Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 097-01-002-22889 N/A Solid ICP 7300 07/02/16 07/07/16 10:31
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.765 0.152 1.02
Arsenic ND 0.765 0.264 1.02
Barium ND 0.510 0.158 1.02
Beryllium ND 0.255 0.140 1.02
Cadmium ND 0.510 0.138 1.02
Chromium ND 0.255 0.145 1.02
Cobalt ND 0.255 0.151 1.02
Copper ND 0.510 0.137 1.02
Lead ND 0.510 0.134 1.02
Molybdenum ND 0.255 0.135 1.02
Nickel ND 0.255 0.148 1.02
Selenium ND 0.765 0.306 1.02
Silver ND 0.255 0.0875 1.02
Thallium ND 0.765 0.155 1.02
Vanadium ND 0.255 0.144 1.02
Zinc ND 1.02 0.181 1.02
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 7 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-20-01 16-06-2030-1-AA 06/28/16
09:47
Solid Mercury 05 07/06/16 07/06/16
15:51
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0194 0.0806 0.00568 1.00 J
BB-20-03 16-06-2030-2-AA 06/28/16
09:49
Solid Mercury 05 07/06/16 07/06/16
15:54
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0182 0.0794 0.00559 1.00 J
BB-21-01 16-06-2030-4-AA 06/28/16
10:24
Solid Mercury 05 07/06/16 07/06/16
15:56
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0177 0.0877 0.00618 1.00 J
BB-21-03 16-06-2030-5-AA 06/28/16
10:26
Solid Mercury 05 07/06/16 07/06/16
15:58
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0192 0.0862 0.00607 1.00 J
BB-22-01 16-06-2030-7-AA 06/28/16
11:02
Solid Mercury 05 07/06/16 07/06/16
16:00
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.0820 0.00578 1.00
BB-22-03 16-06-2030-8-AA 06/28/16
11:04
Solid Mercury 05 07/06/16 07/06/16
16:03
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0184 0.0833 0.00587 1.00 J
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 7471A Total
Method: EPA 7471A
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-16-480-44 N/A Solid Mercury 05 07/06/16 07/06/16 15:27
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.0833 0.00587 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 7471A Total
Method: EPA 7471A
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-21-01 16-06-2030-4-AA 06/28/16
10:24
Solid GC 41 07/05/16 07/08/16
13:01
160705L04
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aldrin ND 5.0 2.2 1.00
Alpha-BHC ND 10 3.7 1.00
Beta-BHC ND 5.0 2.5 1.00
Chlordane 30 50 26 1.00 J
4,4'-DDD ND 5.0 2.4 1.00
4,4'-DDE 7.4 5.0 2.2 1.00
4,4'-DDT ND 5.0 2.2 1.00
Delta-BHC ND 10 4.4 1.00
Dieldrin ND 5.0 2.2 1.00
Endosulfan I ND 5.0 2.0 1.00
Endosulfan II ND 5.0 2.4 1.00
Endosulfan Sulfate ND 5.0 2.6 1.00
Endrin ND 5.0 2.4 1.00
Endrin Aldehyde ND 5.0 3.0 1.00
Endrin Ketone ND 5.0 2.5 1.00
Gamma-BHC ND 5.0 2.2 1.00
Heptachlor ND 5.0 2.2 1.00
Heptachlor Epoxide ND 10 3.7 1.00
Methoxychlor ND 5.0 2.7 1.00
Toxaphene ND 100 45 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 106 24-168
2,4,5,6-Tetrachloro-m-Xylene 79 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8081A
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-12-537-2463 N/A Solid GC 41 07/05/16 07/08/16 11:03
160705L04
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aldrin ND 5.0 2.2 1.00
Alpha-BHC ND 10 3.7 1.00
Beta-BHC ND 5.0 2.5 1.00
Chlordane ND 50 26 1.00
4,4'-DDD ND 5.0 2.4 1.00
4,4'-DDE ND 5.0 2.2 1.00
4,4'-DDT ND 5.0 2.2 1.00
Delta-BHC ND 10 4.4 1.00
Dieldrin ND 5.0 2.2 1.00
Endosulfan I ND 5.0 2.0 1.00
Endosulfan II ND 5.0 2.4 1.00
Endosulfan Sulfate ND 5.0 2.6 1.00
Endrin ND 5.0 2.4 1.00
Endrin Aldehyde ND 5.0 3.0 1.00
Endrin Ketone ND 5.0 2.5 1.00
Gamma-BHC ND 5.0 2.2 1.00
Heptachlor ND 5.0 2.2 1.00
Heptachlor Epoxide ND 10 3.7 1.00
Methoxychlor ND 5.0 2.7 1.00
Toxaphene ND 100 45 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 97 24-168
2,4,5,6-Tetrachloro-m-Xylene 76 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8081A
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-20-01 16-06-2030-1-AA 06/28/16
09:47
Solid GC 58 07/05/16 07/07/16
16:49
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 43 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 31 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 34 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 98 24-168
2,4,5,6-Tetrachloro-m-Xylene 79 25-145
BB-20-03 16-06-2030-2-AA 06/28/16
09:49
Solid GC 58 07/05/16 07/07/16
17:06
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 105 24-168
2,4,5,6-Tetrachloro-m-Xylene 64 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-21-01 16-06-2030-4-AA 06/28/16
10:24
Solid GC 58 07/05/16 07/07/16
17:24
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 43 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 33 50 31 1.00 J
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 34 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 110 24-168
2,4,5,6-Tetrachloro-m-Xylene 89 25-145
BB-21-03 16-06-2030-5-AA 06/28/16
10:26
Solid GC 58 07/05/16 07/07/16
18:18
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 108 24-168
2,4,5,6-Tetrachloro-m-Xylene 83 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-22-01 16-06-2030-7-AA 06/28/16
11:02
Solid GC 58 07/05/16 07/07/16
18:36
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 106 24-168
2,4,5,6-Tetrachloro-m-Xylene 85 25-145
BB-22-03 16-06-2030-8-AA 06/28/16
11:04
Solid GC 58 07/05/16 07/07/16
18:54
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 43 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 31 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 34 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 101 24-168
2,4,5,6-Tetrachloro-m-Xylene 58 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-12-535-3813 N/A Solid GC 58 07/05/16 07/07/16 13:31
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 92 24-168
2,4,5,6-Tetrachloro-m-Xylene 91 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 4 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-20-01 16-06-2030-1-A 06/28/16
09:47
Solid GC/MS Q 06/29/16 06/30/16
15:32
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.4 1.00
Benzene ND 5.2 0.13 1.00
Bromobenzene ND 5.2 0.22 1.00
Bromochloromethane ND 5.2 0.71 1.00
Bromodichloromethane ND 5.2 0.24 1.00
Bromoform ND 5.2 0.82 1.00
Bromomethane ND 26 9.7 1.00
2-Butanone ND 52 3.9 1.00
n-Butylbenzene ND 5.2 0.16 1.00
sec-Butylbenzene ND 5.2 0.60 1.00
tert-Butylbenzene ND 5.2 0.16 1.00
Carbon Disulfide ND 52 0.32 1.00
Carbon Tetrachloride ND 5.2 0.29 1.00
Chlorobenzene ND 5.2 0.23 1.00
Chloroethane ND 5.2 1.5 1.00
Chloroform ND 5.2 0.25 1.00
Chloromethane ND 26 0.31 1.00
2-Chlorotoluene ND 5.2 0.24 1.00
4-Chlorotoluene ND 5.2 0.22 1.00
Dibromochloromethane ND 5.2 0.59 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.2 0.26 1.00
Dibromomethane ND 5.2 0.80 1.00
1,2-Dichlorobenzene ND 5.2 0.24 1.00
1,3-Dichlorobenzene ND 5.2 0.18 1.00
1,4-Dichlorobenzene ND 5.2 0.23 1.00
Dichlorodifluoromethane ND 5.2 0.46 1.00
1,1-Dichloroethane ND 5.2 0.22 1.00
1,2-Dichloroethane ND 5.2 0.32 1.00
1,1-Dichloroethene ND 5.2 0.36 1.00
c-1,2-Dichloroethene ND 5.2 0.29 1.00
t-1,2-Dichloroethene ND 5.2 0.52 1.00
1,2-Dichloropropane ND 5.2 0.45 1.00
1,3-Dichloropropane ND 5.2 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.2 0.34 1.00
1,1-Dichloropropene ND 5.2 0.34 1.00
c-1,3-Dichloropropene ND 5.2 0.26 1.00
t-1,3-Dichloropropene ND 5.2 0.62 1.00
Ethylbenzene ND 5.2 0.16 1.00
2-Hexanone ND 52 1.8 1.00
Isopropylbenzene ND 5.2 0.56 1.00
p-Isopropyltoluene 2.3 5.2 0.65 1.00 J
Methylene Chloride ND 52 1.4 1.00
4-Methyl-2-Pentanone ND 52 4.5 1.00
Naphthalene ND 52 0.84 1.00
n-Propylbenzene ND 5.2 0.52 1.00
Styrene ND 5.2 0.62 1.00
1,1,1,2-Tetrachloroethane ND 5.2 0.25 1.00
1,1,2,2-Tetrachloroethane ND 5.2 0.36 1.00
Tetrachloroethene ND 5.2 0.22 1.00
Toluene ND 5.2 0.53 1.00
1,2,3-Trichlorobenzene ND 10 0.94 1.00
1,2,4-Trichlorobenzene ND 5.2 0.32 1.00
1,1,1-Trichloroethane ND 5.2 0.23 1.00
1,1,2-Trichloroethane ND 5.2 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 52 0.36 1.00
Trichloroethene ND 5.2 0.31 1.00
1,2,3-Trichloropropane ND 5.2 0.86 1.00
1,2,4-Trimethylbenzene ND 5.2 0.60 1.00
Trichlorofluoromethane ND 52 0.39 1.00
1,3,5-Trimethylbenzene ND 5.2 0.57 1.00
Vinyl Acetate ND 52 4.9 1.00
Vinyl Chloride ND 5.2 0.52 1.00
p/m-Xylene ND 5.2 0.28 1.00
o-Xylene ND 5.2 0.57 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.2 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 96 60-132
Dibromofluoromethane 105 63-141
1,2-Dichloroethane-d4 111 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-20-03 16-06-2030-2-A 06/28/16
09:49
Solid GC/MS Q 06/29/16 06/30/16
11:39
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.3 1.00
Benzene ND 5.1 0.13 1.00
Bromobenzene ND 5.1 0.21 1.00
Bromochloromethane ND 5.1 0.70 1.00
Bromodichloromethane ND 5.1 0.24 1.00
Bromoform ND 5.1 0.81 1.00
Bromomethane ND 25 9.6 1.00
2-Butanone ND 51 3.8 1.00
n-Butylbenzene ND 5.1 0.16 1.00
sec-Butylbenzene ND 5.1 0.59 1.00
tert-Butylbenzene ND 5.1 0.15 1.00
Carbon Disulfide ND 51 0.31 1.00
Carbon Tetrachloride ND 5.1 0.29 1.00
Chlorobenzene ND 5.1 0.23 1.00
Chloroethane ND 5.1 1.5 1.00
Chloroform ND 5.1 0.24 1.00
Chloromethane ND 25 0.31 1.00
2-Chlorotoluene ND 5.1 0.23 1.00
4-Chlorotoluene ND 5.1 0.22 1.00
Dibromochloromethane ND 5.1 0.58 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.1 0.26 1.00
Dibromomethane ND 5.1 0.79 1.00
1,2-Dichlorobenzene ND 5.1 0.23 1.00
1,3-Dichlorobenzene ND 5.1 0.18 1.00
1,4-Dichlorobenzene ND 5.1 0.23 1.00
Dichlorodifluoromethane ND 5.1 0.45 1.00
1,1-Dichloroethane ND 5.1 0.21 1.00
1,2-Dichloroethane ND 5.1 0.32 1.00
1,1-Dichloroethene ND 5.1 0.35 1.00
c-1,2-Dichloroethene ND 5.1 0.28 1.00
t-1,2-Dichloroethene ND 5.1 0.51 1.00
1,2-Dichloropropane ND 5.1 0.44 1.00
1,3-Dichloropropane ND 5.1 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.1 0.34 1.00
1,1-Dichloropropene ND 5.1 0.33 1.00
c-1,3-Dichloropropene ND 5.1 0.26 1.00
t-1,3-Dichloropropene ND 5.1 0.61 1.00
Ethylbenzene ND 5.1 0.15 1.00
2-Hexanone ND 51 1.8 1.00
Isopropylbenzene ND 5.1 0.55 1.00
p-Isopropyltoluene ND 5.1 0.64 1.00
Methylene Chloride ND 51 1.4 1.00
4-Methyl-2-Pentanone ND 51 4.4 1.00
Naphthalene ND 51 0.83 1.00
n-Propylbenzene ND 5.1 0.51 1.00
Styrene ND 5.1 0.61 1.00
1,1,1,2-Tetrachloroethane ND 5.1 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.1 0.35 1.00
Tetrachloroethene ND 5.1 0.21 1.00
Toluene ND 5.1 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.93 1.00
1,2,4-Trichlorobenzene ND 5.1 0.31 1.00
1,1,1-Trichloroethane ND 5.1 0.23 1.00
1,1,2-Trichloroethane ND 5.1 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 51 0.36 1.00
Trichloroethene ND 5.1 0.30 1.00
1,2,3-Trichloropropane ND 5.1 0.84 1.00
1,2,4-Trimethylbenzene ND 5.1 0.59 1.00
Trichlorofluoromethane ND 51 0.38 1.00
1,3,5-Trimethylbenzene ND 5.1 0.56 1.00
Vinyl Acetate ND 51 4.8 1.00
Vinyl Chloride ND 5.1 0.51 1.00
p/m-Xylene ND 5.1 0.27 1.00
o-Xylene ND 5.1 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.1 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 96 60-132
Dibromofluoromethane 89 63-141
1,2-Dichloroethane-d4 95 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 4 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-21-01 16-06-2030-4-A 06/28/16
10:24
Solid GC/MS Q 06/29/16 06/30/16
15:59
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone 76 130 6.3 1.00 J
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.80 1.00
Bromomethane ND 25 9.5 1.00
2-Butanone 22 50 3.8 1.00 J
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.23 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.31 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.78 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.45 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.32 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 5 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.26 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene 29 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.82 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.61 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.92 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.84 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.8 1.00
Vinyl Chloride ND 5.0 0.51 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 97 60-132
Dibromofluoromethane 103 63-141
1,2-Dichloroethane-d4 109 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 6 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-21-03 16-06-2030-5-A 06/28/16
10:26
Solid GC/MS Q 06/29/16 06/30/16
16:26
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 4.9 0.13 1.00
Bromobenzene ND 4.9 0.21 1.00
Bromochloromethane ND 4.9 0.68 1.00
Bromodichloromethane ND 4.9 0.23 1.00
Bromoform ND 4.9 0.78 1.00
Bromomethane ND 25 9.3 1.00
2-Butanone ND 49 3.7 1.00
n-Butylbenzene ND 4.9 0.15 1.00
sec-Butylbenzene ND 4.9 0.57 1.00
tert-Butylbenzene ND 4.9 0.15 1.00
Carbon Disulfide ND 49 0.30 1.00
Carbon Tetrachloride ND 4.9 0.28 1.00
Chlorobenzene ND 4.9 0.22 1.00
Chloroethane ND 4.9 1.5 1.00
Chloroform ND 4.9 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 4.9 0.23 1.00
4-Chlorotoluene ND 4.9 0.21 1.00
Dibromochloromethane ND 4.9 0.56 1.00
1,2-Dibromo-3-Chloropropane ND 9.9 1.7 1.00
1,2-Dibromoethane ND 4.9 0.25 1.00
Dibromomethane ND 4.9 0.76 1.00
1,2-Dichlorobenzene ND 4.9 0.23 1.00
1,3-Dichlorobenzene ND 4.9 0.17 1.00
1,4-Dichlorobenzene ND 4.9 0.22 1.00
Dichlorodifluoromethane ND 4.9 0.44 1.00
1,1-Dichloroethane ND 4.9 0.21 1.00
1,2-Dichloroethane ND 4.9 0.31 1.00
1,1-Dichloroethene ND 4.9 0.34 1.00
c-1,2-Dichloroethene ND 4.9 0.28 1.00
t-1,2-Dichloroethene ND 4.9 0.50 1.00
1,2-Dichloropropane ND 4.9 0.43 1.00
1,3-Dichloropropane ND 4.9 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 7 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 4.9 0.33 1.00
1,1-Dichloropropene ND 4.9 0.32 1.00
c-1,3-Dichloropropene ND 4.9 0.25 1.00
t-1,3-Dichloropropene ND 4.9 0.60 1.00
Ethylbenzene ND 4.9 0.15 1.00
2-Hexanone ND 49 1.7 1.00
Isopropylbenzene ND 4.9 0.54 1.00
p-Isopropyltoluene 0.73 4.9 0.62 1.00 J
Methylene Chloride ND 49 1.3 1.00
4-Methyl-2-Pentanone ND 49 4.3 1.00
Naphthalene ND 49 0.80 1.00
n-Propylbenzene ND 4.9 0.49 1.00
Styrene ND 4.9 0.60 1.00
1,1,1,2-Tetrachloroethane ND 4.9 0.24 1.00
1,1,2,2-Tetrachloroethane ND 4.9 0.34 1.00
Tetrachloroethene ND 4.9 0.21 1.00
Toluene ND 4.9 0.51 1.00
1,2,3-Trichlorobenzene ND 9.9 0.90 1.00
1,2,4-Trichlorobenzene ND 4.9 0.31 1.00
1,1,1-Trichloroethane ND 4.9 0.22 1.00
1,1,2-Trichloroethane ND 4.9 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 49 0.35 1.00
Trichloroethene ND 4.9 0.30 1.00
1,2,3-Trichloropropane ND 4.9 0.82 1.00
1,2,4-Trimethylbenzene ND 4.9 0.58 1.00
Trichlorofluoromethane ND 49 0.37 1.00
1,3,5-Trimethylbenzene ND 4.9 0.54 1.00
Vinyl Acetate ND 49 4.7 1.00
Vinyl Chloride ND 4.9 0.50 1.00
p/m-Xylene ND 4.9 0.26 1.00
o-Xylene ND 4.9 0.55 1.00
Methyl-t-Butyl Ether (MTBE) ND 4.9 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 99 60-132
Dibromofluoromethane 104 63-141
1,2-Dichloroethane-d4 107 62-146
Toluene-d8 100 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 8 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-22-01 16-06-2030-7-A 06/28/16
11:02
Solid GC/MS Q 06/29/16 06/30/16
16:52
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.3 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.80 1.00
Bromomethane ND 25 9.5 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.23 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.31 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.78 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.45 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.32 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 9 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.26 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.82 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.61 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.92 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.84 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.8 1.00
Vinyl Chloride ND 5.0 0.51 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 98 60-132
Dibromofluoromethane 103 63-141
1,2-Dichloroethane-d4 109 62-146
Toluene-d8 101 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 10 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-22-03 16-06-2030-8-A 06/28/16
11:04
Solid GC/MS Q 06/29/16 06/30/16
17:20
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.4 1.00
Benzene ND 5.1 0.13 1.00
Bromobenzene ND 5.1 0.22 1.00
Bromochloromethane ND 5.1 0.71 1.00
Bromodichloromethane ND 5.1 0.24 1.00
Bromoform ND 5.1 0.82 1.00
Bromomethane ND 26 9.7 1.00
2-Butanone ND 51 3.9 1.00
n-Butylbenzene ND 5.1 0.16 1.00
sec-Butylbenzene ND 5.1 0.59 1.00
tert-Butylbenzene ND 5.1 0.15 1.00
Carbon Disulfide ND 51 0.31 1.00
Carbon Tetrachloride ND 5.1 0.29 1.00
Chlorobenzene ND 5.1 0.23 1.00
Chloroethane ND 5.1 1.5 1.00
Chloroform ND 5.1 0.25 1.00
Chloromethane ND 26 0.31 1.00
2-Chlorotoluene ND 5.1 0.24 1.00
4-Chlorotoluene ND 5.1 0.22 1.00
Dibromochloromethane ND 5.1 0.59 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.1 0.26 1.00
Dibromomethane ND 5.1 0.80 1.00
1,2-Dichlorobenzene ND 5.1 0.23 1.00
1,3-Dichlorobenzene ND 5.1 0.18 1.00
1,4-Dichlorobenzene ND 5.1 0.23 1.00
Dichlorodifluoromethane ND 5.1 0.46 1.00
1,1-Dichloroethane ND 5.1 0.22 1.00
1,2-Dichloroethane ND 5.1 0.32 1.00
1,1-Dichloroethene ND 5.1 0.36 1.00
c-1,2-Dichloroethene ND 5.1 0.29 1.00
t-1,2-Dichloroethene ND 5.1 0.52 1.00
1,2-Dichloropropane ND 5.1 0.45 1.00
1,3-Dichloropropane ND 5.1 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 11 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.1 0.34 1.00
1,1-Dichloropropene ND 5.1 0.34 1.00
c-1,3-Dichloropropene ND 5.1 0.26 1.00
t-1,3-Dichloropropene ND 5.1 0.62 1.00
Ethylbenzene ND 5.1 0.16 1.00
2-Hexanone ND 51 1.8 1.00
Isopropylbenzene ND 5.1 0.56 1.00
p-Isopropyltoluene ND 5.1 0.65 1.00
Methylene Chloride ND 51 1.4 1.00
4-Methyl-2-Pentanone ND 51 4.4 1.00
Naphthalene ND 51 0.84 1.00
n-Propylbenzene ND 5.1 0.52 1.00
Styrene ND 5.1 0.62 1.00
1,1,1,2-Tetrachloroethane ND 5.1 0.25 1.00
1,1,2,2-Tetrachloroethane ND 5.1 0.35 1.00
Tetrachloroethene ND 5.1 0.22 1.00
Toluene ND 5.1 0.53 1.00
1,2,3-Trichlorobenzene ND 10 0.94 1.00
1,2,4-Trichlorobenzene ND 5.1 0.32 1.00
1,1,1-Trichloroethane ND 5.1 0.23 1.00
1,1,2-Trichloroethane ND 5.1 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 51 0.36 1.00
Trichloroethene ND 5.1 0.31 1.00
1,2,3-Trichloropropane ND 5.1 0.85 1.00
1,2,4-Trimethylbenzene ND 5.1 0.60 1.00
Trichlorofluoromethane ND 51 0.39 1.00
1,3,5-Trimethylbenzene ND 5.1 0.56 1.00
Vinyl Acetate ND 51 4.9 1.00
Vinyl Chloride ND 5.1 0.52 1.00
p/m-Xylene ND 5.1 0.28 1.00
o-Xylene ND 5.1 0.57 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.1 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 99 60-132
Dibromofluoromethane 103 63-141
1,2-Dichloroethane-d4 108 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 12 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
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Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-14-314-572 N/A Solid GC/MS Q 06/30/16 06/30/16 10:44
160630L012
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 13 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 99 60-132
Dibromofluoromethane 102 63-141
1,2-Dichloroethane-d4 105 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 14 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-1 Sample Concrete HPLC 5 07/01/16 07/05/16 19:12 160701S20 16-06-2029-1 Matrix Spike Concrete HPLC 5 07/01/16 07/05/16 18:07 160701S20 16-06-2029-1 Matrix Spike Duplicate Concrete HPLC 5 07/01/16 07/05/16 18:39 160701S20 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Naphthalene ND 100.0 134.6 135 102.9 103 23-167 27 0-46 Acenaphthylene ND 100.0 99.86 100 72.12 72 24-120 32 0-47 Acenaphthene ND 100.0 90.56 91 68.34 68 16-120 28 0-46
Fluorene ND 100.0 88.52 89 67.67 68 32-120 27 0-44
Phenanthrene ND 100.0 90.89 91 74.43 74 34-120 20 0-38
Anthracene ND 100.0 89.23 89 72.31 72 27-120 21 0-45
