276
!-"
1-•
'u
~'t!~
,,
c· . .;.
.......
,, ,. ;-.;
~
jl~l
:x: ;;,..;t
't<:!-~ 1-t•
~·· .. ~. .......
""~ t:f•;
;,:;
:d.J
~
;::1',:1
"tl
I.( I
·~ ·~ :1
!.il
!j~
..... , .,,,
0 :~·{ Jl ot',) 4.
:...._ ---..f:;-------····-···--1-------..l.-------·--'--···--·-----J·-··--·---------- ...---···-··---'-·-···-----L--------___j··-·········--·------L---········· .. ~······--··:····-·····················-i·-···············-··-······-L····-----· ;,:; r ··. ···· .. .I
!
I
c~ I ~ ..... ,
t.:> I
·-.,
--...
·· ... *
· .. _
··-._ · ..
·· ...
.;;.f~''·· .. ,_ ·-... ·-.. __
·-•..
'· ... +
. ··-. '·-..
·-. __
·· •.. _
--~
·- .. ____ 4:.-
·-... ·, __ _
·-..• ·,
· ..
·-..• _
'·

4.~ ·-.. __
'·· ...
'·-.
·-..
·-... _
ATTACHMENT 6 - 3304
4277
Quant Basis: Area
Curve Type: Linear
V-axis Label: Ccncentr'at1on
Corr. Coef. ( r l: C. 9984637
Printed: 23-NOV-19% 0:34:30
Rejection Tolerance: 20/.

Weighting: None
Coef. of Deter•ination (r2l: 0.9969299
Internal Standard: None
Forced Through Origin: No
Equation: ConclHinJ Voii = -8.117287£+!)1 + 9.397962E-0.3 * R Sal!!ple File Halle Valid Calcentration Reseonse Calc'd Concentration X Deviation lPFB CSilPF'B y i.000000£+00 5.4745962£+05 1.012766£+00 -1.26£-tOO lf'Fb CS2lFH y· 1. OOOOOOE+OO 5.1709075£+05 9.556653£-0i 4.64E+OO ~F"F'B CS42F'B r 2. ;)OOOOOE +00 1.1249587£+06 2.098229£+00 -4.bBE+(i0 3PP':: CS73PPB y 3.000000E+OO 1.6116124E+Ob 3.012940E+OO -4.29E-01 4PPB CS104f"PB y 4. OC•OOOOE+OO 2.0551245£+06 3.8465b2E+OO 3.99E+OO SFH CS135PPB y 5.0000COE+OO 2.7080617£+06 5.073B18E+OO -1.45£-rOO Response Factor

9.133094£-03

9.bb9483E-03
a. BS9215E-'i3

9.3074<+1E-03

9. i31771£-ij3

9.231695£-03
ATTACHMENT 6 - 3305
4278
.. -
....

X
0 0
oo
0 0
C~Jonc * I n.,j Vol
·11.. o· .::~. :>< .. -
0 0
0 0
g -=t·--··---.1----------'--···-----'--·-·-·-·-··--'·-····-··---'--··----'--··-·····-··-'-----J ... _______ , _________ .._ ___________ ..J •.. -·-···-...... ··-'--···-······ ~.:- f·· ·· .. ''"'l ·············· ... 0 ... , ·· ..
; .. J- -.. 'If!.'·-- ...... ··-.. _
·-... _
~ I ' "'...- -t ·· ... _
. ~ ' ~ -·~ ·· ....
4:~·· ..
0 0!:1
0 '·· . ...
·····•·····•·· •...
---.. ,_
·-..• ·-.. ,
·-•...
..:t~ .. ··----. _____ _
·-.. __
·-.. ·-..
·, ___ _
'·· .. _
'·· ..• _
·-.,_
·-... ·., __ _
·· •.. _
'···--...
·.,_
--...
..::!) ..
-..• _
·--...
· .. _
ATTACHMENT 6 - 3306
4279
Quant Basis: ikea
Curve Type: Linear
Y-axis Label: Concentt·ahon
Corr. Coef. (r): 0.9924318
Printed: 22-NOV-1990 5:16:33
Rejection Tolerance: 15'
Weighting: None
Coef. of Detereination (r-2): 0. 9849209
Internal Standard: None
Forced Through Origin: No
Equatim: Conctilnj Voll = -1.015590£+03 + 1.729029E-02 * R Swle File Hille Valid Concentration Resppnse ealc'd Cgncentratign :< Deviation lP~B CSllFPB y l.OOOOOOE+OO 3.4393647£+05 9.862346£-01 1.40£+00 !PPB CS21PPB '( l.OOOOOOE+OO 3.3223116E+05 9.457570£-01 5.74E+OO 2PPB CS42PPB y 2.000000£+00 6.7258012£+05 2.122704£+00 -5.78E+OO :PPB CS73PPB y 3.000000E+OO 9.9264125£+05 3.229494£+00 -7.11£+0•) 4PPB CS104PPB y 4.000000£+00 1.1130034E+Ob 3.645990£+00 9.71£+00 5PPB CSi35F'PB y 5. (l!)t)000£+00 1.5248265£+06 5.069822£+00 -1.38£+00 boose Factor

1.45375/E-02

1.50497bE-02

1.4!3081:E-02

1.511120£-02

1. 790B11E-02

1. 639531E-02
ATTACHMENT 6 - 3307
4280
,,
~
!'Y.l
Lr!
l'f.)
~ ....
'"' l,!'l
t'l',l
X
0 0
Cone .:w.- InJ Vol
0 0
(,..)
, . ....,.
0 0 ··t··-........t.·------·...___ _,__ ______ _, _____ .___ ____ _. __________ .. ____ J.--.. -·---... -'--··------J-.-···-··---··-'-·-··--·-·----; ................. ___ J_ .......... . f.:> ! .
-1
r·· .. -I ·· .... ·· ..

I ····· ....
-1 ·· ..... . '""" I ··· ... I ··· ... ~ --; +. 0 l ···· ... I ·· . . , '·· ... 1 I
N 1
. i
f.~> ·-i .;~ I
~ l
1 ~
~ __ J
·o I
-1
I
-i
!
I
itk "l • I
t.::. ·-···1
·O I
··~ '
I
.J
I
I
i
··.
··· ... ·· ..• ··-..
+····· ..·•·· ... ·· .•.. ·· ..
···· ...•
······ .. ,
···· ... +
'······· ...
·· ... \
···• ... ·· •.. : ..... _
·•· ...
·····-.:~i:t-
·· .•.. · ...
·· .. '·.
·· ..
·· .•.
.: ... "'=t""· .. ·· .. ATTACHMENT 6 - 3308
4281
1,4-DiC1BENZENE C~1ib~~ti~~
Quant Basis: Area
Curve Type: Llneaf
Y-axis Label: Concentrat1on
Carr. Coef. <rl: 0.9986501
Printed: 23-NDV-1990 0:34:57
Rejectioo Tolerance: 207.

Weighting: None
Coef. of Deter.ination (r2 l: •}.9973020
Equation: Co1c+<!:1j Voli = -2.219404E+03 + 6.169317£-03 * R Intemal Standard: None
Forced Through Origin: No
Sa!ele File Name Valid Concentration Reseonse Calc'd Concentratioo X Deviation iF"f'B CSllPPf y ~.OOOOOOE+OO 1.0338945£+06 9.972270£-0i 2.78£-01 12PB CS21PPB v 1.000000£+00 1. 0211959£+06 9.795269£-Ql 2.09E+t)(i 2f'FB CS42PPB y :2.000000£+00 1.8306375£+06 2.107778£+00 -5.11£+00 ~.PPB C573f'PB y 3.00000(1£+00 2.4476115£+06 2.967755E+OO L09E+OO 4F~'F CS104PPB y 4.000000E+OO 3.0949910£+06 3. 670 i14E +00 3.36£+00 5PPE CS135PPB y 5.000000E+OO 3.9612770£+06 5.077599£+00 -1. 53E+Xi RespgnS@ Factor

4.836083£-03

4.896220£-;)3

5.462578£-(;3

6.128424£-03

6.4b2054E-C3

6.311096E-03
ATTACHMENT 6 - 3309
4282
Jud•
0 0 0
0 0
:::::. ·-·t--·-·-·-··--.... ·--·-·-·· ..···-..L-.. - .. ·-···-·--·-·-----.l·-·-·---····.....L--··------1--- ....-. ..J.---.. -._.l.. ... _, _________ i. ________ J ___ , .......... - ...... J ••• _____ ,,,,,_J_ ______ _ ..-. I
.... ~ I
!
1·· .. , -·1 . ·· ... i
I ~ --,
I
~~ ·-··1 ···•' I
() !
!
-·1
... !
I
~ ~\) I
0 -~ 6 '
1 ·-l
i
~) l
0 ·--i
() I
l
-·1
~
~:-~
¢ 1
~
j
··· ...
'·· ...
··· ...
····.*··· ...·· ..
'··· ... ·· ...
··· ...
··· ... ··· .. ,
······•· ...•
····•···• ...
'··. .. ·· ..
·••••.. ...J:: ··•... ·r.~7
··· •.. · .. · ..
·•·· ... ·· .. ,_
···· ...
· ...
·· .. ·· ..
···, ·· ... ·.,
······•· ...
·•. ·· •..
·· .. '· ...