Fluoranthene ND 100.0 93.43 93 78.84 79 32-122 17 0-41
Pyrene ND 100.0 102.6 103 85.26 85 31-127 18 0-38
Benzo (a) Anthracene ND 100.0 94.88 95 79.10 79 32-122 18 0-43 Chrysene ND 100.0 91.29 91 75.53 76 30-132 19 0-42
Benzo (b) Fluoranthene ND 100.0 90.36 90 74.88 75 33-120 19 0-44 Benzo (k) Fluoranthene ND 100.0 77.89 78 67.53 68 23-149 14 0-44 Benzo (a) Pyrene ND 100.0 91.67 92 76.13 76 12-132 19 0-48 Dibenz (a,h) Anthracene ND 100.0 87.35 87 72.61 73 29-125 18 0-43 Benzo (g,h,i) Perylene ND 100.0 93.45 93 75.22 75 24-132 22 0-42 Indeno (1,2,3-c,d) Pyrene ND 100.0 92.03 92 75.21 75 29-143 20 0-42 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8310
Project: UTAS - Due Diligence / 43559 Page 1 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2032-8 Sample Solid GC 49 06/30/16 06/30/16 17:31 160630S05 16-06-2032-8 Matrix Spike Solid GC 49 06/30/16 06/30/16 16:21 160630S05 16-06-2032-8 Matrix Spike Duplicate Solid GC 49 06/30/16 06/30/16 16:38 160630S05 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
TPH as Diesel ND 400.0 313.7 78 331.1 83 64-130 5 0-15
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3550B
Method: EPA 8015B (M)
Project: UTAS - Due Diligence / 43559 Page 2 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-1 Sample Concrete ICP 7300 07/02/16 07/05/16 15:34 160702S01 16-06-2029-1 Matrix Spike Concrete ICP 7300 07/02/16 07/05/16 15:35 160702S01 16-06-2029-1 Matrix Spike Duplicate Concrete ICP 7300 07/02/16 07/05/16 15:36 160702S01 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Antimony ND 25.00 3.093 12 4.345 17 50-115 34 0-20 3,4
Arsenic 9.119 25.00 38.33 117 36.34 109 75-125 5 0-20
Barium 151.1 25.00 173.0 4X 173.5 4X 75-125 4X 0-20 Q
Beryllium 0.2746 25.00 27.12 107 28.10 111 75-125 4 0-20 Cadmium ND 25.00 24.61 98 25.29 101 75-125 3 0-20
Chromium 23.99 25.00 50.31 105 51.05 108 75-125 1 0-20
Cobalt 3.240 25.00 27.48 97 28.27 100 75-125 3 0-20
Copper 17.64 25.00 43.27 103 43.61 104 75-125 1 0-20
Lead 1.316 25.00 26.35 100 26.93 102 75-125 2 0-20
Molybdenum 1.885 25.00 27.03 101 27.73 103 75-125 3 0-20 Nickel 5.520 25.00 30.61 100 30.90 102 75-125 1 0-20
Selenium 1.199 25.00 25.62 98 29.12 112 75-125 13 0-20
Silver 0.3734 12.50 13.95 109 14.41 112 75-125 3 0-20
Thallium ND 25.00 14.42 58 16.15 65 75-125 11 0-20 3
Vanadium 18.77 25.00 43.06 97 42.71 96 75-125 1 0-20
Zinc 40.54 25.00 66.09 102 68.68 113 75-125 4 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 3 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-1 Sample Concrete Mercury 05 07/06/16 07/06/16 15:32 160706S02 16-06-2029-1 Matrix Spike Concrete Mercury 05 07/06/16 07/06/16 15:34 160706S02 16-06-2029-1 Matrix Spike Duplicate Concrete Mercury 05 07/06/16 07/06/16 15:36 160706S02 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Mercury ND 0.8350 1.007 121 0.9381 112 75-125 7 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559 Page 4 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2036-1 Sample Solid GC 41 07/05/16 07/08/16 12:16 160705S04 16-06-2036-1 Matrix Spike Solid GC 41 07/05/16 07/08/16 11:46 160705S04 16-06-2036-1 Matrix Spike Duplicate Solid GC 41 07/05/16 07/08/16 12:01 160705S04 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Aldrin ND 25.00 22.96 92 21.95 88 50-135 5 0-25
Alpha-BHC ND 25.00 22.33 89 21.77 87 50-135 3 0-25
Beta-BHC ND 25.00 23.32 93 21.50 86 50-135 8 0-25
4,4'-DDD ND 25.00 26.29 105 25.09 100 50-135 5 0-25
4,4'-DDE ND 25.00 25.85 103 24.52 98 50-135 5 0-25
4,4'-DDT ND 25.00 25.24 101 24.05 96 50-135 5 0-25
Delta-BHC ND 25.00 25.22 101 23.53 94 50-135 7 0-25
Dieldrin ND 25.00 25.48 102 23.80 95 50-135 7 0-25
Endosulfan I ND 25.00 24.07 96 22.98 92 50-135 5 0-25
Endosulfan II ND 25.00 26.14 105 24.52 98 50-135 6 0-25 Endosulfan Sulfate ND 25.00 24.08 96 22.94 92 50-135 5 0-25 Endrin ND 25.00 29.00 116 27.75 111 50-135 4 0-25
Endrin Aldehyde ND 25.00 23.39 94 22.68 91 50-135 3 0-25 Gamma-BHC ND 25.00 23.44 94 22.65 91 50-135 3 0-25
Heptachlor ND 25.00 24.03 96 23.35 93 50-135 3 0-25
Heptachlor Epoxide ND 25.00 23.96 96 22.95 92 50-135 4 0-25 Methoxychlor ND 25.00 25.40 102 25.27 101 50-135 1 0-25 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8081A
Project: UTAS - Due Diligence / 43559 Page 5 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-2 Sample Solid GC 58 07/05/16 07/07/16 15:37 160705S08 16-06-2029-2 Matrix Spike Solid GC 58 07/05/16 07/07/16 14:07 160705S08 16-06-2029-2 Matrix Spike Duplicate Solid GC 58 07/05/16 07/07/16 14:25 160705S08 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Aroclor-1016 ND 100.0 91.50 92 77.00 77 50-135 17 0-20
Aroclor-1260 ND 100.0 98.00 98 83.50 84 50-135 16 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8082
Project: UTAS - Due Diligence / 43559 Page 6 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number BB-20-03 Sample Solid GC/MS Q 06/29/16 06/30/16 11:39 160630S005 BB-20-03 Matrix Spike Solid GC/MS Q 06/29/16 06/30/16 12:05 160630S005 BB-20-03 Matrix Spike Duplicate Solid GC/MS Q 06/29/16 06/30/16 12:32 160630S005 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acetone ND 50.00 46.07 92 45.06 90 70-130 2 0-20
Benzene ND 50.00 43.79 88 43.11 86 61-127 2 0-20
Bromobenzene ND 50.00 43.55 87 42.37 85 70-130 3 0-20
Bromochloromethane ND 50.00 45.56 91 44.48 89 70-130 2 0-20 Bromodichloromethane ND 50.00 44.65 89 43.85 88 70-130 2 0-20 Bromoform ND 50.00 41.54 83 41.21 82 70-130 1 0-20
Bromomethane ND 50.00 40.32 81 41.49 83 70-130 3 0-20
2-Butanone ND 50.00 39.82 80 40.47 81 70-130 2 0-20
n-Butylbenzene ND 50.00 44.49 89 44.87 90 77-123 1 0-25 sec-Butylbenzene ND 50.00 45.16 90 45.76 92 70-130 1 0-20 tert-Butylbenzene ND 50.00 45.46 91 46.06 92 70-130 1 0-20 Carbon Disulfide ND 50.00 45.45 91 44.71 89 70-130 2 0-20 Carbon Tetrachloride ND 50.00 45.64 91 46.21 92 51-135 1 0-29 Chlorobenzene ND 50.00 43.49 87 42.72 85 57-123 2 0-20
Chloroethane ND 50.00 48.76 98 46.41 93 70-130 5 0-20
Chloroform ND 50.00 43.88 88 43.44 87 70-130 1 0-20
Chloromethane ND 50.00 48.92 98 46.80 94 70-130 4 0-20
2-Chlorotoluene ND 50.00 43.35 87 42.92 86 70-130 1 0-20 4-Chlorotoluene ND 50.00 44.95 90 43.52 87 70-130 3 0-20 Dibromochloromethane ND 50.00 42.82 86 41.95 84 70-130 2 0-20 1,2-Dibromo-3-Chloropropane ND 50.00 39.84 80 41.46 83 70-130 4 0-20 1,2-Dibromoethane ND 50.00 44.98 90 44.49 89 64-124 1 0-20 Dibromomethane ND 50.00 44.90 90 43.44 87 70-130 3 0-20 1,2-Dichlorobenzene ND 50.00 42.49 85 42.51 85 35-131 0 0-25 1,3-Dichlorobenzene ND 50.00 42.60 85 42.54 85 70-130 0 0-20 1,4-Dichlorobenzene ND 50.00 41.71 83 41.75 83 70-130 0 0-20 Dichlorodifluoromethane ND 50.00 57.87 116 53.98 108 70-130 7 0-20 1,1-Dichloroethane ND 50.00 44.76 90 44.40 89 70-130 1 0-20 1,2-Dichloroethane ND 50.00 42.58 85 41.64 83 70-130 2 0-20 1,1-Dichloroethene ND 50.00 45.74 91 45.58 91 47-143 0 0-25 c-1,2-Dichloroethene ND 50.00 43.79 88 42.76 86 70-130 2 0-20 t-1,2-Dichloroethene ND 50.00 46.14 92 45.58 91 70-130 1 0-20 1,2-Dichloropropane ND 50.00 44.71 89 43.60 87 79-115 3 0-25 1,3-Dichloropropane ND 50.00 43.99 88 42.62 85 70-130 3 0-20 2,2-Dichloropropane ND 50.00 46.80 94 46.73 93 70-130 0 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 7 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
1,1-Dichloropropene ND 50.00 46.27 93 46.60 93 70-130 1 0-20 c-1,3-Dichloropropene ND 50.00 44.38 89 43.62 87 70-130 2 0-20 t-1,3-Dichloropropene ND 50.00 46.90 94 45.36 91 70-130 3 0-20 Ethylbenzene ND 50.00 45.05 90 44.38 89 57-129 1 0-22
2-Hexanone ND 50.00 39.83 80 38.80 78 70-130 3 0-20
Isopropylbenzene ND 50.00 45.49 91 44.91 90 70-130 1 0-20 p-Isopropyltoluene ND 50.00 45.51 91 45.81 92 70-130 1 0-20 Methylene Chloride ND 50.00 43.55 87 42.56 85 70-130 2 0-20 4-Methyl-2-Pentanone ND 50.00 40.14 80 40.34 81 70-130 1 0-20 Naphthalene ND 50.00 39.34 79 42.02 84 70-130 7 0-20
n-Propylbenzene ND 50.00 44.80 90 44.27 89 70-130 1 0-20 Styrene ND 50.00 44.98 90 44.22 88 70-130 2 0-20
1,1,1,2-Tetrachloroethane ND 50.00 46.05 92 44.94 90 70-130 2 0-20 1,1,2,2-Tetrachloroethane ND 50.00 42.69 85 42.74 85 70-130 0 0-20 Tetrachloroethene ND 50.00 44.82 90 44.18 88 70-130 1 0-20 Toluene ND 50.00 44.90 90 44.10 88 63-123 2 0-20
1,2,3-Trichlorobenzene ND 50.00 38.59 77 41.43 83 70-130 7 0-20 1,2,4-Trichlorobenzene ND 50.00 40.72 81 42.35 85 70-130 4 0-20 1,1,1-Trichloroethane ND 50.00 45.51 91 45.66 91 70-130 0 0-20 1,1,2-Trichloroethane ND 50.00 43.82 88 42.84 86 70-130 2 0-20 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50.00 47.36 95 46.90 94 70-130 1 0-20 Trichloroethene ND 50.00 45.57 91 44.36 89 44-158 3 0-20 1,2,3-Trichloropropane ND 50.00 43.25 86 42.39 85 70-130 2 0-20 1,2,4-Trimethylbenzene ND 50.00 43.55 87 43.83 88 70-130 1 0-20 Trichlorofluoromethane ND 50.00 51.15 102 47.96 96 70-130 6 0-20 1,3,5-Trimethylbenzene ND 50.00 44.88 90 43.83 88 70-130 2 0-20 Vinyl Acetate ND 50.00 12.64 25 10.59 21 70-130 18 0-20 3 Vinyl Chloride ND 50.00 54.79 110 51.17 102 49-139 7 0-47 p/m-Xylene ND 100.0 88.44 88 86.46 86 70-130 2 0-20
o-Xylene ND 50.00 44.99 90 44.33 89 70-130 1 0-20
Methyl-t-Butyl Ether (MTBE) ND 50.00 42.23 84 42.05 84 57-123 0 0-21 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 8 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
16-06-2029-1 Sample Concrete ICP 7300 07/02/16 00:00 07/05/16 15:34 160702S01 16-06-2029-1 PDS Concrete ICP 7300 07/02/16 00:00 07/05/16 15:37 160702S01 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Antimony ND 25.00 21.99 88 75-125
Arsenic 9.119 25.00 36.10 108 75-125
Barium 151.1 25.00 177.5 4X 75-125 Q
Beryllium 0.2746 25.00 26.81 106 75-125
Cadmium ND 25.00 23.90 96 75-125
Chromium 23.99 25.00 49.40 102 75-125
Cobalt 3.240 25.00 26.73 94 75-125
Copper 17.64 25.00 43.28 103 75-125
Lead 1.316 25.00 25.59 97 75-125
Molybdenum 1.885 25.00 26.84 100 75-125
Nickel 5.520 25.00 30.14 98 75-125
Selenium 1.199 25.00 28.36 109 75-125
Silver 0.3734 12.50 13.79 107 75-125
Thallium ND 25.00 23.80 95 75-125
Vanadium 18.77 25.00 44.17 102 75-125
Zinc 40.54 25.00 64.98 98 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 1 of2
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
16-06-2029-1 Sample Concrete Mercury 05 07/06/16 00:00 07/06/16 15:32 160706S02 16-06-2029-1 PDS Concrete Mercury 05 07/06/16 00:00 07/07/16 11:39 160706S02 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Mercury ND 0.8350 0.8524 102 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559 Page 2 of2
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Duplicate Batch Number 16-06-2036-1 Sample Solid N/A 06/29/16 00:00 06/29/16 22:00 G0629MOID6 16-06-2036-1 Sample Duplicate Solid N/A 06/29/16 00:00 06/29/16 22:00 G0629MOID6 Parameter Sample Conc. DUP Conc. RPD RPD CL Qualifiers
Moisture 15.10 15.60 3 0-10
Quality Control - Sample Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: N/A
Method: ASTM D-2216 (M)
Project: UTAS - Due Diligence / 43559 Page 1 of1
RPD: Relative Percent Difference. CL: Control Limits
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Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-07-002-1878 LCS Solid HPLC 5 07/01/16 07/05/16 16:29 160701L20 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Naphthalene 100.0 126.0 126 17-203 0-234
Acenaphthylene 100.0 93.14 93 50-120 38-132
Acenaphthene 100.0 85.65 86 41-120 28-133
Fluorene 100.0 86.18 86 51-120 40-132
Phenanthrene 100.0 89.37 89 56-120 45-131
Anthracene 100.0 86.48 86 49-120 37-132
Fluoranthene 100.0 92.03 92 60-120 50-130
Pyrene 100.0 100.4 100 61-121 51-131
Benzo (a) Anthracene 100.0 95.36 95 61-121 51-131
Chrysene 100.0 91.95 92 61-121 51-131
Benzo (b) Fluoranthene 100.0 90.44 90 61-121 51-131
Benzo (k) Fluoranthene 100.0 85.03 85 57-129 45-141
Benzo (a) Pyrene 100.0 92.84 93 43-120 30-133
Dibenz (a,h) Anthracene 100.0 87.86 88 59-125 48-136
Benzo (g,h,i) Perylene 100.0 95.04 95 57-123 46-134
Indeno (1,2,3-c,d) Pyrene 100.0 91.46 91 64-130 53-141
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8310
Project: UTAS - Due Diligence / 43559 Page 1 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-15-490-2144 LCS Solid GC 49 06/30/16 06/30/16 16:03 160630B05 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers TPH as Diesel 400.0 307.6 77 75-123
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3550B
Method: EPA 8015B (M)
Project: UTAS - Due Diligence / 43559 Page 2 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 097-01-002-22889 LCS Solid ICP 7300 07/02/16 07/05/16 13:22 160702L01U Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Antimony 25.00 24.74 99 80-120 73-127
Arsenic 25.00 24.49 98 80-120 73-127
Barium 25.00 26.41 106 80-120 73-127
Beryllium 25.00 24.22 97 80-120 73-127
Cadmium 25.00 25.25 101 80-120 73-127
Chromium 25.00 25.70 103 80-120 73-127
Cobalt 25.00 26.45 106 80-120 73-127
Copper 25.00 25.58 102 80-120 73-127
Lead 25.00 26.36 105 80-120 73-127
Molybdenum 25.00 24.94 100 80-120 73-127
Nickel 25.00 26.86 107 80-120 73-127
Selenium 25.00 23.47 94 80-120 73-127
Silver 12.50 12.44 100 80-120 73-127
Thallium 25.00 26.17 105 80-120 73-127
Vanadium 25.00 24.31 97 80-120 73-127
Zinc 25.00 26.06 104 80-120 73-127
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 3 of8
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-480-44 LCS Solid Mercury 05 07/06/16 07/06/16 15:29 160706L02 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers Mercury 0.8350 0.9333 112 80-120
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559 Page 4 of8
RPD: Relative Percent Difference. CL: Control Limits
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Total number of LCS compounds: 17
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-12-537-2463 LCS Solid GC 41 07/05/16 07/08/16 13:31 160705L04 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Aldrin 25.00 21.00 84 50-135 36-149
Alpha-BHC 25.00 20.87 83 50-135 36-149
Beta-BHC 25.00 21.05 84 50-135 36-149
4,4'-DDD 25.00 26.47 106 50-135 36-149
4,4'-DDE 25.00 23.99 96 50-135 36-149
4,4'-DDT 25.00 26.34 105 50-135 36-149
Delta-BHC 25.00 23.55 94 50-135 36-149
Dieldrin 25.00 23.98 96 50-135 36-149
Endosulfan I 25.00 22.01 88 50-135 36-149
Endosulfan II 25.00 27.68 111 50-135 36-149
Endosulfan Sulfate 25.00 27.28 109 50-135 36-149
Endrin 25.00 26.76 107 50-135 36-149
Endrin Aldehyde 25.00 25.67 103 50-135 36-149
Gamma-BHC 25.00 21.41 86 50-135 36-149
Heptachlor 25.00 22.91 92 50-135 36-149
Heptachlor Epoxide 25.00 22.78 91 50-135 36-149
Methoxychlor 25.00 30.50 122 50-135 36-149
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8081A
Project: UTAS - Due Diligence / 43559 Page 5 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-12-535-3813 LCS Solid GC 58 07/05/16 07/07/16 13:49 160705L08 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers Aroclor-1016 100.0 99.00 99 50-135
Aroclor-1260 100.0 91.00 91 50-135
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 3545
Method: EPA 8082
Project: UTAS - Due Diligence / 43559 Page 6 of8
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-14-314-572 LCS Solid GC/MS Q 06/30/16 06/30/16 09:36 160630L012 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Acetone 50.00 46.68 93 70-130 60-140
Benzene 50.00 43.57 87 78-120 71-127
Bromobenzene 50.00 45.63 91 70-130 60-140
Bromochloromethane 50.00 41.68 83 70-130 60-140
Bromodichloromethane 50.00 43.92 88 70-130 60-140
Bromoform 50.00 45.72 91 70-130 60-140
Bromomethane 50.00 36.36 73 70-130 60-140
2-Butanone 50.00 43.62 87 70-130 60-140
n-Butylbenzene 50.00 46.58 93 77-123 69-131
sec-Butylbenzene 50.00 47.24 94 70-130 60-140
tert-Butylbenzene 50.00 48.31 97 70-130 60-140
Carbon Disulfide 50.00 42.41 85 70-130 60-140
Carbon Tetrachloride 50.00 44.70 89 49-139 34-154
Chlorobenzene 50.00 44.36 89 79-120 72-127
Chloroethane 50.00 43.74 87 70-130 60-140
Chloroform 50.00 40.98 82 70-130 60-140
Chloromethane 50.00 44.11 88 70-130 60-140
2-Chlorotoluene 50.00 45.36 91 70-130 60-140
4-Chlorotoluene 50.00 45.93 92 70-130 60-140
Dibromochloromethane 50.00 43.90 88 70-130 60-140
1,2-Dibromo-3-Chloropropane 50.00 48.29 97 70-130 60-140 1,2-Dibromoethane 50.00 45.92 92 70-130 60-140
Dibromomethane 50.00 44.38 89 70-130 60-140
1,2-Dichlorobenzene 50.00 45.94 92 75-120 68-128
1,3-Dichlorobenzene 50.00 46.19 92 70-130 60-140
1,4-Dichlorobenzene 50.00 44.71 89 70-130 60-140
Dichlorodifluoromethane 50.00 52.20 104 70-130 60-140
1,1-Dichloroethane 50.00 42.29 85 70-130 60-140
1,2-Dichloroethane 50.00 42.22 84 70-130 60-140
1,1-Dichloroethene 50.00 42.84 86 74-122 66-130
c-1,2-Dichloroethene 50.00 41.40 83 70-130 60-140
t-1,2-Dichloroethene 50.00 43.98 88 70-130 60-140
1,2-Dichloropropane 50.00 45.86 92 79-115 73-121
1,3-Dichloropropane 50.00 44.25 89 70-130 60-140
2,2-Dichloropropane 50.00 45.53 91 70-130 60-140
1,1-Dichloropropene 50.00 44.80 90 70-130 60-140
c-1,3-Dichloropropene 50.00 47.00 94 70-130 60-140
t-1,3-Dichloropropene 50.00 48.49 97 70-130 60-140
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 7 of8
RPD: Relative Percent Difference. CL: Control Limits
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Total number of LCS compounds: 66
Total number of ME compounds: 0
Total number of ME compounds allowed: 3
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Ethylbenzene 50.00 46.04 92 76-120 69-127
2-Hexanone 50.00 49.98 100 70-130 60-140
Isopropylbenzene 50.00 46.87 94 70-130 60-140
p-Isopropyltoluene 50.00 47.96 96 70-130 60-140
Methylene Chloride 50.00 41.03 82 70-130 60-140
4-Methyl-2-Pentanone 50.00 48.06 96 70-130 60-140
Naphthalene 50.00 45.72 91 70-130 60-140
n-Propylbenzene 50.00 46.28 93 70-130 60-140
Styrene 50.00 46.45 93 70-130 60-140
1,1,1,2-Tetrachloroethane 50.00 48.28 97 70-130 60-140
1,1,2,2-Tetrachloroethane 50.00 45.68 91 70-130 60-140
Tetrachloroethene 50.00 44.27 89 70-130 60-140
Toluene 50.00 46.17 92 77-120 70-127
1,2,3-Trichlorobenzene 50.00 46.05 92 70-130 60-140
1,2,4-Trichlorobenzene 50.00 49.48 99 70-130 60-140
1,1,1-Trichloroethane 50.00 43.27 87 70-130 60-140
1,1,2-Trichloroethane 50.00 44.40 89 70-130 60-140
1,1,2-Trichloro-1,2,2-Trifluoroethane 50.00 44.44 89 70-130 60-140 Trichloroethene 50.00 45.56 91 70-130 60-140
1,2,3-Trichloropropane 50.00 47.38 95 70-130 60-140
1,2,4-Trimethylbenzene 50.00 46.20 92 70-130 60-140
Trichlorofluoromethane 50.00 45.22 90 70-130 60-140
1,3,5-Trimethylbenzene 50.00 47.41 95 70-130 60-140
Vinyl Acetate 50.00 39.26 79 70-130 60-140
Vinyl Chloride 50.00 47.91 96 68-122 59-131
p/m-Xylene 100.0 92.01 92 70-130 60-140
o-Xylene 50.00 47.30 95 70-130 60-140
Methyl-t-Butyl Ether (MTBE) 50.00 44.45 89 77-120 70-127 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2030
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 8 of8
RPD: Relative Percent Difference. CL: Control Limits
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Method Extraction Chemist ID Instrument Analytical Location ASTM D-2216 (M) N/A 1009 N/A 1
EPA 6010B EPA 3050B 935 ICP 7300 1
EPA 7471A EPA 7471A Total 868 Mercury 05 1
EPA 8015B (M) EPA 3550B 972 GC 49 1
EPA 8081A EPA 3545 669 GC 41 1
EPA 8082 EPA 3545 944 GC 58 1
EPA 8260B EPA 5030C 1055 GC/MS Q 2
EPA 8310 EPA 3545 960 HPLC 5 1
Sample Analysis Summary Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2030 Page 1 of1
Location 1: 7440 Lincoln Way, Garden Grove, CA 92841
Location 2: 7445 Lampson Avenue, Garden Grove, CA 92841 Return to Contents
Qualifiers Definition
* See applicable analysis comment.
< Less than the indicated value.
> Greater than the indicated value.
1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clarification.
2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clarification. 3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
4 The MS/MSD RPD was out of control due to suspected matrix interference. 5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference. 6 Surrogate recovery below the acceptance limit.
7 Surrogate recovery above the acceptance limit.
B Analyte was present in the associated method blank.
BU Sample analyzed after holding time expired.
BV Sample received after holding time expired.
CI See case narrative.
E Concentration exceeds the calibration range.
ET Sample was extracted past end of recommended max. holding time.
HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.
HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons were also present (or detected).
HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detected).
J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated.
JA Analyte positively identified but quantitation is an estimate.
ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
ND Parameter not detected at the indicated reporting limit.
Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater.
SG The sample extract was subjected to Silica Gel treatment prior to analysis.
X % Recovery and/or RPD out-of-range.
Z Analyte presence was not confirmed by second column or GC/MS analysis.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations.
Glossary of Terms and Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2030 Page 1 of1
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WORK ORDER NUMBER: 16-06-2031
Analytical Report For
Client: Haley & Aldrich, Inc,
Client Project Name: UTAS - Due Diligence / 43559
Attention: Robert K. Scott
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Approved for release on by:
Virendra Patel
Project Manager
AIR SOIL WATER MARINE CHEMISTRY
Eurofins Calscience, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached to this report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of this report is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Calscience is not responsible, legally or otherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise. 07/13/2016
Contents
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client Project Name: UTAS - Due Diligence / 43559
Work Order Number: 16-06-2031
1 Work Order Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2 Case Narrative 16-06-2031. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 3 Sample Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 4 Detections Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 5 Client Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
5.1 EPA 8310 Polynuclear Aromatic Hydrocarbons (Solid). . . . . . . . . . . . . . . . . . . . . . . 12
5.2 ASTM D-2216 (M) Moisture Content (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
5.3 EPA 8015B (M) C6-C44 (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
5.4 EPA 6010B/7471A CAC Title 22 Metals (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
5.5 EPA 6010B ICP Metals (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
5.6 EPA 7470A Mercury (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
5.7 EPA 7471A Mercury (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
5.8 EPA 8081A Organochlorine Pesticides (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
5.9 EPA 8082 PCB Aroclors (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
5.10 EPA 8260B Volatile Organics (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
5.11 EPA 8260B Volatile Organics (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48 6 Quality Control Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
6.1 MS/MSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
6.2 PDS/PDSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
6.3 Sample Duplicate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
6.4 LCS/LCSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80 7 Sample Analysis Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93 8 Glossary of Terms and Qualifiers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94 9 Chain-of-Custody/Sample Receipt Form. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
Condition Upon Receipt:
Samples were received under Chain-of-Custody (COC) on 06/28/16. They were assigned to Work Order 16-06-2031.
Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are integral elements of the analytical report and are presented at the back of the report.
Holding Times:
All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
Quality Control:
All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or described further within this report.
Subcontractor Information:
Unless otherwise noted below (or on the subcontract form), no samples were subcontracted.
Additional Comments:
Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from mass/sample basis to mass/volume basis using client-supplied air volumes.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are always reported on a wet weight basis.
Work Order Narrative
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2031 Page 1 of1
Return to Contents
CASE NARRATIVE
Eurofins Calscience Work Order 16-06-2031
EPA Method 6010B Total Metals:
Project Required Detection Limit (PRDL):
The PRDL’s were analyzed as required per the project QAPP. The low level calibration check performed post the sample batch is outside acceptable range for Silver, Selenium, Thallium and Zinc on 07/01/16.
The PRDL’s were analyzed as required per the project QAPP. The low level calibration check performed post the sample batch is outside acceptable range for Chromium, Antimony, Selenium, and Zinc on 07/05/16.
EPA Method 8260B Volatile Organics:
Table A: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160629S007 2-Chloro Vinyl Ether3
160630S002 Carbon Disulfide3, Dichlorodifluoromethane3, 1,2-Dichloropropane3and Vinyl Acetate3
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
Table B: Laboratory Control Sample (LCS) / LCS Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160629L007 Isobutyl AlcoholME
160630L003 Carbon DisulfideME, and DichlorodifluoromethaneME ME: LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
EPA Method 8310 PAHs:
Table C: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 8310
Batch # Analytes(s)
160702S06 Benzo (a) Anthracene3,4, Dibenz (a,h) Anthracence3and Indeno (1,2,3-c,d) Pyrene3
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control. 4: The MS/MSD RPD was out of control due to suspected matrix interference. 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Return to Contents
Sample Identification Lab Number Collection Date and Time Number of Containers
Matrix
BB-17-01 16-06-2031-1 06/28/16 09:52 1 Solid
BB-17-04 16-06-2031-2 06/28/16 09:54 1 Solid
BB-17-10 16-06-2031-3 06/28/16 09:56 1 Solid
BB-17-GW 16-06-2031-4 06/28/16 10:10 6 Aqueous
BB-18-01 16-06-2031-5 06/28/16 10:36 1 Solid
BB-18-04 16-06-2031-6 06/28/16 10:38 1 Solid
BB-18-10 16-06-2031-7 06/28/16 10:40 1 Solid
BB-19-01 16-06-2031-8 06/28/16 12:21 1 Solid
BB-19-03 16-06-2031-9 06/28/16 12:23 1 Solid
BB-19-10 16-06-2031-10 06/28/16 12:25 1 Solid
Sample Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
PO Number:
Date/Time
Received:
06/28/16 19:00
Number of
Containers:
15 Attn: Robert K. Scott
Return to Contents
BB-17-01 (16-06-2031-1)
Moisture 3.5 0.10 % ASTM D-2216 (M) N/A
Arsenic 3.25 0.754 mg/kg EPA 6010B EPA 3050B
Barium 72.6 0.503 mg/kg EPA 6010B EPA 3050B
Beryllium 0.239 J 0.138* mg/kg EPA 6010B EPA 3050B
Cadmium 0.407 J 0.136* mg/kg EPA 6010B EPA 3050B
Chromium 12.8 0.251 mg/kg EPA 6010B EPA 3050B
Cobalt 4.42 0.251 mg/kg EPA 6010B EPA 3050B
Copper 7.64 0.503 mg/kg EPA 6010B EPA 3050B
Lead 9.76 0.503 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.425 0.251 mg/kg EPA 6010B EPA 3050B
Nickel 5.91 0.251 mg/kg EPA 6010B EPA 3050B
Selenium 0.903 0.754 mg/kg EPA 6010B EPA 3050B
Thallium 0.252 J 0.152* mg/kg EPA 6010B EPA 3050B
Vanadium 29.6 0.251 mg/kg EPA 6010B EPA 3050B
Zinc 33.0 1.01 mg/kg EPA 6010B EPA 3050B
Mercury 0.00945 J 0.00597* mg/kg EPA 7471A EPA 7471A Total C25-C28 2.9 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C29-C32 13 4.9 mg/kg EPA 8015B (M) EPA 3550B
C33-C36 19 4.9 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 4.3 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 39 5.0 mg/kg EPA 8015B (M) EPA 3550B
4,4'-DDT 4.8 J 2.2* ug/kg EPA 8081A EPA 3545
Aroclor-1254 120 50 ug/kg EPA 8082 EPA 3545
BB-17-04 (16-06-2031-2)
Moisture 3.8 0.10 % ASTM D-2216 (M) N/A
Arsenic 1.38 0.732 mg/kg EPA 6010B EPA 3050B
Barium 69.5 0.488 mg/kg EPA 6010B EPA 3050B
Beryllium 0.309 0.244 mg/kg EPA 6010B EPA 3050B
Cadmium 0.335 J 0.132* mg/kg EPA 6010B EPA 3050B
Chromium 16.3 0.244 mg/kg EPA 6010B EPA 3050B
Cobalt 9.81 0.244 mg/kg EPA 6010B EPA 3050B
Copper 10.0 0.488 mg/kg EPA 6010B EPA 3050B
Lead 4.17 0.488 mg/kg EPA 6010B EPA 3050B
Nickel 7.24 0.244 mg/kg EPA 6010B EPA 3050B
Selenium 0.368 J 0.292* mg/kg EPA 6010B EPA 3050B
Vanadium 51.5 0.244 mg/kg EPA 6010B EPA 3050B
Zinc 24.8 0.976 mg/kg EPA 6010B EPA 3050B
Mercury 0.0215 J 0.00559* mg/kg EPA 7471A EPA 7471A Total Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 1 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-17-GW (16-06-2031-4)
Arsenic 0.0149 0.0100 mg/L EPA 6010B EPA 3005A Filt.
Barium 0.0430 0.0100 mg/L EPA 6010B EPA 3005A Filt.
Cobalt 0.0211 0.0100 mg/L EPA 6010B EPA 3005A Filt.
Copper 0.00481 J 0.00267* mg/L EPA 6010B EPA 3005A Filt.
Molybdenum 0.105 B 0.0100 mg/L EPA 6010B EPA 3005A Filt.
Nickel 0.0125 0.0100 mg/L EPA 6010B EPA 3005A Filt.
Selenium 0.0164 0.0150 mg/L EPA 6010B EPA 3005A Filt.
Silver 0.00156 J 0.00139* mg/L EPA 6010B EPA 3005A Filt.
Zinc 0.0119 0.0100 mg/L EPA 6010B EPA 3005A Filt.
Acetone 5.1 J 3.5* ug/L EPA 8260B EPA 5030C
Bromomethane 0.88 J 0.38* ug/L EPA 8260B EPA 5030C
Chloroform 1.5 0.50 ug/L EPA 8260B EPA 5030C
Chloromethane 0.24 J 0.22* ug/L EPA 8260B EPA 5030C
Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 2 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-18-01 (16-06-2031-5)
Moisture 5.0 0.10 % ASTM D-2216 (M) N/A
Arsenic 5.58 0.765 mg/kg EPA 6010B EPA 3050B
Barium 79.4 0.510 mg/kg EPA 6010B EPA 3050B
Beryllium 0.242 J 0.140* mg/kg EPA 6010B EPA 3050B
Cadmium 0.451 J 0.138* mg/kg EPA 6010B EPA 3050B
Chromium 17.5 0.255 mg/kg EPA 6010B EPA 3050B
Cobalt 3.74 0.255 mg/kg EPA 6010B EPA 3050B
Copper 10.9 0.510 mg/kg EPA 6010B EPA 3050B
Lead 17.6 0.510 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.863 0.255 mg/kg EPA 6010B EPA 3050B
Nickel 5.92 0.255 mg/kg EPA 6010B EPA 3050B
Silver 0.185 J 0.0875* mg/kg EPA 6010B EPA 3050B
Thallium 0.470 J 0.155* mg/kg EPA 6010B EPA 3050B
Vanadium 23.9 0.255 mg/kg EPA 6010B EPA 3050B
Zinc 48.2 1.02 mg/kg EPA 6010B EPA 3050B
Mercury 0.0239 J 0.00597* mg/kg EPA 7471A EPA 7471A Total C29-C32 32 25 mg/kg EPA 8015B (M) EPA 3550B
C33-C36 35 25 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 29 25 mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 97 5.0 mg/kg EPA 8015B (M) EPA 3550B
Phenanthrene 23 10 ug/kg EPA 8310 EPA 3545
Anthracene 8.2 J 2.0* ug/kg EPA 8310 EPA 3545
Fluoranthene 54 10 ug/kg EPA 8310 EPA 3545
Pyrene 32 10 ug/kg EPA 8310 EPA 3545
Benzo (a) Anthracene 5.5 J 2.5* ug/kg EPA 8310 EPA 3545 Chrysene 20 10 ug/kg EPA 8310 EPA 3545
Benzo (b) Fluoranthene 21 10 ug/kg EPA 8310 EPA 3545
Benzo (k) Fluoranthene 47 10 ug/kg EPA 8310 EPA 3545
Benzo (a) Pyrene 19 10 ug/kg EPA 8310 EPA 3545
Dibenz (a,h) Anthracene 60 10 ug/kg EPA 8310 EPA 3545
Benzo (g,h,i) Perylene 28 10 ug/kg EPA 8310 EPA 3545
Indeno (1,2,3-c,d) Pyrene 110 10 ug/kg EPA 8310 EPA 3545 Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 3 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-18-04 (16-06-2031-6)
Moisture 6.3 0.10 % ASTM D-2216 (M) N/A
Arsenic 1.77 0.765 mg/kg EPA 6010B EPA 3050B
Barium 74.9 0.510 mg/kg EPA 6010B EPA 3050B
Beryllium 0.318 0.255 mg/kg EPA 6010B EPA 3050B
Cadmium 0.881 0.510 mg/kg EPA 6010B EPA 3050B
Chromium 17.0 0.255 mg/kg EPA 6010B EPA 3050B
Cobalt 9.32 0.255 mg/kg EPA 6010B EPA 3050B
Copper 23.5 0.510 mg/kg EPA 6010B EPA 3050B
Lead 22.7 0.510 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.147 J 0.135* mg/kg EPA 6010B EPA 3050B
Nickel 8.92 0.255 mg/kg EPA 6010B EPA 3050B
Selenium 0.467 J 0.306* mg/kg EPA 6010B EPA 3050B
Thallium 0.181 J 0.155* mg/kg EPA 6010B EPA 3050B
Vanadium 49.6 0.255 mg/kg EPA 6010B EPA 3050B
Zinc 55.5 1.02 mg/kg EPA 6010B EPA 3050B
Mercury 0.0234 J 0.00597* mg/kg EPA 7471A EPA 7471A Total Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 4 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-19-01 (16-06-2031-8)
Moisture 3.1 0.10 % ASTM D-2216 (M) N/A
Arsenic 6.75 0.761 mg/kg EPA 6010B EPA 3050B
Barium 92.9 0.508 mg/kg EPA 6010B EPA 3050B
Beryllium 0.282 0.254 mg/kg EPA 6010B EPA 3050B
Cadmium 0.432 J 0.137* mg/kg EPA 6010B EPA 3050B
Chromium 14.3 0.254 mg/kg EPA 6010B EPA 3050B
Cobalt 4.55 0.254 mg/kg EPA 6010B EPA 3050B
Copper 13.6 0.508 mg/kg EPA 6010B EPA 3050B
Lead 14.5 0.508 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.884 0.254 mg/kg EPA 6010B EPA 3050B
Nickel 7.50 0.254 mg/kg EPA 6010B EPA 3050B
Selenium 1.16 0.761 mg/kg EPA 6010B EPA 3050B
Thallium 0.734 J 0.154* mg/kg EPA 6010B EPA 3050B
Vanadium 27.2 0.254 mg/kg EPA 6010B EPA 3050B
Zinc 56.9 1.02 mg/kg EPA 6010B EPA 3050B
Mercury 0.0218 J 0.00618* mg/kg EPA 7471A EPA 7471A Total C29-C32 57 50 mg/kg EPA 8015B (M) EPA 3550B
C33-C36 66 50 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 42 J 13* mg/kg EPA 8015B (M) EPA 3550B
C41-C44 29 J 13* mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 190 5.0 mg/kg EPA 8015B (M) EPA 3550B
Chlordane 33 J 26* ug/kg EPA 8081A EPA 3545
4,4'-DDE 2.4 J 2.2* ug/kg EPA 8081A EPA 3545
4,4'-DDT 4.1 J 2.2* ug/kg EPA 8081A EPA 3545
Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 5 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
Subcontracted analyses, if any, are not included in this summary.
BB-19-03 (16-06-2031-9)
Moisture 3.4 0.10 % ASTM D-2216 (M) N/A
Arsenic 2.06 0.732 mg/kg EPA 6010B EPA 3050B
Barium 83.4 0.488 mg/kg EPA 6010B EPA 3050B
Beryllium 0.326 0.244 mg/kg EPA 6010B EPA 3050B
Cadmium 0.510 0.488 mg/kg EPA 6010B EPA 3050B
Chromium 16.9 0.244 mg/kg EPA 6010B EPA 3050B
Cobalt 9.24 0.244 mg/kg EPA 6010B EPA 3050B
Copper 20.4 0.488 mg/kg EPA 6010B EPA 3050B
Lead 14.9 0.488 mg/kg EPA 6010B EPA 3050B
Nickel 7.51 0.244 mg/kg EPA 6010B EPA 3050B
Thallium 0.223 J 0.148* mg/kg EPA 6010B EPA 3050B
Vanadium 49.8 0.244 mg/kg EPA 6010B EPA 3050B
Zinc 43.6 0.976 mg/kg EPA 6010B EPA 3050B
Mercury 0.0235 J 0.00618* mg/kg EPA 7471A EPA 7471A Total Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2031
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 6 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-01 16-06-2031-5-AA 06/28/16
10:36
Solid HPLC 5 07/02/16 07/06/16
06:03
160702L06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Naphthalene ND 15 4.0 1.00
Acenaphthylene ND 30 4.2 1.00
Acenaphthene ND 15 4.0 1.00
Fluorene ND 10 1.7 1.00
Phenanthrene 23 10 2.1 1.00
Anthracene 8.2 10 2.0 1.00 J
Fluoranthene 54 10 2.1 1.00
Pyrene 32 10 2.9 1.00
Benzo (a) Anthracene 5.5 10 2.5 1.00 J
Chrysene 20 10 2.1 1.00
Benzo (b) Fluoranthene 21 10 2.1 1.00
Benzo (k) Fluoranthene 47 10 1.7 1.00
Benzo (a) Pyrene 19 10 2.0 1.00
Dibenz (a,h) Anthracene 60 10 2.9 1.00
Benzo (g,h,i) Perylene 28 10 1.8 1.00
Indeno (1,2,3-c,d) Pyrene 110 10 2.2 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decafluorobiphenyl 68 8-120
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8310
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-07-002-1879 N/A Solid HPLC 5 07/02/16 07/05/16 17:02
160702L06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Naphthalene ND 15 4.0 1.00
Acenaphthylene ND 30 4.2 1.00
Acenaphthene ND 15 4.0 1.00
Fluorene ND 10 1.7 1.00
Phenanthrene ND 10 2.1 1.00
Anthracene ND 10 2.0 1.00
Fluoranthene ND 10 2.1 1.00
Pyrene ND 10 2.9 1.00
Benzo (a) Anthracene ND 10 2.5 1.00
Chrysene ND 10 2.1 1.00
Benzo (b) Fluoranthene ND 10 2.1 1.00
Benzo (k) Fluoranthene ND 10 1.7 1.00
Benzo (a) Pyrene ND 10 2.0 1.00
Dibenz (a,h) Anthracene ND 10 3.0 1.00
Benzo (g,h,i) Perylene ND 10 1.8 1.00
Indeno (1,2,3-c,d) Pyrene ND 10 2.2 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decafluorobiphenyl 61 8-120
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8310
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-AA 06/28/16
09:52
Solid N/A 06/29/16 06/29/16
19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 3.5 0.10 0.10 1.00
BB-17-04 16-06-2031-2-AA 06/28/16
09:54
Solid N/A 06/29/16 06/29/16
19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 3.8 0.10 0.10 1.00
BB-18-01 16-06-2031-5-AA 06/28/16
10:36
Solid N/A 06/29/16 06/29/16
19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 5.0 0.10 0.10 1.00
BB-18-04 16-06-2031-6-AA 06/28/16
10:38
Solid N/A 06/29/16 06/29/16
19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 6.3 0.10 0.10 1.00
BB-19-01 16-06-2031-8-AA 06/28/16
12:21
Solid N/A 06/29/16 06/29/16
19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 3.1 0.10 0.10 1.00
BB-19-03 16-06-2031-9-AA 06/28/16
12:23
Solid N/A 06/29/16 06/29/16
19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 3.4 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-05-014-6079 N/A Solid N/A 06/29/16 06/29/16 19:00
G0629MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture ND 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-AA 06/28/16
09:52
Solid GC 49 06/30/16 06/30/16
21:22
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 4.9 1.2 1.00
C7 ND 4.9 1.2 1.00
C8 ND 4.9 1.2 1.00
C9-C10 ND 4.9 1.2 1.00
C11-C12 ND 4.9 1.2 1.00
C13-C14 ND 4.9 1.2 1.00
C15-C16 ND 4.9 1.2 1.00
C17-C18 ND 4.9 1.2 1.00
C19-C20 ND 4.9 1.2 1.00
C21-C22 ND 4.9 1.2 1.00
C23-C24 ND 4.9 1.2 1.00
C25-C28 2.9 4.9 1.2 1.00 J
C29-C32 13 4.9 1.2 1.00
C33-C36 19 4.9 1.2 1.00
C37-C40 4.3 4.9 1.2 1.00 J
C41-C44 ND 4.9 1.2 1.00
C6-C44 Total 39 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 80 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-04 16-06-2031-2-AA 06/28/16
09:54
Solid GC 49 06/30/16 07/01/16
14:15
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 92 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-01 16-06-2031-5-AA 06/28/16
10:36
Solid GC 49 06/30/16 06/30/16
21:40
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 25 6.3 5.00
C7 ND 25 6.3 5.00
C8 ND 25 6.3 5.00
C9-C10 ND 25 6.3 5.00
C11-C12 ND 25 6.3 5.00
C13-C14 ND 25 6.3 5.00
C15-C16 ND 25 6.3 5.00
C17-C18 ND 25 6.3 5.00
C19-C20 ND 25 6.3 5.00
C21-C22 ND 25 6.3 5.00
C23-C24 ND 25 6.3 5.00
C25-C28 ND 25 6.3 5.00
C29-C32 32 25 6.3 5.00
C33-C36 35 25 6.3 5.00
C37-C40 29 25 6.3 5.00
C41-C44 ND 25 6.3 5.00
C6-C44 Total 97 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 88 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 3 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-04 16-06-2031-6-AA 06/28/16
10:38
Solid GC 49 06/30/16 06/30/16
18:07
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.1 1.3 1.00
C7 ND 5.1 1.3 1.00
C8 ND 5.1 1.3 1.00
C9-C10 ND 5.1 1.3 1.00
C11-C12 ND 5.1 1.3 1.00
C13-C14 ND 5.1 1.3 1.00
C15-C16 ND 5.1 1.3 1.00
C17-C18 ND 5.1 1.3 1.00
C19-C20 ND 5.1 1.3 1.00
C21-C22 ND 5.1 1.3 1.00
C23-C24 ND 5.1 1.3 1.00
C25-C28 ND 5.1 1.3 1.00
C29-C32 ND 5.1 1.3 1.00
C33-C36 ND 5.1 1.3 1.00
C37-C40 ND 5.1 1.3 1.00
C41-C44 ND 5.1 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 91 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 4 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-01 16-06-2031-8-AA 06/28/16
12:21
Solid GC 49 06/30/16 06/30/16
22:33
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 50 13 10.0
C7 ND 50 13 10.0
C8 ND 50 13 10.0
C9-C10 ND 50 13 10.0
C11-C12 ND 50 13 10.0
C13-C14 ND 50 13 10.0
C15-C16 ND 50 13 10.0
C17-C18 ND 50 13 10.0
C19-C20 ND 50 13 10.0
C21-C22 ND 50 13 10.0
C23-C24 ND 50 13 10.0
C25-C28 ND 50 13 10.0
C29-C32 57 50 13 10.0
C33-C36 66 50 13 10.0
C37-C40 42 50 13 10.0 J
C41-C44 29 50 13 10.0 J
C6-C44 Total 190 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 66 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 5 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-03 16-06-2031-9-AA 06/28/16
12:23
Solid GC 49 06/30/16 07/01/16
14:32
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 4.9 1.2 1.00
C7 ND 4.9 1.2 1.00
C8 ND 4.9 1.2 1.00
C9-C10 ND 4.9 1.2 1.00
C11-C12 ND 4.9 1.2 1.00
C13-C14 ND 4.9 1.2 1.00
C15-C16 ND 4.9 1.2 1.00
C17-C18 ND 4.9 1.2 1.00
C19-C20 ND 4.9 1.2 1.00
C21-C22 ND 4.9 1.2 1.00
C23-C24 ND 4.9 1.2 1.00
C25-C28 ND 4.9 1.2 1.00
C29-C32 ND 4.9 1.2 1.00
C33-C36 ND 4.9 1.2 1.00
C37-C40 ND 4.9 1.2 1.00
C41-C44 ND 4.9 1.2 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 92 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 6 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-15-490-2144 N/A Solid GC 49 06/30/16 06/30/16 15:45
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 92 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 7 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-AA 06/28/16
09:52
Solid ICP 7300 07/02/16 07/05/16
15:53
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.754 0.150 1.01
Arsenic 3.25 0.754 0.260 1.01
Barium 72.6 0.503 0.155 1.01
Beryllium 0.239 0.251 0.138 1.01 J
Cadmium 0.407 0.503 0.136 1.01 J
Chromium 12.8 0.251 0.143 1.01
Cobalt 4.42 0.251 0.149 1.01
Copper 7.64 0.503 0.135 1.01
Lead 9.76 0.503 0.132 1.01
Molybdenum 0.425 0.251 0.133 1.01
Nickel 5.91 0.251 0.145 1.01
Selenium 0.903 0.754 0.301 1.01
Silver ND 0.251 0.0861 1.01
Thallium 0.252 0.754 0.152 1.01 J
Vanadium 29.6 0.251 0.142 1.01
Zinc 33.0 1.01 0.178 1.01
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-04 16-06-2031-2-AA 06/28/16
09:54
Solid ICP 7300 07/02/16 07/05/16
15:54
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.732 0.145 0.976
Arsenic 1.38 0.732 0.253 0.976
Barium 69.5 0.488 0.151 0.976
Beryllium 0.309 0.244 0.134 0.976
Cadmium 0.335 0.488 0.132 0.976 J
Chromium 16.3 0.244 0.139 0.976
Cobalt 9.81 0.244 0.144 0.976
Copper 10.0 0.488 0.131 0.976
Lead 4.17 0.488 0.128 0.976
Molybdenum ND 0.244 0.129 0.976
Nickel 7.24 0.244 0.141 0.976
Selenium 0.368 0.732 0.292 0.976 J
Silver ND 0.244 0.0836 0.976
Thallium ND 0.732 0.148 0.976
Vanadium 51.5 0.244 0.138 0.976
Zinc 24.8 0.976 0.173 0.976
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-01 16-06-2031-5-AA 06/28/16
10:36
Solid ICP 7300 07/02/16 07/05/16
15:55
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.765 0.152 1.02
Arsenic 5.58 0.765 0.264 1.02
Barium 79.4 0.510 0.158 1.02
Beryllium 0.242 0.255 0.140 1.02 J
Cadmium 0.451 0.510 0.138 1.02 J
Chromium 17.5 0.255 0.145 1.02
Cobalt 3.74 0.255 0.151 1.02
Copper 10.9 0.510 0.137 1.02
Lead 17.6 0.510 0.134 1.02
Molybdenum 0.863 0.255 0.135 1.02
Nickel 5.92 0.255 0.148 1.02
Selenium ND 0.765 0.306 1.02
Silver 0.185 0.255 0.0875 1.02 J
Thallium 0.470 0.765 0.155 1.02 J
Vanadium 23.9 0.255 0.144 1.02
Zinc 48.2 1.02 0.181 1.02
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 3 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-04 16-06-2031-6-AA 06/28/16
10:38
Solid ICP 7300 07/02/16 07/05/16
15:56
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.765 0.152 1.02
Arsenic 1.77 0.765 0.264 1.02
Barium 74.9 0.510 0.158 1.02
Beryllium 0.318 0.255 0.140 1.02
Cadmium 0.881 0.510 0.138 1.02
Chromium 17.0 0.255 0.145 1.02
Cobalt 9.32 0.255 0.151 1.02
Copper 23.5 0.510 0.137 1.02
Lead 22.7 0.510 0.134 1.02
Molybdenum 0.147 0.255 0.135 1.02 J
Nickel 8.92 0.255 0.148 1.02
Selenium 0.467 0.765 0.306 1.02 J
Silver ND 0.255 0.0875 1.02
Thallium 0.181 0.765 0.155 1.02 J
Vanadium 49.6 0.255 0.144 1.02
Zinc 55.5 1.02 0.181 1.02
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 4 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-01 16-06-2031-8-AA 06/28/16
12:21
Solid ICP 7300 07/02/16 07/05/16
16:03
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.761 0.151 1.02
Arsenic 6.75 0.761 0.263 1.02
Barium 92.9 0.508 0.157 1.02
Beryllium 0.282 0.254 0.139 1.02
Cadmium 0.432 0.508 0.137 1.02 J
Chromium 14.3 0.254 0.144 1.02
Cobalt 4.55 0.254 0.150 1.02
Copper 13.6 0.508 0.137 1.02
Lead 14.5 0.508 0.134 1.02
Molybdenum 0.884 0.254 0.134 1.02
Nickel 7.50 0.254 0.147 1.02
Selenium 1.16 0.761 0.304 1.02
Silver ND 0.254 0.0870 1.02
Thallium 0.734 0.761 0.154 1.02 J
Vanadium 27.2 0.254 0.143 1.02
Zinc 56.9 1.02 0.180 1.02
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 5 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-03 16-06-2031-9-AA 06/28/16
12:23
Solid ICP 7300 07/02/16 07/05/16
16:04
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.732 0.145 0.976
Arsenic 2.06 0.732 0.253 0.976
Barium 83.4 0.488 0.151 0.976
Beryllium 0.326 0.244 0.134 0.976
Cadmium 0.510 0.488 0.132 0.976
Chromium 16.9 0.244 0.139 0.976
Cobalt 9.24 0.244 0.144 0.976
Copper 20.4 0.488 0.131 0.976
Lead 14.9 0.488 0.128 0.976
Molybdenum ND 0.244 0.129 0.976
Nickel 7.51 0.244 0.141 0.976
Selenium ND 0.732 0.292 0.976
Silver ND 0.244 0.0836 0.976
Thallium 0.223 0.732 0.148 0.976 J
Vanadium 49.8 0.244 0.138 0.976
Zinc 43.6 0.976 0.173 0.976
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 6 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 097-01-002-22889 N/A Solid ICP 7300 07/02/16 07/07/16 10:31
160702L01U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.765 0.152 1.02
Arsenic ND 0.765 0.264 1.02
Barium ND 0.510 0.158 1.02
Beryllium ND 0.255 0.140 1.02
Cadmium ND 0.510 0.138 1.02
Chromium ND 0.255 0.145 1.02
Cobalt ND 0.255 0.151 1.02
Copper ND 0.510 0.137 1.02
Lead ND 0.510 0.134 1.02
Molybdenum ND 0.255 0.135 1.02
Nickel ND 0.255 0.148 1.02
Selenium ND 0.765 0.306 1.02
Silver ND 0.255 0.0875 1.02
Thallium ND 0.765 0.155 1.02
Vanadium ND 0.255 0.144 1.02
Zinc ND 1.02 0.181 1.02
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 7 of7
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-GW 16-06-2031-4-F 06/28/16
10:10
Aqueous ICP 7300 06/30/16 07/01/16
13:11
160630LA2U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.0150 0.00787 1.00
Arsenic 0.0149 0.0100 0.00438 1.00
Barium 0.0430 0.0100 0.00296 1.00
Beryllium ND 0.0100 0.00262 1.00
Cadmium ND 0.0100 0.00269 1.00
Chromium ND 0.0100 0.00271 1.00
Cobalt 0.0211 0.0100 0.00295 1.00
Copper 0.00481 0.0100 0.00267 1.00 J
Lead ND 0.0100 0.00406 1.00
Molybdenum 0.105 0.0100 0.00278 1.00 B
Nickel 0.0125 0.0100 0.00298 1.00
Selenium 0.0164 0.0150 0.00699 1.00
Silver 0.00156 0.00500 0.00139 1.00 J
Thallium ND 0.0150 0.00291 1.00
Vanadium ND 0.0100 0.00244 1.00
Zinc 0.0119 0.0100 0.00352 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3005A Filt.