ATTACHMENT 6 - 3310
4283
1,2-DiC1BENZENE C~1ibr~ti~~ R~p~rt
Quant Basis: Area
Curve Type: Linear
Y-axis Label: Concentt'ation
Carr. Coef. <rl: 0.9943514
Printed: 22-NOV-1990 5:17:15
Rejection Tolerance: 15~
Weighting: None
Coef. of Deteraination {r-2): 0. 9887348
Intemal Standard: None
Forced Through Origin: No
Equation: Cone* <Inj Vol l = -2. 818205£+03 + 7 .1585B2E-Q3 * R Swle File Halle Valid Concentration Response ealc'd Concentration % Deviation 1PPB CSllPPB y 1. OOOOOOE+OO 1.0696696£+06 9.678224£-01 3.32E+(l(J 1PPB CS21PPB y 1. OOOOOOE +00 1.1089495£+06 1. (i24060E+OO -2.35£+00 2PPB CS42PPB y 2. OOOOOOE +00 1.7985671£+06 2.011397£+00 -5.67E-01 3PFB CS73PPB y 3.000000E+OO 2.6468250E+06 3.225862E+OO -7.00£+00 4PPB CS104PPB y 4. OO;jOOOE +00 2.9757300£+06 3.696760£+00 8.20£+00 5PPB CS135PPB y 5. OOt)QOOE +00 3.9377497£+06 5.074100£+00 -1.46£+00 Response Factor

4.674340£-1).3

4.50877:'E-Q3

5.559982£-03

5.667167E-Q3

6.721040E-03

6.34B804E-03
ATTACHMENT 6 - 3311
4284
MAXIMA 820 METHOD REPORT
Printed: 22-NOV-1990 07:49

HALOG&AROMATIC VOLATILE ORGANIC
~--------------:
: Sample Queue :
:--------------:

Queue Parameter's
F1le Path: D:\MAX\8010-200
Starting Index: 1
Raw Sample Weight: :l..UOO
Volume of Extract: 1.000
Stripchart Parameters
Scaling: F~t to highest valid peak x-Axis limits: 0.0-6144 Peak Labels: Retent1on ~1mes y-Axis limits: 0.0-1.000
Regions: 1
Options: basel. ine·o.;;, s:;tat-·ts/ends, ma:-;ima
Sample Queue Table
# Name :ry~e:Source: File Na~e :IndexllnJ.Volume Amount I I Dilution
REAGENT BLANr=: lUNKNi ARCH I
I RB112090 5.000£+03 '") lPPB lSTND: DISK I CSllPPB I
.. I I 5.000£+03
3 1PPB :srND: DISK : CS21PF'B 5.000E+03 I '
4 2PPB :STND: DBK CS42PPB 5.000£+03 I
I
5 :)pf'ij lSTNJl DIS!< C573PPB 5.000£+03 j
I
6 4Pf'B !STND: DISK CS104PPB 5.000E+O~, I
I
7 I SPPB , SHill: DISK I CS135PPB ; ' 5.01)0£+03 ' I I I ' I & BOR-05000i lUNKNi ARCH I EMA14902 2 I
I I I 5.000£+03
9 I BOfH50005 lUNKN: ARCH I EI'IA14903 .,. I I ..:· i 5.000£+03 10 j BOR-050010 lUNK.I>4: ARCH I EMA14904 I 4 I
I I I I 5.000E+03
11 I BOR-020C{l i il.iNKN: ARCH I EMAi4905 ' 5 I 5.1YJOET03 I

I I I I I
12 I BOR-020005 :UNKN; ARCH i El1A1490b i b ' 5.000£+03 I I I i I
13 I BOR-020010 :UNKN: Afi'CH I I I El1A14907 7 5,•)00E+03 14 BOR-040001 :uNt:J~: ARCH EMA14908 8 5.0WE+03
15 BOR-040005 :tJNKN: ARCH EMA14909 9 5.000£+03
16 BOR-040010 :UNKN: ARCH EMA14910 10 5.000£+03
17 BOR-03t)00 1 :UNrJ~: ARCH EHA14911 11 5.Ci()0E+03
18 ' BDR-030001 DUP :UN¥-N: AACH I EM14911D 12 I
I I I 5.0(10£+03 f5~
ATTACHMENT 6 - 3312
4285
19 SPIKE : UNKN: ARCH : SP1120'10 I
I 13 : 5.000£+03
20 SPIKE : UNKN: ARCH : SP11209A : 14 : 5.000£+03
: 21 BOR-030005 :IJNKN: ARCH : EI'!A14912 15 : 5.000£+03 : 22 : BOR-030010 : UNKN: ARCH : Et'IA14913 16 : 5.000£+03 :
: 23 : BOR-o60001 :IJ-41<'-N: ARCH : EI1A14914 17 : 5.000E+03 :
: 24 : BOR-Q60005 : l!NKf'l: ARCH : EHA14915 18 : 5.000£+03 :
25 : BOR-060010 :UNKN: ARCH : EI1A14916 : 19 : 5.000£+03 :
26 : BOR-010001 :lJNKN: ARCH : El'IA14917 : 20 : 5.000£+03 :
27 : BOR-Q1 0005 :UNKN: ARCH EI'IA14918 : 21 : 5.000E+03 :
2B I BOR-010010 : UNKN: ARCH EI1Al4919 .,.~ I L..4 : 2.000£+03 ':!Q
.... : REAGENT BLANK : !.f~KN: ARCH RB11209A ,.,.,
i..,J : 5.000E+03
30 : CAL CK. 4PPB lUNKN: DISK CCS11219 : : 5.000£+03
31 : LAB CONT. 4PPB :UNKN: DISK LC511219 : : 5.000E+03 :

Standard Concentrations
CO!IIflonent 1PPB 1PP3 2PPB 3PPB 4PPB 5PPB
DiC IDiFHEiHANE I
I t.OOOE+OO 1.000£+00 2.000£+00 3.000£+00 4 • OOOE +i)l) 5.000£+00 I I CHLOROI'ETHAt£ 1.000£+00 l.OOOE+OO 2.000E+OO 3.000E+OO 4.000£+00 S.OOOE+JO I I VINYL CHLRD 1.000E+OO i.OOOE+OO 2.000E+OO .3.000£--00 4.000£+00 S.OOC:E+OO I I BROMOI'IETHANE 1.000£+00 1.000£+00 2.000£+00 3.000E+OO 4.000£-H)O 5.000E+OO CHUJROETHANE 1.000£+00 1.000£+00 2.000E+OO 3.000E+OO 4.000£+00 5.000E+OO 1,1-DiClETHYLEN: 1.000E+OO 1.000£+00 2.000E+OO 3.000E+OO 4.000E+OO 5.00('£+00 METHYLENE CHLRD: 1.000£+0') l.OOOE+OO 2.000E+OO 3.000E+OO 4.000E+OO 5.000£+00 tns-1,2-DiClENE: l.OOOE+OO l.OOOE+OO 2.000£+(10 3.000£+00 4.000£+00 5.0iXiE+OO 1,1-DiClETHANE I I 1.000E+OO 1.000£+00 2.000E+OO 3. (11)0£+1)0 4.000E+OO S.OOOE+OO I I P10D1 1.000E+OO l.OOOE+OO 2.000£+00 3.0i)(}E+OO 4. OOCJE+i)l) S.OOOE+OQ CHLOROF!Jfi'l'l 1.000E+OO l.OOOE+OO 2.000£+00 3.000E+OO 4.000E+OO 5.000E+OO 1,1,1-TriClETHAl l.OOOE+OO 1.000E+OO 2.000E+OO 3.000£+00 4.000E+OO S.OOOE+OO CARBN TETRACHLR: 1.000E+OO l.OOOE+OO 2.000E+OO 3.000E+OO 4.000E+OO 5.;)00E+OO 1,2-DiClETHANE I I l.OOOE+OO 1.000E+OO 2. 00(1£+00 3,00i)E+OO 4.000E+OC• 5.000E+00 TCE 1.000£+00 1.tX10E+OO 2.000£+00 ),(11)1)£+(10 4. (I(II)E+OO 5.000E+(H) 1,2-DiClPROPANE: l.OOOE+OO 1.000£+00 2.000£+(1(1 3,(1(10£+00 4.000£+00 5.0(11)£+00 BrDiClMETHANE : 1.000£+00 1.000£+00 2.000E+OO 3.000£+00 4.000E+CO 5. ·:)OOE+OO I I cis-1,3-DiClPENl 1.000£+0(; l.OOOE+OO 2.000£+00 3.00C'E+OO 4. OOC'f+OO 5.000E+OO tns-1,3-DiClPENl l.OOOE+OO 1.000£+00 2 .00(1£ +00 3.000£+00 4. OOOE +OC• 5.0GOE+Oi:· 1,1,2-Tt'iClETHAl l.OOOE+OO l.OOtl£+00 2.000E+OO 3.000£+00 4.000E+OO 5.000E+OO PCE l.OOOE+OO l.OOOE+OO 2.000E+OO 3.000E+(X= 4.001)£+00 5.000£+01) I I DiBrCUlETHANE l.OOOE+OO l.i)I)0£+00 2.000E+OO 3.000E+OO 4.000E+OO 5.0COE+,)0 I I CHLOROBENZENE 1. ()(If)£ +00 l.OOOE+OCI 2,(H)0E+OO 3.00')£+00 4.UOOE+OO 5. OO•)E +00 : BROMOFOJ;:M 1.000£+00 l.OIX•E+OO 2.000E+OO :).0(10£+00 4.•)00£+00 5.000E+OO l,l,Z,2-Cl4ETHA: 1.000E+OO 1.00(1£+00 2. i)f)0£+00 3.000£+00 4.000E+OO 5.000E+OO ATTACHMENT 6 - 3313
4286
; 1,4-DlClBENZENE: l.OOCE+OO l.OOOE+OO 2.000E+OO 3.000E+OO 4.000E+OO 5.000E+OO 1,2-DlClBENZENE: l.OOOE+OO l.OOOE+OO 2.000E+OO 3.000E+OO <i.OOOE+OO S.OOOE+OO ATTACHMENT 6 - 3314
4287
, .....
0 .....
(::'t
.
0 C;J (_;::.