Method: EPA 6010B
Units: mg/L
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-16-460-98 N/A Aqueous ICP 7300 06/30/16 07/01/16 12:28
160630LA2U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony 0.0413 0.0150 0.00787 1.00
Arsenic ND 0.0100 0.00438 1.00
Barium ND 0.0100 0.00296 1.00
Beryllium ND 0.0100 0.00262 1.00
Cadmium ND 0.0100 0.00269 1.00
Chromium ND 0.0100 0.00271 1.00
Cobalt ND 0.0100 0.00295 1.00
Copper ND 0.0100 0.00267 1.00
Lead ND 0.0100 0.00406 1.00
Molybdenum 0.00769 0.0100 0.00278 1.00 J
Nickel ND 0.0100 0.00298 1.00
Selenium ND 0.0150 0.00699 1.00
Silver ND 0.00500 0.00139 1.00
Thallium 0.00605 0.0150 0.00291 1.00 J
Vanadium ND 0.0100 0.00244 1.00
Zinc ND 0.0100 0.00352 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3005A Filt.
Method: EPA 6010B
Units: mg/L
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-GW 16-06-2031-4-F 06/28/16
10:10
Aqueous Mercury 04 07/06/16 07/06/16
15:25
160706LA1F
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.000500 0.0000453 1.00
Method Blank 099-16-456-3 N/A Aqueous Mercury 04 07/06/16 07/06/16 15:14
160706LA1F
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.000500 0.0000453 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7470A Filt.
Method: EPA 7470A
Units: mg/L
Project: UTAS - Due Diligence / 43559 Page 1 of1
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-AA 06/28/16
09:52
Solid Mercury 05 07/06/16 07/07/16
11:35
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.00945 0.0847 0.00597 1.00 J
BB-17-04 16-06-2031-2-AA 06/28/16
09:54
Solid Mercury 05 07/06/16 07/06/16
16:05
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0215 0.0794 0.00559 1.00 J
BB-18-01 16-06-2031-5-AA 06/28/16
10:36
Solid Mercury 05 07/06/16 07/06/16
16:07
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0239 0.0847 0.00597 1.00 J
BB-18-04 16-06-2031-6-AA 06/28/16
10:38
Solid Mercury 05 07/06/16 07/06/16
16:09
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0234 0.0847 0.00597 1.00 J
BB-19-01 16-06-2031-8-AA 06/28/16
12:21
Solid Mercury 05 07/06/16 07/07/16
11:28
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0218 0.0877 0.00618 1.00 J
BB-19-03 16-06-2031-9-AA 06/28/16
12:23
Solid Mercury 05 07/06/16 07/07/16
11:31
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury 0.0235 0.0877 0.00618 1.00 J
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7471A Total
Method: EPA 7471A
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-16-480-44 N/A Solid Mercury 05 07/06/16 07/06/16 15:27
160706L02
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.0833 0.00587 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7471A Total
Method: EPA 7471A
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-AA 06/28/16
09:52
Solid GC 44 07/05/16 07/09/16
11:13
160705L04
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aldrin ND 5.0 2.2 1.00
Alpha-BHC ND 10 3.7 1.00
Beta-BHC ND 5.0 2.5 1.00
Chlordane ND 50 26 1.00
4,4'-DDD ND 5.0 2.4 1.00
4,4'-DDE ND 5.0 2.2 1.00
4,4'-DDT 4.8 5.0 2.2 1.00 J
Delta-BHC ND 10 4.4 1.00
Dieldrin ND 5.0 2.2 1.00
Endosulfan I ND 5.0 2.0 1.00
Endosulfan II ND 5.0 2.4 1.00
Endosulfan Sulfate ND 5.0 2.6 1.00
Endrin ND 5.0 2.4 1.00
Endrin Aldehyde ND 5.0 3.0 1.00
Endrin Ketone ND 5.0 2.5 1.00
Gamma-BHC ND 5.0 2.2 1.00
Heptachlor ND 5.0 2.2 1.00
Heptachlor Epoxide ND 10 3.7 1.00
Methoxychlor ND 5.0 2.7 1.00
Toxaphene ND 100 45 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 98 24-168
2,4,5,6-Tetrachloro-m-Xylene 79 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8081A
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of3
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-01 16-06-2031-8-AA 06/28/16
12:21
Solid GC 44 07/05/16 07/09/16
11:28
160705L04
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aldrin ND 5.0 2.2 1.00
Alpha-BHC ND 10 3.7 1.00
Beta-BHC ND 5.0 2.5 1.00
Chlordane 33 50 26 1.00 J
4,4'-DDD ND 5.0 2.4 1.00
4,4'-DDE 2.4 5.0 2.2 1.00 J
4,4'-DDT 4.1 5.0 2.2 1.00 J
Delta-BHC ND 10 4.4 1.00
Dieldrin ND 5.0 2.2 1.00
Endosulfan I ND 5.0 2.0 1.00
Endosulfan II ND 5.0 2.3 1.00
Endosulfan Sulfate ND 5.0 2.6 1.00
Endrin ND 5.0 2.3 1.00
Endrin Aldehyde ND 5.0 3.0 1.00
Endrin Ketone ND 5.0 2.5 1.00
Gamma-BHC ND 5.0 2.2 1.00
Heptachlor ND 5.0 2.2 1.00
Heptachlor Epoxide ND 10 3.7 1.00
Methoxychlor ND 5.0 2.7 1.00
Toxaphene ND 100 45 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 98 24-168
2,4,5,6-Tetrachloro-m-Xylene 82 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8081A
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of3
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-12-537-2463 N/A Solid GC 41 07/05/16 07/08/16 11:03
160705L04
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aldrin ND 5.0 2.2 1.00
Alpha-BHC ND 10 3.7 1.00
Beta-BHC ND 5.0 2.5 1.00
Chlordane ND 50 26 1.00
4,4'-DDD ND 5.0 2.4 1.00
4,4'-DDE ND 5.0 2.2 1.00
4,4'-DDT ND 5.0 2.2 1.00
Delta-BHC ND 10 4.4 1.00
Dieldrin ND 5.0 2.2 1.00
Endosulfan I ND 5.0 2.0 1.00
Endosulfan II ND 5.0 2.4 1.00
Endosulfan Sulfate ND 5.0 2.6 1.00
Endrin ND 5.0 2.4 1.00
Endrin Aldehyde ND 5.0 3.0 1.00
Endrin Ketone ND 5.0 2.5 1.00
Gamma-BHC ND 5.0 2.2 1.00
Heptachlor ND 5.0 2.2 1.00
Heptachlor Epoxide ND 10 3.7 1.00
Methoxychlor ND 5.0 2.7 1.00
Toxaphene ND 100 45 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 97 24-168
2,4,5,6-Tetrachloro-m-Xylene 76 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8081A
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of3
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-AA 06/28/16
09:52
Solid GC 58 07/05/16 07/07/16
19:12
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 120 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 114 24-168
2,4,5,6-Tetrachloro-m-Xylene 87 25-145
BB-17-04 16-06-2031-2-AA 06/28/16
09:54
Solid GC 58 07/05/16 07/07/16
19:30
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 112 24-168
2,4,5,6-Tetrachloro-m-Xylene 58 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-01 16-06-2031-5-AA 06/28/16
10:36
Solid GC 58 07/05/16 07/07/16
19:48
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 115 24-168
2,4,5,6-Tetrachloro-m-Xylene 93 25-145
BB-18-04 16-06-2031-6-AA 06/28/16
10:38
Solid GC 58 07/05/16 07/07/16
20:06
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 108 24-168
2,4,5,6-Tetrachloro-m-Xylene 57 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-01 16-06-2031-8-AA 06/28/16
12:21
Solid GC 58 07/05/16 07/07/16
20:24
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 115 24-168
2,4,5,6-Tetrachloro-m-Xylene 85 25-145
BB-19-03 16-06-2031-9-AA 06/28/16
12:23
Solid GC 58 07/05/16 07/07/16
20:42
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 108 24-168
2,4,5,6-Tetrachloro-m-Xylene 71 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-12-535-3813 N/A Solid GC 58 07/05/16 07/07/16 13:31
160705L08
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Aroclor-1016 ND 50 21 1.00
Aroclor-1221 ND 50 42 1.00
Aroclor-1232 ND 50 25 1.00
Aroclor-1242 ND 50 37 1.00
Aroclor-1248 ND 50 32 1.00
Aroclor-1254 ND 50 32 1.00
Aroclor-1260 ND 50 30 1.00
Aroclor-1262 ND 50 35 1.00
Aroclor-1268 ND 50 33 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decachlorobiphenyl 92 24-168
2,4,5,6-Tetrachloro-m-Xylene 91 25-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8082
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 4 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-GW 16-06-2031-4-A 06/28/16
10:10
Aqueous GC/MS L 06/29/16 06/29/16
19:39
160629L007
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone 5.1 10 3.5 1.00 J
Benzene ND 0.50 0.32 1.00
Bromobenzene ND 0.50 0.33 1.00
Bromochloromethane ND 1.0 0.38 1.00
Bromodichloromethane ND 0.50 0.20 1.00
Bromoform ND 0.50 0.34 1.00
Bromomethane 0.88 1.0 0.38 1.00 J
2-Butanone ND 5.0 2.9 1.00
n-Butylbenzene ND 0.50 0.34 1.00
sec-Butylbenzene ND 0.50 0.23 1.00
tert-Butylbenzene ND 0.50 0.38 1.00
Carbon Disulfide ND 1.0 0.44 1.00
Carbon Tetrachloride ND 0.50 0.22 1.00
Chlorobenzene ND 0.50 0.14 1.00
Chloroethane ND 0.50 0.34 1.00
2-Chloroethyl Vinyl Ether ND 5.0 3.1 1.00
Chloroform 1.5 0.50 0.22 1.00
Chloromethane 0.24 0.50 0.22 1.00 J
2-Chlorotoluene ND 0.50 0.34 1.00
4-Chlorotoluene ND 0.50 0.33 1.00
Dibromochloromethane ND 0.50 0.24 1.00
1,2-Dibromo-3-Chloropropane ND 5.0 2.9 1.00
1,2-Dibromoethane ND 0.50 0.34 1.00
Dibromomethane ND 0.50 0.34 1.00
1,2-Dichlorobenzene ND 0.50 0.17 1.00
1,3-Dichlorobenzene ND 0.50 0.17 1.00
1,4-Dichlorobenzene ND 0.50 0.31 1.00
Dichlorodifluoromethane ND 1.0 0.24 1.00
1,1-Dichloroethane ND 0.50 0.19 1.00
1,2-Dichloroethane ND 0.50 0.18 1.00
1,1-Dichloroethene ND 0.50 0.20 1.00
c-1,2-Dichloroethene ND 0.50 0.24 1.00
t-1,2-Dichloroethene ND 0.50 0.26 1.00
Acetonitrile ND 10 2.2 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559 Page 1 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
1,2-Dichloropropane ND 0.50 0.24 1.00
Acrolein ND 20 8.8 1.00
Acrylonitrile ND 10 5.2 1.00
1,3-Dichloropropane ND 1.0 0.24 1.00
2,2-Dichloropropane ND 1.0 0.42 1.00
Allyl Chloride ND 1.0 0.36 1.00
1,1-Dichloropropene ND 0.50 0.28 1.00
c-1,3-Dichloropropene ND 0.50 0.18 1.00
t-1,3-Dichloropropene ND 0.50 0.35 1.00
Ethylbenzene ND 0.50 0.32 1.00
2-Hexanone ND 10 2.6 1.00
Isopropylbenzene ND 0.50 0.42 1.00
p-Isopropyltoluene ND 0.50 0.14 1.00
Methylene Chloride ND 1.0 0.38 1.00
4-Methyl-2-Pentanone ND 5.0 2.7 1.00
Naphthalene ND 1.0 0.41 1.00
n-Propylbenzene ND 0.50 0.38 1.00
Styrene ND 0.50 0.32 1.00
Chloroprene ND 0.50 0.24 1.00
1,1,1,2-Tetrachloroethane ND 0.50 0.24 1.00
1,1,2,2-Tetrachloroethane ND 0.50 0.22 1.00
Tetrachloroethene ND 0.50 0.22 1.00
Toluene ND 0.50 0.26 1.00
1,2,3-Trichlorobenzene ND 0.50 0.25 1.00
Ethyl Methacrylate ND 5.0 1.4 1.00
1,2,4-Trichlorobenzene ND 0.50 0.25 1.00
1,1,1-Trichloroethane ND 0.50 0.19 1.00
Hexachloro-1,3-Butadiene ND 2.0 0.48 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 0.50 0.26 1.00 1,1,2-Trichloroethane ND 0.50 0.32 1.00
Iodomethane ND 10 6.8 1.00
Trichloroethene ND 0.50 0.23 1.00
Trichlorofluoromethane ND 0.50 0.25 1.00
Isobutyl Alcohol ND 10 6.7 1.00
1,2,3-Trichloropropane ND 1.0 0.25 1.00
1,2,4-Trimethylbenzene ND 0.50 0.15 1.00
Methacrylonitrile ND 10 2.5 1.00
Methyl Methacrylate ND 5.0 1.3 1.00
1,3,5-Trimethylbenzene ND 0.50 0.33 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559 Page 2 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
Vinyl Acetate ND 5.0 2.2 1.00
Vinyl Chloride ND 0.50 0.27 1.00
p/m-Xylene ND 0.50 0.24 1.00
o-Xylene ND 0.50 0.39 1.00
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.29 1.00
t-1,4-Dichloro-2-Butene ND 5.0 3.0 1.00
Tetrahydrofuran ND 5.0 2.2 1.00
Propionitrile ND 10 3.1 1.00
Tert-Butyl Alcohol (TBA) ND 10 4.1 1.00
Diisopropyl Ether (DIPE) ND 0.50 0.24 1.00
Ethyl-t-Butyl Ether (ETBE) ND 0.50 0.22 1.00
Tert-Amyl-Methyl Ether (TAME) ND 0.50 0.24 1.00
Ethanol ND 50 17 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 96 68-120
Dibromofluoromethane 106 71-135
1,2-Dichloroethane-d4 109 64-139
Toluene-d8 102 72-128
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559 Page 3 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-16-446-105 N/A Aqueous GC/MS L 06/29/16 06/29/16 10:33
160629L007
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 10 3.5 1.00
Benzene ND 0.50 0.32 1.00
Bromobenzene ND 0.50 0.33 1.00
Bromochloromethane ND 1.0 0.38 1.00
Bromodichloromethane ND 0.50 0.20 1.00
Bromoform ND 0.50 0.34 1.00
Bromomethane ND 1.0 0.38 1.00
2-Butanone ND 5.0 2.9 1.00
n-Butylbenzene ND 0.50 0.34 1.00
sec-Butylbenzene ND 0.50 0.23 1.00
tert-Butylbenzene ND 0.50 0.38 1.00
Carbon Disulfide ND 1.0 0.44 1.00
Carbon Tetrachloride ND 0.50 0.22 1.00
Chlorobenzene ND 0.50 0.14 1.00
Chloroethane ND 0.50 0.34 1.00
2-Chloroethyl Vinyl Ether ND 5.0 3.1 1.00
Chloroform ND 0.50 0.22 1.00
Chloromethane ND 0.50 0.22 1.00
2-Chlorotoluene ND 0.50 0.34 1.00
4-Chlorotoluene ND 0.50 0.33 1.00
Dibromochloromethane ND 0.50 0.24 1.00
1,2-Dibromo-3-Chloropropane ND 5.0 2.9 1.00
1,2-Dibromoethane ND 0.50 0.34 1.00
Dibromomethane ND 0.50 0.34 1.00
1,2-Dichlorobenzene ND 0.50 0.17 1.00
1,3-Dichlorobenzene ND 0.50 0.17 1.00
1,4-Dichlorobenzene ND 0.50 0.31 1.00
Dichlorodifluoromethane ND 1.0 0.24 1.00
1,1-Dichloroethane ND 0.50 0.19 1.00
1,2-Dichloroethane ND 0.50 0.18 1.00
1,1-Dichloroethene ND 0.50 0.20 1.00
c-1,2-Dichloroethene ND 0.50 0.24 1.00
t-1,2-Dichloroethene ND 0.50 0.26 1.00
Acetonitrile ND 10 2.2 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559 Page 4 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
1,2-Dichloropropane ND 0.50 0.24 1.00
Acrolein ND 20 8.8 1.00
Acrylonitrile ND 10 5.2 1.00
1,3-Dichloropropane ND 1.0 0.24 1.00
2,2-Dichloropropane ND 1.0 0.42 1.00
Allyl Chloride ND 1.0 0.36 1.00
1,1-Dichloropropene ND 0.50 0.28 1.00
c-1,3-Dichloropropene ND 0.50 0.18 1.00
t-1,3-Dichloropropene ND 0.50 0.35 1.00
Ethylbenzene ND 0.50 0.32 1.00
2-Hexanone ND 10 2.6 1.00
Isopropylbenzene ND 0.50 0.42 1.00
p-Isopropyltoluene ND 0.50 0.14 1.00
Methylene Chloride ND 1.0 0.38 1.00
4-Methyl-2-Pentanone ND 5.0 2.7 1.00
Naphthalene ND 1.0 0.41 1.00
n-Propylbenzene ND 0.50 0.38 1.00
Styrene ND 0.50 0.32 1.00
Chloroprene ND 0.50 0.24 1.00
1,1,1,2-Tetrachloroethane ND 0.50 0.24 1.00
1,1,2,2-Tetrachloroethane ND 0.50 0.22 1.00
Tetrachloroethene ND 0.50 0.22 1.00
Toluene ND 0.50 0.26 1.00
1,2,3-Trichlorobenzene ND 0.50 0.25 1.00
Ethyl Methacrylate ND 5.0 1.4 1.00
1,2,4-Trichlorobenzene ND 0.50 0.25 1.00
1,1,1-Trichloroethane ND 0.50 0.19 1.00
Hexachloro-1,3-Butadiene ND 2.0 0.48 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 0.50 0.26 1.00 1,1,2-Trichloroethane ND 0.50 0.32 1.00
Iodomethane ND 10 6.8 1.00
Trichloroethene ND 0.50 0.23 1.00
Trichlorofluoromethane ND 0.50 0.25 1.00
Isobutyl Alcohol ND 10 6.7 1.00
1,2,3-Trichloropropane ND 1.0 0.25 1.00
1,2,4-Trimethylbenzene ND 0.50 0.15 1.00
Methacrylonitrile ND 10 2.5 1.00
Methyl Methacrylate ND 5.0 1.3 1.00
1,3,5-Trimethylbenzene ND 0.50 0.33 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559 Page 5 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
Vinyl Acetate ND 5.0 2.2 1.00
Vinyl Chloride ND 0.50 0.27 1.00
p/m-Xylene ND 0.50 0.24 1.00
o-Xylene ND 0.50 0.39 1.00
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.29 1.00
t-1,4-Dichloro-2-Butene ND 5.0 3.0 1.00
Tetrahydrofuran ND 5.0 2.2 1.00
Propionitrile ND 10 3.1 1.00
Tert-Butyl Alcohol (TBA) ND 10 4.1 1.00
Diisopropyl Ether (DIPE) ND 0.50 0.24 1.00
Ethyl-t-Butyl Ether (ETBE) ND 0.50 0.22 1.00
Tert-Amyl-Methyl Ether (TAME) ND 0.50 0.24 1.00
Ethanol ND 50 17 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 94 68-120
Dibromofluoromethane 99 71-135
1,2-Dichloroethane-d4 99 64-139
Toluene-d8 97 72-128
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559 Page 6 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-01 16-06-2031-1-A 06/28/16
09:52
Solid GC/MS BB 06/29/16 06/30/16
16:40
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.4 1.00
Benzene ND 5.1 0.13 1.00
Bromobenzene ND 5.1 0.22 1.00
Bromochloromethane ND 5.1 0.71 1.00
Bromodichloromethane ND 5.1 0.24 1.00
Bromoform ND 5.1 0.82 1.00
Bromomethane ND 26 9.7 1.00
2-Butanone ND 51 3.9 1.00
n-Butylbenzene ND 5.1 0.16 1.00
sec-Butylbenzene ND 5.1 0.59 1.00
tert-Butylbenzene ND 5.1 0.15 1.00
Carbon Disulfide ND 51 0.31 1.00
Carbon Tetrachloride ND 5.1 0.29 1.00
Chlorobenzene ND 5.1 0.23 1.00
Chloroethane ND 5.1 1.5 1.00
Chloroform ND 5.1 0.25 1.00
Chloromethane ND 26 0.31 1.00
2-Chlorotoluene ND 5.1 0.24 1.00
4-Chlorotoluene ND 5.1 0.22 1.00
Dibromochloromethane ND 5.1 0.59 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.1 0.26 1.00
Dibromomethane ND 5.1 0.80 1.00
1,2-Dichlorobenzene ND 5.1 0.23 1.00
1,3-Dichlorobenzene ND 5.1 0.18 1.00
1,4-Dichlorobenzene ND 5.1 0.23 1.00
Dichlorodifluoromethane ND 5.1 0.46 1.00
1,1-Dichloroethane ND 5.1 0.22 1.00
1,2-Dichloroethane ND 5.1 0.32 1.00
1,1-Dichloroethene ND 5.1 0.36 1.00
c-1,2-Dichloroethene ND 5.1 0.29 1.00
t-1,2-Dichloroethene ND 5.1 0.52 1.00
1,2-Dichloropropane ND 5.1 0.45 1.00
1,3-Dichloropropane ND 5.1 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.1 0.34 1.00
1,1-Dichloropropene ND 5.1 0.34 1.00
c-1,3-Dichloropropene ND 5.1 0.26 1.00
t-1,3-Dichloropropene ND 5.1 0.62 1.00
Ethylbenzene ND 5.1 0.16 1.00
2-Hexanone ND 51 1.8 1.00
Isopropylbenzene ND 5.1 0.56 1.00
p-Isopropyltoluene ND 5.1 0.65 1.00
Methylene Chloride ND 51 1.4 1.00
4-Methyl-2-Pentanone ND 51 4.4 1.00
Naphthalene ND 51 0.84 1.00
n-Propylbenzene ND 5.1 0.52 1.00
Styrene ND 5.1 0.62 1.00
1,1,1,2-Tetrachloroethane ND 5.1 0.25 1.00
1,1,2,2-Tetrachloroethane ND 5.1 0.35 1.00
Tetrachloroethene ND 5.1 0.22 1.00
Toluene ND 5.1 0.53 1.00
1,2,3-Trichlorobenzene ND 10 0.94 1.00
1,2,4-Trichlorobenzene ND 5.1 0.32 1.00
1,1,1-Trichloroethane ND 5.1 0.23 1.00
1,1,2-Trichloroethane ND 5.1 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 51 0.36 1.00
Trichloroethene ND 5.1 0.31 1.00
1,2,3-Trichloropropane ND 5.1 0.85 1.00
1,2,4-Trimethylbenzene ND 5.1 0.60 1.00
Trichlorofluoromethane ND 51 0.39 1.00
1,3,5-Trimethylbenzene ND 5.1 0.56 1.00
Vinyl Acetate ND 51 4.9 1.00
Vinyl Chloride ND 5.1 0.52 1.00
p/m-Xylene ND 5.1 0.28 1.00
o-Xylene ND 5.1 0.57 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.1 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 94 60-132
Dibromofluoromethane 93 63-141
1,2-Dichloroethane-d4 93 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-17-04 16-06-2031-2-A 06/28/16
09:54
Solid GC/MS BB 06/29/16 06/30/16
17:07
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.3 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.80 1.00
Bromomethane ND 25 9.5 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.31 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.78 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.45 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.32 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.26 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.82 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.61 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.92 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.8 1.00
Vinyl Chloride ND 5.0 0.51 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 94 60-132
Dibromofluoromethane 94 63-141
1,2-Dichloroethane-d4 92 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 4 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-01 16-06-2031-5-A 06/28/16
10:36
Solid GC/MS BB 06/29/16 06/30/16
17:35
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 5 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 94 60-132
Dibromofluoromethane 94 63-141
1,2-Dichloroethane-d4 94 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 6 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-18-04 16-06-2031-6-A 06/28/16
10:38
Solid GC/MS BB 06/29/16 06/30/16
18:02
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.1 1.00
Benzene ND 4.9 0.13 1.00
Bromobenzene ND 4.9 0.21 1.00
Bromochloromethane ND 4.9 0.68 1.00
Bromodichloromethane ND 4.9 0.23 1.00
Bromoform ND 4.9 0.78 1.00
Bromomethane ND 25 9.2 1.00
2-Butanone ND 49 3.7 1.00
n-Butylbenzene ND 4.9 0.15 1.00
sec-Butylbenzene ND 4.9 0.57 1.00
tert-Butylbenzene ND 4.9 0.15 1.00
Carbon Disulfide ND 49 0.30 1.00
Carbon Tetrachloride ND 4.9 0.28 1.00
Chlorobenzene ND 4.9 0.22 1.00
Chloroethane ND 4.9 1.5 1.00
Chloroform ND 4.9 0.23 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 4.9 0.23 1.00
4-Chlorotoluene ND 4.9 0.21 1.00
Dibromochloromethane ND 4.9 0.56 1.00
1,2-Dibromo-3-Chloropropane ND 9.8 1.7 1.00
1,2-Dibromoethane ND 4.9 0.25 1.00
Dibromomethane ND 4.9 0.76 1.00
1,2-Dichlorobenzene ND 4.9 0.22 1.00
1,3-Dichlorobenzene ND 4.9 0.17 1.00
1,4-Dichlorobenzene ND 4.9 0.22 1.00
Dichlorodifluoromethane ND 4.9 0.43 1.00
1,1-Dichloroethane ND 4.9 0.21 1.00
1,2-Dichloroethane ND 4.9 0.31 1.00
1,1-Dichloroethene ND 4.9 0.34 1.00
c-1,2-Dichloroethene ND 4.9 0.27 1.00
t-1,2-Dichloroethene ND 4.9 0.50 1.00
1,2-Dichloropropane ND 4.9 0.43 1.00
1,3-Dichloropropane ND 4.9 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 7 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 4.9 0.32 1.00
1,1-Dichloropropene ND 4.9 0.32 1.00
c-1,3-Dichloropropene ND 4.9 0.25 1.00
t-1,3-Dichloropropene ND 4.9 0.59 1.00
Ethylbenzene ND 4.9 0.15 1.00
2-Hexanone ND 49 1.7 1.00
Isopropylbenzene ND 4.9 0.54 1.00
p-Isopropyltoluene ND 4.9 0.62 1.00
Methylene Chloride ND 49 1.3 1.00
4-Methyl-2-Pentanone ND 49 4.2 1.00
Naphthalene ND 49 0.80 1.00
n-Propylbenzene ND 4.9 0.49 1.00
Styrene ND 4.9 0.59 1.00
1,1,1,2-Tetrachloroethane ND 4.9 0.24 1.00
1,1,2,2-Tetrachloroethane ND 4.9 0.34 1.00
Tetrachloroethene ND 4.9 0.21 1.00
Toluene ND 4.9 0.51 1.00
1,2,3-Trichlorobenzene ND 9.8 0.90 1.00
1,2,4-Trichlorobenzene ND 4.9 0.30 1.00
1,1,1-Trichloroethane ND 4.9 0.22 1.00
1,1,2-Trichloroethane ND 4.9 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 49 0.35 1.00
Trichloroethene ND 4.9 0.29 1.00
1,2,3-Trichloropropane ND 4.9 0.81 1.00
1,2,4-Trimethylbenzene ND 4.9 0.57 1.00
Trichlorofluoromethane ND 49 0.37 1.00
1,3,5-Trimethylbenzene ND 4.9 0.54 1.00
Vinyl Acetate ND 49 4.7 1.00
Vinyl Chloride ND 4.9 0.49 1.00
p/m-Xylene ND 4.9 0.26 1.00
o-Xylene ND 4.9 0.55 1.00
Methyl-t-Butyl Ether (MTBE) ND 4.9 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 95 60-132
Dibromofluoromethane 94 63-141
1,2-Dichloroethane-d4 94 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 8 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-01 16-06-2031-8-A 06/28/16
12:21
Solid GC/MS BB 06/29/16 06/30/16
18:29
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.5 1.00
Benzene ND 5.2 0.14 1.00
Bromobenzene ND 5.2 0.22 1.00
Bromochloromethane ND 5.2 0.72 1.00
Bromodichloromethane ND 5.2 0.24 1.00
Bromoform ND 5.2 0.83 1.00
Bromomethane ND 26 9.8 1.00
2-Butanone ND 52 3.9 1.00
n-Butylbenzene ND 5.2 0.16 1.00
sec-Butylbenzene ND 5.2 0.60 1.00
tert-Butylbenzene ND 5.2 0.16 1.00
Carbon Disulfide ND 52 0.32 1.00
Carbon Tetrachloride ND 5.2 0.29 1.00
Chlorobenzene ND 5.2 0.23 1.00
Chloroethane ND 5.2 1.6 1.00
Chloroform ND 5.2 0.25 1.00
Chloromethane ND 26 0.32 1.00
2-Chlorotoluene ND 5.2 0.24 1.00
4-Chlorotoluene ND 5.2 0.22 1.00
Dibromochloromethane ND 5.2 0.59 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.2 0.27 1.00
Dibromomethane ND 5.2 0.81 1.00
1,2-Dichlorobenzene ND 5.2 0.24 1.00
1,3-Dichlorobenzene ND 5.2 0.18 1.00
1,4-Dichlorobenzene ND 5.2 0.23 1.00
Dichlorodifluoromethane ND 5.2 0.46 1.00
1,1-Dichloroethane ND 5.2 0.22 1.00
1,2-Dichloroethane ND 5.2 0.33 1.00
1,1-Dichloroethene ND 5.2 0.36 1.00
c-1,2-Dichloroethene ND 5.2 0.29 1.00
t-1,2-Dichloroethene ND 5.2 0.53 1.00
1,2-Dichloropropane ND 5.2 0.46 1.00
1,3-Dichloropropane ND 5.2 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 9 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.2 0.34 1.00
1,1-Dichloropropene ND 5.2 0.34 1.00
c-1,3-Dichloropropene ND 5.2 0.27 1.00
t-1,3-Dichloropropene ND 5.2 0.63 1.00
Ethylbenzene ND 5.2 0.16 1.00
2-Hexanone ND 52 1.8 1.00
Isopropylbenzene ND 5.2 0.57 1.00
p-Isopropyltoluene ND 5.2 0.66 1.00
Methylene Chloride ND 52 1.4 1.00
4-Methyl-2-Pentanone ND 52 4.5 1.00
Naphthalene ND 52 0.85 1.00
n-Propylbenzene ND 5.2 0.52 1.00
Styrene ND 5.2 0.63 1.00
1,1,1,2-Tetrachloroethane ND 5.2 0.25 1.00
1,1,2,2-Tetrachloroethane ND 5.2 0.36 1.00
Tetrachloroethene ND 5.2 0.22 1.00
Toluene ND 5.2 0.54 1.00
1,2,3-Trichlorobenzene ND 10 0.95 1.00
1,2,4-Trichlorobenzene ND 5.2 0.32 1.00
1,1,1-Trichloroethane ND 5.2 0.23 1.00
1,1,2-Trichloroethane ND 5.2 0.37 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 52 0.37 1.00
Trichloroethene ND 5.2 0.31 1.00
1,2,3-Trichloropropane ND 5.2 0.86 1.00
1,2,4-Trimethylbenzene ND 5.2 0.61 1.00
Trichlorofluoromethane ND 52 0.39 1.00
1,3,5-Trimethylbenzene ND 5.2 0.57 1.00
Vinyl Acetate ND 52 4.9 1.00
Vinyl Chloride ND 5.2 0.52 1.00
p/m-Xylene ND 5.2 0.28 1.00
o-Xylene ND 5.2 0.58 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.2 0.31 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 95 60-132
Dibromofluoromethane 94 63-141
1,2-Dichloroethane-d4 93 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 10 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-19-03 16-06-2031-9-A 06/28/16
12:23
Solid GC/MS BB 06/29/16 06/30/16
18:57
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.4 1.00
Benzene ND 5.2 0.13 1.00
Bromobenzene ND 5.2 0.22 1.00
Bromochloromethane ND 5.2 0.71 1.00
Bromodichloromethane ND 5.2 0.24 1.00
Bromoform ND 5.2 0.82 1.00
Bromomethane ND 26 9.7 1.00
2-Butanone ND 52 3.9 1.00
n-Butylbenzene ND 5.2 0.16 1.00
sec-Butylbenzene ND 5.2 0.60 1.00
tert-Butylbenzene ND 5.2 0.16 1.00
Carbon Disulfide ND 52 0.32 1.00
Carbon Tetrachloride ND 5.2 0.29 1.00
Chlorobenzene ND 5.2 0.23 1.00
Chloroethane ND 5.2 1.5 1.00
Chloroform ND 5.2 0.25 1.00
Chloromethane ND 26 0.31 1.00
2-Chlorotoluene ND 5.2 0.24 1.00
4-Chlorotoluene ND 5.2 0.22 1.00
Dibromochloromethane ND 5.2 0.59 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.2 0.26 1.00
Dibromomethane ND 5.2 0.80 1.00
1,2-Dichlorobenzene ND 5.2 0.24 1.00
1,3-Dichlorobenzene ND 5.2 0.18 1.00
1,4-Dichlorobenzene ND 5.2 0.23 1.00
Dichlorodifluoromethane ND 5.2 0.46 1.00
1,1-Dichloroethane ND 5.2 0.22 1.00
1,2-Dichloroethane ND 5.2 0.32 1.00
1,1-Dichloroethene ND 5.2 0.36 1.00
c-1,2-Dichloroethene ND 5.2 0.29 1.00
t-1,2-Dichloroethene ND 5.2 0.52 1.00
1,2-Dichloropropane ND 5.2 0.45 1.00
1,3-Dichloropropane ND 5.2 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 11 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.2 0.34 1.00
1,1-Dichloropropene ND 5.2 0.34 1.00
c-1,3-Dichloropropene ND 5.2 0.26 1.00
t-1,3-Dichloropropene ND 5.2 0.62 1.00
Ethylbenzene ND 5.2 0.16 1.00
2-Hexanone ND 52 1.8 1.00
Isopropylbenzene ND 5.2 0.56 1.00
p-Isopropyltoluene ND 5.2 0.65 1.00
Methylene Chloride ND 52 1.4 1.00
4-Methyl-2-Pentanone ND 52 4.5 1.00
Naphthalene ND 52 0.84 1.00
n-Propylbenzene ND 5.2 0.52 1.00
Styrene ND 5.2 0.62 1.00
1,1,1,2-Tetrachloroethane ND 5.2 0.25 1.00
1,1,2,2-Tetrachloroethane ND 5.2 0.36 1.00
Tetrachloroethene ND 5.2 0.22 1.00
Toluene ND 5.2 0.53 1.00
1,2,3-Trichlorobenzene ND 10 0.94 1.00
1,2,4-Trichlorobenzene ND 5.2 0.32 1.00
1,1,1-Trichloroethane ND 5.2 0.23 1.00
1,1,2-Trichloroethane ND 5.2 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 52 0.36 1.00
Trichloroethene ND 5.2 0.31 1.00
1,2,3-Trichloropropane ND 5.2 0.86 1.00
1,2,4-Trimethylbenzene ND 5.2 0.60 1.00
Trichlorofluoromethane ND 52 0.39 1.00
1,3,5-Trimethylbenzene ND 5.2 0.57 1.00
Vinyl Acetate ND 52 4.9 1.00
Vinyl Chloride ND 5.2 0.52 1.00
p/m-Xylene ND 5.2 0.28 1.00
o-Xylene ND 5.2 0.57 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.2 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 94 60-132
Dibromofluoromethane 94 63-141
1,2-Dichloroethane-d4 94 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 12 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-14-314-571 N/A Solid GC/MS BB 06/30/16 06/30/16 09:55
160630L003
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 13 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 95 60-132
Dibromofluoromethane 100 63-141
1,2-Dichloroethane-d4 105 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 14 of14
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2175-31 Sample Solid HPLC 5 07/02/16 07/06/16 12:01 160702S06 16-06-2175-31 Matrix Spike Solid HPLC 5 07/02/16 07/06/16 19:06 160702S06 16-06-2175-31 Matrix Spike Duplicate Solid HPLC 5 07/02/16 07/06/16 19:38 160702S06 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Naphthalene ND 100.0 91.88 92 84.31 84 23-167 9 0-46
Acenaphthylene ND 100.0 85.70 86 76.37 76 24-120 12 0-47 Acenaphthene ND 100.0 80.70 81 71.95 72 16-120 11 0-46
Fluorene ND 100.0 72.76 73 67.08 67 32-120 8 0-44
Phenanthrene ND 100.0 70.62 71 65.40 65 34-120 8 0-38
Anthracene ND 100.0 69.44 69 64.42 64 27-120 8 0-45
Fluoranthene ND 100.0 60.43 60 56.64 57 32-122 6 0-41
Pyrene ND 100.0 56.63 57 50.54 51 31-127 11 0-38
Benzo (a) Anthracene ND 100.0 21.01 21 8.489 8 32-122 85 0-43 3,4 Chrysene ND 100.0 67.53 68 63.16 63 30-132 7 0-42
Benzo (b) Fluoranthene 15.17 100.0 98.38 83 65.26 50 33-120 40 0-44 Benzo (k) Fluoranthene 31.49 100.0 60.33 29 67.32 36 23-149 11 0-44 Benzo (a) Pyrene 15.48 100.0 112.6 97 97.57 82 12-132 14 0-48 Dibenz (a,h) Anthracene 188.1 100.0 268.1 80 183.3 0 29-125 38 0-43 3 Benzo (g,h,i) Perylene 18.28 100.0 95.51 77 64.44 46 24-132 39 0-42 Indeno (1,2,3-c,d) Pyrene 332.6 100.0 322.3 0 237.9 0 29-143 30 0-42 3 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8310
Project: UTAS - Due Diligence / 43559 Page 1 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2032-8 Sample Solid GC 49 06/30/16 06/30/16 17:31 160630S05 16-06-2032-8 Matrix Spike Solid GC 49 06/30/16 06/30/16 16:21 160630S05 16-06-2032-8 Matrix Spike Duplicate Solid GC 49 06/30/16 06/30/16 16:38 160630S05 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
TPH as Diesel ND 400.0 313.7 78 331.1 83 64-130 5 0-15
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Project: UTAS - Due Diligence / 43559 Page 2 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-1 Sample Concrete ICP 7300 07/02/16 07/05/16 15:34 160702S01 16-06-2029-1 Matrix Spike Concrete ICP 7300 07/02/16 07/05/16 15:35 160702S01 16-06-2029-1 Matrix Spike Duplicate Concrete ICP 7300 07/02/16 07/05/16 15:36 160702S01 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Antimony ND 25.00 3.093 12 4.345 17 50-115 34 0-20 3,4
Arsenic 9.119 25.00 38.33 117 36.34 109 75-125 5 0-20
Barium 151.1 25.00 173.0 4X 173.5 4X 75-125 4X 0-20 Q
Beryllium 0.2746 25.00 27.12 107 28.10 111 75-125 4 0-20 Cadmium ND 25.00 24.61 98 25.29 101 75-125 3 0-20
Chromium 23.99 25.00 50.31 105 51.05 108 75-125 1 0-20
Cobalt 3.240 25.00 27.48 97 28.27 100 75-125 3 0-20
Copper 17.64 25.00 43.27 103 43.61 104 75-125 1 0-20
Lead 1.316 25.00 26.35 100 26.93 102 75-125 2 0-20
Molybdenum 1.885 25.00 27.03 101 27.73 103 75-125 3 0-20 Nickel 5.520 25.00 30.61 100 30.90 102 75-125 1 0-20
Selenium 1.199 25.00 25.62 98 29.12 112 75-125 13 0-20
Silver 0.3734 12.50 13.95 109 14.41 112 75-125 3 0-20
Thallium ND 25.00 14.42 58 16.15 65 75-125 11 0-20 3
Vanadium 18.77 25.00 43.06 97 42.71 96 75-125 1 0-20
Zinc 40.54 25.00 66.09 102 68.68 113 75-125 4 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 3 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-10 Sample Aqueous ICP 7300 06/30/16 07/01/16 13:00 160630SA2 16-06-2029-10 Matrix Spike Aqueous ICP 7300 06/30/16 07/01/16 13:02 160630SA2 16-06-2029-10 Matrix Spike Duplicate Aqueous ICP 7300 06/30/16 07/01/16 13:03 160630SA2 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Antimony ND 0.5000 0.5226 105 0.5360 107 75-125 3 0-20
Arsenic ND 0.5000 0.5284 106 0.5320 106 75-125 1 0-20
Barium 0.02259 0.5000 0.5364 103 0.5367 103 75-125 0 0-20 Beryllium ND 0.5000 0.5139 103 0.5169 103 75-125 1 0-20 Cadmium ND 0.5000 0.5197 104 0.5262 105 75-125 1 0-20
Chromium ND 0.5000 0.5098 102 0.5176 104 75-125 2 0-20
Cobalt ND 0.5000 0.5358 107 0.5441 109 75-125 2 0-20
Copper ND 0.5000 0.5309 106 0.5374 107 75-125 1 0-20
Lead ND 0.5000 0.4982 100 0.5074 101 75-125 2 0-20
Molybdenum 0.02077 0.5000 0.5355 103 0.5498 106 75-125 3 0-20 Nickel ND 0.5000 0.5063 101 0.5163 103 75-125 2 0-20
Selenium ND 0.5000 0.5189 104 0.5145 103 75-125 1 0-20
Silver ND 0.2500 0.2597 104 0.2590 104 75-125 0 0-20
Thallium ND 0.5000 0.5004 100 0.5071 101 75-125 1 0-20
Vanadium 0.05304 0.5000 0.5661 103 0.5756 105 75-125 2 0-20 Zinc 0.01178 0.5000 0.5634 110 0.5672 111 75-125 1 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3005A Filt.
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 4 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2033-10 Sample Aqueous Mercury 04 07/06/16 07/06/16 15:19 160706SA1 16-06-2033-10 Matrix Spike Aqueous Mercury 04 07/06/16 07/06/16 15:21 160706SA1 16-06-2033-10 Matrix Spike Duplicate Aqueous Mercury 04 07/06/16 07/06/16 15:23 160706SA1 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Mercury ND 0.01000 0.009027 90 0.009054 91 75-125 0 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7470A Filt.