Suple: REAGENT BLANK Olannel: 6C#l ELCD Ch#1
Acquired: 20-NOV-90 7:0o Jllethod: D: \l'1AX\B010-20D\801 0-2011 Inj Vol: 5000.00
0 0 0:::) .

C\,'1 .::. 0'•
0 0 0
e ..
'XI
·~~
Filena~~e: RB112090
~erator: cv.:
'"'"'
0 0
ATTACHMENT 6 - 3315
4288
MAX~MA ic,1990 Dynamic Solut1ons, Division of M1llipore MAXIMA 820 CONCENTRATION REPORT
Pl'inted: 22-NOV-1990 7:55:29
SAtRE: REAGENT BLANK
11 in Metnod: HAL06&AHOMATIC VOLATILE ORGANIC
Acquired: 2o-NUV-1990 7:06
Rate: 5. 1) points/sec
Dur'ation: 30.000 minutes
Opet'atot': CYC
DETECTOR: GC#l ELCD Ch#l
Pl(i IDi Retention Ti• Type Peak Height Peak Area
!minutesl !microvolt l !microvolt-sec)
--------- --------- ------- ---------- -------------- TOTAL 0 0 Area Percent
----------
Type: UNKN
InstrWiient: 6CI1 PlJR6E&IRAf-'
Filename: RB-112090
Inde::: 1
Injection Volume: 5000.0
Code Base Solution Cone Colponent Hue
--------- ---------- ------------ 0
ATTACHMENT 6 - 3316
4289
....
t.;:> ......
0 ··~
~· I ~-1 0
Salple: 1PF'B Channel: GCil ELCD Ch#l
Acquired: 2HIDV-90 7:33 l'ethod: D: \I'!AX'\8010-20D\B010-20M Inj Vol: 5000.00
::1-{ .1. 0 -··- ·
1- 'V 0 1 t: :5
0 Filenue: CS11PPB
Operator: eve
ATTACHMENT 6 - 3317
4290
t'lAXlMA (cl1990 Dynamic Solut1ons 1 Division of Millipore MAXIMA 820 CONCENTRATION REPORT
Printed: 22-NOV-1990 7:57:.:.5
SAtRE: 1PPB Type: STND
12 in Method: HALOG&ARCI'1ATIC VOLATILE ORGANIC Instt'Uftlent: GCI1 PURGE& TRAP Acquired: 21-NOV-1990 7:33 Filena11e: CS11PPB
Rate: 5.0 points/sec Index: Disk
Dut'ation: 30.000 minutes InJection Volu.e: 5000.0
Operator: CYC
DETECTCR: GC#l ELCD Chtl
PKI IDI Retention Tile Type Peak Height Peak Area Area Percent Code Base Solution Cone Colponent Hue <•inutesl <•icrovol tl <•icrovolt-secl
-------- ------ ----- ---- ------- ------------- 3.170 BP 147.10428 2335.1673 0.01 EXT AREA 1.0000000 DiClDiFMETHANE 2 ..,
.. 3.473 pp 1909.4946 24871.163 0.12 EXT AREA 1.0000000 CHLOROt1ETHANE "T ·.) 3 4.093 pp 15155.794 537690.73 2.61 EXT AREA 1.0000000 VINYL CHLRD 4 4 4.920 PP 21196.368 731580.95 3.56 EXT AREA 1.0000000 BROMOMETHAI£ " 5 5.950 pp 3104.4487 255457.59 1.24 EXT AREA 1.0000000 CHLOROETriANE ,J 6 6 t..777 pp 59076.435 1512408.7 7 -:rc;; .. ...;..., EXT AREA 1. i)OOI)(J(i(i 1,~-DiCIETHYLEN ? i 8.163 pp 43547.755 1476335.2 7.18 EXT AREA 1.0000000 METHYLEr£ CHLRD 8 8 8.937 PF' 74092.874 166'1764.0 8.12 EXT AREA 1.0000000 tns-1,2-DiClENE 9 9 10. !)67 PB 24497.b31 688813.14 3.35 EXT Afi'EA 1.001)0000 11 1-DiCIETHANE 10 10 11.363 BB 2162.0991 31277.304 0.15 EXT AREA 1.0000000 P10D1 ll 11 11393 BP 19616.368 215302.93 i.OS EXT AREA i • (1000t)i)(l CHLORCfORM 12 12 12.323 PP 69472.202 '698867.01 3.40 EXT AREA 1.0000000 1,1,1-TriClETHA 13 13 12.710 pp 10255.815 264010.95 1.28 EXT AREA 1.0000000 CARBN TETRACHLR 14 14 13.013 f'P 93034.755 1342727.7 6.53 EXT AREA 1.0000000 112-DiClETHANE 15 15 1-+.143 pp 158567.69 1427657.1 6.94 EXT AREA 1.0000000 TCE lb 16 14.480 PP 119510.07 1459915.2 7.10 EXT AREA 1.0000000 1,2-DlCIPROPANE 17 17 14.960 pp 26233.915 535455.13 2.60 EXT AREA 1.0000000 BrDiCiMETHANE 18 18 15.673 pp 39273.624 572380.35 2.78 EXT AREA 1.0000000 cis-1,3-DiClPEN 19 19 1t..530 r·P 17184.617 157820.53 0.77 EXT AREA 1.0000000 tns-1,3-DiClPEN 20 20 16.780 pp 124123.47 999141.86 4.86 EXT AREA 1.0000000 1,1,2-TriClETHA 21 21 17.050 PP 161127.94 1541081.6 7.49 EXT AREA 1.0000000 PCE ·";li . .,..., ..... ... .. 17.387 pp 29252.533 570147.23 2.77 EXT AREA 1.0000000 DiBrClMETHANE 23 1")1'

1..-..J 18.327 PB 53616.888 647284.28 3.15 EXT AREA 1.0000000 CHLOROBENZENE :-24 24 19.460 BB 391.36414 4205.0607 0.02 EXT AREA 1.0000000 BR0110FORM 25 25 20.190 BB 42776.590 547459.65 2.66 EXT AREA 1.0000000 1,1,2,2-cl4ETHA 26 26 21.6.37 BP 72589.833 343936.45 1.67 EXT AREA 1. 0(l(JOO(li) 1,3-DiClBENZENE '"1"7 ·"1"7 21.753 PF' 106799.26 1240520.7 6.03 EXT AREA 1.0000000 1,4-DiClBENZENE J../ ~~ 28 28 22.313 PB 88530.670 1069669.6 5.20 EXT AREA 1.0000000 1,2-DiClBENZENE ---------- ------------- ------------ TOTAL 1477247.7 20568117 28.000000 ATTACHMENT 6 - 3318
4291
;'I)
l/1
Salple: 1PPB Channel: 6C!U ELCD Chlt1
Acquired: 21-NOV-90 8:15 ltethod: D: \HAX\801Q-20D\8(J1Q-20t1 Inj Vol: 5000.00
~ 0 ~ 0 0 0 0
Filenue: CS21PF'B
Operator: CYC
(,.::. ··-r-··r...__ ______ .. __ _j __ ,_,_, ...... ,_._ .. _ .... L.---··-·-·-.. -.l---·-............ ..1.-... - ............... _ ................ .l. ... _ .. ,, ............................. l .......... _, __ .... , 0 I I
I
.1 I !-~· 3.19 DiClDiFMETHANE
1 ·-:r...r-_ 3. 57 CHLORDI'IETHANE
<::) ~-~"':.' -· 4.09 VINYL CHLRD .~ ! ·: ... ~
1',.11 ·-i :: ~- -- 4. 93 BROMOMETHANE o I ..... --.)h.'lj!!:
':, . ,.-::':. 5. 99 CHLOROETHANE
I ··*~"------.... _______ b.81 11 1-DiClETHYLEN I ~ ,........-----· .. ·-·---........ ·1 ~:~~-· --·---::::;::::r· ..... 8. 18 METHYLENE CHLRD :.... I 'j-- ............ -~~:=~~ .. :::_:::::::::::::::::;:;;:::::::::::::::::'"""::::::c-~- ·- 8. 96 tns-1, 2-D iClENE 0 ·-~ l·--ll-~~;~"""""' .... 10.09 1,1-DiClETHANE . C• i ·, ..............

I ~ ..... 11.40 ?1001
•.,j"
I '4-':::.jj:=tiC.:::= .... . ... __ 12.34 1 1 1-TriClETHA "i ! .......... :.:.;.;rM-··--·--· ...... "''!: 74 CARll TETRACHLR ' ' I j·-::::::::::==.:::::::::=---.. ·-:::::=--=:=-·----- 13.03 1,2-DiClETHANE ....,. -:-~t~ .. - ............. -.. ·--.... - -.. .- .. - _____ .. ____ .... 14 16 TCE • 1 : .......................... ~ 1 --·· - - -- · - - 14 50 1 .., DiClPROPA~•E • --1 : .............. -~- ......... ' • .. ,..::- . ~.JI . ! i .....-···•"" . 0 1-~~:;:::::::.::;:::::.==--- ..... 15.69 cis-1,3-DiClPEN ~~~~ifl~~-~:;-~;;;;;:;. ~-:;:;·;==z:::::.:::-=·.:;....L!.!:f:..t.:.·7!.:z9~1!J.•.!.J1,t£;_2-I!:lflEJHr .06 PCE -"~>....._ ... _ .. - - 18.34 CHLOROBENZENE ,; ..,..,., ...... .--- '1( 19. 80 BROI'IJFORH ·-to-ilot-·--·--:,···---·- ~rr.:, .. -·- ..... 2C1 "0 1 1 7 2-C14ETHA ..... --... __ .. ..... ' ,., . i
! -!11~: : •. ~···· .. ~·····~"·-·rr······""~""~' ·-.. -·-·---··-~=-•OOH ........ ........._ _______ ____ , ... __ ··· i. -~1 • 76 1 4-D 1 ClBENZEN~ t. ; ..... ~ .,.--:.:::::::-~ _ .:. . --22.32 1,2-DiClBENiENE . I ,ll: ___ _ ~~ --1 {
0 J I
I I
ATTACHMENT 6 - 3319
4292
f'(AX II'IA \cl1990 Dynam1c Solutions, Div1sion of M!llipore MAX IMA 8:20 CONCENTRATION REPORT
Pt'lnted: 22-NOV-1990 8:05:20
SAtRE: lPPB Type: STND
#:. ln Method: HALOG&AROMATIC VOLATILE OR~~IC Instrument: GCil PUR6E&TRAP Acquired: 21-NOV-1990 8:15 F i l enill'.e: CS21PPB
r Rate: 5.0 points/sec Index: Disk
ilur·at ion: 30.000 minutes Injection Volume: 5000.0
Operator·: eve
DETECTt:R: GCIH ELCD Ch#l
PKI IDI Retention TiE Type Peak Height Peak Area Area Percent Code Base Solution Cone C01ponent Halle <•inutes) laicrovoltl (aicrovolt-sec)
--------- ------ ---- ----- ------- ---------- .~ .• 193 BB 14.185907 250.75678 0.00 EXT AREA 1.(1000000 D1ClDiF!1£THANE 2 ., 3.573 BP 1192.5b99 21310.107 0.10 EXT AREA 1.0000000 CHLOROMETHANE i. 3 3 4.093 PP 14403.226 515259.59 2.50 EXT AREA 1.0000(100 VINYL CHLRD 4 4 4.933 pp 20967.844 716084.70 3.47 EXT AREA 1.0000000 BROI10i1ETHANE 5 " 5.990 PB 3008.3o60 251950.89 1 ?" EXT AREA 1.0000000 CHl.OROETHAt£ .J ·~.l. 6 6 6.807 BP 43909.317 1223087.8 5.93 EXT AREA 1.0000000 11 1-DiClETHYLEN 7 7 8.18.3 PP 42351.013 1408935.2 6.83 EXT AREA 1.0000000 METHYLENE CHLRD 8 ,. .. , 8.957 pp 73541.292 1709517.6 8.29 EXT AREA 1.0000000 tns-1,2-DiClENE 0 ~ 9 10.090 PP 25056.604 786549.37 3.81 EXT AREA 1.0000000 1,1-DiClETHANE 10 10 11.400 PB 3495.9320 57095.144 0.28 EXT AREA 1.0000000 PlOD1 :1 11 12.010 BP 16788.008 187166.20 0.91 En AREA 1.0000000 CHLOROFORM 12 12 12.340 PF 66607.364 710710.31 3.45 EXT AREA 1.0000000 1,1,1-TriCIETHA F 13 12.743 Pf' 10110.141 239741.75 1.16 EXT AREA 1.0000000 CA~:BN TETF:ACHLR 14 14 13.027 PP 91582.309 1363940.8 6.61 EXT AREA 1.0000000 1,2-DiClETHANE 15 15 14.157 PP 155429.98 1406429.9 6.82 EXT AfiEA 1.0000000 TCE 16 16 14.497 pp 11820.3.18 1478457.9 7.17 EXT AREA 1.0000000 1,2-DiClPROPANE 17 17 14.977 FP 26650.551 564803.36 2.74 EXT AREA 1.0000000 BrDiClMETHANE 113 18 15.687 FP 38504.724 618492.23 3.1Xl EXT AREA 1. OO(li)(i00 cis-1,3-DiClPHt 19 1~ 1a.557 FP 17804.267 173883.27 0.84 EXT AREA 1.0000000 tns-1,3-DiClPEN 2J 20 16.790 pp 122836.b0 999744.97 4.85 EXT AREA 1.00000UO 1,1,2-TriClETHA 21 21 17.0o3 pp 159170.41 1569280.7 7.61 EXT AREA i . ()()1)0000 PCE ·""':';• ... , i7.80C~ pp 8982.5402 659557.74 3.20 EXT AREA 1.0000000 DilkClMETHANE ,;....;. 23 ·"':a't 16.340 pp 53065.426 754035.70 3.66 E"' AREA 1.0000000 CHLOROBENZENE ._._. !\; 24 24 19.800 PB 3b8.83359 17811.182 0.09 EXT AREA 1.0000000 BROI''!OFORM 25 25 20.203 BB 41592.007 517090.74 2.~i1 EXT AREA 1.0000000 11 112,2-Gl4ETHA 2o ?~ ~u 21.650 BP 69491.991 332231.15 1.61 EXT AREA 1.0000000 1,3-DiClBENZEN£ 27 27 21.763 pp 103831.66 1228802.8 5.96 En AREA 1.0000000 1,4-DiCIBENZENE 28 28 . .., ... 7.,'7'
u PB 85838.567 1108949.5 5.38 EXT AREA l.OOOOOOtj 1,2-DiClBENZENE . .JL,) ----------- -------------- ------------ TOTAL 1414798.9 20621177 28.000000 ATTACHMENT 6 - 3320
4293
~ ....

Salple: 2PPB Channel: OCI1 ELCD Ch#l Filen.ue: CS42PPB
Acquired: 21-NOV-90 8:57 l'lethod: D: \I'IAX\B010-20D\B010-20H Operator: eve lnj Vol: 5000.00
}-( 1. 0-- .1. volt:S
0 I- 1-" 1:\.~ N w
;:.1'1 0 ::J1 0 1'JI 0 C! 0 r.*•· .,.. 0 0 0 <:> g ··-··r·····-, ...... ·--·············---l ......... ···-····--··'--···-············.1··-·-··-····-···················--·-·-··-L············-···-····-·-··-···-·-····J ____ ........................................ !. .........................•.•.................. _ .. !.. ... . -~~ j- 3.17 DiCIDiFlE11/ANE
•-::r -~~ -flj_.,... __

3.59 . __ ::.