Method: EPA 7470A
Project: UTAS - Due Diligence / 43559 Page 5 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-1 Sample Concrete Mercury 05 07/06/16 07/06/16 15:32 160706S02 16-06-2029-1 Matrix Spike Concrete Mercury 05 07/06/16 07/06/16 15:34 160706S02 16-06-2029-1 Matrix Spike Duplicate Concrete Mercury 05 07/06/16 07/06/16 15:36 160706S02 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Mercury ND 0.8350 1.007 121 0.9381 112 75-125 7 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559 Page 6 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2036-1 Sample Solid GC 41 07/05/16 07/08/16 12:16 160705S04 16-06-2036-1 Matrix Spike Solid GC 41 07/05/16 07/08/16 11:46 160705S04 16-06-2036-1 Matrix Spike Duplicate Solid GC 41 07/05/16 07/08/16 12:01 160705S04 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Aldrin ND 25.00 22.96 92 21.95 88 50-135 5 0-25
Alpha-BHC ND 25.00 22.33 89 21.77 87 50-135 3 0-25
Beta-BHC ND 25.00 23.32 93 21.50 86 50-135 8 0-25
4,4'-DDD ND 25.00 26.29 105 25.09 100 50-135 5 0-25
4,4'-DDE ND 25.00 25.85 103 24.52 98 50-135 5 0-25
4,4'-DDT ND 25.00 25.24 101 24.05 96 50-135 5 0-25
Delta-BHC ND 25.00 25.22 101 23.53 94 50-135 7 0-25
Dieldrin ND 25.00 25.48 102 23.80 95 50-135 7 0-25
Endosulfan I ND 25.00 24.07 96 22.98 92 50-135 5 0-25
Endosulfan II ND 25.00 26.14 105 24.52 98 50-135 6 0-25 Endosulfan Sulfate ND 25.00 24.08 96 22.94 92 50-135 5 0-25 Endrin ND 25.00 29.00 116 27.75 111 50-135 4 0-25
Endrin Aldehyde ND 25.00 23.39 94 22.68 91 50-135 3 0-25 Gamma-BHC ND 25.00 23.44 94 22.65 91 50-135 3 0-25
Heptachlor ND 25.00 24.03 96 23.35 93 50-135 3 0-25
Heptachlor Epoxide ND 25.00 23.96 96 22.95 92 50-135 4 0-25 Methoxychlor ND 25.00 25.40 102 25.27 101 50-135 1 0-25 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8081A
Project: UTAS - Due Diligence / 43559 Page 7 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2029-2 Sample Solid GC 58 07/05/16 07/07/16 15:37 160705S08 16-06-2029-2 Matrix Spike Solid GC 58 07/05/16 07/07/16 14:07 160705S08 16-06-2029-2 Matrix Spike Duplicate Solid GC 58 07/05/16 07/07/16 14:25 160705S08 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Aroclor-1016 ND 100.0 91.50 92 77.00 77 50-135 17 0-20
Aroclor-1260 ND 100.0 98.00 98 83.50 84 50-135 16 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8082
Project: UTAS - Due Diligence / 43559 Page 8 of13
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-1543-12 Sample Aqueous GC/MS L 06/29/16 06/29/16 12:19 160629S007 16-06-1543-12 Matrix Spike Aqueous GC/MS L 06/29/16 06/29/16 13:53 160629S007 16-06-1543-12 Matrix Spike Duplicate Aqueous GC/MS L 06/29/16 06/29/16 14:24 160629S007 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acetone ND 10.00 11.74 117 11.88 119 51-163 1 0-82
Benzene ND 10.00 10.16 102 10.15 102 77-121 0 0-21
Bromobenzene ND 10.00 10.35 104 10.39 104 78-120 0 0-20 Bromochloromethane ND 10.00 10.17 102 10.31 103 71-135 1 0-28 Bromodichloromethane ND 10.00 10.35 103 10.36 104 72-129 0 0-26 Bromoform ND 10.00 9.546 95 9.841 98 61-140 3 0-22
Bromomethane ND 10.00 10.66 107 10.54 105 63-140 1 0-36 2-Butanone ND 10.00 10.28 103 10.46 105 55-138 2 0-45
n-Butylbenzene ND 10.00 11.32 113 11.35 114 67-127 0 0-26 sec-Butylbenzene ND 10.00 11.02 110 10.94 109 66-122 1 0-26 tert-Butylbenzene ND 10.00 10.84 108 10.75 108 73-120 1 0-26 Carbon Disulfide ND 10.00 8.722 87 9.757 98 27-170 11 0-36 Carbon Tetrachloride ND 10.00 10.05 101 10.56 106 64-135 5 0-31 Chlorobenzene ND 10.00 10.11 101 10.26 103 80-120 1 0-20 Chloroethane ND 10.00 11.45 115 11.07 111 67-131 3 0-35 2-Chloroethyl Vinyl Ether ND 10.00 0.8532 9 0.5528 6 60-139 43 0-90 3 Chloroform ND 10.00 10.57 106 10.46 105 75-126 1 0-20
Chloromethane ND 10.00 11.05 110 10.66 107 54-143 4 0-41 2-Chlorotoluene ND 10.00 10.64 106 10.59 106 64-123 0 0-34 4-Chlorotoluene ND 10.00 10.59 106 10.68 107 67-126 1 0-23 Dibromochloromethane ND 10.00 9.774 98 9.916 99 76-132 1 0-23 1,2-Dibromo-3-Chloropropane ND 10.00 9.577 96 9.838 98 65-125 3 0-31 1,2-Dibromoethane ND 10.00 9.761 98 10.03 100 74-130 3 0-22 Dibromomethane ND 10.00 9.911 99 9.887 99 75-127 0 0-29 1,2-Dichlorobenzene ND 10.00 10.36 104 10.33 103 78-120 0 0-19 1,3-Dichlorobenzene ND 10.00 10.42 104 10.19 102 75-120 2 0-22 1,4-Dichlorobenzene ND 10.00 10.04 100 10.22 102 78-120 2 0-21 Dichlorodifluoromethane ND 10.00 11.94 119 11.08 111 25-168 8 0-41 1,1-Dichloroethane ND 10.00 10.62 106 10.17 102 63-144 4 0-32 1,2-Dichloroethane ND 10.00 9.950 100 10.21 102 72-130 3 0-25 1,1-Dichloroethene ND 10.00 10.53 105 10.29 103 66-130 2 0-32 c-1,2-Dichloroethene ND 10.00 10.54 105 10.33 103 76-123 2 0-32 t-1,2-Dichloroethene ND 10.00 9.698 97 10.62 106 67-129 9 0-35 Acetonitrile ND 20.00 16.55 83 19.77 99 70-130 18 0-35
1,2-Dichloropropane ND 10.00 10.23 102 10.42 104 74-122 2 0-24 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 9 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acrolein ND 20.00 23.33 117 22.96 115 70-130 2 0-35
Acrylonitrile ND 10.00 8.277 83 10.22 102 65-149 21 0-89 1,3-Dichloropropane ND 10.00 9.987 100 10.03 100 74-128 0 0-21 2,2-Dichloropropane ND 10.00 11.16 112 11.09 111 68-125 1 0-40 Allyl Chloride ND 10.00 8.716 87 9.516 95 70-130 9 0-35 1,1-Dichloropropene ND 10.00 10.25 103 10.48 105 68-119 2 0-26 c-1,3-Dichloropropene ND 10.00 9.948 99 9.989 100 76-126 0 0-24 t-1,3-Dichloropropene ND 10.00 10.02 100 10.02 100 71-127 0 0-22 Ethylbenzene ND 10.00 10.67 107 10.54 105 78-120 1 0-23 2-Hexanone ND 10.00 9.637 96 10.39 104 61-137 8 0-36
Isopropylbenzene ND 10.00 10.87 109 10.78 108 71-123 1 0-24 p-Isopropyltoluene ND 10.00 11.39 114 11.59 116 68-122 2 0-25 Methylene Chloride ND 10.00 9.550 96 10.46 105 71-129 9 0-30 4-Methyl-2-Pentanone ND 10.00 9.456 95 9.934 99 60-136 5 0-41 Naphthalene ND 10.00 10.35 104 10.72 107 55-159 3 0-30
n-Propylbenzene ND 10.00 10.87 109 10.75 107 64-125 1 0-35 Styrene ND 10.00 10.68 107 10.79 108 77-120 1 0-23
Chloroprene ND 10.00 10.93 109 10.51 105 70-130 4 0-35
1,1,1,2-Tetrachloroethane ND 10.00 10.35 104 10.36 104 79-123 0 0-20 1,1,2,2-Tetrachloroethane ND 10.00 9.976 100 10.12 101 67-132 1 0-25 Tetrachloroethene ND 10.00 9.576 96 9.480 95 72-119 1 0-24 Toluene ND 10.00 10.43 104 10.39 104 78-120 0 0-25
1,2,3-Trichlorobenzene ND 10.00 10.22 102 10.36 104 70-129 1 0-27 Ethyl Methacrylate ND 10.00 9.956 100 10.13 101 70-130 2 0-35 1,2,4-Trichlorobenzene ND 10.00 10.30 103 10.44 104 71-128 1 0-26 1,1,1-Trichloroethane ND 10.00 10.24 102 10.55 105 66-130 3 0-30 Hexachloro-1,3-Butadiene ND 10.00 11.67 117 11.45 115 52-128 2 0-30 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10.00 11.62 116 11.35 113 52-145 2 0-35 1,1,2-Trichloroethane ND 10.00 9.952 100 9.959 100 77-124 0 0-25 Iodomethane ND 20.00 17.58 88 18.93 95 70-130 7 0-35
Trichloroethene 2.601 10.00 12.51 99 12.49 99 75-116 0 0-24 Trichlorofluoromethane ND 10.00 11.94 119 11.48 115 62-146 4 0-36 Isobutyl Alcohol ND 20.00 15.57 78 14.49 72 70-130 7 0-35 1,2,3-Trichloropropane ND 10.00 10.08 101 10.49 105 80-120 4 0-20 1,2,4-Trimethylbenzene ND 10.00 11.31 113 11.36 114 70-127 1 0-23 Methacrylonitrile ND 10.00 9.128 91 9.625 96 70-130 5 0-35 Methyl Methacrylate ND 10.00 9.504 95 9.867 99 70-130 4 0-35 1,3,5-Trimethylbenzene ND 10.00 11.20 112 11.21 112 72-124 0 0-23 Vinyl Acetate ND 10.00 7.621 76 9.153 92 45-164 18 0-74 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 10 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Vinyl Chloride ND 10.00 11.76 118 11.26 113 60-141 4 0-34 p/m-Xylene ND 20.00 21.42 107 21.27 106 74-122 1 0-23
o-Xylene ND 10.00 10.75 107 10.74 107 74-122 0 0-24
Methyl-t-Butyl Ether (MTBE) ND 10.00 9.430 94 10.28 103 57-144 9 0-31 t-1,4-Dichloro-2-Butene ND 10.00 9.896 99 10.24 102 70-130 3 0-35 Tetrahydrofuran ND 10.00 9.481 95 9.641 96 70-130 2 0-35 Propionitrile ND 10.00 9.682 97 10.38 104 70-130 7 0-35 Tert-Butyl Alcohol (TBA) ND 50.00 59.30 119 52.60 105 43-170 12 0-38 Diisopropyl Ether (DIPE) ND 10.00 10.77 108 9.933 99 70-130 8 0-35 Ethyl-t-Butyl Ether (ETBE) ND 10.00 10.06 101 9.893 99 70-130 2 0-35 Tert-Amyl-Methyl Ether (TAME) ND 10.00 9.197 92 9.550 95 70-130 4 0-35 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 11 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2035-1 Sample Solid GC/MS BB 06/29/16 06/30/16 12:43 160630S002 16-06-2035-1 Matrix Spike Solid GC/MS BB 06/29/16 06/30/16 11:22 160630S002 16-06-2035-1 Matrix Spike Duplicate Solid GC/MS BB 06/29/16 06/30/16 11:49 160630S002 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acetone ND 50.00 45.05 90 46.69 93 70-130 4 0-20
Benzene ND 50.00 35.96 72 39.37 79 61-127 9 0-20
Bromobenzene ND 50.00 40.25 80 44.61 89 70-130 10 0-20
Bromochloromethane ND 50.00 37.16 74 40.69 81 70-130 9 0-20 Bromodichloromethane ND 50.00 41.03 82 46.19 92 70-130 12 0-20 Bromoform ND 50.00 40.73 81 45.68 91 70-130 11 0-20
Bromomethane ND 50.00 44.98 90 43.81 88 70-130 3 0-20
2-Butanone ND 50.00 42.42 85 45.88 92 70-130 8 0-20
n-Butylbenzene ND 50.00 38.82 78 42.62 85 77-123 9 0-25 sec-Butylbenzene ND 50.00 38.98 78 42.32 85 70-130 8 0-20 tert-Butylbenzene ND 50.00 39.10 78 43.11 86 70-130 10 0-20 Carbon Disulfide ND 50.00 27.77 56 30.81 62 70-130 10 0-20 3 Carbon Tetrachloride ND 50.00 39.84 80 44.51 89 51-135 11 0-29 Chlorobenzene ND 50.00 37.60 75 42.54 85 57-123 12 0-20 Chloroethane ND 50.00 48.52 97 45.77 92 70-130 6 0-20
Chloroform ND 50.00 39.77 80 43.31 87 70-130 9 0-20
Chloromethane ND 50.00 36.09 72 35.37 71 70-130 2 0-20
2-Chlorotoluene ND 50.00 39.93 80 44.03 88 70-130 10 0-20 4-Chlorotoluene ND 50.00 39.29 79 43.20 86 70-130 9 0-20 Dibromochloromethane ND 50.00 40.90 82 45.95 92 70-130 12 0-20 1,2-Dibromo-3-Chloropropane ND 50.00 44.54 89 48.09 96 70-130 8 0-20 1,2-Dibromoethane ND 50.00 39.97 80 45.47 91 64-124 13 0-20 Dibromomethane ND 50.00 40.33 81 43.70 87 70-130 8 0-20 1,2-Dichlorobenzene ND 50.00 40.17 80 43.20 86 35-131 7 0-25 1,3-Dichlorobenzene ND 50.00 39.56 79 42.66 85 70-130 8 0-20 1,4-Dichlorobenzene ND 50.00 39.07 78 42.35 85 70-130 8 0-20 Dichlorodifluoromethane ND 50.00 31.57 63 30.23 60 70-130 4 0-20 3 1,1-Dichloroethane ND 50.00 38.55 77 42.69 85 70-130 10 0-20 1,2-Dichloroethane ND 50.00 38.89 78 42.16 84 70-130 8 0-20 1,1-Dichloroethene ND 50.00 34.79 70 38.39 77 47-143 10 0-25 c-1,2-Dichloroethene ND 50.00 36.66 73 40.78 82 70-130 11 0-20 t-1,2-Dichloroethene ND 50.00 35.49 71 38.79 78 70-130 9 0-20 1,2-Dichloropropane ND 50.00 39.24 78 43.33 87 79-115 10 0-25 3 1,3-Dichloropropane ND 50.00 39.64 79 43.42 87 70-130 9 0-20 2,2-Dichloropropane ND 50.00 39.13 78 43.66 87 70-130 11 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 12 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
1,1-Dichloropropene ND 50.00 35.90 72 38.92 78 70-130 8 0-20 c-1,3-Dichloropropene ND 50.00 38.85 78 42.86 86 70-130 10 0-20 t-1,3-Dichloropropene ND 50.00 41.20 82 46.32 93 70-130 12 0-20 Ethylbenzene ND 50.00 37.96 76 42.50 85 57-129 11 0-22
2-Hexanone ND 50.00 41.66 83 46.94 94 70-130 12 0-20
Isopropylbenzene ND 50.00 39.30 79 44.27 89 70-130 12 0-20 p-Isopropyltoluene ND 50.00 39.56 79 43.06 86 70-130 8 0-20 Methylene Chloride ND 50.00 37.69 75 41.82 84 70-130 10 0-20 4-Methyl-2-Pentanone ND 50.00 41.63 83 46.18 92 70-130 10 0-20 Naphthalene ND 50.00 40.92 82 45.49 91 70-130 11 0-20
n-Propylbenzene ND 50.00 38.55 77 43.20 86 70-130 11 0-20 Styrene ND 50.00 39.38 79 44.41 89 70-130 12 0-20
1,1,1,2-Tetrachloroethane ND 50.00 42.69 85 48.88 98 70-130 14 0-20 1,1,2,2-Tetrachloroethane ND 50.00 41.29 83 45.17 90 70-130 9 0-20 Tetrachloroethene ND 50.00 37.04 74 45.44 91 70-130 20 0-20 Toluene ND 50.00 36.71 73 40.53 81 63-123 10 0-20
1,2,3-Trichlorobenzene ND 50.00 41.04 82 44.60 89 70-130 8 0-20 1,2,4-Trichlorobenzene ND 50.00 40.73 81 44.26 89 70-130 8 0-20 1,1,1-Trichloroethane ND 50.00 39.01 78 43.55 87 70-130 11 0-20 1,1,2-Trichloroethane ND 50.00 39.82 80 44.36 89 70-130 11 0-20 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50.00 36.58 73 40.85 82 70-130 11 0-20 Trichloroethene ND 50.00 37.57 75 41.37 83 44-158 10 0-20 1,2,3-Trichloropropane ND 50.00 43.76 88 48.76 98 70-130 11 0-20 1,2,4-Trimethylbenzene ND 50.00 38.35 77 41.88 84 70-130 9 0-20 Trichlorofluoromethane ND 50.00 47.14 94 44.61 89 70-130 6 0-20 1,3,5-Trimethylbenzene ND 50.00 39.66 79 44.39 89 70-130 11 0-20 Vinyl Acetate ND 50.00 33.91 68 36.83 74 70-130 8 0-20 3 Vinyl Chloride ND 50.00 42.77 86 40.89 82 49-139 5 0-47 p/m-Xylene ND 100.0 76.11 76 85.38 85 70-130 11 0-20
o-Xylene ND 50.00 39.05 78 43.78 88 70-130 11 0-20
Methyl-t-Butyl Ether (MTBE) ND 50.00 39.96 80 44.15 88 57-123 10 0-21 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 13 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
16-06-2029-1 Sample Concrete ICP 7300 07/02/16 00:00 07/05/16 15:34 160702S01 16-06-2029-1 PDS Concrete ICP 7300 07/02/16 00:00 07/05/16 15:37 160702S01 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Antimony ND 25.00 21.99 88 75-125
Arsenic 9.119 25.00 36.10 108 75-125
Barium 151.1 25.00 177.5 4X 75-125 Q
Beryllium 0.2746 25.00 26.81 106 75-125
Cadmium ND 25.00 23.90 96 75-125
Chromium 23.99 25.00 49.40 102 75-125
Cobalt 3.240 25.00 26.73 94 75-125
Copper 17.64 25.00 43.28 103 75-125
Lead 1.316 25.00 25.59 97 75-125
Molybdenum 1.885 25.00 26.84 100 75-125
Nickel 5.520 25.00 30.14 98 75-125
Selenium 1.199 25.00 28.36 109 75-125
Silver 0.3734 12.50 13.79 107 75-125
Thallium ND 25.00 23.80 95 75-125
Vanadium 18.77 25.00 44.17 102 75-125
Zinc 40.54 25.00 64.98 98 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 1 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
16-06-2029-10 Sample Aqueous ICP 7300 06/30/16 00:00 07/01/16 13:00 160630SA2 16-06-2029-10 PDS Aqueous ICP 7300 06/30/16 00:00 07/01/16 13:04 160630SA2 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Antimony ND 0.5000 0.5056 101 75-125
Arsenic ND 0.5000 0.5028 101 75-125
Barium 0.02259 0.5000 0.5211 100 75-125
Beryllium ND 0.5000 0.4994 100 75-125
Cadmium ND 0.5000 0.5080 102 75-125
Chromium ND 0.5000 0.4975 99 75-125
Cobalt ND 0.5000 0.5163 103 75-125
Copper ND 0.5000 0.5165 103 75-125
Lead ND 0.5000 0.4830 97 75-125
Molybdenum 0.02077 0.5000 0.5206 100 75-125
Nickel ND 0.5000 0.4890 98 75-125
Selenium ND 0.5000 0.4911 98 75-125
Silver ND 0.2500 0.2516 101 75-125
Thallium ND 0.5000 0.4828 97 75-125
Vanadium 0.05304 0.5000 0.5554 100 75-125
Zinc 0.01178 0.5000 0.5512 108 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3005A Filt.
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 2 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
16-06-2033-10 Sample Aqueous Mercury 04 07/06/16 00:00 07/06/16 15:19 160706SA1 16-06-2033-10 PDS Aqueous Mercury 04 07/06/16 00:00 07/06/16 15:50 160706SA1 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Mercury ND 0.01000 0.008861 89 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7470A Filt.
Method: EPA 7470A
Project: UTAS - Due Diligence / 43559 Page 3 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
16-06-2029-1 Sample Concrete Mercury 05 07/06/16 00:00 07/06/16 15:32 160706S02 16-06-2029-1 PDS Concrete Mercury 05 07/06/16 00:00 07/07/16 11:39 160706S02 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Mercury ND 0.8350 0.8524 102 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559 Page 4 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Duplicate Batch Number BB-17-01 Sample Solid N/A 06/29/16 00:00 06/29/16 19:00 G0629MOID4 BB-17-01 Sample Duplicate Solid N/A 06/29/16 00:00 06/29/16 19:00 G0629MOID4 Parameter Sample Conc. DUP Conc. RPD RPD CL Qualifiers
Moisture 3.500 3.400 3 0-10
Quality Control - Sample Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: N/A
Method: ASTM D-2216 (M)
Project: UTAS - Due Diligence / 43559 Page 1 of1
RPD: Relative Percent Difference. CL: Control Limits
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Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-07-002-1879 LCS Solid HPLC 5 07/02/16 07/05/16 17:34 160702L06 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Naphthalene 100.0 111.0 111 17-203 0-234
Acenaphthylene 100.0 74.49 74 50-120 38-132
Acenaphthene 100.0 67.86 68 41-120 28-133
Fluorene 100.0 68.67 69 51-120 40-132
Phenanthrene 100.0 72.34 72 56-120 45-131
Anthracene 100.0 68.27 68 49-120 37-132
Fluoranthene 100.0 76.06 76 60-120 50-130
Pyrene 100.0 84.09 84 61-121 51-131
Benzo (a) Anthracene 100.0 82.09 82 61-121 51-131
Chrysene 100.0 79.59 80 61-121 51-131
Benzo (b) Fluoranthene 100.0 78.09 78 61-121 51-131
Benzo (k) Fluoranthene 100.0 73.51 74 57-129 45-141
Benzo (a) Pyrene 100.0 75.84 76 43-120 30-133
Dibenz (a,h) Anthracene 100.0 76.90 77 59-125 48-136
Benzo (g,h,i) Perylene 100.0 83.03 83 57-123 46-134
Indeno (1,2,3-c,d) Pyrene 100.0 79.05 79 64-130 53-141
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8310
Project: UTAS - Due Diligence / 43559 Page 1 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-15-490-2144 LCS Solid GC 49 06/30/16 06/30/16 16:03 160630B05 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers TPH as Diesel 400.0 307.6 77 75-123
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3550B
Method: EPA 8015B (M)
Project: UTAS - Due Diligence / 43559 Page 2 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 097-01-002-22889 LCS Solid ICP 7300 07/02/16 07/05/16 13:22 160702L01U Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Antimony 25.00 24.74 99 80-120 73-127
Arsenic 25.00 24.49 98 80-120 73-127
Barium 25.00 26.41 106 80-120 73-127
Beryllium 25.00 24.22 97 80-120 73-127
Cadmium 25.00 25.25 101 80-120 73-127
Chromium 25.00 25.70 103 80-120 73-127
Cobalt 25.00 26.45 106 80-120 73-127
Copper 25.00 25.58 102 80-120 73-127
Lead 25.00 26.36 105 80-120 73-127
Molybdenum 25.00 24.94 100 80-120 73-127
Nickel 25.00 26.86 107 80-120 73-127
Selenium 25.00 23.47 94 80-120 73-127
Silver 12.50 12.44 100 80-120 73-127
Thallium 25.00 26.17 105 80-120 73-127
Vanadium 25.00 24.31 97 80-120 73-127
Zinc 25.00 26.06 104 80-120 73-127
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 3 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-460-98 LCS Aqueous ICP 7300 06/30/16 07/01/16 12:29 160630LA2U Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Antimony 0.5000 0.4709 94 80-120 73-127
Arsenic 0.5000 0.4486 90 80-120 73-127
Barium 0.5000 0.4910 98 80-120 73-127
Beryllium 0.5000 0.4458 89 80-120 73-127
Cadmium 0.5000 0.4796 96 80-120 73-127
Chromium 0.5000 0.4805 96 80-120 73-127
Cobalt 0.5000 0.5087 102 80-120 73-127
Copper 0.5000 0.4784 96 80-120 73-127
Lead 0.5000 0.4913 98 80-120 73-127
Molybdenum 0.5000 0.4732 95 80-120 73-127
Nickel 0.5000 0.4797 96 80-120 73-127
Selenium 0.5000 0.4394 88 80-120 73-127
Silver 0.2500 0.2368 95 80-120 73-127
Thallium 0.5000 0.4896 98 80-120 73-127
Vanadium 0.5000 0.4589 92 80-120 73-127
Zinc 0.5000 0.4847 97 80-120 73-127
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3005A Filt.