CHL~THANE - 4. 09 VINYL CHLRD
• I!·····~ I'JI ··-1 ·: ........ ~.::;;...-,. ..... 4. 90 BR0f10METHANE •O 'j ,./~ 5. 92 DI..OROETHANE
I ~ :L-..~---·--·-··----·-·-------- - 6. 80 1! 1-DiClETHYLEN i : ,....------"-·---··--·--···-- ·, ·~··-!!:::f"'"-:.___ ____ .=- - 8.18 METHYLENE CHLP.D 1- I ~;······ .. ··· .. ~::-..::::~;_-:::;;:::::::::.=.:::=--==~-· --a. 97 tns-1,2-DiCIENE 0 ··-i ':_--~---~,:::;:::.-.-- 10.08 1,1-0iClETHANE
o I ~~~·. 3~- P~.oD1_ --
1 ....... •., -···----··- ·-· .... ~ ·- 12.34 1, 1,1-TriCIETHA ... i ~:···~~ ~-:~=::::~~~~=~ .. :.. ... JZ=!]b ~BN ~TRACH.R ---··- 1"' 0., 1 ., o·~lETHANE :~ .,.. .. - .... --~---· .. -·------·----·-.. ............. .J• .:.· , J..- lL 1-" I -~~~~-:-:-:-:7:·:-:-:··:-:-:7::·_...---·--.-·-·:;::::-~-=='"-::.=-::.==::.=:====---·-···--····-···-···-·········-····-- ..... 14.16 TCE I ~············-Hot=:.:-·· -· _ ·-· . -- 14.50 1,2-DlCIPROPANE t:.~l ·1 : . -·-··· ·- o I i-~t·..,.-;;:-.::.~-":;-::::::==-":::.=-·--··-· ·- 15.68 cis-1,3-DiClPEN . -~ I ..:...~::- . 1::::::~~=~~====···-~::::"===---:- --····: ·'=·---·'=~-----· --·-~-::::.~.J.k~~J.l.2.:_~rl_Cfr~~ PCE -~ .l~t-..j;.-.::::::_ ........... ,..... ··- _ --·- 18.34 CHLOROBENZENE I ) ... ....- ,_.._, ... ...-- !:,,_:, ,. c~ __ 1
. ~ , ... ·- 19. 57 BROriJF(F.M
··•~-:.;._.....- -·=------~-· -20.20 1, 1 ,2,2-Cl4ETHA o I .. ,... tt- l ~·~~ .. '" ,.,.~ ... ~"~' _,_, -=~~~-.e!!!!· !!!!!. ~~~,.,---.··-·-···---· --· 21.77 1 4-DiClBENZENE (.l'f
0 j ····· -:-..::::=... - 22.33 1,2-DiCliNZEt.l£ =: .......... .....---.. ······ i'ol-·
/
I
.I
,I
ATTACHMENT 6 - 3321
4294
MAXIMA icl1990 Dynamic Solutions, Divis1on of Millipore MAXIMA 820 CONCENTRATION REPORT
Printed: 22-NOV-1990 8:06:20
SAtRE: 2PPB
14 1n 11e~: HALOG&AROMATIC VOLATILE ORGANIC
Acquired: 21-NDV-1990 6:57
Rate: 5.0 points/sec
Dur·atioo: 30.000 minutes
Operator: CYC
DETECTOR: iJC#l ELCD Ch#l
PKI IDI Retention Tille Type Peak Height Peak Area
(ainutes) <aicrovolt) (aicrovolt-sec)
--------- ------- --------- 3.167 BB 70.452699 6004.3941 -~ .:. 2 3.590 BF' 1206.7558 22423.796 ~ ~ 4.087 pp 27782.682 96BB28.b5 ·-· .J 4 4 4.900 PP 40223.007 1228463.7 <: 5 5.920 pp 7029.2958 767419.33 ..., 0 b 6.803 PP 110551.25 2739755.7
7 7 8.183 PP 76456.914 2630781.6
a B 3.967 pp 131095.19 2907869.3
9 9 10.083 pp 51350.004 1574150.7
:o li) 11.373 PB 7721.7827 115171.60
11 11 11.997 BP 70954.689 689880.49 j·")
... 12 i2.340 pp 152737.87 1655863.3
t: 13 12.76(; PP 19902.351 425396.99
14 14 1.3.030 FP 169516.35 2298292.0
15 15 1-f.lb3 PP 264762.43 2328769.9
16 16 i4.503 PP 200599.46 2356055.5
17 17 14.967 PP 81867.824 1267611.0
i8 18 15.683 PP 92633.854 1219457.8
19 1f 16.537 PP 53716.308 447462.83
20 20 16.797 PP 222268.97 1750747.0 ,, ..,, .... .!..i 17 .07(! pp 272139.82 2521359.7 .-.. .-.~ 17.410 PF 71771.273 1290407.7 ..;.,:.. ,:..~ ::3 ..,1' 18.337 FP 103010.91 1272194.7 .. ..,
:4 24 19.573 pp 8362.6519 123061.77 '")C:.
4'-' '"' L...J 20.197 PB 100208.89 1134090.1
26 26 21.65i) BP 137158.17 672580.12 ,.,.., ':.7 21.770 pp 181663.::3 2014680.1 i.l ... , 28 28 22.327 PB 155978.94 1798567.1
----------- ------------- TOTAL 2812741.6 36227347
Area Percent
------ 0.02

0.06 2.53

3.21 2.01

7.17 6.88

7.61 4.12

0.30 i.80

4.33 !.11

6.01 6.09

6.16 3.32

3.19 1.17

4.58 6.60

3.38 3.33

0.32 2.97

1. 76

5.27 4.70
Type: snm
lnstruilent: 6Cil f'URGE&TRAP
Filename: CS42PPB
Index: Disk
Injection Volume: 5000.0
Code Base Solution Cone ColpooentNalll!
------- ------------ EXT AREA 2.0000000 DiCHiiFMETHAN£
EXT AREA 2.0000000 CHLOROMETHANE
EXT AREA 2. 000(1()(1( VINYL CHLRD
EXT AREA 2.00COOOO BR0110M£TiiANE
EXT AREA 2.00000C~) CHLORO£THANE
EXT AREA 2.0000000 1,1-DiCIETHYLEN
EXT AREA 2.0000000 METHYLENE CHUm
EXT AREA 2.0000000 tns-1,2-DiClENE
EXT AREA 2.0000000 1,1-DiClETHANE
EXT AREA 2.0000000 ?lODl
EXT AREA 2.0000000 CHLOROFORM
EXT AREA 2.0000000 1,1,1-TriClETHA
EH AREA 2.0000000 CARBN TETRACHLR
EA:T AREA 2.00000()0 1,2-DiClETHkNE
EXi AREA 2.0000000 TCE
EXT AREA 2.0000000 1,2-DiClPROPANE
EXT AREA 2.0000000 BrDiClMETHANE
EXT HREA 2.0000000 Cls-1,3-DiClPEN
EH AREA 2.0000000 tns-1,3-DiClPEN
EXT AREA 2.0000000 11 112-TriClETHA
EXT Afo:EA 2.0000000 PCE
EXT AREA 2.0000000 DiBrClMETHANE
EXT AREA 2.0000000 CHLOROBENZENE
EXT AREA 2.0000000 BRO!'IOFORH
EXT AREA 2.0000000 1,1,2,2-Ci4ETHA
EXT AREA 2.0000000 1,3-DlClBENZENE
EXT ARE?. 2.0000000 1,4-DiCiBEUZENE
E.XT AREA 2.0000000 1,2-DlClBENZENE
-----------
5b.OOOOOO
ATTACHMENT 6 - 3322
4295
.....
:t
,..
.-
Salple: 3PPB Channel: GC#l ELCD CM1
Acquired: 21-NOV-91
) 9:3!:1 l'lethod: D:\I'IAX\B010-20D\8010-2Cit1
Inj Vol: 5000.00
X .1.()--.:t 'VO 1 t:s
Filena.e: CS73PPB
Operator: eve
0 0 0 0 0 0 0 0 0 0 -·-r-·T'-.. -· .... -.... --.•----·--.. L--.--'--.... -....l. ... - ..... - ............. _,_ • .J._, .. ___ .... _._J..,._......._ ___ .L ..... -.... _ ... _ ...... - .. o.. ......... - •• -'-·--...... J ....... . 0 II
'I J -3.22 DiCIDiFIET- ·-·~~ 3. 55 CHLOROt1ETHANE ? I ·=i ... :·~~' -· 4.06 VINYL CHLRD (.1'1 ····1 L .. .. . . . . .. .. Jt..+< .. ....::;;:: ·- 4. 91 BROMOMETHANE O · : ,... .... ~~;. 92 CHLOROETHANE I -;-lrlll::::._. _____ =::::.r• .... b,82 1,1-DiC}fTHYLEN .. :: ..... -... ..:-"'""'"'',....
j
;: .... .;, oi:::·-·-··-···-:~::::-.::::;:::;:::o- - 8. 20 METHYLENE CHLRD t- ; ............... -~~-~==-~=--::::=:::::::=:::~~::::=:::=-· .. - ·-· 8.98 tns-1,2-DiClENE 0 ·- 1 ~ ... ~:~:;:::·.::~-=::::;pooL- 10.09 1, 1-DiCIETHANE ( o I ·. ........ ......... 1 ~--Hl::~·- 11.37 P10Dl I -:-~:~: ........ -.... ---:=:=====-·""'"" ..... 12 -rc:: 1 1 1 ~ 'CIETHA :::::::: -~~~:::::=:..":::::::::::::::~="- 1 A "7 CARliN TETRACHLR _.. 'vw ' ' - 1 r 1 (.1'1 ·-
0 1:\:1
0 ~:::. I
i ... I
~·~ J
~ I
I
.! ... -~· . ...,.::::....~----·-··-----............ '-• I ,_ -- 1 ~ 04 t ., D. CIETHANE L.~-----.. ~::==-~~===-·~~~ .. .;.. ·~--~---~ .... -------- -- 14.18 TCE , ........................ _.~ ~ - ... :::-·- ·· -~·---: '4 51 1 "-D.CIP~OPANE ~ .......... .:~ .. .!o_::.,...... w~. _ 1 • ,... 1 H . ~ -·~·-:::.:::::;::::::::::::::~-::::==--==----·----·- -· 15.69 cis-1,3-DiCIPEN 1~~--· .. ·- 16.81 11 2-TriCIETHA :::::::: ........ :-:· ....... ::::. ~:n=~~~~~~§_§_.~~~;;;;; ... ~-;;_;;. ;;.;;:;;;;;;;;;;:::::. ==-·=-- -·----~1: ...... 1",, 08 PCE =·······················-l::il::!~ ·- ~:::::---=:=--=--=---··~~--·-- : ,............-.-· .. -- -18. 35 CHLOROBENZEiol£ ~~:- ..... 19. 57 BROI'KIFORM
~::::=====-------
1~~~··~-~~:.:.:.:::.:.:.:.:.:.:.:::.:······;····:_:..::::li ... !l!:::- ~~=---:::.·---~- 21.78 !,_4-DiClBE.!;IZENE ~··- - .. -- .. _ .. ,... ---~ - 22.34 1,2-DiClt~t:.NZENE ATTACHMENT 6 - 3323
4296
t'.AX!i'IA (cl 1990 Dynamic Soluhon;, Division of Millipore MAXIMA 820 CONCENTRATION REPORT
Printed; 22-t-lOV-1990 8;07:22
SAI'IPLE: 3FPB
115 in Method: HALOG&AROMATIC VOLATILE ORGANIC
Acquit•ed; il-NOV-1990 9:39
Rate: 5.0 pc;ints/sec
Dt.wation: 30.000 m1nutes
O!Jerato:-: CI'C
DETECTOR: GC#l tLCD Cnlll
PK# IDI Retention Time Type Peak Height Peak Area
(ainutesl (aicrovoltl (aicrovol t-sec)
---------- ------- ------- "T ?')"'! •.h ... i..oJ BP 224.11349 3217.5070 <. .... 3.553 PP 1737.1180 25494.578 .,. .:=I 4.063 PP 43514.018 1417410.9 .j 4 4 4.913 pp 61769.374 2071170.4
5 "" 5.917 PP 13256.901 1147875.6 . .J
0 6 6.817 PP 76388.368 2982314.4 ..,
I 7 8.197 PP 104789.51 3699429.2
8 8 8.980 pp 187978.77 4314851.0
9 9 10.087 pp 84261.189 2880470.8
lO 10 11. 37(1 PP 201.30.041 501240.48
11 11 12.010 pp 89256.059 944548.96 ,, 12 1:2.350 PF' 219456.82 2442053.5 ..... i'":! 1.3 12.770 PF 34080.867 698711.28 ... ._.
14 14 13.040 pp 248467.59 3631293.3
15 15 14.177 pp 367190.05 3290139.2
1t: lb 14.513 Pf· 284539.61 3326505.!
17 F 14.977 pp 126078.14 1967161.5
18 18 15.693 pp 149809.02 2001726.1
19 19 16.543 pp 94317.328 775966.68
20 20 16.807 pp 317009.96 2512400.1
21 21 17.080 pp 376172.59 3451980.4 .-.·--:: ,.,.., ..:...&... 1..i. 17.413 F'P 101952.92 1835926.8

2.3 -.-,. .;_.,j 18.347 F'P 151533.38 1841107.7
..;;>+ 24 19.567 pp 12608.530 161012.96 .-c;
..:..! 25 20.203 PB 156341.93 1617218.1
2b 26 21.b57 BP 200549.39 992641.24
;:.! '!-!
~~ 21.777 FP 254997.40 2744055.5
28 :28 22.337 PB 220788.74 2646825.1
----------- --------------- TOTi4L .)999199. 7 55924738 Area Percent
------- 0.01

0.05 2.53

3.70 2.05

5.33 6.62

7.72 5.15

0.90 1.69

4.37 1.25

6.49 5.88

5.95 3.52

3.58 1.39

4.49 6.17

3.28 3.29
0 ., ... ai-.7

2.89 1. 77

4.91 4.73
Type: snm
Instrument: GC#l PURGE&TRAf'
Filename; CS73PPB
Inde::: Dist::

In.jection Valuate: 5000.0
Code &se Solution Cone Caltponent Hale
----- --------- EXT AREA 3.0000000 DiC1DiFI1ETHANE
EXT AREA 3.0000000 CHLOROMETHANE
EXT AREA 3.000000(1 VWYL CHLRD
EXT AREA 3.0000000 BROt101'1ETHAN£
EXT AREA 3.0000000 CHLOROETHANE
EXT AREA 3.0000000 1,1-DiClETHYLEN
EXT AREA 3.0000000 !'ETHYLENE CHLRD
EXT AREA 3.0000000 tns-1,2-DlClENE
EXT AREA 3.0(100000 1, 1-lhClETHANE
EXT AREA 3.0000000 P10Di
EXT AREA 3.000(1000 CHLOROFORM
EXT AREA 3.0000000 1,1,1-TrlClErHA
EXT AREA 3.0000000 CARB~J TETRACHLR
EXT AREA 3.0000000 112-DiClETHANE
EXT AREA 3.00000(10 TCE
EXT AREA 3.0000000 1, 2-DiClPROF'fiN£
EXT AREA 3.000:)000 BrDiClMETHANE
EXT AREA 3. iY.JOOOOO cis-1,3-DlClPEN
EXT AREA 3.0000000 tns-1,3-DiClPEN
EXT AREA 3.0000000 1,1,2-TriClETHA
EXT AREA 3.0000000 PCE
EXT AREA 3.0000000 DiBrClMETHANE
EXT AREA 3.0000000 CHLOROBENlErE
EXT AREA 3.0000000 BfiONOFORM
EXT AREA 3.0000000 1,1,2,2-Cl4ETHA
EXT AREA 3.0000000 1,3-DiClBENZENE
EXT AREA 3.0000000 114-DiClBENZEHE
EXT AREA 3.0000000 1,2-DiClBENZENE
-------------

84.000000
ATTACHMENT 6 - 3324
4297
>::
1-"
0 1-'·
:J
.....
~
\!:
o!'+- 1 .,.,
Ll'1
Salple: 4PPB Channel: 6C#1 ELCD Ch#l
Acquired: 21-NOV-90 10:21 lfethod: D:\lfAX\8010-20D\8010-201'1 Inj Vol: 5000.00
Filena.e: C5E14PPP
Operator: eve
0 0 0 0 0 0 0 0 0
g
• li·- ' 1 • -' .L.--·-·--·'------l·-··--...1. .. __ ; __ , ........ -- -·--'---'----'-·-.. ·--·l·-·-··J.·-···---·-·········-·-····--··--··--·-·-;···-·······-·-' ... ,
! 3.20 DiClDiFMETHANE
~ ·~~ - 3. 59 CHLOOOt1£THANE ? l~=::;:;_;;=·- 4.03 VINYL CHLRD -- ·, ---::;:::;:::;::;o ..... 4. 90 Bfi'OMOI1ETHANE 1!.1'1 ···········-::H .. 0 : .......-· I
~ ... ·· .... 5. 9: CHLOROEiHANE ~-11-fi::;: __ ~·~ _ 6.83 1,1-DiClETHYLEN 1 . '· ,....,...... ·-·· i ! .. ·--r.•:;4.. .. __ ... ____ -::::o.-- 8.21 METHYLENE CHLRD ...-
...... lj : ~·················~·-=~=-·-······-··--···-::::: _.....-----····--····- _ ... --8 99 t 1 "D'ClENE .... - ........... - • ns- ,t..- 1 0 ····1 1· .. ·--l'-.c'~~~:::;.:..--::::::--=- ··- 10.09 1, 1-DiC!ETHANE 0 I ~ ,.........-·- :-~~ _ 11.38 P10D1
I !;·:':.~:·:+~=::~m·-:::- -·· _ 12.36 1,1 1 1-TnClETHA ... , ......... ~.. ··· -·--··-- ··· 1"~ 78 ctiRBN fEtRAtli.R I l····:~ ...... --::::.-=.-=-..:=-'7 .. -:==--·-...!:.:.....- _,,_ - 13.05 1 I 2-DiClETHANE 1-" I :-·(hl(uo. - ·--·---- 14.18 TCE
• j ~: . .'.".'.'.'.'.'.'.'.'.'.'.'~·;~~·· .. ~~- --·-· - - · -· 14.52 1,2-DiClPROFANE I:JI ., ~ .---·-·----- 0 I 1· ~.,. - - 15.70 cis-1,3-DiClPEN
_I ;l·t·f::F:!:~:=;p=.z;;·· I ~ .....---····~··· I ~f-............... ·=.======-------- 18.35 CHUIROBENZENE ~·!,) 1 ~,: ···- 19. 57 BRCHOFORI'I
·- 16.81 1.1.12-TriClETHA ___ ___._ -- 17. 09 PCE
8 .. I . ~::.:-. ...--.. --::=:::.- -· ··c------- -20.21 11 11212-Cl4ETHA J -f~ -·~;;~~~~: .. :~ ·~:· .. ·_:=·--= .. ki::=··-==~·-·:_:_...:_-=:_~-·=-=~.22-. 34 --1, i.:l{da~f&JBENZENE I ~ , .. --- 1 ,:,..-·· ~ -·-· ,r.-
0 I I
~ I
I I
ATTACHMENT 6 - 3325
4298
M?!X IMA ici 1990 Dynuic Solutions, Division of fhlllpor-e MAXIMA 8:20 CONCENTRATION REPORT
Pr1nted: 22-NOV-1990 8:08:24
SAtRE: 4PFB Type: STND
16 in Method: HALDG&AROMATIC VOLATILE ORGANIC Instruent: GCil PUf<6E&TRAf' ikquire.:l: 21-NOV-1990 10:21 Fi lenaae: CS104PPB
Rate: 5.0 points/sec Index: Disk
l!twation: 30.000 m1nutes Injection Vollllle: 5000.0
Operator·: CYC
DETECT~: 6Ci1 ELCD Chl1
PKI Illi Retention Till! Type Peak Heisht Peak Area Area Percent Code Base Solution Cone ColponentNue (einutesl (eicrovoltl (eicrovolt-secl
-----
1 3.203 BB -2.145767 1172.8408 o.oo EXT AREA 4.0000000 DiClDiFMETHANE 2 2 3.590 BP 1426.3393 25148.146 0.04 EXT AREA 4.0000000 CHLORIJ'IETHANE ' ..,. 4.033 PP 47485.715 1553945.9 2.49 EXT AREA 4.0000000 VINYL CHLRD ·.J .:,. 4 4 4.903 pp 69083.103 2274699.4 3.64 EXT AAEA 4.0000000 BR1J'IOMETHANE 5 c 5.913 PP 15726.330 1382259.0 2.21 EXT AREA 4.0000000 CHLOROETHANE ..! 6 0 6.830 PP 84630.261 3281379.1 5.26 EXT AREA 4.0000000 1,1-DiClETHYLEN 7 7 8.207 F'P 117800.49 3952679.4. 6.33 EXT AREA 4.0000000 METHYLENE CHLRD I 8 8 8.993 PP 213558.82 4909145.4 7.87 EXT AREA 4.0000000 tns-1,2-DiClENE 9 9 10.093 ?P 98926.556 3285962.9 5.27 EXT AREA 4.0000000 11 1-DiClETHANE 10 l\) 11.300 PP 23801.926 586581.14 0.94 EXT AREA 4.0000000 P10Dl 11 11 12.020 pp 107119.57 1113887.4 1. 78 EXT AREA 4.0000000 CHLOROFORM 12 12 12.363 pp 248272.09 2752034.5 4.41 EXT AREA 4.0000000 1,1,1-TriClETHA 13 13 12.783 PP 39083.485 790156.36 1.27 EXT AREA 4.0000000 CARBN TETRACiiLR 14 14 13.053 pp 280354.89 4045655.0 6.48 EXT AREA 4.0000000 1,2-DiClETHANE 15 15 14.183 pp 405853.80 3627-l89. 7 5.81 EXT AREA 4.0000000 TCE 16 16 14.523 pp 315061.73 3678878.7 5.89 EXT AREA 4.0000000 1,2-DiClPROPANE 17 17 14.987 PP 141697.78 2160682.9 3.46 EXT AREA 4.0000000 BrDiCll'iETHANE 18 18 15.700 pp 170088.91 2234681.3 3.58 EXT AREA 4.0000000 cis-1,3-DiClPEN 19 19 16.550 pp 110743.42 900366.84 1.44 EXT AREA 4.0000000 tns-1,3-DiClPEN 20 20 16.8i3 PP 354351.44 2801662.9 4.49 EXT AREA 4.0000000 1,1,2-TriClETHA 21 21 17.090 PP 416400.12 3849135.5 6.17 EXT AREA 4.0000000 PCE .;.-, 22 17.423 pp 109456.91 1973465.9 3.16 EXT AREA 4.0000000 DiBrClMETHAI-lE .;_,;;. ~,.,. ":•1' 18.353 pp 170110.13 2059026.1 3.30 EXT AREA 4.0000000 CHLOROBENZENE ~.,j ... .., 24 24 19.573 pp 12792.946 183346.91 0.29 EXT AREA 4.0000000 BROMOFORM ~.~:
i...J 25 20.210 PB 182722.71 1910728.4 3.06 EXT AREA 4.0000000 1,1,2,2-Cl4EThA 2o 26 21.667 BP 222818.28 1113083.4 1.78 EXT AREA 4.0000000 1,3-DiCIBENZENE "1., i.i 27 21.787 pp 281669.65 2984048.6 4.78 EXT AREA 4.0000000 1,4-DiClBENZENE 28 28 22.343 PB 247677.83 2975729.9 4.77 EXT AREA 4.0000000 1,2-DiClBENZEN£ ----------- ------------ ------------ TOTAL 448B717.4 b2407033 112.00000 ATTACHMENT 6 - 3326
4299
,.,,,
Salple: 5PPB Channel: GCI1 ELCD Ch#1
Acquired: 21-NOV-90 11:03 l'tethod: D: \I'IAX\B010-20D\801(1-2(JM Inj Vol: 5000.00
N
0 0
0 0
Filena~~e: CS135P:::'B
Operator: C\C
0 0
;."!! -·-r····-r-·---•·····--.I. ........ .J_ .... -•··---'----'--·--L-.. •----··'···-·-'-·-··..L--•·-·····--'·--····..._ ___ .J •..... -'··----..1..-·-····•-·-L. __ ._ ....... .L.-.. . o!~ I I
I I
I I ·I I
I ~t 3. 6!J CHI..OOOMETHANE o::~ I ~, "'=---·-~:;:;:- ··- 4. 06 VINYL CHI..RD • I : · · · · · · -·-!>·!If.: ••
l
: -····-····::· -·· 4. 91 BROI'OIETHANE
(JI :·······~
O ! .... ··'"'··· 5. 94 CHI..OROETHANE
t•*'::.-·------::::=--=- ... 6. 84 1, 1-DiClETHYI..EN
·i ·: .. ........---- ' 1 .. ....._·--·--·--·---_,... ·- 8.23 METHYLENE CHI..RD I
: __ .. _ 1- i ................. ~ ~:=::=::--====-=--==-=---- ..... 9.00 tns-1,2-DiClENE 0 ... ~ j-···-+<~=---==-- 10.11 1, 1-DiClETHANE o:::~,: ..--- .... . i· -~:. _ 11.40 P10D1 ···I' 1:~::7:·:~~=-t~~~--:=::: -- ___...... I : .....--~~- T!!'omtiJ.2.37 11 11 1-TriClETHA
• 7 CARBN TE •
·- 13.06 1,2-DiClETHANE
: ...... ,
1 F~=:::::··~··; .... -fHk ~-§· §-~;;._ ;; ... ~~~;; .. _;;_~~=======~---~· !;'44"':. 53;-1;-,: i=lliClPROP~~19 TCE
<:> '!······-io·~-=---=· .. -·-------· ... - 15.71 cis-1,3-DiClPEN 1 ~~·-~ ....... -~ ~ ~ . I , ......... :::m==~ -- - -- ····-·::::-.::::.. ·--·--·---··--· -··· 16.8..:. 11.tt., .. -TrlCIETHA ,:~;~~==-==~--~~~-~-, "17.10 PCE
! ~- ..... 19.57 BROMOFG"RM
g- r.C=-~-= .....
-
...
-
... -._· .. _-__ -_-_-_--- 20.22 1,1,2,2-cl4ETHA
........ =- ·--· .. -• ... ···----·-·- 21.79 1d,-DiClBENZENE ~-····~---- =----~--- -· 22.35 1,2-DiCltitNZENE : -:~.-::::--"1!. 98
':.-'
~· !<1-
::..rl- II
0 J I
'+29.30
ATTACHMENT 6 - 3327
4300
MAXI~q icl1990 Dynamic Solutions, Division of Mill1pore MAXIMA 820 CONCENTRATION REPORT
Printed: 22-NOV-1990 8:09:26
SAf1PLE: 5PPB
17 in Method: HALOG&AROMATIC VOLATILE ORGANIC
Acquit•ed: 21-NOV-1990 11:(;3
Rate: 5.0 points/sec
Dur·ation: 30.000 minutes
Opet·ator: CYC
DETECT~: GC#1 ELCD C.llll
Pkl IDI Retention Ti• Type Peak Height Peik Arei
l•inutes) l•icrovol t) <•icrovolt-sec)
--------- ------- -------- .,. ........... .J • ..)..;,~I &P 243.18698 2447.7724 2 2 3.61)0 pp 1739.3830 3.3994.919
3 'l'
·.1 4.057 pp 63490.518 20811b6.8
4 4 4.910 pp 89952.837 3101588.0 1:
.! 5 5.9-l3 pp 20602.467 1779966.9
6 b 6.843 pp 122275.25 4623328.4 "7 7 8.230 PP 156110.90 5389541.8 ; 8 s 9.000 PP 273535.40 6271999.7
9 9 10.110 pp 134981.89 4671246.8
10 lt) 11.403 pp 3.3380.989 832879.88
ll 11 12.027 pp 204283.38 2084042.3 ~ .-,
i~ 12 12.370 pp 346633.24 3885173.3
13 1.3 12. 7t)0 pp 100722.80 1410524.0
14 14 13.060 PF' 372245.71 5495383.6
15 15 14.193 F'P 518011.63 4650526.8
16 16 14.533 pp 408338.36 4740b49.8
17 17 14.990 pp 232271.58 3350283.6
18 18 15.707 pp 248718.b5 3304498.9
19 19 16.553 F"P 179328.34 1447223.0
·•·· . 20 16.820 PP 466670.09 3731041.2 .::,1_;
.....
.:.l 21 17.100 pp 535987.68 4906786.8 .-,""\ ....... ~~.. :..~ 17.430 PP 175707.84 30676bb.2 ·-=., ":11' t...J .;..-,J 18.360 pp 227814.46 2993589.9 24 24 19.570 pp 36237.006 449852.50 .-.c
.a:..J 25 20.217 pp 272026.33 3289156.9
26 26 :21.673 pp :!.01187.55 152482b.5 ,..,,
""' 27 21.793 pp 36~262.98 3961276.9 ·i,',
.:.o 28 22.353 PB 32b727.07 3937749.8 ·"":-0 22.980 ss 12338.401 42412.872 ~· 30 29.300 BB 926.61392 1599.3240
----------- --------------- TOTAL 6231752.5 87062425
Arei Percent
------- o.oo

0.04 2.39

3.56 2.04

5.31 6.19

7.20 5.37

0.96 2.39

4.46 1.62

6.31 5.34

5.45 3.85

3.80 1.66

4.29 5.64

3.52 3.44

0.52 3.78

1. 75

4.55 4.52

0.05 1). !);)
Type: STND
Instrument: 6CI1 PURSE&TRAP
Filename: CS135PPB
Index: Disk
Inject1on Volume: 5000.0
Code Base Solution Cone Colponent NMe
------ ---------- EXT AREA 5.0000000 D1ClDiFI£THANE
EXT AREA 5.0000000 CHLOROMETHANE
EXT AREA 5.0000000 VINYL CHLRD
EXT AREA 5.0000000 BROf10METHANE
EXT AREA 5.000000v CHLOI\'OETHANE
EXT AREA 5. (101)0000 1~1-DiClETHV'LEN
EXT AREA 5.0000000 METHYLEI£ CHLRD
EXT AREA 5.0000000 tns-1,2-DiClENE
EXT AREA 5.0000000 1,1-DiClETHANE
EH AREA 5. 000001..'~0 ?10D1
EXT AREA 5.0000000 CHLORCIFORM
EXT AREA 5.0000000 1,1,1-TriClETHA
EXT AREA 5.0000000 CARBN TEiRACHLR
EXT AREA 5.0000000 1,2-DiClETHANE
EXT AREA 5.0000000 TCE
EXT AREA 5.0000000 1,2-DiClPROPANE
EH AREA 5.0000000 &t·D iC li'IETHANE
EXT AREA 5.0000000 cis-1,3-DiClPEN
EXT AREA 5.0000000 tns-1,3-DiClPEI~
EXT AREA 5.0000000 11 112-TnClETHA
EXT AREA 5.0000000 PCE
EXT AREA 5.0000000 DiEtrClMETHANE
EXT AREA 5.0000000 CliLOROBENZENE
EXT AREA 5.0000000 BR0110FOHM
EXT AREA 5.0000000 1, 1,2, 2-Cl4ETHA
EXT AREA 5.0000000 1,3-DlClBENZENE
EXT AREA 5.0000000 1,4-DiClBENZENE
EXT AREA 5.0000000 11 2-DiClBENZENE
-----------
140.00000
f.-::to-...

ATTACHMENT 6 - 3328
4301
Salple: BOR-050001 Channel: SCil ELCD Ch#l
Acquired: 20-NOV-90 7:49 1'1ethod: D: \HAX\8Q10-20D\6010-20P1 Inj Vol: 5000.00
vo 1 t:s
0 0 <:> . . 0
Filena~e: EHA14902
(ferator: CYC
0 N • ~ 00 0
0 0 0 o:::. 0 0 C• g r~ _ _l ____ ...... __ _._ __ .... ______ .l___ .. L---·-'-··......__t. ____ .... __ __,_ _ __, ____ J _______ , ___ __, __________ ... _________ .I l.J..._ ~ Q'") c· r, ..) .... ~--·II
0 I I
~ ~ I
ATTACHMENT 6 - 3329
4302
MAXIMA (cl1990 Dtnamic Solutions, Division of ~illipore MAXIMA 820 CONCENTRATION REPORT
Printed: 22-NOV-1990 8:24:12
SAttPL.E: 00R-05(Ji)01
#8 in l'tethod: HALOG&AAOI1ATIC VOLATILE ORGANIC
Acqu1red: 20-t~V-1990 7:49
Rate: 5.0 points/sec
Duration: 30.000 minutes
Operator: eve
DETECTOR: GCtl ELCD Chtl
PI< I IDI Retention Tille Type Peak Height Peak Area
<•inutesl (•icrovoltl (•icrovolt-secl
-------- ---- ------ 3.920 BB 42.319303 29.659276
----------- -------------- TOTAL 42.319303 '29.659276
Type: UNKN
Instrument: 6CI1 PURGE&TRHP
Filename: EI1A14902
Index: 2
InJechon Volume: 5000.0
Area Percent Code Base Solution Cone Coaponent Naill!
100.00
0 ATTACHMENT 6 - 3330
4303
Sallple: BOR-050005 Channel: 6C#t aco Ch#l
Acquired: 20-NOV-90 8:31 !'lethod: D: \HAX\8010-20D\B010-2011 lnj Vol: 5000.00

0. .......
......
·~
Filenaae: EMA14903
Operator: CYC
ATTACHMENT 6 - 3331
4304
MAXIi·lA icl 1990 Dynaauc Solutions, Division of Millipore MAXIMA 820 CONCENTRATION REPORT
Pt•inted: 22-NOV-1990 8:24:56
SAI'f'LE: BOR-0500(;5
#9 in Method: HALGG&P.ROMATIC VOLATILE ORGANIC
Acquit·ed: 2()-NOV-1991) 8:31
Rate: 5.0 paints/sec
Dut·ation: 30.000 minutes
Operator·: Ci'C
DETECTOR: GC#l ELCD Chif1
PKI IDI Retentioo TiE Type Peak Height
<minutes) <•icrovol t)
----------- -------- 3.873 BB 175.11847
----------- TOiAL 175.11847
Peak Area
<•icrovolt-secl
----------- 102.59153
--------------- 102.59153
Type: UNKN
Instrument: GCI1 PUR6E&TRAP
Filename: £MA14903
Index: 3
Injection Volume: 5000.0
Area Percent Code Base Solutioo Cone Coapooent Naale
100.00
0 ATTACHMENT 6 - 3332
4305
Salple: BOR-050010 Channel: GC#l ELCD Chll
Acquired: 20-NOV-90 9: i3 ltethod: D: \11AX\8010-20D\8010-201'1 Inj Vol: 5000.00
volt::!.:;:
0 0 0
Filena~~e: EI'IA14904
Operator: CYC
0 N A ~ ~ 0 <:",i~•O. 0 <'.) .;;,',:0 0 <:> o +r_. ___ _,_ ___ ... _____ _t_ ___ _,_ __ _.. ___ _. _____ ..J ________ ..._ __ J·--·······....__J._ .• _.__ .......___._ ____ L. __ _._ __ .. _._ ... _._ ... _.J o I'
l I .. 1,
0 . fl .tt- ! '" 9(1 .,), . • I
r..r: I
0 o ~t ..... ! I
0 I [
-~
I
ATTACHMENT 6 - 3333
4306
MAXIMA (cll990 Dynamic Solutions, Division of Millipore MAXIMA 820 CONCENTRATION REPORT
F'rinted: 22-NOV-1990 8:27:19
SMU: BOR-Q50010
iiO :on l'lethoci: HALOG&AROMATIC VOLATILE ORGANIC
Acquired: 20-NOV-1990 9:13
Rate: 5.0 points/sec
Dut•ation: 30.000 minutes
Opet·ator: CYC
DETECTOR: GCil ELCD Cnw1
PI< I IDI Retention Tille Type Peak Height Peak Area
<•inutesl <•icrovoltl <•icrovolt-secl
-------- ------ ------ 3.897 BB 212.43098 368.89917
---------- ------------- TOTAL 212.43098 368.89917
Type: IJNI(N
InstrUIIent: 6Cil PURGE&TRAf'
Filename: EI'IA14904
Index: 4
Injection Volume: 5000.0
Area Percent Code Base Solution Cane Colpanent Halle
100.00
0 ATTACHMENT 6 - 3334
4307
Salple: BOR-020001 Channel: GC#l ELCD Chit~
Acquired: 2o-NOV-90 9:55 l'lethad: D:\I'IAX\8010-20D\8010-20M Inj Vol: 5000.00
VO 1 -t:s
0 0 0 0 0
()!)
<='•
Filena~e: EMA14905
Operator: CYC
"'""
0 ·:~~
ATTACHMENT 6 - 3335
4308
;'JAXIMA (c! 199tj Dynamic Solutions, Division of i'hllipore MAXIMA 820 CONCENTRATION REPORT
Ft·inted: 22-NOV-1990 8:28:03
SAfftE: BOF:-020001
#11 in Method: HALGG&AROMATIC VOLATILE ORGANIC
Acquu-ed: 2i)-NOV-19% 9:55
Rate: 5.0 pointsisec
Duration: 30.000 minutes
Operator: C\'C
DETECTOR: GCil ELCD Ch#l
PKI IDI Retention Time Type Peak Height Peak Area
<•inutesl (microvolt! <•icrovol t-sec I
------------ ------ ---------- 9.333 BE 147.93875 713.42004 ----------- --------------- TOTAi.. 147.93875 713.42004 Type: UNKN
Instrument: GC#l PURSE&TRAP
Filename: EMA14905
Index: 5
Injection Volume: 5000.0
Area Percent Code Base Solution Cone Component lilalle
100.00
ATTACHMENT 6 - 3336
4309
Salple: BOR-020005 Channel: GC#l ELCD Ch#l
Acquired: 20-NOV-90 10:37 lfethod: D:\11AX\8010-20D\8010-20M Inj Vol: 5000.00
volts
0 0 0 0
Filena.e: EMA149C~
Operator: CYC
ATTACHMENT 6 - 3337
4310
i1AAIMA ic) 1990 Dynamic Solutlons, Division of l'lillipore MAXIMA 820 CONCENTRATION REPORT
Printed: 22-NOV-1990 8:30:26
~: BOR-020005
if12 in Method: Hiil.f.IG&AROHATIC VOLATILE (J<GANlC
Acquired: 2o-NOV-1990 10:37
Rate: 5. i) pointsisec
Duration: 30.000 ~inutes
Operator: CrC
DETECT~: GCIH ELCD Chl1
PKI IDI Retention TiE Type Peak Heisht Peak Area
<•inutesl <•icrovoltl <•icrovolt-secl
----- --- 3.943 BB 172.61507 304.88973
--------- ------------- TOTAL 172.61507 304.88973
Area Percent
100.00
Type: UNKt~
Instrwaent: 6CI1 PURGE& TRAP
Filenaae: EMA14906
Inde:{: 6
Injection Volute: 5000.0
Code Base Solution Cone Colpanent NHe
------------- 0
ATTACHMENT 6 - 3338
4311
.....