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559 Page 4 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-456-3 LCS Aqueous Mercury 04 07/06/16 07/06/16 15:16 160706LA1F Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers Mercury 0.01000 0.01003 100 80-120
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7470A Filt.
Method: EPA 7470A
Project: UTAS - Due Diligence / 43559 Page 5 of13
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-480-44 LCS Solid Mercury 05 07/06/16 07/06/16 15:29 160706L02 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers Mercury 0.8350 0.9333 112 80-120
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559 Page 6 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 17
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-12-537-2463 LCS Solid GC 41 07/05/16 07/08/16 13:31 160705L04 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Aldrin 25.00 21.00 84 50-135 36-149
Alpha-BHC 25.00 20.87 83 50-135 36-149
Beta-BHC 25.00 21.05 84 50-135 36-149
4,4'-DDD 25.00 26.47 106 50-135 36-149
4,4'-DDE 25.00 23.99 96 50-135 36-149
4,4'-DDT 25.00 26.34 105 50-135 36-149
Delta-BHC 25.00 23.55 94 50-135 36-149
Dieldrin 25.00 23.98 96 50-135 36-149
Endosulfan I 25.00 22.01 88 50-135 36-149
Endosulfan II 25.00 27.68 111 50-135 36-149
Endosulfan Sulfate 25.00 27.28 109 50-135 36-149
Endrin 25.00 26.76 107 50-135 36-149
Endrin Aldehyde 25.00 25.67 103 50-135 36-149
Gamma-BHC 25.00 21.41 86 50-135 36-149
Heptachlor 25.00 22.91 92 50-135 36-149
Heptachlor Epoxide 25.00 22.78 91 50-135 36-149
Methoxychlor 25.00 30.50 122 50-135 36-149
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8081A
Project: UTAS - Due Diligence / 43559 Page 7 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-12-535-3813 LCS Solid GC 58 07/05/16 07/07/16 13:49 160705L08 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers Aroclor-1016 100.0 99.00 99 50-135
Aroclor-1260 100.0 91.00 91 50-135
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 3545
Method: EPA 8082
Project: UTAS - Due Diligence / 43559 Page 8 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-446-105 LCS Aqueous GC/MS L 06/29/16 06/29/16 09:49 160629L007 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Acetone 10.00 7.899 79 51-163 32-182
Benzene 10.00 9.933 99 77-121 70-128
Bromobenzene 10.00 9.753 98 78-120 71-127
Bromochloromethane 10.00 9.752 98 71-135 60-146
Bromodichloromethane 10.00 10.10 101 72-129 62-138
Bromoform 10.00 10.16 102 61-140 48-153
Bromomethane 10.00 9.643 96 63-140 50-153
2-Butanone 10.00 8.586 86 55-138 41-152
n-Butylbenzene 10.00 10.75 108 67-127 57-137
sec-Butylbenzene 10.00 10.70 107 66-122 57-131
tert-Butylbenzene 10.00 10.48 105 73-120 65-128
Carbon Disulfide 10.00 10.27 103 27-170 3-194
Carbon Tetrachloride 10.00 10.68 107 64-135 52-147
Chlorobenzene 10.00 9.780 98 80-120 73-127
Chloroethane 10.00 9.801 98 67-131 56-142
2-Chloroethyl Vinyl Ether 10.00 8.017 80 60-139 47-152
Chloroform 10.00 9.652 97 75-126 66-134
Chloromethane 10.00 8.904 89 54-143 39-158
2-Chlorotoluene 10.00 10.10 101 64-123 54-133
4-Chlorotoluene 10.00 10.18 102 67-126 57-136
Dibromochloromethane 10.00 9.944 99 76-132 67-141
1,2-Dibromo-3-Chloropropane 10.00 8.819 88 65-125 55-135 1,2-Dibromoethane 10.00 9.358 94 74-130 65-139
Dibromomethane 10.00 9.141 91 75-127 66-136
1,2-Dichlorobenzene 10.00 9.775 98 78-120 71-127
1,3-Dichlorobenzene 10.00 9.981 100 75-120 68-128
1,4-Dichlorobenzene 10.00 9.745 97 78-120 71-127
Dichlorodifluoromethane 10.00 10.26 103 25-168 1-192
1,1-Dichloroethane 10.00 10.17 102 63-144 50-158
1,2-Dichloroethane 10.00 9.141 91 72-130 62-140
1,1-Dichloroethene 10.00 9.924 99 66-130 55-141
c-1,2-Dichloroethene 10.00 10.03 100 76-123 68-131
t-1,2-Dichloroethene 10.00 10.50 105 67-129 57-139
Acetonitrile 20.00 20.18 101 70-130 60-140
1,2-Dichloropropane 10.00 9.933 99 74-122 66-130
Acrolein 20.00 19.97 100 70-130 60-140
Acrylonitrile 10.00 8.527 85 65-149 51-163
1,3-Dichloropropane 10.00 9.231 92 74-128 65-137
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 9 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers 2,2-Dichloropropane 10.00 11.34 113 68-125 58-134
Allyl Chloride 10.00 10.15 101 70-130 60-140
1,1-Dichloropropene 10.00 10.06 101 68-119 60-128
c-1,3-Dichloropropene 10.00 10.15 102 76-126 68-134
t-1,3-Dichloropropene 10.00 10.06 101 71-127 62-136
Ethylbenzene 10.00 10.25 102 78-120 71-127
2-Hexanone 10.00 8.384 84 61-137 48-150
Isopropylbenzene 10.00 10.36 104 71-123 62-132
p-Isopropyltoluene 10.00 10.90 109 68-122 59-131
Methylene Chloride 10.00 9.785 98 71-129 61-139
4-Methyl-2-Pentanone 10.00 8.251 83 60-136 47-149
Naphthalene 10.00 8.975 90 55-159 38-176
n-Propylbenzene 10.00 10.34 103 64-125 54-135
Styrene 10.00 10.01 100 77-120 70-127
Chloroprene 10.00 10.65 106 70-130 60-140
1,1,1,2-Tetrachloroethane 10.00 10.74 107 79-123 72-130 1,1,2,2-Tetrachloroethane 10.00 8.972 90 67-132 56-143
Tetrachloroethene 10.00 9.873 99 72-119 64-127
Toluene 10.00 10.11 101 78-120 71-127
1,2,3-Trichlorobenzene 10.00 9.135 91 70-129 60-139
Ethyl Methacrylate 10.00 8.650 86 70-130 60-140
1,2,4-Trichlorobenzene 10.00 9.776 98 71-128 62-138
1,1,1-Trichloroethane 10.00 9.944 99 66-130 55-141
Hexachloro-1,3-Butadiene 10.00 11.21 112 52-128 39-141
1,1,2-Trichloro-1,2,2-Trifluoroethane 10.00 11.23 112 52-145 36-160 1,1,2-Trichloroethane 10.00 9.087 91 77-124 69-132
Iodomethane 20.00 21.56 108 70-130 60-140
Trichloroethene 10.00 10.11 101 75-116 68-123
Trichlorofluoromethane 10.00 10.30 103 62-146 48-160
Isobutyl Alcohol 20.00 11.98 60 70-130 60-140 ME
1,2,3-Trichloropropane 10.00 9.192 92 80-120 73-127
1,2,4-Trimethylbenzene 10.00 10.32 103 70-127 60-136
Methacrylonitrile 10.00 8.606 86 70-130 60-140
Methyl Methacrylate 10.00 8.555 86 70-130 60-140
1,3,5-Trimethylbenzene 10.00 10.42 104 72-124 63-133
Vinyl Acetate 10.00 8.130 81 45-164 25-184
Vinyl Chloride 10.00 9.833 98 60-141 46-154
p/m-Xylene 20.00 20.53 103 74-122 66-130
o-Xylene 10.00 10.20 102 74-122 66-130
Methyl-t-Butyl Ether (MTBE) 10.00 9.055 91 57-144 42-158 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 10 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 85
Total number of ME compounds: 1
Total number of ME compounds allowed: 4
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers t-1,4-Dichloro-2-Butene 10.00 9.473 95 70-130 60-140
Tetrahydrofuran 10.00 8.469 85 70-130 60-140
Propionitrile 10.00 8.426 84 70-130 60-140
Tert-Butyl Alcohol (TBA) 50.00 52.59 105 43-170 22-191
Diisopropyl Ether (DIPE) 10.00 10.05 101 70-130 60-140
Ethyl-t-Butyl Ether (ETBE) 10.00 9.513 95 70-130 60-140 Tert-Amyl-Methyl Ether (TAME) 10.00 8.821 88 70-130 60-140 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 11 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-14-314-571 LCS Solid GC/MS BB 06/30/16 06/30/16 08:59 160630L003 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Acetone 50.00 49.99 100 70-130 60-140
Benzene 50.00 40.86 82 78-120 71-127
Bromobenzene 50.00 46.07 92 70-130 60-140
Bromochloromethane 50.00 40.82 82 70-130 60-140
Bromodichloromethane 50.00 46.67 93 70-130 60-140
Bromoform 50.00 45.87 92 70-130 60-140
Bromomethane 50.00 46.08 92 70-130 60-140
2-Butanone 50.00 46.18 92 70-130 60-140
n-Butylbenzene 50.00 45.88 92 77-123 69-131
sec-Butylbenzene 50.00 44.85 90 70-130 60-140
tert-Butylbenzene 50.00 45.52 91 70-130 60-140
Carbon Disulfide 50.00 33.65 67 70-130 60-140 ME
Carbon Tetrachloride 50.00 46.51 93 49-139 34-154
Chlorobenzene 50.00 43.96 88 79-120 72-127
Chloroethane 50.00 49.50 99 70-130 60-140
Chloroform 50.00 44.63 89 70-130 60-140
Chloromethane 50.00 37.72 75 70-130 60-140
2-Chlorotoluene 50.00 46.15 92 70-130 60-140
4-Chlorotoluene 50.00 44.49 89 70-130 60-140
Dibromochloromethane 50.00 47.17 94 70-130 60-140
1,2-Dibromo-3-Chloropropane 50.00 50.26 101 70-130 60-140 1,2-Dibromoethane 50.00 45.45 91 70-130 60-140
Dibromomethane 50.00 43.88 88 70-130 60-140
1,2-Dichlorobenzene 50.00 45.16 90 75-120 68-128
1,3-Dichlorobenzene 50.00 44.55 89 70-130 60-140
1,4-Dichlorobenzene 50.00 44.01 88 70-130 60-140
Dichlorodifluoromethane 50.00 32.37 65 70-130 60-140 ME 1,1-Dichloroethane 50.00 43.61 87 70-130 60-140
1,2-Dichloroethane 50.00 42.57 85 70-130 60-140
1,1-Dichloroethene 50.00 40.12 80 74-122 66-130
c-1,2-Dichloroethene 50.00 42.17 84 70-130 60-140
t-1,2-Dichloroethene 50.00 40.25 80 70-130 60-140
1,2-Dichloropropane 50.00 44.03 88 79-115 73-121
1,3-Dichloropropane 50.00 44.35 89 70-130 60-140
2,2-Dichloropropane 50.00 46.31 93 70-130 60-140
1,1-Dichloropropene 50.00 40.79 82 70-130 60-140
c-1,3-Dichloropropene 50.00 44.26 89 70-130 60-140
t-1,3-Dichloropropene 50.00 47.67 95 70-130 60-140
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 12 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 66
Total number of ME compounds: 2
Total number of ME compounds allowed: 3
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Ethylbenzene 50.00 44.52 89 76-120 69-127
2-Hexanone 50.00 47.98 96 70-130 60-140
Isopropylbenzene 50.00 46.09 92 70-130 60-140
p-Isopropyltoluene 50.00 45.40 91 70-130 60-140
Methylene Chloride 50.00 42.75 86 70-130 60-140
4-Methyl-2-Pentanone 50.00 45.69 91 70-130 60-140
Naphthalene 50.00 48.00 96 70-130 60-140
n-Propylbenzene 50.00 45.30 91 70-130 60-140
Styrene 50.00 45.99 92 70-130 60-140
1,1,1,2-Tetrachloroethane 50.00 49.65 99 70-130 60-140
1,1,2,2-Tetrachloroethane 50.00 44.79 90 70-130 60-140
Tetrachloroethene 50.00 41.54 83 70-130 60-140
Toluene 50.00 41.67 83 77-120 70-127
1,2,3-Trichlorobenzene 50.00 47.68 95 70-130 60-140
1,2,4-Trichlorobenzene 50.00 48.04 96 70-130 60-140
1,1,1-Trichloroethane 50.00 45.82 92 70-130 60-140
1,1,2-Trichloroethane 50.00 45.20 90 70-130 60-140
1,1,2-Trichloro-1,2,2-Trifluoroethane 50.00 41.62 83 70-130 60-140 Trichloroethene 50.00 42.16 84 70-130 60-140
1,2,3-Trichloropropane 50.00 48.08 96 70-130 60-140
1,2,4-Trimethylbenzene 50.00 43.93 88 70-130 60-140
Trichlorofluoromethane 50.00 46.82 94 70-130 60-140
1,3,5-Trimethylbenzene 50.00 46.41 93 70-130 60-140
Vinyl Acetate 50.00 40.30 81 70-130 60-140
Vinyl Chloride 50.00 43.77 88 68-122 59-131
p/m-Xylene 100.0 88.61 89 70-130 60-140
o-Xylene 50.00 45.29 91 70-130 60-140
Methyl-t-Butyl Ether (MTBE) 50.00 44.55 89 77-120 70-127 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2031
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 13 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Method Extraction Chemist ID Instrument Analytical Location ASTM D-2216 (M) N/A 1009 N/A 1
EPA 6010B EPA 3005A Filt. 935 ICP 7300 1
EPA 6010B EPA 3050B 935 ICP 7300 1
EPA 7470A EPA 7470A Filt. 868 Mercury 04 1
EPA 7471A EPA 7471A Total 868 Mercury 05 1
EPA 8015B (M) EPA 3550B 972 GC 49 1
EPA 8081A EPA 3545 669 GC 44 1
EPA 8082 EPA 3545 944 GC 58 1
EPA 8260B EPA 5030C 316 GC/MS L 2
EPA 8260B EPA 5030C 867 GC/MS BB 2
EPA 8310 EPA 3545 960 HPLC 5 1
Sample Analysis Summary Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2031 Page 1 of1
Location 1: 7440 Lincoln Way, Garden Grove, CA 92841
Location 2: 7445 Lampson Avenue, Garden Grove, CA 92841 Return to Contents
Qualifiers Definition
* See applicable analysis comment.
< Less than the indicated value.
> Greater than the indicated value.
1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clarification.
2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clarification. 3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
4 The MS/MSD RPD was out of control due to suspected matrix interference. 5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference. 6 Surrogate recovery below the acceptance limit.
7 Surrogate recovery above the acceptance limit.
B Analyte was present in the associated method blank.
BU Sample analyzed after holding time expired.
BV Sample received after holding time expired.
CI See case narrative.
E Concentration exceeds the calibration range.
ET Sample was extracted past end of recommended max. holding time.
HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.
HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons were also present (or detected).
HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detected).
J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated.
JA Analyte positively identified but quantitation is an estimate.
ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
ND Parameter not detected at the indicated reporting limit.
Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater.
SG The sample extract was subjected to Silica Gel treatment prior to analysis.
X % Recovery and/or RPD out-of-range.
Z Analyte presence was not confirmed by second column or GC/MS analysis.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations.
Glossary of Terms and Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2031 Page 1 of1
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WORK ORDER NUMBER: 16-06-2032
Analytical Report For
Client: Haley & Aldrich, Inc,
Client Project Name: UTAS - Due Diligence / 43559
Attention: Robert K. Scott
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Approved for release on by:
Virendra Patel
Project Manager
AIR SOIL WATER MARINE CHEMISTRY
Eurofins Calscience, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached to this report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of this report is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Calscience is not responsible, legally or otherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise. 08/26/2016
Supplemental Report 1
The original report has been
revised/corrected.
Contents
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client Project Name: UTAS - Due Diligence / 43559
Work Order Number: 16-06-2032
1 Work Order Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2 Case Narrative 16-06-2032_s1. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 3 Sample Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 4 Detections Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 5 Client Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
5.1 EPA 8310 Polynuclear Aromatic Hydrocarbons (Solid). . . . . . . . . . . . . . . . . . . . . . . 13
5.2 ASTM D-2216 (M) Moisture Content (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
5.3 EPA 8015B (M) C6-C44 (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
5.4 EPA 6010B/7471A CAC Title 22 Metals (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
5.5 EPA 7471A Mercury (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
5.6 EPA 8081A Organochlorine Pesticides (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
5.7 EPA 8082 PCB Aroclors (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
5.8 EPA 8260B Volatile Organics (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 6 Quality Control Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
6.1 MS/MSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
6.2 PDS/PDSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
6.3 Sample Duplicate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
6.4 LCS/LCSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77 7 Sample Analysis Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91 8 Glossary of Terms and Qualifiers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92 9 Chain-of-Custody/Sample Receipt Form. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93
Condition Upon Receipt:
Samples were received under Chain-of-Custody (COC) on 06/28/16. They were assigned to Work Order 16-06-2032.
Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are integral elements of the analytical report and are presented at the back of the report.
Holding Times:
All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
Quality Control:
All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or described further within this report.
Subcontractor Information:
Unless otherwise noted below (or on the subcontract form), no samples were subcontracted.
Additional Comments:
Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from mass/sample basis to mass/volume basis using client-supplied air volumes.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are always reported on a wet weight basis.
For sample #7, BB-14-01 - the EPA 7471A results were released with error. Due to a data entry error, the prep factor on this sample was incorrectly entered in our database. The oversight has been corrected and the data is included in the attached analytical report.
Work Order Narrative
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2032 Page 1 of1
Return to Contents
CASE NARRATIVE
Eurofins Calscience Work Order 16-06-2032
EPA Method 6010B Total Metals:
Project Required Detection Limit (PRDL):
The PRDL’s were analyzed as required per the project QAPP. The low level calibration check performed post the sample batch is outside acceptable range for Chromium, Antimony, Selenium, and Zinc on 07/05/16.
The PRDL’s were analyzed as required per the project QAPP. The low level calibration check performed post the sample batch is outside acceptable range for Copper, Molybdenum, Selenium and Zinc on 07/13/16.
Table A: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 6010B
Batch # Analytes(s)
160702S02 Antimony3and Barium3
160709S04 Antimony3, Barium3, Thallium3and Zinc3
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
EPA Method 7471A Mercury:
For sample #7, BB-14-01 - the EPA 7471A results were released with error. Due to a data entry error, the prep factor on this sample was incorrectly entered in our database. The oversight has been corrected and the data is included in the supplemental report.
EPA Method 8260B Volatile Organics:
Table B: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160629S033 2-Butanone3, n-Butylbenzene3, tert-Butylbenzene3, Carbon Disulfide3, Chloroethane4, Chloromethane3, 4-Chlorotoluene3, 1,2-Dibromo-3- Chloropropane3,4, Dibromomethane3,4, 1,3-Dichlorobenzene3, 1,4- Dichlorobenzene3, Dichlorodifluoromethane3, 2,2-Dichloropropane3,4, c-1,3- Dichloropropene3,4, t-1,3-Dichloropropene3,4, p-isopropyltoluene3, Naphthalene3, 1,1,2,2-Tetrachloroethane3,4, 1,2,3-Trichlorobenzene3, 1,2,4- Trichlorobenzene3, Vinyl Acetate3,4 and Methyl-t-Butyl Ether (MTBE)4 160707S001 n-Butylbenzene3, Carbon Disulfide3, Chloromethane3, 1,3-Dichlorobenzene3, 1,4-Dichlorobenzene3, Dichlorodifluoromethane3, 2-Hexanone4, 4-Methyl-2- Pentanone4, Naphthalene3, n-Propylbenzene3, 1,2,3-Trichlorobenzene3, 1,2,4-Trichlorobenzene3, Vinyl Acetate3,4
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control. 4: The MS/MSD RPD was out of control due to suspected matrix interference. 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Return to Contents
Table C: Laboratory Control Sample (LCS) / LCS Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160629L062 Carbon DisulfideME, ChloromethaneME, Dichlorodifluoromethane and Vinyl AcetateME
160707L001 DichlorodifluoromethaneME
ME: LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
EPA Method 8310 Polynuclear Aromatic Hydrocarbons:
Table D: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 8310
Batch # Analytes(s)
160702S06 Benzo (a) Anthracene3,4, Dibenz (a,h) Anthracene3and Indeno (1,2,3-c,d) Pyrene3
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control. 4: The MS/MSD RPD was out of control due to suspected matrix interference.
The LCS/LCSD recoveries for the associated sample batches are within acceptable control limits, therefore, the results have been released without any further action or qualification. 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Return to Contents
Sample Identification Lab Number Collection Date and Time Number of Containers
Matrix
BB-16-01 16-06-2032-1 06/28/16 08:27 1 Solid
BB-16-03 16-06-2032-2 06/28/16 08:29 1 Solid
BB-16-10 16-06-2032-3 06/28/16 08:30 1 Solid
BB-15-01 16-06-2032-4 06/28/16 08:48 1 Solid
BB-15-03 16-06-2032-5 06/28/16 08:50 1 Solid
BB-15-10 16-06-2032-6 06/28/16 08:52 1 Solid
BB-14-01 16-06-2032-7 06/28/16 09:10 1 Solid
BB-14-05 16-06-2032-8 06/28/16 09:09 1 Solid
BB-14-10 16-06-2032-9 06/28/16 09:14 1 Solid
BB-14-03 16-06-2032-10 06/28/16 09:12 1 Solid
Sample Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
PO Number:
Date/Time
Received:
06/28/16 19:00
Number of
Containers:
10 Attn: Robert K. Scott
Return to Contents
BB-16-01 (16-06-2032-1)
Moisture 6.6 0.10 % ASTM D-2216 (M) N/A
Arsenic 3.85 0.773 mg/kg EPA 6010B EPA 3050B
Barium 94.5 0.515 mg/kg EPA 6010B EPA 3050B
Beryllium 0.366 0.258 mg/kg EPA 6010B EPA 3050B
Cadmium 0.513 J 0.140* mg/kg EPA 6010B EPA 3050B
Chromium 17.3 0.258 mg/kg EPA 6010B EPA 3050B
Cobalt 8.75 0.258 mg/kg EPA 6010B EPA 3050B
Copper 13.9 0.515 mg/kg EPA 6010B EPA 3050B
Lead 13.9 0.515 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.269 0.258 mg/kg EPA 6010B EPA 3050B
Nickel 8.26 0.258 mg/kg EPA 6010B EPA 3050B
Selenium 2.12 0.773 mg/kg EPA 6010B EPA 3050B
Thallium 0.769 J 0.156* mg/kg EPA 6010B EPA 3050B
Vanadium 47.3 0.258 mg/kg EPA 6010B EPA 3050B
Zinc 51.1 B 1.03 mg/kg EPA 6010B EPA 3050B
Mercury 0.0152 J 0.00578* mg/kg EPA 7471A EPA 7471A Total C29-C32 22 J 6.3* mg/kg EPA 8015B (M) EPA 3550B
C33-C36 29 25 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 28 25 mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 79 5.0 mg/kg EPA 8015B (M) EPA 3550B
Aroclor-1260 33 J 30* ug/kg EPA 8082 EPA 3545
Phenanthrene 12 9.9 ug/kg EPA 8310 EPA 3545
Fluoranthene 20 9.9 ug/kg EPA 8310 EPA 3545
Pyrene 39 9.9 ug/kg EPA 8310 EPA 3545
Benzo (a) Anthracene 6.3 J 2.4* ug/kg EPA 8310 EPA 3545 Chrysene 8.4 J 2.0* ug/kg EPA 8310 EPA 3545
Benzo (b) Fluoranthene 16 9.9 ug/kg EPA 8310 EPA 3545
Benzo (k) Fluoranthene 7.8 J 1.7* ug/kg EPA 8310 EPA 3545 Benzo (a) Pyrene 12 9.9 ug/kg EPA 8310 EPA 3545
Dibenz (a,h) Anthracene 54 9.9 ug/kg EPA 8310 EPA 3545
Benzo (g,h,i) Perylene 26 9.9 ug/kg EPA 8310 EPA 3545
Indeno (1,2,3-c,d) Pyrene 100 9.9 ug/kg EPA 8310 EPA 3545 Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 1 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-16-03 (16-06-2032-2)
Moisture 7.5 0.10 % ASTM D-2216 (M) N/A
Arsenic 1.95 0.765 mg/kg EPA 6010B EPA 3050B
Barium 62.3 0.510 mg/kg EPA 6010B EPA 3050B
Beryllium 0.323 0.255 mg/kg EPA 6010B EPA 3050B
Cadmium 0.415 J 0.138* mg/kg EPA 6010B EPA 3050B
Chromium 15.0 0.255 mg/kg EPA 6010B EPA 3050B
Cobalt 9.65 0.255 mg/kg EPA 6010B EPA 3050B
Copper 12.0 0.510 mg/kg EPA 6010B EPA 3050B
Lead 6.82 0.510 mg/kg EPA 6010B EPA 3050B
Nickel 6.80 0.255 mg/kg EPA 6010B EPA 3050B
Thallium 0.425 J 0.155* mg/kg EPA 6010B EPA 3050B
Vanadium 48.0 0.255 mg/kg EPA 6010B EPA 3050B
Zinc 28.5 B 1.02 mg/kg EPA 6010B EPA 3050B
Mercury 0.0174 J 0.00568* mg/kg EPA 7471A EPA 7471A Total Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 2 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-15-01 (16-06-2032-4)
Moisture 2.9 0.10 % ASTM D-2216 (M) N/A
Arsenic 3.07 0.758 mg/kg EPA 6010B EPA 3050B
Barium 62.1 0.505 mg/kg EPA 6010B EPA 3050B
Beryllium 0.250 J 0.138* mg/kg EPA 6010B EPA 3050B
Cadmium 1.03 0.505 mg/kg EPA 6010B EPA 3050B
Chromium 11.4 0.253 mg/kg EPA 6010B EPA 3050B
Cobalt 6.04 0.253 mg/kg EPA 6010B EPA 3050B
Copper 9.20 0.505 mg/kg EPA 6010B EPA 3050B
Lead 11.1 0.505 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.351 0.253 mg/kg EPA 6010B EPA 3050B
Nickel 6.96 0.253 mg/kg EPA 6010B EPA 3050B
Vanadium 29.1 0.253 mg/kg EPA 6010B EPA 3050B
Zinc 39.2 1.01 mg/kg EPA 6010B EPA 3050B
Mercury 0.0153 J 0.00578* mg/kg EPA 7471A EPA 7471A Total C9-C10 3.4 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C11-C12 1.5 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C19-C20 1.4 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C21-C22 3.3 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C25-C28 4.4 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C29-C32 26 5.0 mg/kg EPA 8015B (M) EPA 3550B
C33-C36 34 5.0 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 41 5.0 mg/kg EPA 8015B (M) EPA 3550B
C41-C44 24 5.0 mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 140 5.0 mg/kg EPA 8015B (M) EPA 3550B
4,4'-DDT 2.7 J 2.2* ug/kg EPA 8081A EPA 3545
Aroclor-1254 94 50 ug/kg EPA 8082 EPA 3545
Methylene Chloride 1.9 J 1.4* ug/kg EPA 8260B EPA 5030C p/m-Xylene 0.45 J 0.27* ug/kg EPA 8260B EPA 5030C
Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 3 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-15-03 (16-06-2032-5)
Moisture 5.0 0.10 % ASTM D-2216 (M) N/A
Arsenic 3.44 0.728 mg/kg EPA 6010B EPA 3050B
Barium 66.2 0.485 mg/kg EPA 6010B EPA 3050B
Beryllium 0.280 0.243 mg/kg EPA 6010B EPA 3050B
Cadmium 0.734 0.485 mg/kg EPA 6010B EPA 3050B
Chromium 14.9 0.243 mg/kg EPA 6010B EPA 3050B
Cobalt 7.51 0.243 mg/kg EPA 6010B EPA 3050B
Copper 27.9 0.485 mg/kg EPA 6010B EPA 3050B
Lead 21.3 0.485 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.201 J 0.128* mg/kg EPA 6010B EPA 3050B
Nickel 8.20 0.243 mg/kg EPA 6010B EPA 3050B
Vanadium 40.4 0.243 mg/kg EPA 6010B EPA 3050B
Zinc 61.3 B 0.971 mg/kg EPA 6010B EPA 3050B
Mercury 0.0440 J 0.00578* mg/kg EPA 7471A EPA 7471A Total C29-C32 3.3 J 1.3* mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 3.3 J 1.3* mg/kg EPA 8015B (M) EPA 3550B
Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 4 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
BB-14-01 (16-06-2032-7)
Moisture 4.2 0.10 % ASTM D-2216 (M) N/A
Arsenic 4.73 0.773 mg/kg EPA 6010B EPA 3050B
Barium 80.6 0.515 mg/kg EPA 6010B EPA 3050B
Beryllium 0.258 J 0.141* mg/kg EPA 6010B EPA 3050B
Cadmium 0.438 J 0.140* mg/kg EPA 6010B EPA 3050B
Chromium 16.6 0.258 mg/kg EPA 6010B EPA 3050B
Cobalt 3.84 0.258 mg/kg EPA 6010B EPA 3050B
Copper 8.82 0.515 mg/kg EPA 6010B EPA 3050B
Lead 13.5 0.515 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.580 0.258 mg/kg EPA 6010B EPA 3050B
Nickel 7.75 0.258 mg/kg EPA 6010B EPA 3050B
Thallium 0.503 J 0.156* mg/kg EPA 6010B EPA 3050B
Vanadium 29.0 0.258 mg/kg EPA 6010B EPA 3050B
Zinc 39.5 B 1.03 mg/kg EPA 6010B EPA 3050B
Mercury 0.0221 J 0.00578* mg/kg EPA 7471A EPA 7471A Total C29-C32 38 25 mg/kg EPA 8015B (M) EPA 3550B
C33-C36 38 25 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 33 25 mg/kg EPA 8015B (M) EPA 3550B
C41-C44 12 J 6.3* mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 120 5.0 mg/kg EPA 8015B (M) EPA 3550B
Aroclor-1254 160 50 ug/kg EPA 8082 EPA 3545
Aroclor-1260 110 50 ug/kg EPA 8082 EPA 3545
Acetone 15 J 6.1* ug/kg EPA 8260B EPA 5030C
p/m-Xylene 0.82 J 0.26* ug/kg EPA 8260B EPA 5030C
Phenanthrene 11 10 ug/kg EPA 8310 EPA 3545
Fluoranthene 17 10 ug/kg EPA 8310 EPA 3545
Pyrene 18 10 ug/kg EPA 8310 EPA 3545
Benzo (a) Anthracene 5.8 J 2.5* ug/kg EPA 8310 EPA 3545 Chrysene 13 10 ug/kg EPA 8310 EPA 3545
Benzo (b) Fluoranthene 31 10 ug/kg EPA 8310 EPA 3545
Benzo (k) Fluoranthene 12 10 ug/kg EPA 8310 EPA 3545
Benzo (a) Pyrene 23 10 ug/kg EPA 8310 EPA 3545
Dibenz (a,h) Anthracene 47 10 ug/kg EPA 8310 EPA 3545
Benzo (g,h,i) Perylene 23 10 ug/kg EPA 8310 EPA 3545
Indeno (1,2,3-c,d) Pyrene 83 10 ug/kg EPA 8310 EPA 3545 Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 5 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
Subcontracted analyses, if any, are not included in this summary.
BB-14-05 (16-06-2032-8)
Moisture 6.5 0.10 % ASTM D-2216 (M) N/A
Arsenic 3.11 0.725 mg/kg EPA 6010B EPA 3050B
Barium 68.2 0.483 mg/kg EPA 6010B EPA 3050B
Beryllium 0.315 0.242 mg/kg EPA 6010B EPA 3050B
Cadmium 0.449 J 0.131* mg/kg EPA 6010B EPA 3050B
Chromium 16.9 0.242 mg/kg EPA 6010B EPA 3050B
Cobalt 9.21 0.242 mg/kg EPA 6010B EPA 3050B
Copper 18.7 0.483 mg/kg EPA 6010B EPA 3050B
Lead 10.7 0.483 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.136 J 0.128* mg/kg EPA 6010B EPA 3050B
Nickel 7.64 0.242 mg/kg EPA 6010B EPA 3050B
Selenium 0.334 J 0.289* mg/kg EPA 6010B EPA 3050B
Vanadium 48.8 0.242 mg/kg EPA 6010B EPA 3050B
Zinc 39.1 B 0.966 mg/kg EPA 6010B EPA 3050B
Mercury 0.0300 J 0.00587* mg/kg EPA 7471A EPA 7471A Total Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2032
Project Name: UTAS - Due Diligence / 43559
Received: 06/28/16
Attn: Robert K. Scott Page 6 of6
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-16-01 16-06-2032-1-AA 06/28/16
08:27
Solid HPLC 5 07/02/16 07/06/16
06:35
160702L06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Naphthalene ND 15 4.0 1.00
Acenaphthylene ND 30 4.1 1.00
Acenaphthene ND 15 4.0 1.00
Fluorene ND 9.9 1.7 1.00
Phenanthrene 12 9.9 2.1 1.00
Anthracene ND 9.9 2.0 1.00
Fluoranthene 20 9.9 2.1 1.00
Pyrene 39 9.9 2.9 1.00
Benzo (a) Anthracene 6.3 9.9 2.4 1.00 J
Chrysene 8.4 9.9 2.0 1.00 J
Benzo (b) Fluoranthene 16 9.9 2.1 1.00
Benzo (k) Fluoranthene 7.8 9.9 1.7 1.00 J
Benzo (a) Pyrene 12 9.9 2.0 1.00
Dibenz (a,h) Anthracene 54 9.9 2.9 1.00
Benzo (g,h,i) Perylene 26 9.9 1.8 1.00
Indeno (1,2,3-c,d) Pyrene 100 9.9 2.2 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decafluorobiphenyl 68 8-120
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3545
Method: EPA 8310
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of3
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-14-01 16-06-2032-7-AA 06/28/16
09:10
Solid HPLC 5 07/02/16 07/06/16
07:08
160702L06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Naphthalene ND 15 4.0 1.00
Acenaphthylene ND 30 4.2 1.00
Acenaphthene ND 15 4.0 1.00
Fluorene ND 10 1.7 1.00
Phenanthrene 11 10 2.1 1.00
Anthracene ND 10 2.0 1.00
Fluoranthene 17 10 2.1 1.00
Pyrene 18 10 2.9 1.00
Benzo (a) Anthracene 5.8 10 2.5 1.00 J
Chrysene 13 10 2.1 1.00
Benzo (b) Fluoranthene 31 10 2.1 1.00
Benzo (k) Fluoranthene 12 10 1.7 1.00
Benzo (a) Pyrene 23 10 2.0 1.00
Dibenz (a,h) Anthracene 47 10 2.9 1.00
Benzo (g,h,i) Perylene 23 10 1.8 1.00
Indeno (1,2,3-c,d) Pyrene 83 10 2.2 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decafluorobiphenyl 82 8-120
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3545
Method: EPA 8310
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of3
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-07-002-1879 N/A Solid HPLC 5 07/02/16 07/05/16 17:02
160702L06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Naphthalene ND 15 4.0 1.00
Acenaphthylene ND 30 4.2 1.00
Acenaphthene ND 15 4.0 1.00
Fluorene ND 10 1.7 1.00
Phenanthrene ND 10 2.1 1.00
Anthracene ND 10 2.0 1.00
Fluoranthene ND 10 2.1 1.00
Pyrene ND 10 2.9 1.00
Benzo (a) Anthracene ND 10 2.5 1.00
Chrysene ND 10 2.1 1.00
Benzo (b) Fluoranthene ND 10 2.1 1.00
Benzo (k) Fluoranthene ND 10 1.7 1.00
Benzo (a) Pyrene ND 10 2.0 1.00
Dibenz (a,h) Anthracene ND 10 3.0 1.00
Benzo (g,h,i) Perylene ND 10 1.8 1.00
Indeno (1,2,3-c,d) Pyrene ND 10 2.2 1.00
Surrogate Rec. (%) Control Limits Qualifiers
Decafluorobiphenyl 61 8-120
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3545
Method: EPA 8310
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of3
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-16-01 16-06-2032-1-AA 06/28/16
08:27
Solid N/A 06/29/16 06/29/16
21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 6.6 0.10 0.10 1.00
BB-16-03 16-06-2032-2-AA 06/28/16
08:29
Solid N/A 06/29/16 06/29/16
21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 7.5 0.10 0.10 1.00
BB-15-01 16-06-2032-4-AA 06/28/16
08:48
Solid N/A 06/29/16 06/29/16
21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 2.9 0.10 0.10 1.00
BB-15-03 16-06-2032-5-AA 06/28/16
08:50
Solid N/A 06/29/16 06/29/16
21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 5.0 0.10 0.10 1.00
BB-14-01 16-06-2032-7-AA 06/28/16
09:10
Solid N/A 06/29/16 06/29/16
21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 4.2 0.10 0.10 1.00
BB-14-05 16-06-2032-8-AA 06/28/16
09:09
Solid N/A 06/29/16 06/29/16
21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 6.5 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-05-014-6082 N/A Solid N/A 06/29/16 06/29/16 21:30
G0629MOIB5
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture ND 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-16-01 16-06-2032-1-AA 06/28/16
08:27
Solid GC 49 06/30/16 06/30/16
20:47
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 25 6.3 5.00
C7 ND 25 6.3 5.00
C8 ND 25 6.3 5.00
C9-C10 ND 25 6.3 5.00
C11-C12 ND 25 6.3 5.00
C13-C14 ND 25 6.3 5.00
C15-C16 ND 25 6.3 5.00
C17-C18 ND 25 6.3 5.00
C19-C20 ND 25 6.3 5.00
C21-C22 ND 25 6.3 5.00
C23-C24 ND 25 6.3 5.00
C25-C28 ND 25 6.3 5.00
C29-C32 22 25 6.3 5.00 J
C33-C36 29 25 6.3 5.00
C37-C40 28 25 6.3 5.00
C41-C44 ND 25 6.3 5.00
C6-C44 Total 79 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 71 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-16-03 16-06-2032-2-AA 06/28/16
08:29
Solid GC 49 06/30/16 06/30/16
16:56
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 4.9 1.2 1.00
C7 ND 4.9 1.2 1.00
C8 ND 4.9 1.2 1.00
C9-C10 ND 4.9 1.2 1.00
C11-C12 ND 4.9 1.2 1.00
C13-C14 ND 4.9 1.2 1.00
C15-C16 ND 4.9 1.2 1.00
C17-C18 ND 4.9 1.2 1.00
C19-C20 ND 4.9 1.2 1.00
C21-C22 ND 4.9 1.2 1.00
C23-C24 ND 4.9 1.2 1.00
C25-C28 ND 4.9 1.2 1.00
C29-C32 ND 4.9 1.2 1.00
C33-C36 ND 4.9 1.2 1.00
C37-C40 ND 4.9 1.2 1.00
C41-C44 ND 4.9 1.2 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 88 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-15-01 16-06-2032-4-AA 06/28/16
08:48
Solid GC 45 07/08/16 07/11/16
12:36
160708B11A
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.2 1.00
C7 ND 5.0 1.2 1.00
C8 ND 5.0 1.2 1.00
C9-C10 3.4 5.0 1.2 1.00 J
C11-C12 1.5 5.0 1.2 1.00 J
C13-C14 ND 5.0 1.2 1.00
C15-C16 ND 5.0 1.2 1.00
C17-C18 ND 5.0 1.2 1.00
C19-C20 1.4 5.0 1.2 1.00 J
C21-C22 3.3 5.0 1.2 1.00 J
C23-C24 ND 5.0 1.2 1.00
C25-C28 4.4 5.0 1.2 1.00 J
C29-C32 26 5.0 1.2 1.00
C33-C36 34 5.0 1.2 1.00
C37-C40 41 5.0 1.2 1.00
C41-C44 24 5.0 1.2 1.00
C6-C44 Total 140 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 99 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 3 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-15-03 16-06-2032-5-AA 06/28/16
08:50
Solid GC 49 06/30/16 06/30/16
17:13
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 3.3 5.0 1.3 1.00 J
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total 3.3 5.0 1.3 1.00 J
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 91 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 4 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-14-01 16-06-2032-7-AA 06/28/16
09:10
Solid GC 49 06/30/16 06/30/16
21:05
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 25 6.3 5.00
C7 ND 25 6.3 5.00
C8 ND 25 6.3 5.00
C9-C10 ND 25 6.3 5.00
C11-C12 ND 25 6.3 5.00
C13-C14 ND 25 6.3 5.00
C15-C16 ND 25 6.3 5.00
C17-C18 ND 25 6.3 5.00
C19-C20 ND 25 6.3 5.00
C21-C22 ND 25 6.3 5.00
C23-C24 ND 25 6.3 5.00
C25-C28 ND 25 6.3 5.00
C29-C32 38 25 6.3 5.00
C33-C36 38 25 6.3 5.00
C37-C40 33 25 6.3 5.00
C41-C44 12 25 6.3 5.00 J
C6-C44 Total 120 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 63 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 5 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-14-05 16-06-2032-8-AA 06/28/16
09:09
Solid GC 49 06/30/16 06/30/16
17:31
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 89 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 6 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-15-490-2144 N/A Solid GC 49 06/30/16 06/30/16 15:45
160630B05
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 92 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 7 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-15-490-2156 N/A Solid GC 45 07/08/16 07/08/16 20:16
160708B11A
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 78 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 8 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-16-01 16-06-2032-1-AA 06/28/16
08:27
Solid ICP 7300 07/02/16 07/05/16
14:00
160702L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.773 0.154 1.03
Arsenic 3.85 0.773 0.267 1.03
Barium 94.5 0.515 0.159 1.03
Beryllium 0.366 0.258 0.141 1.03
Cadmium 0.513 0.515 0.140 1.03 J
Chromium 17.3 0.258 0.147 1.03
Cobalt 8.75 0.258 0.153 1.03
Copper 13.9 0.515 0.139 1.03
Lead 13.9 0.515 0.136 1.03
Molybdenum 0.269 0.258 0.136 1.03
Nickel 8.26 0.258 0.149 1.03
Selenium 2.12 0.773 0.309 1.03
Silver ND 0.258 0.0884 1.03
Thallium 0.769 0.773 0.156 1.03 J
Vanadium 47.3 0.258 0.146 1.03
Zinc 51.1 1.03 0.183 1.03 B
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-16-03 16-06-2032-2-AA 06/28/16
08:29
Solid ICP 7300 07/02/16 07/05/16
14:01
160702L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.765 0.152 1.02
Arsenic 1.95 0.765 0.264 1.02
Barium 62.3 0.510 0.158 1.02
Beryllium 0.323 0.255 0.140 1.02
Cadmium 0.415 0.510 0.138 1.02 J
Chromium 15.0 0.255 0.145 1.02
Cobalt 9.65 0.255 0.151 1.02
Copper 12.0 0.510 0.137 1.02
Lead 6.82 0.510 0.134 1.02
Molybdenum ND 0.255 0.135 1.02
Nickel 6.80 0.255 0.148 1.02
Selenium ND 0.765 0.306 1.02
Silver ND 0.255 0.0875 1.02
Thallium 0.425 0.765 0.155 1.02 J
Vanadium 48.0 0.255 0.144 1.02
Zinc 28.5 1.02 0.181 1.02 B
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-15-01 16-06-2032-4-AA 06/28/16
08:48
Solid ICP 7300 07/09/16 07/13/16
19:57
160709L04U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.758 0.150 1.01
Arsenic 3.07 0.758 0.262 1.01
Barium 62.1 0.505 0.156 1.01
Beryllium 0.250 0.253 0.138 1.01 J
Cadmium 1.03 0.505 0.137 1.01
Chromium 11.4 0.253 0.144 1.01
Cobalt 6.04 0.253 0.150 1.01
Copper 9.20 0.505 0.136 1.01
Lead 11.1 0.505 0.133 1.01
Molybdenum 0.351 0.253 0.133 1.01
Nickel 6.96 0.253 0.146 1.01
Selenium ND 0.758 0.303 1.01
Silver ND 0.253 0.0866 1.01
Thallium ND 0.758 0.153 1.01
Vanadium 29.1 0.253 0.143 1.01
Zinc 39.2 1.01 0.179 1.01
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 3 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-15-03 16-06-2032-5-AA 06/28/16
08:50
Solid ICP 7300 07/02/16 07/05/16
13:56
160702L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.728 0.145 0.971
Arsenic 3.44 0.728 0.252 0.971
Barium 66.2 0.485 0.150 0.971
Beryllium 0.280 0.243 0.133 0.971
Cadmium 0.734 0.485 0.131 0.971
Chromium 14.9 0.243 0.138 0.971
Cobalt 7.51 0.243 0.144 0.971
Copper 27.9 0.485 0.131 0.971
Lead 21.3 0.485 0.128 0.971
Molybdenum 0.201 0.243 0.128 0.971 J
Nickel 8.20 0.243 0.141 0.971
Selenium ND 0.728 0.291 0.971
Silver ND 0.243 0.0832 0.971
Thallium ND 0.728 0.147 0.971
Vanadium 40.4 0.243 0.137 0.971
Zinc 61.3 0.971 0.172 0.971 B
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 4 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
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Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-14-01 16-06-2032-7-AA 06/28/16
09:10
Solid ICP 7300 07/02/16 07/05/16
14:02
160702L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.773 0.154 1.03
Arsenic 4.73 0.773 0.267 1.03
Barium 80.6 0.515 0.159 1.03
Beryllium 0.258 0.258 0.141 1.03 J
Cadmium 0.438 0.515 0.140 1.03 J
Chromium 16.6 0.258 0.147 1.03
Cobalt 3.84 0.258 0.153 1.03
Copper 8.82 0.515 0.139 1.03
Lead 13.5 0.515 0.136 1.03
Molybdenum 0.580 0.258 0.136 1.03
Nickel 7.75 0.258 0.149 1.03
Selenium ND 0.773 0.309 1.03
Silver ND 0.258 0.0884 1.03
Thallium 0.503 0.773 0.156 1.03 J
Vanadium 29.0 0.258 0.146 1.03
Zinc 39.5 1.03 0.183 1.03 B
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 5 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-14-05 16-06-2032-8-AA 06/28/16
09:09
Solid ICP 7300 07/02/16 07/05/16
14:03
160702L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.725 0.144 0.966
Arsenic 3.11 0.725 0.250 0.966
Barium 68.2 0.483 0.149 0.966
Beryllium 0.315 0.242 0.132 0.966
Cadmium 0.449 0.483 0.131 0.966 J
Chromium 16.9 0.242 0.137 0.966
Cobalt 9.21 0.242 0.143 0.966
Copper 18.7 0.483 0.130 0.966
Lead 10.7 0.483 0.127 0.966
Molybdenum 0.136 0.242 0.128 0.966 J
Nickel 7.64 0.242 0.140 0.966
Selenium 0.334 0.725 0.289 0.966 J
Silver ND 0.242 0.0828 0.966
Thallium ND 0.725 0.147 0.966
Vanadium 48.8 0.242 0.136 0.966
Zinc 39.1 0.966 0.172 0.966 B
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 6 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 097-01-002-22886 N/A Solid ICP 7300 07/02/16 07/05/16 13:23
160702L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.765 0.152 1.02
Arsenic ND 0.765 0.264 1.02
Barium ND 0.510 0.158 1.02
Beryllium ND 0.255 0.140 1.02
Cadmium ND 0.510 0.138 1.02
Chromium ND 0.255 0.145 1.02
Cobalt ND 0.255 0.151 1.02
Copper ND 0.510 0.137 1.02
Lead ND 0.510 0.134 1.02
Molybdenum ND 0.255 0.135 1.02
Nickel ND 0.255 0.148 1.02
Selenium ND 0.765 0.306 1.02
Silver ND 0.255 0.0875 1.02
Thallium ND 0.765 0.155 1.02
Vanadium ND 0.255 0.144 1.02
Zinc 1.16 1.02 0.181 1.02
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 7 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 097-01-002-22917 N/A Solid ICP 7300 07/09/16 07/13/16 19:53
160709L04U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony 0.514 0.750 0.149 1.00 J
Arsenic ND 0.750 0.259 1.00
Barium ND 0.500 0.154 1.00
Beryllium ND 0.250 0.137 1.00
Cadmium ND 0.500 0.135 1.00
Chromium ND 0.250 0.142 1.00
Cobalt ND 0.250 0.148 1.00
Copper ND 0.500 0.135 1.00
Lead ND 0.500 0.132 1.00
Molybdenum ND 0.250 0.132 1.00
Nickel ND 0.250 0.145 1.00
Selenium ND 0.750 0.300 1.00
Silver ND 0.250 0.0857 1.00
Thallium ND 0.750 0.152 1.00
Vanadium ND 0.250 0.141 1.00
Zinc ND 1.00 0.178 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2032
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 8 of8
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents