Total number of LCS compounds: 85
Total number of ME compounds: 1
Total number of ME compounds allowed: 4
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers t-1,4-Dichloro-2-Butene 10.00 8.856 89 70-130 60-140
Tetrahydrofuran 10.00 7.772 78 70-130 60-140
Propionitrile 10.00 8.447 84 70-130 60-140
Tert-Butyl Alcohol (TBA) 50.00 52.06 104 43-170 22-191
Diisopropyl Ether (DIPE) 10.00 8.576 86 70-130 60-140
Ethyl-t-Butyl Ether (ETBE) 10.00 8.101 81 70-130 60-140 Tert-Amyl-Methyl Ether (TAME) 10.00 7.546 75 70-130 60-140 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2037
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 11 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-14-314-574 LCS Solid GC/MS BB 07/01/16 07/01/16 09:30 160701L002 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Acetone 50.00 50.63 101 70-130 60-140
Benzene 50.00 49.15 98 78-120 71-127
Bromobenzene 50.00 54.83 110 70-130 60-140
Bromochloromethane 50.00 46.58 93 70-130 60-140
Bromodichloromethane 50.00 51.26 103 70-130 60-140
Bromoform 50.00 49.85 100 70-130 60-140
Bromomethane 50.00 58.91 118 70-130 60-140
2-Butanone 50.00 39.58 79 70-130 60-140
n-Butylbenzene 50.00 52.14 104 77-123 69-131
sec-Butylbenzene 50.00 51.30 103 70-130 60-140
tert-Butylbenzene 50.00 51.77 104 70-130 60-140
Carbon Disulfide 50.00 58.70 117 70-130 60-140
Carbon Tetrachloride 50.00 50.40 101 49-139 34-154
Chlorobenzene 50.00 51.57 103 79-120 72-127
Chloroethane 50.00 67.04 134 70-130 60-140 ME
Chloroform 50.00 47.44 95 70-130 60-140
Chloromethane 50.00 54.36 109 70-130 60-140
2-Chlorotoluene 50.00 52.90 106 70-130 60-140
4-Chlorotoluene 50.00 50.48 101 70-130 60-140
Dibromochloromethane 50.00 51.19 102 70-130 60-140
1,2-Dibromo-3-Chloropropane 50.00 46.53 93 70-130 60-140 1,2-Dibromoethane 50.00 50.31 101 70-130 60-140
Dibromomethane 50.00 47.90 96 70-130 60-140
1,2-Dichlorobenzene 50.00 51.17 102 75-120 68-128
1,3-Dichlorobenzene 50.00 51.81 104 70-130 60-140
1,4-Dichlorobenzene 50.00 50.91 102 70-130 60-140
Dichlorodifluoromethane 50.00 43.69 87 70-130 60-140
1,1-Dichloroethane 50.00 47.14 94 70-130 60-140
1,2-Dichloroethane 50.00 44.89 90 70-130 60-140
1,1-Dichloroethene 50.00 51.67 103 74-122 66-130
c-1,2-Dichloroethene 50.00 47.39 95 70-130 60-140
t-1,2-Dichloroethene 50.00 48.75 98 70-130 60-140
1,2-Dichloropropane 50.00 49.03 98 79-115 73-121
1,3-Dichloropropane 50.00 47.78 96 70-130 60-140
2,2-Dichloropropane 50.00 48.28 97 70-130 60-140
1,1-Dichloropropene 50.00 47.00 94 70-130 60-140
c-1,3-Dichloropropene 50.00 50.46 101 70-130 60-140
t-1,3-Dichloropropene 50.00 52.30 105 70-130 60-140
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2037
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 12 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 66
Total number of ME compounds: 2
Total number of ME compounds allowed: 3
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Ethylbenzene 50.00 52.10 104 76-120 69-127
2-Hexanone 50.00 42.55 85 70-130 60-140
Isopropylbenzene 50.00 53.73 107 70-130 60-140
p-Isopropyltoluene 50.00 52.39 105 70-130 60-140
Methylene Chloride 50.00 47.80 96 70-130 60-140
4-Methyl-2-Pentanone 50.00 43.63 87 70-130 60-140
Naphthalene 50.00 49.83 100 70-130 60-140
n-Propylbenzene 50.00 53.35 107 70-130 60-140
Styrene 50.00 53.66 107 70-130 60-140
1,1,1,2-Tetrachloroethane 50.00 54.29 109 70-130 60-140 1,1,2,2-Tetrachloroethane 50.00 45.65 91 70-130 60-140
Tetrachloroethene 50.00 51.50 103 70-130 60-140
Toluene 50.00 49.84 100 77-120 70-127
1,2,3-Trichlorobenzene 50.00 51.83 104 70-130 60-140
1,2,4-Trichlorobenzene 50.00 53.58 107 70-130 60-140
1,1,1-Trichloroethane 50.00 47.99 96 70-130 60-140
1,1,2-Trichloroethane 50.00 47.67 95 70-130 60-140
1,1,2-Trichloro-1,2,2-Trifluoroethane 50.00 52.41 105 70-130 60-140 Trichloroethene 50.00 50.25 100 70-130 60-140
1,2,3-Trichloropropane 50.00 48.99 98 70-130 60-140
1,2,4-Trimethylbenzene 50.00 50.12 100 70-130 60-140
Trichlorofluoromethane 50.00 54.42 109 70-130 60-140
1,3,5-Trimethylbenzene 50.00 54.06 108 70-130 60-140
Vinyl Acetate 50.00 37.89 76 70-130 60-140
Vinyl Chloride 50.00 63.37 127 68-122 59-131 ME
p/m-Xylene 100.0 104.6 105 70-130 60-140
o-Xylene 50.00 52.72 105 70-130 60-140
Methyl-t-Butyl Ether (MTBE) 50.00 45.76 92 77-120 70-127 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/28/16
Work Order: 16-06-2037
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 13 of13
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Method Extraction Chemist ID Instrument Analytical Location ASTM D-2216 (M) N/A 1009 N/A 1
EPA 6010B EPA 3005A Filt. 935 ICP 7300 1
EPA 6010B EPA 3050B 935 ICP 7300 1
EPA 7470A EPA 7470A Filt. 868 Mercury 04 1
EPA 7471A EPA 7471A Total 868 Mercury 05 1
EPA 8015B (M) EPA 3550B 682 GC 46 1
EPA 8015B (M) EPA 3550B 682 GC 48 1
EPA 8081A EPA 3545 669 GC 44 1
EPA 8082 EPA 3545 944 GC 58 1
EPA 8260B EPA 5030C 316 GC/MS L 2
EPA 8260B EPA 5030C 867 GC/MS BB 2
EPA 8310 EPA 3545 960 HPLC 5 1
Sample Analysis Summary Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2037 Page 1 of1
Location 1: 7440 Lincoln Way, Garden Grove, CA 92841
Location 2: 7445 Lampson Avenue, Garden Grove, CA 92841 Return to Contents
Qualifiers Definition
* See applicable analysis comment.
< Less than the indicated value.
> Greater than the indicated value.
1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clarification.
2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clarification. 3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
4 The MS/MSD RPD was out of control due to suspected matrix interference. 5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference. 6 Surrogate recovery below the acceptance limit.
7 Surrogate recovery above the acceptance limit.
B Analyte was present in the associated method blank.
BU Sample analyzed after holding time expired.
BV Sample received after holding time expired.
CI See case narrative.
E Concentration exceeds the calibration range.
ET Sample was extracted past end of recommended max. holding time.
HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.
HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons were also present (or detected).
HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detected).
J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated.
JA Analyte positively identified but quantitation is an estimate.
ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
ND Parameter not detected at the indicated reporting limit.
Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater.
SG The sample extract was subjected to Silica Gel treatment prior to analysis.
X % Recovery and/or RPD out-of-range.
Z Analyte presence was not confirmed by second column or GC/MS analysis.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations.
Glossary of Terms and Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2037 Page 1 of1
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WORK ORDER NUMBER: 16-06-2174
Analytical Report For
Client: Haley & Aldrich, Inc,
Client Project Name: UTAS - Due Diligence / 43559
Attention: Robert K. Scott
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Approved for release on by:
Virendra Patel
Project Manager
AIR SOIL WATER MARINE CHEMISTRY
Eurofins Calscience, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached to this report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of this report is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Calscience is not responsible, legally or otherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise. 07/14/2016
Contents
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client Project Name: UTAS - Due Diligence / 43559
Work Order Number: 16-06-2174
1 Work Order Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2 Case Narrative 16-06-2174. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 3 Sample Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 4 Detections Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 5 Client Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
5.1 ASTM D-2216 (M) Moisture Content (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
5.2 EPA 8015B (M) C6-C44 (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
5.3 EPA 8260B Volatile Organics (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 6 Quality Control Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
6.1 MS/MSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
6.2 Sample Duplicate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
6.3 LCS/LCSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41 7 Sample Analysis Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 8 Glossary of Terms and Qualifiers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45 9 Chain-of-Custody/Sample Receipt Form. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Condition Upon Receipt:
Samples were received under Chain-of-Custody (COC) on 06/29/16. They were assigned to Work Order 16-06-2174.
Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are integral elements of the analytical report and are presented at the back of the report.
Holding Times:
All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
Quality Control:
All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or described further within this report.
Subcontractor Information:
Unless otherwise noted below (or on the subcontract form), no samples were subcontracted.
Additional Comments:
Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from mass/sample basis to mass/volume basis using client-supplied air volumes.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are always reported on a wet weight basis.
Work Order Narrative
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2174 Page 1 of1
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CASE NARRATIVE
Eurofins Calscience Work Order 16-06-2174
EPA Method 8260B Volatile Organics:
Table A: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160701S005 Vinyl Acetate3
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control. 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Return to Contents
Sample Identification Lab Number Collection Date and Time Number of Containers
Matrix
BB-08A-01 16-06-2174-1 06/28/16 15:35 1 Solid
BB-08A-04 16-06-2174-2 06/28/16 15:37 1 Solid
BB-08A-08 16-06-2174-3 06/28/16 15:38 1 Solid
BB-08A-10 16-06-2174-4 06/28/16 15:39 1 Solid
BB-08B-01 16-06-2174-5 06/28/16 15:54 1 Solid
BB-08B-04 16-06-2174-6 06/28/16 15:56 1 Solid
BB-08B-08 16-06-2174-7 06/28/16 15:57 1 Solid
BB-08B-10 16-06-2174-8 06/28/16 15:58 1 Solid
BB-08C-04 16-06-2174-9 06/28/16 16:21 1 Solid
BB-08C-01 16-06-2174-10 06/28/16 16:19 1 Solid
BB-08C-08 16-06-2174-11 06/28/16 16:22 1 Solid
BB-08C-10 16-06-2174-12 06/28/16 16:23 1 Solid
Sample Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2174
Project Name: UTAS - Due Diligence / 43559
PO Number:
Date/Time
Received:
06/29/16 19:45
Number of
Containers:
12 Attn: Robert K. Scott
Return to Contents
BB-08A-04 (16-06-2174-2)
Moisture 23 0.10 % ASTM D-2216 (M) N/A
C13-C14 2.7 J 1.2* mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 2.7 J 1.3* mg/kg EPA 8015B (M) EPA 3550B
BB-08A-08 (16-06-2174-3)
Moisture 13 0.10 % ASTM D-2216 (M) N/A
BB-08A-10 (16-06-2174-4)
Moisture 15 0.10 % ASTM D-2216 (M) N/A
1,1-Dichloroethane 0.37 J 0.21* ug/kg EPA 8260B EPA 5030C c-1,2-Dichloroethene 0.61 J 0.28* ug/kg EPA 8260B EPA 5030C Trichloroethene 5.8 4.9 ug/kg EPA 8260B EPA 5030C
BB-08B-04 (16-06-2174-6)
Moisture 21 0.10 % ASTM D-2216 (M) N/A
BB-08B-08 (16-06-2174-7)
Moisture 15 0.10 % ASTM D-2216 (M) N/A
Trichloroethene 2.1 J 0.31* ug/kg EPA 8260B EPA 5030C
BB-08B-10 (16-06-2174-8)
Moisture 18 0.10 % ASTM D-2216 (M) N/A
Trichloroethene 0.69 J 0.30* ug/kg EPA 8260B EPA 5030C
BB-08C-04 (16-06-2174-9)
Moisture 11 0.10 % ASTM D-2216 (M) N/A
C9-C10 1.7 J 1.3* mg/kg EPA 8015B (M) EPA 3550B
C13-C14 1.9 J 1.3* mg/kg EPA 8015B (M) EPA 3550B
C15-C16 4.4 J 1.3* mg/kg EPA 8015B (M) EPA 3550B
C17-C18 5.7 5.0 mg/kg EPA 8015B (M) EPA 3550B
C19-C20 15 5.0 mg/kg EPA 8015B (M) EPA 3550B
C21-C22 7.8 5.0 mg/kg EPA 8015B (M) EPA 3550B
C23-C24 23 5.0 mg/kg EPA 8015B (M) EPA 3550B
C25-C28 14 5.0 mg/kg EPA 8015B (M) EPA 3550B
C29-C32 47 5.0 mg/kg EPA 8015B (M) EPA 3550B
C33-C36 21 5.0 mg/kg EPA 8015B (M) EPA 3550B
C37-C40 13 5.0 mg/kg EPA 8015B (M) EPA 3550B
C6-C44 Total 160 5.0 mg/kg EPA 8015B (M) EPA 3550B
Acetone 26 J 6.3* ug/kg EPA 8260B EPA 5030C
c-1,2-Dichloroethene 7.1 5.1 ug/kg EPA 8260B EPA 5030C
Trichloroethene 2.0 J 0.31* ug/kg EPA 8260B EPA 5030C
BB-08C-08 (16-06-2174-11)
Moisture 5.6 0.10 % ASTM D-2216 (M) N/A
Acetone 17 J 6.2* ug/kg EPA 8260B EPA 5030C
Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2174
Project Name: UTAS - Due Diligence / 43559
Received: 06/29/16
Attn: Robert K. Scott Page 1 of2
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
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Subcontracted analyses, if any, are not included in this summary.
Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-06-2174
Project Name: UTAS - Due Diligence / 43559
Received: 06/29/16
Attn: Robert K. Scott Page 2 of2
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
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Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-04 16-06-2174-2-A 06/28/16
15:37
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 23 0.10 0.10 1.00
BB-08A-08 16-06-2174-3-A 06/28/16
15:38
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 13 0.10 0.10 1.00
BB-08A-10 16-06-2174-4-A 06/28/16
15:39
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 15 0.10 0.10 1.00
BB-08B-04 16-06-2174-6-A 06/28/16
15:56
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 21 0.10 0.10 1.00
BB-08B-08 16-06-2174-7-A 06/28/16
15:57
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 15 0.10 0.10 1.00
BB-08B-10 16-06-2174-8-A 06/28/16
15:58
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 18 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
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Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08C-04 16-06-2174-9-A 06/28/16
16:21
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 11 0.10 0.10 1.00
BB-08C-08 16-06-2174-11-A 06/28/16
16:22
Solid N/A 06/30/16 06/30/16
23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 5.6 0.10 0.10 1.00
Method Blank 099-05-014-6086 N/A Solid N/A 06/30/16 06/30/16 23:00
G0630MOIB2
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture ND 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-04 16-06-2174-2-AA 06/28/16
15:37
Solid GC 49 07/06/16 07/07/16
10:08
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.2 1.00
C7 ND 5.0 1.2 1.00
C8 ND 5.0 1.2 1.00
C9-C10 ND 5.0 1.2 1.00
C11-C12 ND 5.0 1.2 1.00
C13-C14 2.7 5.0 1.2 1.00 J
C15-C16 ND 5.0 1.2 1.00
C17-C18 ND 5.0 1.2 1.00
C19-C20 ND 5.0 1.2 1.00
C21-C22 ND 5.0 1.2 1.00
C23-C24 ND 5.0 1.2 1.00
C25-C28 ND 5.0 1.2 1.00
C29-C32 ND 5.0 1.2 1.00
C33-C36 ND 5.0 1.2 1.00
C37-C40 ND 5.0 1.2 1.00
C41-C44 ND 5.0 1.2 1.00
C6-C44 Total 2.7 5.0 1.3 1.00 J
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 97 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 1 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-08 16-06-2174-3-AA 06/28/16
15:38
Solid GC 49 07/06/16 07/07/16
10:26
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 92 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 2 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-10 16-06-2174-4-AA 06/28/16
15:39
Solid GC 49 07/06/16 07/07/16
10:43
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 96 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 3 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08B-04 16-06-2174-6-AA 06/28/16
15:56
Solid GC 49 07/06/16 07/07/16
11:01
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.2 1.00
C7 ND 5.0 1.2 1.00
C8 ND 5.0 1.2 1.00
C9-C10 ND 5.0 1.2 1.00
C11-C12 ND 5.0 1.2 1.00
C13-C14 ND 5.0 1.2 1.00
C15-C16 ND 5.0 1.2 1.00
C17-C18 ND 5.0 1.2 1.00
C19-C20 ND 5.0 1.2 1.00
C21-C22 ND 5.0 1.2 1.00
C23-C24 ND 5.0 1.2 1.00
C25-C28 ND 5.0 1.2 1.00
C29-C32 ND 5.0 1.2 1.00
C33-C36 ND 5.0 1.2 1.00
C37-C40 ND 5.0 1.2 1.00
C41-C44 ND 5.0 1.2 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 100 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 4 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08B-08 16-06-2174-7-AA 06/28/16
15:57
Solid GC 49 07/06/16 07/07/16
11:35
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.2 1.00
C7 ND 5.0 1.2 1.00
C8 ND 5.0 1.2 1.00
C9-C10 ND 5.0 1.2 1.00
C11-C12 ND 5.0 1.2 1.00
C13-C14 ND 5.0 1.2 1.00
C15-C16 ND 5.0 1.2 1.00
C17-C18 ND 5.0 1.2 1.00
C19-C20 ND 5.0 1.2 1.00
C21-C22 ND 5.0 1.2 1.00
C23-C24 ND 5.0 1.2 1.00
C25-C28 ND 5.0 1.2 1.00
C29-C32 ND 5.0 1.2 1.00
C33-C36 ND 5.0 1.2 1.00
C37-C40 ND 5.0 1.2 1.00
C41-C44 ND 5.0 1.2 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 97 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 5 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08B-10 16-06-2174-8-AA 06/28/16
15:58
Solid GC 49 07/06/16 07/07/16
11:53
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 103 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 6 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08C-04 16-06-2174-9-AA 06/28/16
16:21
Solid GC 49 07/06/16 07/07/16
12:10
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 1.7 5.0 1.3 1.00 J
C11-C12 ND 5.0 1.3 1.00
C13-C14 1.9 5.0 1.3 1.00 J
C15-C16 4.4 5.0 1.3 1.00 J
C17-C18 5.7 5.0 1.3 1.00
C19-C20 15 5.0 1.3 1.00
C21-C22 7.8 5.0 1.3 1.00
C23-C24 23 5.0 1.3 1.00
C25-C28 14 5.0 1.3 1.00
C29-C32 47 5.0 1.3 1.00
C33-C36 21 5.0 1.3 1.00
C37-C40 13 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total 160 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 97 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 7 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08C-08 16-06-2174-11-AA 06/28/16
16:22
Solid GC 49 07/06/16 07/07/16
12:28
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag. - The total concentration includes individual carbon range concentrations (estimated), if any, below the RL reported as ND.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.2 1.00
C7 ND 5.0 1.2 1.00
C8 ND 5.0 1.2 1.00
C9-C10 ND 5.0 1.2 1.00
C11-C12 ND 5.0 1.2 1.00
C13-C14 ND 5.0 1.2 1.00
C15-C16 ND 5.0 1.2 1.00
C17-C18 ND 5.0 1.2 1.00
C19-C20 ND 5.0 1.2 1.00
C21-C22 ND 5.0 1.2 1.00
C23-C24 ND 5.0 1.2 1.00
C25-C28 ND 5.0 1.2 1.00
C29-C32 ND 5.0 1.2 1.00
C33-C36 ND 5.0 1.2 1.00
C37-C40 ND 5.0 1.2 1.00
C41-C44 ND 5.0 1.2 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 95 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 8 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-15-490-2152 N/A Solid GC 49 07/06/16 07/07/16 05:48
160706B06
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
C6 ND 5.0 1.3 1.00
C7 ND 5.0 1.3 1.00
C8 ND 5.0 1.3 1.00
C9-C10 ND 5.0 1.3 1.00
C11-C12 ND 5.0 1.3 1.00
C13-C14 ND 5.0 1.3 1.00
C15-C16 ND 5.0 1.3 1.00
C17-C18 ND 5.0 1.3 1.00
C19-C20 ND 5.0 1.3 1.00
C21-C22 ND 5.0 1.3 1.00
C23-C24 ND 5.0 1.3 1.00
C25-C28 ND 5.0 1.3 1.00
C29-C32 ND 5.0 1.3 1.00
C33-C36 ND 5.0 1.3 1.00
C37-C40 ND 5.0 1.3 1.00
C41-C44 ND 5.0 1.3 1.00
C6-C44 Total ND 5.0 1.3 1.00
Surrogate Rec. (%) Control Limits Qualifiers
n-Octacosane 96 61-145
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Units: mg/kg
Project: UTAS - Due Diligence / 43559 Page 9 of9
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-04 16-06-2174-2-A 06/28/16
15:37
Solid GC/MS Q 06/30/16 07/01/16
14:43
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.3 1.00
Benzene ND 5.1 0.13 1.00
Bromobenzene ND 5.1 0.21 1.00
Bromochloromethane ND 5.1 0.70 1.00
Bromodichloromethane ND 5.1 0.24 1.00
Bromoform ND 5.1 0.81 1.00
Bromomethane ND 25 9.6 1.00
2-Butanone ND 51 3.8 1.00
n-Butylbenzene ND 5.1 0.16 1.00
sec-Butylbenzene ND 5.1 0.59 1.00
tert-Butylbenzene ND 5.1 0.15 1.00
Carbon Disulfide ND 51 0.31 1.00
Carbon Tetrachloride ND 5.1 0.29 1.00
Chlorobenzene ND 5.1 0.23 1.00
Chloroethane ND 5.1 1.5 1.00
Chloroform ND 5.1 0.24 1.00
Chloromethane ND 25 0.31 1.00
2-Chlorotoluene ND 5.1 0.23 1.00
4-Chlorotoluene ND 5.1 0.22 1.00
Dibromochloromethane ND 5.1 0.58 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.1 0.26 1.00
Dibromomethane ND 5.1 0.79 1.00
1,2-Dichlorobenzene ND 5.1 0.23 1.00
1,3-Dichlorobenzene ND 5.1 0.18 1.00
1,4-Dichlorobenzene ND 5.1 0.23 1.00
Dichlorodifluoromethane ND 5.1 0.45 1.00
1,1-Dichloroethane ND 5.1 0.21 1.00
1,2-Dichloroethane ND 5.1 0.32 1.00
1,1-Dichloroethene ND 5.1 0.35 1.00
c-1,2-Dichloroethene ND 5.1 0.28 1.00
t-1,2-Dichloroethene ND 5.1 0.51 1.00
1,2-Dichloropropane ND 5.1 0.44 1.00
1,3-Dichloropropane ND 5.1 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 1 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.1 0.34 1.00
1,1-Dichloropropene ND 5.1 0.33 1.00
c-1,3-Dichloropropene ND 5.1 0.26 1.00
t-1,3-Dichloropropene ND 5.1 0.61 1.00
Ethylbenzene ND 5.1 0.15 1.00
2-Hexanone ND 51 1.8 1.00
Isopropylbenzene ND 5.1 0.55 1.00
p-Isopropyltoluene ND 5.1 0.64 1.00
Methylene Chloride ND 51 1.4 1.00
4-Methyl-2-Pentanone ND 51 4.4 1.00
Naphthalene ND 51 0.83 1.00
n-Propylbenzene ND 5.1 0.51 1.00
Styrene ND 5.1 0.61 1.00
1,1,1,2-Tetrachloroethane ND 5.1 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.1 0.35 1.00
Tetrachloroethene ND 5.1 0.21 1.00
Toluene ND 5.1 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.93 1.00
1,2,4-Trichlorobenzene ND 5.1 0.31 1.00
1,1,1-Trichloroethane ND 5.1 0.23 1.00
1,1,2-Trichloroethane ND 5.1 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 51 0.36 1.00
Trichloroethene ND 5.1 0.30 1.00
1,2,3-Trichloropropane ND 5.1 0.84 1.00
1,2,4-Trimethylbenzene ND 5.1 0.59 1.00
Trichlorofluoromethane ND 51 0.38 1.00
1,3,5-Trimethylbenzene ND 5.1 0.56 1.00
Vinyl Acetate ND 51 4.8 1.00
Vinyl Chloride ND 5.1 0.51 1.00
p/m-Xylene ND 5.1 0.27 1.00
o-Xylene ND 5.1 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.1 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 99 60-132
Dibromofluoromethane 104 63-141
1,2-Dichloroethane-d4 109 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 2 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-08 16-06-2174-3-A 06/28/16
15:38
Solid GC/MS Q 06/30/16 07/01/16
16:29
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 4.9 0.13 1.00
Bromobenzene ND 4.9 0.21 1.00
Bromochloromethane ND 4.9 0.68 1.00
Bromodichloromethane ND 4.9 0.23 1.00
Bromoform ND 4.9 0.78 1.00
Bromomethane ND 25 9.3 1.00
2-Butanone ND 49 3.7 1.00
n-Butylbenzene ND 4.9 0.15 1.00
sec-Butylbenzene ND 4.9 0.57 1.00
tert-Butylbenzene ND 4.9 0.15 1.00
Carbon Disulfide ND 49 0.30 1.00
Carbon Tetrachloride ND 4.9 0.28 1.00
Chlorobenzene ND 4.9 0.22 1.00
Chloroethane ND 4.9 1.5 1.00
Chloroform ND 4.9 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 4.9 0.23 1.00
4-Chlorotoluene ND 4.9 0.21 1.00
Dibromochloromethane ND 4.9 0.56 1.00
1,2-Dibromo-3-Chloropropane ND 9.9 1.7 1.00
1,2-Dibromoethane ND 4.9 0.25 1.00
Dibromomethane ND 4.9 0.77 1.00
1,2-Dichlorobenzene ND 4.9 0.23 1.00
1,3-Dichlorobenzene ND 4.9 0.17 1.00
1,4-Dichlorobenzene ND 4.9 0.22 1.00
Dichlorodifluoromethane ND 4.9 0.44 1.00
1,1-Dichloroethane ND 4.9 0.21 1.00
1,2-Dichloroethane ND 4.9 0.31 1.00
1,1-Dichloroethene ND 4.9 0.34 1.00
c-1,2-Dichloroethene ND 4.9 0.28 1.00
t-1,2-Dichloroethene ND 4.9 0.50 1.00
1,2-Dichloropropane ND 4.9 0.43 1.00
1,3-Dichloropropane ND 4.9 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 3 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 4.9 0.33 1.00
1,1-Dichloropropene ND 4.9 0.32 1.00
c-1,3-Dichloropropene ND 4.9 0.25 1.00
t-1,3-Dichloropropene ND 4.9 0.60 1.00
Ethylbenzene ND 4.9 0.15 1.00
2-Hexanone ND 49 1.7 1.00
Isopropylbenzene ND 4.9 0.54 1.00
p-Isopropyltoluene ND 4.9 0.62 1.00
Methylene Chloride ND 49 1.3 1.00
4-Methyl-2-Pentanone ND 49 4.3 1.00
Naphthalene ND 49 0.80 1.00
n-Propylbenzene ND 4.9 0.50 1.00
Styrene ND 4.9 0.60 1.00
1,1,1,2-Tetrachloroethane ND 4.9 0.24 1.00
1,1,2,2-Tetrachloroethane ND 4.9 0.34 1.00
Tetrachloroethene ND 4.9 0.21 1.00
Toluene ND 4.9 0.51 1.00
1,2,3-Trichlorobenzene ND 9.9 0.90 1.00
1,2,4-Trichlorobenzene ND 4.9 0.31 1.00
1,1,1-Trichloroethane ND 4.9 0.22 1.00
1,1,2-Trichloroethane ND 4.9 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 49 0.35 1.00
Trichloroethene ND 4.9 0.30 1.00
1,2,3-Trichloropropane ND 4.9 0.82 1.00
1,2,4-Trimethylbenzene ND 4.9 0.58 1.00
Trichlorofluoromethane ND 49 0.37 1.00
1,3,5-Trimethylbenzene ND 4.9 0.54 1.00
Vinyl Acetate ND 49 4.7 1.00
Vinyl Chloride ND 4.9 0.50 1.00
p/m-Xylene ND 4.9 0.26 1.00
o-Xylene ND 4.9 0.55 1.00
Methyl-t-Butyl Ether (MTBE) ND 4.9 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 98 60-132
Dibromofluoromethane 104 63-141
1,2-Dichloroethane-d4 109 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 4 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08A-10 16-06-2174-4-A 06/28/16
15:39
Solid GC/MS Q 06/30/16 07/01/16
16:56
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 4.9 0.13 1.00
Bromobenzene ND 4.9 0.21 1.00
Bromochloromethane ND 4.9 0.68 1.00
Bromodichloromethane ND 4.9 0.23 1.00
Bromoform ND 4.9 0.78 1.00
Bromomethane ND 25 9.3 1.00
2-Butanone ND 49 3.7 1.00
n-Butylbenzene ND 4.9 0.15 1.00
sec-Butylbenzene ND 4.9 0.57 1.00
tert-Butylbenzene ND 4.9 0.15 1.00
Carbon Disulfide ND 49 0.30 1.00
Carbon Tetrachloride ND 4.9 0.28 1.00
Chlorobenzene ND 4.9 0.22 1.00
Chloroethane ND 4.9 1.5 1.00
Chloroform ND 4.9 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 4.9 0.23 1.00
4-Chlorotoluene ND 4.9 0.21 1.00
Dibromochloromethane ND 4.9 0.56 1.00
1,2-Dibromo-3-Chloropropane ND 9.9 1.7 1.00
1,2-Dibromoethane ND 4.9 0.25 1.00
Dibromomethane ND 4.9 0.77 1.00
1,2-Dichlorobenzene ND 4.9 0.23 1.00
1,3-Dichlorobenzene ND 4.9 0.17 1.00
1,4-Dichlorobenzene ND 4.9 0.22 1.00
Dichlorodifluoromethane ND 4.9 0.44 1.00
1,1-Dichloroethane 0.37 4.9 0.21 1.00 J
1,2-Dichloroethane ND 4.9 0.31 1.00
1,1-Dichloroethene ND 4.9 0.34 1.00
c-1,2-Dichloroethene 0.61 4.9 0.28 1.00 J
t-1,2-Dichloroethene ND 4.9 0.50 1.00
1,2-Dichloropropane ND 4.9 0.43 1.00
1,3-Dichloropropane ND 4.9 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 5 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 4.9 0.33 1.00
1,1-Dichloropropene ND 4.9 0.32 1.00
c-1,3-Dichloropropene ND 4.9 0.25 1.00
t-1,3-Dichloropropene ND 4.9 0.60 1.00
Ethylbenzene ND 4.9 0.15 1.00
2-Hexanone ND 49 1.7 1.00
Isopropylbenzene ND 4.9 0.54 1.00
p-Isopropyltoluene ND 4.9 0.62 1.00
Methylene Chloride ND 49 1.3 1.00
4-Methyl-2-Pentanone ND 49 4.3 1.00
Naphthalene ND 49 0.80 1.00
n-Propylbenzene ND 4.9 0.50 1.00
Styrene ND 4.9 0.60 1.00
1,1,1,2-Tetrachloroethane ND 4.9 0.24 1.00
1,1,2,2-Tetrachloroethane ND 4.9 0.34 1.00
Tetrachloroethene ND 4.9 0.21 1.00
Toluene ND 4.9 0.51 1.00
1,2,3-Trichlorobenzene ND 9.9 0.90 1.00
1,2,4-Trichlorobenzene ND 4.9 0.31 1.00
1,1,1-Trichloroethane ND 4.9 0.22 1.00
1,1,2-Trichloroethane ND 4.9 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 49 0.35 1.00
Trichloroethene 5.8 4.9 0.30 1.00
1,2,3-Trichloropropane ND 4.9 0.82 1.00
1,2,4-Trimethylbenzene ND 4.9 0.58 1.00
Trichlorofluoromethane ND 49 0.37 1.00
1,3,5-Trimethylbenzene ND 4.9 0.54 1.00
Vinyl Acetate ND 49 4.7 1.00
Vinyl Chloride ND 4.9 0.50 1.00
p/m-Xylene ND 4.9 0.26 1.00
o-Xylene ND 4.9 0.55 1.00
Methyl-t-Butyl Ether (MTBE) ND 4.9 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 98 60-132
Dibromofluoromethane 103 63-141
1,2-Dichloroethane-d4 107 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 6 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08B-04 16-06-2174-6-A 06/28/16
15:56
Solid GC/MS Q 06/30/16 07/01/16
17:22
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.1 1.00
Benzene ND 4.9 0.13 1.00
Bromobenzene ND 4.9 0.21 1.00
Bromochloromethane ND 4.9 0.68 1.00
Bromodichloromethane ND 4.9 0.23 1.00
Bromoform ND 4.9 0.78 1.00
Bromomethane ND 25 9.2 1.00
2-Butanone ND 49 3.7 1.00
n-Butylbenzene ND 4.9 0.15 1.00
sec-Butylbenzene ND 4.9 0.57 1.00
tert-Butylbenzene ND 4.9 0.15 1.00
Carbon Disulfide ND 49 0.30 1.00
Carbon Tetrachloride ND 4.9 0.28 1.00
Chlorobenzene ND 4.9 0.22 1.00
Chloroethane ND 4.9 1.5 1.00
Chloroform ND 4.9 0.23 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 4.9 0.23 1.00
4-Chlorotoluene ND 4.9 0.21 1.00
Dibromochloromethane ND 4.9 0.56 1.00
1,2-Dibromo-3-Chloropropane ND 9.8 1.7 1.00
1,2-Dibromoethane ND 4.9 0.25 1.00
Dibromomethane ND 4.9 0.76 1.00
1,2-Dichlorobenzene ND 4.9 0.22 1.00
1,3-Dichlorobenzene ND 4.9 0.17 1.00
1,4-Dichlorobenzene ND 4.9 0.22 1.00
Dichlorodifluoromethane ND 4.9 0.43 1.00
1,1-Dichloroethane ND 4.9 0.21 1.00
1,2-Dichloroethane ND 4.9 0.31 1.00
1,1-Dichloroethene ND 4.9 0.34 1.00
c-1,2-Dichloroethene ND 4.9 0.27 1.00
t-1,2-Dichloroethene ND 4.9 0.50 1.00
1,2-Dichloropropane ND 4.9 0.43 1.00
1,3-Dichloropropane ND 4.9 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 7 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 4.9 0.32 1.00
1,1-Dichloropropene ND 4.9 0.32 1.00
c-1,3-Dichloropropene ND 4.9 0.25 1.00
t-1,3-Dichloropropene ND 4.9 0.59 1.00
Ethylbenzene ND 4.9 0.15 1.00
2-Hexanone ND 49 1.7 1.00
Isopropylbenzene ND 4.9 0.54 1.00
p-Isopropyltoluene ND 4.9 0.62 1.00
Methylene Chloride ND 49 1.3 1.00
4-Methyl-2-Pentanone ND 49 4.2 1.00
Naphthalene ND 49 0.80 1.00
n-Propylbenzene ND 4.9 0.49 1.00
Styrene ND 4.9 0.59 1.00
1,1,1,2-Tetrachloroethane ND 4.9 0.24 1.00
1,1,2,2-Tetrachloroethane ND 4.9 0.34 1.00
Tetrachloroethene ND 4.9 0.21 1.00
Toluene ND 4.9 0.51 1.00
1,2,3-Trichlorobenzene ND 9.8 0.90 1.00
1,2,4-Trichlorobenzene ND 4.9 0.30 1.00
1,1,1-Trichloroethane ND 4.9 0.22 1.00
1,1,2-Trichloroethane ND 4.9 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 49 0.35 1.00
Trichloroethene ND 4.9 0.29 1.00
1,2,3-Trichloropropane ND 4.9 0.81 1.00
1,2,4-Trimethylbenzene ND 4.9 0.57 1.00
Trichlorofluoromethane ND 49 0.37 1.00
1,3,5-Trimethylbenzene ND 4.9 0.54 1.00
Vinyl Acetate ND 49 4.7 1.00
Vinyl Chloride ND 4.9 0.49 1.00
p/m-Xylene ND 4.9 0.26 1.00
o-Xylene ND 4.9 0.55 1.00
Methyl-t-Butyl Ether (MTBE) ND 4.9 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 97 60-132
Dibromofluoromethane 105 63-141
1,2-Dichloroethane-d4 113 62-146
Toluene-d8 100 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 8 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08B-08 16-06-2174-7-A 06/28/16
15:57
Solid GC/MS Q 06/30/16 07/01/16
17:49
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 130 6.4 1.00
Benzene ND 5.1 0.13 1.00
Bromobenzene ND 5.1 0.21 1.00
Bromochloromethane ND 5.1 0.70 1.00
Bromodichloromethane ND 5.1 0.24 1.00
Bromoform ND 5.1 0.81 1.00
Bromomethane ND 26 9.6 1.00
2-Butanone ND 51 3.8 1.00
n-Butylbenzene ND 5.1 0.16 1.00
sec-Butylbenzene ND 5.1 0.59 1.00
tert-Butylbenzene ND 5.1 0.15 1.00
Carbon Disulfide ND 51 0.31 1.00
Carbon Tetrachloride ND 5.1 0.29 1.00
Chlorobenzene ND 5.1 0.23 1.00
Chloroethane ND 5.1 1.5 1.00
Chloroform ND 5.1 0.24 1.00
Chloromethane ND 26 0.31 1.00
2-Chlorotoluene ND 5.1 0.24 1.00
4-Chlorotoluene ND 5.1 0.22 1.00
Dibromochloromethane ND 5.1 0.58 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.1 0.26 1.00
Dibromomethane ND 5.1 0.79 1.00
1,2-Dichlorobenzene ND 5.1 0.23 1.00
1,3-Dichlorobenzene ND 5.1 0.18 1.00
1,4-Dichlorobenzene ND 5.1 0.23 1.00
Dichlorodifluoromethane ND 5.1 0.45 1.00
1,1-Dichloroethane ND 5.1 0.22 1.00
1,2-Dichloroethane ND 5.1 0.32 1.00
1,1-Dichloroethene ND 5.1 0.35 1.00
c-1,2-Dichloroethene ND 5.1 0.29 1.00
t-1,2-Dichloroethene ND 5.1 0.52 1.00
1,2-Dichloropropane ND 5.1 0.45 1.00
1,3-Dichloropropane ND 5.1 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 9 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.1 0.34 1.00
1,1-Dichloropropene ND 5.1 0.33 1.00
c-1,3-Dichloropropene ND 5.1 0.26 1.00
t-1,3-Dichloropropene ND 5.1 0.62 1.00
Ethylbenzene ND 5.1 0.15 1.00
2-Hexanone ND 51 1.8 1.00
Isopropylbenzene ND 5.1 0.56 1.00
p-Isopropyltoluene ND 5.1 0.64 1.00
Methylene Chloride ND 51 1.4 1.00
4-Methyl-2-Pentanone ND 51 4.4 1.00
Naphthalene ND 51 0.83 1.00
n-Propylbenzene ND 5.1 0.51 1.00
Styrene ND 5.1 0.62 1.00
1,1,1,2-Tetrachloroethane ND 5.1 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.1 0.35 1.00
Tetrachloroethene ND 5.1 0.21 1.00
Toluene ND 5.1 0.53 1.00
1,2,3-Trichlorobenzene ND 10 0.93 1.00
1,2,4-Trichlorobenzene ND 5.1 0.32 1.00
1,1,1-Trichloroethane ND 5.1 0.23 1.00
1,1,2-Trichloroethane ND 5.1 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 51 0.36 1.00
Trichloroethene 2.1 5.1 0.31 1.00 J
1,2,3-Trichloropropane ND 5.1 0.85 1.00
1,2,4-Trimethylbenzene ND 5.1 0.60 1.00
Trichlorofluoromethane ND 51 0.38 1.00
1,3,5-Trimethylbenzene ND 5.1 0.56 1.00
Vinyl Acetate ND 51 4.8 1.00
Vinyl Chloride ND 5.1 0.51 1.00
p/m-Xylene ND 5.1 0.27 1.00
o-Xylene ND 5.1 0.57 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.1 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 99 60-132
Dibromofluoromethane 104 63-141
1,2-Dichloroethane-d4 111 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 10 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08B-10 16-06-2174-8-A 06/28/16
15:58
Solid GC/MS Q 06/30/16 07/01/16
18:15
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.25 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.50 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 11 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.60 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.51 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.22 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene 0.69 5.0 0.30 1.00 J
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.37 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 97 60-132
Dibromofluoromethane 105 63-141
1,2-Dichloroethane-d4 111 62-146
Toluene-d8 100 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 12 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08C-04 16-06-2174-9-A 06/28/16
16:21
Solid GC/MS Q 06/30/16 07/01/16
18:42
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone 26 130 6.3 1.00 J
Benzene ND 5.1 0.13 1.00
Bromobenzene ND 5.1 0.21 1.00
Bromochloromethane ND 5.1 0.70 1.00
Bromodichloromethane ND 5.1 0.24 1.00
Bromoform ND 5.1 0.81 1.00
Bromomethane ND 25 9.6 1.00
2-Butanone ND 51 3.8 1.00
n-Butylbenzene ND 5.1 0.16 1.00
sec-Butylbenzene ND 5.1 0.59 1.00
tert-Butylbenzene ND 5.1 0.15 1.00
Carbon Disulfide ND 51 0.31 1.00
Carbon Tetrachloride ND 5.1 0.29 1.00
Chlorobenzene ND 5.1 0.23 1.00
Chloroethane ND 5.1 1.5 1.00
Chloroform ND 5.1 0.24 1.00
Chloromethane ND 25 0.31 1.00
2-Chlorotoluene ND 5.1 0.24 1.00
4-Chlorotoluene ND 5.1 0.22 1.00
Dibromochloromethane ND 5.1 0.58 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.8 1.00
1,2-Dibromoethane ND 5.1 0.26 1.00
Dibromomethane ND 5.1 0.79 1.00
1,2-Dichlorobenzene ND 5.1 0.23 1.00
1,3-Dichlorobenzene ND 5.1 0.18 1.00
1,4-Dichlorobenzene ND 5.1 0.23 1.00
Dichlorodifluoromethane ND 5.1 0.45 1.00
1,1-Dichloroethane ND 5.1 0.21 1.00
1,2-Dichloroethane ND 5.1 0.32 1.00
1,1-Dichloroethene ND 5.1 0.35 1.00
c-1,2-Dichloroethene 7.1 5.1 0.28 1.00
t-1,2-Dichloroethene ND 5.1 0.51 1.00
1,2-Dichloropropane ND 5.1 0.45 1.00
1,3-Dichloropropane ND 5.1 0.26 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 13 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.1 0.34 1.00
1,1-Dichloropropene ND 5.1 0.33 1.00
c-1,3-Dichloropropene ND 5.1 0.26 1.00
t-1,3-Dichloropropene ND 5.1 0.62 1.00
Ethylbenzene ND 5.1 0.15 1.00
2-Hexanone ND 51 1.8 1.00
Isopropylbenzene ND 5.1 0.56 1.00
p-Isopropyltoluene ND 5.1 0.64 1.00
Methylene Chloride ND 51 1.4 1.00
4-Methyl-2-Pentanone ND 51 4.4 1.00
Naphthalene ND 51 0.83 1.00
n-Propylbenzene ND 5.1 0.51 1.00
Styrene ND 5.1 0.61 1.00
1,1,1,2-Tetrachloroethane ND 5.1 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.1 0.35 1.00
Tetrachloroethene ND 5.1 0.21 1.00
Toluene ND 5.1 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.93 1.00
1,2,4-Trichlorobenzene ND 5.1 0.32 1.00
1,1,1-Trichloroethane ND 5.1 0.23 1.00
1,1,2-Trichloroethane ND 5.1 0.36 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 51 0.36 1.00
Trichloroethene 2.0 5.1 0.31 1.00 J
1,2,3-Trichloropropane ND 5.1 0.84 1.00
1,2,4-Trimethylbenzene ND 5.1 0.60 1.00
Trichlorofluoromethane ND 51 0.38 1.00
1,3,5-Trimethylbenzene ND 5.1 0.56 1.00
Vinyl Acetate ND 51 4.8 1.00
Vinyl Chloride ND 5.1 0.51 1.00
p/m-Xylene ND 5.1 0.27 1.00
o-Xylene ND 5.1 0.57 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.1 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 95 60-132
Dibromofluoromethane 106 63-141
1,2-Dichloroethane-d4 112 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 14 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
BB-08C-08 16-06-2174-11-A 06/28/16
16:22
Solid GC/MS Q 06/30/16 07/01/16
19:08
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone 17 120 6.2 1.00 J
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.68 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.3 1.00
2-Butanone ND 50 3.7 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.57 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.30 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 9.9 1.7 1.00
1,2-Dibromoethane ND 5.0 0.25 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.17 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.34 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.50 1.00
1,2-Dichloropropane ND 5.0 0.43 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 15 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.60 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.7 1.00
Isopropylbenzene ND 5.0 0.54 1.00
p-Isopropyltoluene ND 5.0 0.62 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.34 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.51 1.00
1,2,3-Trichlorobenzene ND 9.9 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.22 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.82 1.00
1,2,4-Trimethylbenzene ND 5.0 0.58 1.00
Trichlorofluoromethane ND 50 0.37 1.00
1,3,5-Trimethylbenzene ND 5.0 0.54 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.55 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.29 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 97 60-132
Dibromofluoromethane 105 63-141
1,2-Dichloroethane-d4 114 62-146
Toluene-d8 99 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 16 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-14-314-575 N/A Solid GC/MS Q 07/01/16 07/01/16 13:50
160701L013
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 17 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 98 60-132
Dibromofluoromethane 103 63-141
1,2-Dichloroethane-d4 111 62-146
Toluene-d8 97 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559 Page 18 of18
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-06-2175-51 Sample Solid GC 49 07/06/16 07/07/16 09:51 160706S06 16-06-2175-51 Matrix Spike Solid GC 49 07/06/16 07/07/16 06:23 160706S06 16-06-2175-51 Matrix Spike Duplicate Solid GC 49 07/06/16 07/07/16 06:40 160706S06 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
TPH as Diesel ND 400.0 357.2 89 365.8 91 64-130 2 0-15
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Project: UTAS - Due Diligence / 43559 Page 1 of3
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number BB-08A-04 Sample Solid GC/MS Q 06/30/16 07/01/16 14:43 160701S005 BB-08A-04 Matrix Spike Solid GC/MS Q 06/30/16 07/01/16 15:09 160701S005 BB-08A-04 Matrix Spike Duplicate Solid GC/MS Q 06/30/16 07/01/16 15:36 160701S005 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acetone ND 50.00 52.04 104 46.61 93 70-130 11 0-20
Benzene ND 50.00 44.00 88 40.08 80 61-127 9 0-20
Bromobenzene ND 50.00 46.86 94 42.40 85 70-130 10 0-20
Bromochloromethane ND 50.00 48.15 96 44.71 89 70-130 7 0-20 Bromodichloromethane ND 50.00 48.64 97 45.68 91 70-130 6 0-20 Bromoform ND 50.00 45.70 91 42.30 85 70-130 8 0-20
Bromomethane ND 50.00 44.69 89 41.48 83 70-130 7 0-20
2-Butanone ND 50.00 44.50 89 42.48 85 70-130 5 0-20
n-Butylbenzene ND 50.00 46.23 92 41.40 83 77-123 11 0-25 sec-Butylbenzene ND 50.00 45.96 92 41.75 83 70-130 10 0-20 tert-Butylbenzene ND 50.00 46.46 93 41.77 84 70-130 11 0-20 Carbon Disulfide ND 50.00 42.59 85 39.13 78 70-130 8 0-20 Carbon Tetrachloride ND 50.00 46.01 92 42.99 86 51-135 7 0-29 Chlorobenzene ND 50.00 45.03 90 41.10 82 57-123 9 0-20
Chloroethane ND 50.00 48.55 97 46.94 94 70-130 3 0-20
Chloroform ND 50.00 46.34 93 42.21 84 70-130 9 0-20
Chloromethane ND 50.00 47.30 95 46.31 93 70-130 2 0-20
2-Chlorotoluene ND 50.00 46.00 92 41.38 83 70-130 11 0-20 4-Chlorotoluene ND 50.00 47.22 94 41.35 83 70-130 13 0-20 Dibromochloromethane ND 50.00 47.39 95 44.29 89 70-130 7 0-20 1,2-Dibromo-3-Chloropropane ND 50.00 45.76 92 45.08 90 70-130 2 0-20 1,2-Dibromoethane ND 50.00 48.47 97 44.72 89 64-124 8 0-20 Dibromomethane ND 50.00 47.83 96 45.28 91 70-130 5 0-20 1,2-Dichlorobenzene ND 50.00 47.10 94 43.28 87 35-131 8 0-25 1,3-Dichlorobenzene ND 50.00 45.77 92 41.86 84 70-130 9 0-20 1,4-Dichlorobenzene ND 50.00 45.39 91 41.32 83 70-130 9 0-20 Dichlorodifluoromethane ND 50.00 57.60 115 55.88 112 70-130 3 0-20 1,1-Dichloroethane ND 50.00 45.55 91 42.03 84 70-130 8 0-20 1,2-Dichloroethane ND 50.00 46.49 93 44.19 88 70-130 5 0-20 1,1-Dichloroethene ND 50.00 44.24 88 41.31 83 47-143 7 0-25 c-1,2-Dichloroethene ND 50.00 45.09 90 42.02 84 70-130 7 0-20 t-1,2-Dichloroethene ND 50.00 44.96 90 42.39 85 70-130 6 0-20 1,2-Dichloropropane ND 50.00 46.07 92 42.48 85 79-115 8 0-25 1,3-Dichloropropane ND 50.00 46.66 93 42.67 85 70-130 9 0-20 2,2-Dichloropropane ND 50.00 46.71 93 42.84 86 70-130 9 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 2 of3
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
1,1-Dichloropropene ND 50.00 45.95 92 42.47 85 70-130 8 0-20 c-1,3-Dichloropropene ND 50.00 47.08 94 43.69 87 70-130 7 0-20 t-1,3-Dichloropropene ND 50.00 50.47 101 46.23 92 70-130 9 0-20 Ethylbenzene ND 50.00 45.82 92 41.13 82 57-129 11 0-22
2-Hexanone ND 50.00 41.96 84 41.74 83 70-130 1 0-20
Isopropylbenzene ND 50.00 45.73 91 41.27 83 70-130 10 0-20 p-Isopropyltoluene ND 50.00 47.15 94 42.30 85 70-130 11 0-20 Methylene Chloride ND 50.00 45.10 90 42.41 85 70-130 6 0-20 4-Methyl-2-Pentanone ND 50.00 41.82 84 41.33 83 70-130 1 0-20 Naphthalene ND 50.00 45.47 91 44.32 89 70-130 3 0-20
n-Propylbenzene ND 50.00 45.64 91 40.91 82 70-130 11 0-20 Styrene ND 50.00 47.03 94 41.88 84 70-130 12 0-20
1,1,1,2-Tetrachloroethane ND 50.00 49.39 99 44.87 90 70-130 10 0-20 1,1,2,2-Tetrachloroethane ND 50.00 45.02 90 43.15 86 70-130 4 0-20 Tetrachloroethene ND 50.00 48.71 97 43.81 88 70-130 11 0-20 Toluene ND 50.00 44.86 90 41.48 83 63-123 8 0-20
1,2,3-Trichlorobenzene ND 50.00 46.78 94 43.37 87 70-130 8 0-20 1,2,4-Trichlorobenzene ND 50.00 47.72 95 43.79 88 70-130 9 0-20 1,1,1-Trichloroethane ND 50.00 46.23 92 42.95 86 70-130 7 0-20 1,1,2-Trichloroethane ND 50.00 46.58 93 43.95 88 70-130 6 0-20 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50.00 45.77 92 42.11 84 70-130 8 0-20 Trichloroethene ND 50.00 45.50 91 42.47 85 44-158 7 0-20 1,2,3-Trichloropropane ND 50.00 47.06 94 43.79 88 70-130 7 0-20 1,2,4-Trimethylbenzene ND 50.00 45.62 91 41.67 83 70-130 9 0-20 Trichlorofluoromethane ND 50.00 54.57 109 52.04 104 70-130 5 0-20 1,3,5-Trimethylbenzene ND 50.00 46.44 93 41.53 83 70-130 11 0-20 Vinyl Acetate ND 50.00 34.75 70 31.62 63 70-130 9 0-20 3 Vinyl Chloride ND 50.00 52.01 104 49.78 100 49-139 4 0-47 p/m-Xylene ND 100.0 90.44 90 81.18 81 70-130 11 0-20
o-Xylene ND 50.00 46.64 93 42.13 84 70-130 10 0-20
Methyl-t-Butyl Ether (MTBE) ND 50.00 46.12 92 43.25 87 57-123 6 0-21 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 3 of3
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Duplicate Batch Number BB-08A-04 Sample Solid N/A 06/30/16 00:00 06/30/16 23:00 G0630MOID2 BB-08A-04 Sample Duplicate Solid N/A 06/30/16 00:00 06/30/16 23:00 G0630MOID2 Parameter Sample Conc. DUP Conc. RPD RPD CL Qualifiers
Moisture 23.30 24.20 4 0-10
Quality Control - Sample Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: N/A
Method: ASTM D-2216 (M)
Project: UTAS - Due Diligence / 43559 Page 1 of1
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-15-490-2152 LCS Solid GC 49 07/06/16 07/07/16 06:06 160706B06 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers TPH as Diesel 400.0 358.4 90 75-123
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 3550B
Method: EPA 8015B (M)
Project: UTAS - Due Diligence / 43559 Page 1 of3
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-14-314-575 LCS Solid GC/MS Q 07/01/16 07/01/16 12:44 160701L013 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Acetone 50.00 42.15 84 70-130 60-140
Benzene 50.00 42.99 86 78-120 71-127
Bromobenzene 50.00 46.11 92 70-130 60-140
Bromochloromethane 50.00 42.34 85 70-130 60-140
Bromodichloromethane 50.00 46.53 93 70-130 60-140
Bromoform 50.00 46.16 92 70-130 60-140
Bromomethane 50.00 39.09 78 70-130 60-140
2-Butanone 50.00 46.04 92 70-130 60-140
n-Butylbenzene 50.00 47.63 95 77-123 69-131
sec-Butylbenzene 50.00 46.91 94 70-130 60-140
tert-Butylbenzene 50.00 48.52 97 70-130 60-140
Carbon Disulfide 50.00 40.92 82 70-130 60-140
Carbon Tetrachloride 50.00 46.56 93 49-139 34-154
Chlorobenzene 50.00 44.86 90 79-120 72-127
Chloroethane 50.00 42.93 86 70-130 60-140
Chloroform 50.00 42.62 85 70-130 60-140
Chloromethane 50.00 42.51 85 70-130 60-140
2-Chlorotoluene 50.00 45.67 91 70-130 60-140
4-Chlorotoluene 50.00 46.76 94 70-130 60-140
Dibromochloromethane 50.00 44.46 89 70-130 60-140
1,2-Dibromo-3-Chloropropane 50.00 50.61 101 70-130 60-140 1,2-Dibromoethane 50.00 46.03 92 70-130 60-140
Dibromomethane 50.00 44.23 88 70-130 60-140
1,2-Dichlorobenzene 50.00 46.51 93 75-120 68-128
1,3-Dichlorobenzene 50.00 46.38 93 70-130 60-140
1,4-Dichlorobenzene 50.00 45.72 91 70-130 60-140
Dichlorodifluoromethane 50.00 52.25 104 70-130 60-140
1,1-Dichloroethane 50.00 42.71 85 70-130 60-140
1,2-Dichloroethane 50.00 44.78 90 70-130 60-140
1,1-Dichloroethene 50.00 43.18 86 74-122 66-130
c-1,2-Dichloroethene 50.00 41.30 83 70-130 60-140
t-1,2-Dichloroethene 50.00 43.32 87 70-130 60-140
1,2-Dichloropropane 50.00 44.24 88 79-115 73-121
1,3-Dichloropropane 50.00 44.15 88 70-130 60-140
2,2-Dichloropropane 50.00 46.05 92 70-130 60-140
1,1-Dichloropropene 50.00 45.08 90 70-130 60-140
c-1,3-Dichloropropene 50.00 47.36 95 70-130 60-140
t-1,3-Dichloropropene 50.00 48.00 96 70-130 60-140
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 2 of3
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 66
Total number of ME compounds: 0
Total number of ME compounds allowed: 3
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Ethylbenzene 50.00 46.83 94 76-120 69-127
2-Hexanone 50.00 48.04 96 70-130 60-140
Isopropylbenzene 50.00 46.68 93 70-130 60-140
p-Isopropyltoluene 50.00 48.14 96 70-130 60-140
Methylene Chloride 50.00 40.23 80 70-130 60-140
4-Methyl-2-Pentanone 50.00 48.08 96 70-130 60-140
Naphthalene 50.00 46.00 92 70-130 60-140
n-Propylbenzene 50.00 45.56 91 70-130 60-140
Styrene 50.00 46.05 92 70-130 60-140
1,1,1,2-Tetrachloroethane 50.00 48.99 98 70-130 60-140
1,1,2,2-Tetrachloroethane 50.00 46.77 94 70-130 60-140
Tetrachloroethene 50.00 44.87 90 70-130 60-140
Toluene 50.00 46.58 93 77-120 70-127
1,2,3-Trichlorobenzene 50.00 48.15 96 70-130 60-140
1,2,4-Trichlorobenzene 50.00 50.19 100 70-130 60-140
1,1,1-Trichloroethane 50.00 45.37 91 70-130 60-140
1,1,2-Trichloroethane 50.00 43.67 87 70-130 60-140
1,1,2-Trichloro-1,2,2-Trifluoroethane 50.00 45.23 90 70-130 60-140 Trichloroethene 50.00 45.70 91 70-130 60-140
1,2,3-Trichloropropane 50.00 47.15 94 70-130 60-140
1,2,4-Trimethylbenzene 50.00 46.96 94 70-130 60-140
Trichlorofluoromethane 50.00 48.59 97 70-130 60-140
1,3,5-Trimethylbenzene 50.00 47.22 94 70-130 60-140
Vinyl Acetate 50.00 36.86 74 70-130 60-140
Vinyl Chloride 50.00 46.30 93 68-122 59-131
p/m-Xylene 100.0 91.12 91 70-130 60-140
o-Xylene 50.00 46.77 94 70-130 60-140
Methyl-t-Butyl Ether (MTBE) 50.00 44.46 89 77-120 70-127 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 06/29/16
Work Order: 16-06-2174
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559 Page 3 of3
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Method Extraction Chemist ID Instrument Analytical Location ASTM D-2216 (M) N/A 1009 N/A 1
EPA 8015B (M) EPA 3550B 682 GC 49 1
EPA 8260B EPA 5030C 1055 GC/MS Q 2
Sample Analysis Summary Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2174 Page 1 of1
Location 1: 7440 Lincoln Way, Garden Grove, CA 92841
Location 2: 7445 Lampson Avenue, Garden Grove, CA 92841 Return to Contents
Qualifiers Definition
* See applicable analysis comment.
< Less than the indicated value.
> Greater than the indicated value.
1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clarification.
2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clarification. 3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
4 The MS/MSD RPD was out of control due to suspected matrix interference. 5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference. 6 Surrogate recovery below the acceptance limit.
7 Surrogate recovery above the acceptance limit.
B Analyte was present in the associated method blank.
BU Sample analyzed after holding time expired.
BV Sample received after holding time expired.
CI See case narrative.
E Concentration exceeds the calibration range.
ET Sample was extracted past end of recommended max. holding time.
HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.
HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons were also present (or detected).
HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detected).
J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated.
JA Analyte positively identified but quantitation is an estimate.
ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
ND Parameter not detected at the indicated reporting limit.
Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater.
SG The sample extract was subjected to Silica Gel treatment prior to analysis.
X % Recovery and/or RPD out-of-range.
Z Analyte presence was not confirmed by second column or GC/MS analysis.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations.
Glossary of Terms and Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-06-2174 Page 1 of1
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1 Virendra Patel
From: Foster, Keith <[email protected]>
Sent: Thursday, June 30, 2016 10:45 AM
To: Erick Ovalle
Cc: Scott, Bob; Burns, Tyree; Virendra Patel
Subject: RE: Sample receipt confirmation / 16-06-2174 / UTAS - Due Diligence / 43559 Attachments: DOC018.pdf
Eric,
Please see the attached COC with the matrix type and number of containers updated.
Please run the requested analyses on BB‐08A‐01
From: Erick Ovalle [mailto:[email protected]]
Sent: Thursday, June 30, 2016 10:35 AM
To: Scott, Bob; Foster, Keith; Burns, Tyree
Cc: Virendra Patel
Subject: Sample receipt confirmation / 16-06-2174 / UTAS - Due Diligence / 43559 Sample receipt confirmation attached. Please review and advise of any changes required. • Sample 1 (BB-08A-01): Water was present inside the sleeve. • The matrix type and number of containers was not filled out.
Please call with any questions or concerns.
Best Regards,
Erick Ovalle
Project Manager Assistant
Eurofins Calscience,Inc.
7440 Lincoln Way
Garden Grove, CA 92841‐1427
USA
Phone: +1 (714) 895‐5494
PRIVACY NOTICE:
This email (and/or the documents attached to it) is intended only for the use of the individual or entity to which it is addressed and may contain information that is privileged, confidential, or exempt from disclosure under applicable Federal or State law. If the reader of this message is not the intended recipient or the employee or agent responsible for delivering the message to the intended recipient, you are hereby notified that any dissemination, distribution, or copying of this communication is strictly prohibited. If you have received this communication in error, please notify us immediately and delete this e-mail and all attachments.
Notify us here to report this email as spam.
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Revised COC received from Keith
Foster (H&A) on 06/30/16 at 10:45am. - Virendra (ECI)
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WORK ORDER NUMBER: 16-07-0873
Analytical Report For
Client: Haley & Aldrich, Inc,
Client Project Name: UTAS - Due Diligence / 43559-013
Attention: Robert K. Scott
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Approved for release on by:
Virendra Patel
Project Manager
AIR SOIL WATER MARINE CHEMISTRY
Eurofins Calscience, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation is required or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached to this report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of this report is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Calscience is not responsible, legally or otherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise. 07/26/2016
Contents
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client Project Name: UTAS - Due Diligence / 43559-013
Work Order Number: 16-07-0873
1 Work Order Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 2 Case Narrative 16-07-0873. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 3 Sample Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 4 Detections Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 5 Client Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
5.1 ASTM D-2216 (M) Moisture Content (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
5.2 EPA 6010B/7471A CAC Title 22 Metals (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
5.3 EPA 6010B ICP Metals (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
5.4 EPA 7470A Mercury (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
5.5 EPA 7471A Mercury (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
5.6 EPA 8260B Volatile Organics (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
5.7 EPA 8260B Volatile Organics (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 6 Quality Control Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
6.1 MS/MSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
6.2 PDS/PDSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
6.3 Sample Duplicate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
6.4 LCS/LCSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38 7 Sample Analysis Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 8 Glossary of Terms and Qualifiers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48 9 Chain-of-Custody/Sample Receipt Form. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49 Condition Upon Receipt:
Samples were received under Chain-of-Custody (COC) on 07/13/16. They were assigned to Work Order 16-07-0873.
Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are integral elements of the analytical report and are presented at the back of the report.
Holding Times:
All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
Quality Control:
All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or described further within this report.
Subcontractor Information:
Unless otherwise noted below (or on the subcontract form), no samples were subcontracted.
Additional Comments:
Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from mass/sample basis to mass/volume basis using client-supplied air volumes.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are always reported on a wet weight basis.
Work Order Narrative
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-07-0873 Page 1 of1
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CASE NARRATIVE
Eurofins Calscience Work Order 16-07-0873
EPA Method 6010B Total Metals:
Project Required Detection Limit (PRDL):
The PRDL’s were analyzed as required per the project QAPP. The low level calibration check performed post the sample batch is outside acceptable range for Arsenic and Thallium on 07/21/16 for soil samples.
The PRDL’s were analyzed as required per the project QAPP. The low level calibration check performed post the sample batch is outside acceptable range for Antimony on 07/22/16 for soil samples.
Table A: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 6010B
Batch # Analytes(s)
160719S03 Antimony3,4, Barium3, Vanadium3and Zinc3
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control. 4: The MS/MSD RPD was out of control due to suspected matrix interference.
The LCS/LCSD recoveries for the associated sample batches are within acceptable control limits, therefore, the results have been released without any further action or qualification.
EPA Method 8260B Volatile Organics:
Continuing Calibration:
The continuing calibration (CC) was performed on 07/14/16 on GC/MS L. The percent RSDs in the continuing calibration was > 40% for 2-Chloroethyl Vinyl Ether and Chloromethane.
Table B: Matrix Spike / Matrix Spike Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160714S005 2-Chloroethyl Vinyl Ether3
160714S003 Bromomethane3, n-Butylbenzene3, Carbon Disulfide4, 1,4-Dichlorobenzene4, Dichlorodifluoromethane4, Methylene Chloride4, Napthalene3, 1,2,3-Trichlorobenzene3, 1,2,4-Trichlorobenzene3,
Trichlorofluoromethane4and Vinyl Acetate3,4
3: Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control. 4: The MS/MSD RPD was out of control due to suspected matrix interference. 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Return to Contents
Table C: Laboratory Control Sample (LCS) / LCS Duplicate outside acceptable limits EPA Method 8260B
Batch # Analytes(s)
160714L002 BromomethaneME and 2-Chloroethyl Vinyl EtherME ME: LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean). 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Return to Contents
Sample Identification Lab Number Collection Date and Time Number of Containers
Matrix
IDW - Soil 16-07-0873-1 07/12/16 13:30 2 Solid
IDW - Water 16-07-0873-2 07/12/16 13:40 6 Aqueous
Sample Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-07-0873
Project Name: UTAS - Due Diligence / 43559-013
PO Number:
Date/Time
Received:
07/13/16 19:20
Number of
Containers:
8 Attn: Robert K. Scott
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Subcontracted analyses, if any, are not included in this summary.
IDW - Soil (16-07-0873-1)
Moisture 11 0.10 % ASTM D-2216 (M) N/A
Arsenic 1.62 0.789 mg/kg EPA 6010B EPA 3050B
Barium 66.9 0.526 mg/kg EPA 6010B EPA 3050B
Beryllium 0.271 0.263 mg/kg EPA 6010B EPA 3050B
Cadmium 0.205 J 0.143* mg/kg EPA 6010B EPA 3050B
Chromium 13.6 0.263 mg/kg EPA 6010B EPA 3050B
Cobalt 7.34 0.263 mg/kg EPA 6010B EPA 3050B
Copper 7.80 0.526 mg/kg EPA 6010B EPA 3050B
Lead 3.48 0.526 mg/kg EPA 6010B EPA 3050B
Molybdenum 0.343 0.263 mg/kg EPA 6010B EPA 3050B
Nickel 5.56 0.263 mg/kg EPA 6010B EPA 3050B
Vanadium 46.8 0.263 mg/kg EPA 6010B EPA 3050B
Zinc 27.2 1.05 mg/kg EPA 6010B EPA 3050B
IDW - Water (16-07-0873-2)
Arsenic 0.0107 0.0100 mg/L EPA 6010B EPA 3010A Total
Barium 0.0287 0.0100 mg/L EPA 6010B EPA 3010A Total
Chromium 0.00542 J 0.00271* mg/L EPA 6010B EPA 3010A Total Copper 0.0165 0.0100 mg/L EPA 6010B EPA 3010A Total
Molybdenum 0.0658 0.0100 mg/L EPA 6010B EPA 3010A Total Nickel 0.0100 0.0100 mg/L EPA 6010B EPA 3010A Total
Thallium 0.00805 B,J 0.00291* mg/L EPA 6010B EPA 3010A Total Vanadium 0.0251 0.0100 mg/L EPA 6010B EPA 3010A Total
Zinc 0.0235 0.0100 mg/L EPA 6010B EPA 3010A Total
Acetone 7.0 J 3.5* ug/L EPA 8260B EPA 5030C
Bromodichloromethane 0.21 J 0.20* ug/L EPA 8260B EPA 5030C Bromoform 0.49 J 0.34* ug/L EPA 8260B EPA 5030C
Carbon Disulfide 1.1 1.0 ug/L EPA 8260B EPA 5030C
Dibromochloromethane 1.2 0.50 ug/L EPA 8260B EPA 5030C
Tert-Butyl Alcohol (TBA) 5.7 J 4.1* ug/L EPA 8260B EPA 5030C Detections Summary
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Client: Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Work Order: 16-07-0873
Project Name: UTAS - Due Diligence / 43559-013
Received: 07/13/16
Attn: Robert K. Scott Page 1 of1
Client SampleID
Analyte Result Qualifiers RL Units Method Extraction
* MDL is shown
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Soil 16-07-0873-1-A 07/12/16
13:30
Solid N/A 07/14/16 07/15/16
11:00
G0715MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture 11 0.10 0.10 1.00
Method Blank 099-05-014-6123 N/A Solid N/A 07/14/16 07/15/16 11:00
G0715MOIB4
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Moisture ND 0.10 0.10 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: N/A
Method: ASTM D-2216 (M)
Units: %
Project: UTAS - Due Diligence / 43559-013 Page 1 of1
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Soil 16-07-0873-1-AA 07/12/16
13:30
Solid ICP 7300 07/19/16 07/21/16
11:06
160719L03U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.789 0.157 1.05
Arsenic 1.62 0.789 0.273 1.05
Barium 66.9 0.526 0.163 1.05
Beryllium 0.271 0.263 0.144 1.05
Cadmium 0.205 0.526 0.143 1.05 J
Chromium 13.6 0.263 0.150 1.05
Cobalt 7.34 0.263 0.156 1.05
Copper 7.80 0.526 0.142 1.05
Lead 3.48 0.526 0.139 1.05
Molybdenum 0.343 0.263 0.139 1.05
Nickel 5.56 0.263 0.152 1.05
Selenium ND 0.789 0.315 1.05
Silver ND 0.263 0.0902 1.05
Thallium ND 0.789 0.160 1.05
Vanadium 46.8 0.263 0.149 1.05
Zinc 27.2 1.05 0.187 1.05
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559-013 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 097-01-002-22971 N/A Solid ICP 7300 07/19/16 07/21/16 11:02
160719L03U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.758 0.150 1.01
Arsenic ND 0.758 0.262 1.01
Barium ND 0.505 0.156 1.01
Beryllium ND 0.253 0.138 1.01
Cadmium ND 0.505 0.137 1.01
Chromium ND 0.253 0.144 1.01
Cobalt ND 0.253 0.150 1.01
Copper ND 0.505 0.136 1.01
Lead ND 0.505 0.133 1.01
Molybdenum ND 0.253 0.133 1.01
Nickel ND 0.253 0.146 1.01
Selenium ND 0.758 0.303 1.01
Silver ND 0.253 0.0866 1.01
Thallium 0.321 0.758 0.153 1.01 J
Vanadium ND 0.253 0.143 1.01
Zinc ND 1.01 0.179 1.01
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3050B
Method: EPA 6010B
Units: mg/kg
Project: UTAS - Due Diligence / 43559-013 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Water 16-07-0873-2-F 07/12/16
13:40
Aqueous ICP 7300 07/16/16 07/21/16
10:51
160716LA1U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.0150 0.00787 1.00
Arsenic 0.0107 0.0100 0.00438 1.00
Barium 0.0287 0.0100 0.00296 1.00
Beryllium ND 0.0100 0.000561 1.00
Cadmium ND 0.0100 0.00269 1.00
Chromium 0.00542 0.0100 0.00271 1.00 J
Cobalt ND 0.0100 0.00295 1.00
Copper 0.0165 0.0100 0.00267 1.00
Lead ND 0.0100 0.00406 1.00
Molybdenum 0.0658 0.0100 0.00278 1.00
Nickel 0.0100 0.0100 0.00298 1.00
Selenium ND 0.0150 0.00699 1.00
Silver ND 0.00500 0.00139 1.00
Thallium 0.00805 0.0150 0.00291 1.00 B,J
Vanadium 0.0251 0.0100 0.00244 1.00
Zinc 0.0235 0.0100 0.00352 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3010A Total
Method: EPA 6010B
Units: mg/L
Project: UTAS - Due Diligence / 43559-013 Page 1 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-16-458-46 N/A Aqueous ICP 7300 07/16/16 07/22/16 10:48
160716LA1U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Antimony ND 0.0150 0.00787 1.00
Arsenic ND 0.0100 0.00438 1.00
Barium ND 0.0100 0.00296 1.00
Beryllium ND 0.0100 0.000561 1.00
Cadmium ND 0.0100 0.00269 1.00
Chromium ND 0.0100 0.00271 1.00
Cobalt ND 0.0100 0.00295 1.00
Copper ND 0.0100 0.00267 1.00
Lead ND 0.0100 0.00406 1.00
Molybdenum ND 0.0100 0.00278 1.00
Nickel ND 0.0100 0.00298 1.00
Selenium ND 0.0150 0.00699 1.00
Silver ND 0.00500 0.00139 1.00
Thallium 0.00297 0.0150 0.00291 1.00 J
Vanadium ND 0.0100 0.00244 1.00
Zinc ND 0.0100 0.00352 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3010A Total
Method: EPA 6010B
Units: mg/L
Project: UTAS - Due Diligence / 43559-013 Page 2 of2
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Water 16-07-0873-2-F 07/12/16
13:40
Aqueous Mercury 04 07/20/16 07/21/16
12:08
160720LA3
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.000500 0.0000453 1.00
Method Blank 099-04-008-7926 N/A Aqueous Mercury 04 07/20/16 07/21/16 12:02
160720LA3
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.000500 0.0000453 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7470A Total
Method: EPA 7470A
Units: mg/L
Project: UTAS - Due Diligence / 43559-013 Page 1 of1
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Soil 16-07-0873-1-AA 07/12/16
13:30
Solid Mercury 05 07/20/16 07/20/16
15:29
160720L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.0806 0.00568 1.00
Method Blank 099-16-480-51 N/A Solid Mercury 05 07/20/16 07/20/16 15:24
160720L02U
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Mercury ND 0.0833 0.00587 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7471A Total
Method: EPA 7471A
Units: mg/kg
Project: UTAS - Due Diligence / 43559-013 Page 1 of1
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Water 16-07-0873-2-A 07/12/16
13:40
Aqueous GC/MS L 07/14/16 07/14/16
19:16
160714L002
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone 7.0 10 3.5 1.00 J
Benzene ND 0.50 0.32 1.00
Bromobenzene ND 0.50 0.33 1.00
Bromochloromethane ND 1.0 0.38 1.00
Bromodichloromethane 0.21 0.50 0.20 1.00 J
Bromoform 0.49 0.50 0.34 1.00 J
Bromomethane ND 1.0 0.38 1.00
2-Butanone ND 5.0 2.9 1.00
n-Butylbenzene ND 0.50 0.34 1.00
sec-Butylbenzene ND 0.50 0.23 1.00
tert-Butylbenzene ND 0.50 0.38 1.00
Carbon Disulfide 1.1 1.0 0.44 1.00
Carbon Tetrachloride ND 0.50 0.22 1.00
Chlorobenzene ND 0.50 0.14 1.00
Chloroethane ND 0.50 0.34 1.00
2-Chloroethyl Vinyl Ether ND 5.0 3.1 1.00
Chloroform ND 0.50 0.22 1.00
Chloromethane ND 0.50 0.22 1.00
2-Chlorotoluene ND 0.50 0.34 1.00
4-Chlorotoluene ND 0.50 0.33 1.00
Dibromochloromethane 1.2 0.50 0.24 1.00
1,2-Dibromo-3-Chloropropane ND 5.0 2.9 1.00
1,2-Dibromoethane ND 0.50 0.34 1.00
Dibromomethane ND 0.50 0.34 1.00
1,2-Dichlorobenzene ND 0.50 0.17 1.00
1,3-Dichlorobenzene ND 0.50 0.17 1.00
1,4-Dichlorobenzene ND 0.50 0.31 1.00
Dichlorodifluoromethane ND 1.0 0.24 1.00
1,1-Dichloroethane ND 0.50 0.19 1.00
1,2-Dichloroethane ND 0.50 0.18 1.00
1,1-Dichloroethene ND 0.50 0.20 1.00
c-1,2-Dichloroethene ND 0.50 0.24 1.00
t-1,2-Dichloroethene ND 0.50 0.26 1.00
Acetonitrile ND 10 2.2 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559-013 Page 1 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
1,2-Dichloropropane ND 0.50 0.24 1.00
Acrolein ND 20 8.8 1.00
Acrylonitrile ND 10 5.2 1.00
1,3-Dichloropropane ND 1.0 0.24 1.00
2,2-Dichloropropane ND 1.0 0.42 1.00
Allyl Chloride ND 1.0 0.36 1.00
1,1-Dichloropropene ND 0.50 0.28 1.00
c-1,3-Dichloropropene ND 0.50 0.18 1.00
t-1,3-Dichloropropene ND 0.50 0.35 1.00
Ethylbenzene ND 0.50 0.32 1.00
2-Hexanone ND 10 2.6 1.00
Isopropylbenzene ND 0.50 0.42 1.00
p-Isopropyltoluene ND 0.50 0.14 1.00
Methylene Chloride ND 1.0 0.38 1.00
4-Methyl-2-Pentanone ND 5.0 2.7 1.00
Naphthalene ND 1.0 0.41 1.00
n-Propylbenzene ND 0.50 0.38 1.00
Styrene ND 0.50 0.32 1.00
Chloroprene ND 0.50 0.24 1.00
1,1,1,2-Tetrachloroethane ND 0.50 0.24 1.00
1,1,2,2-Tetrachloroethane ND 0.50 0.22 1.00
Tetrachloroethene ND 0.50 0.22 1.00
Toluene ND 0.50 0.26 1.00
1,2,3-Trichlorobenzene ND 0.50 0.25 1.00
Ethyl Methacrylate ND 5.0 1.4 1.00
1,2,4-Trichlorobenzene ND 0.50 0.25 1.00
1,1,1-Trichloroethane ND 0.50 0.19 1.00
Hexachloro-1,3-Butadiene ND 2.0 0.48 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 0.50 0.26 1.00 1,1,2-Trichloroethane ND 0.50 0.32 1.00
Iodomethane ND 10 6.8 1.00
Trichloroethene ND 0.50 0.23 1.00
Trichlorofluoromethane ND 0.50 0.25 1.00
Isobutyl Alcohol ND 10 6.7 1.00
1,2,3-Trichloropropane ND 1.0 0.25 1.00
1,2,4-Trimethylbenzene ND 0.50 0.15 1.00
Methacrylonitrile ND 10 2.5 1.00
Methyl Methacrylate ND 5.0 1.3 1.00
1,3,5-Trimethylbenzene ND 0.50 0.33 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559-013 Page 2 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
Vinyl Acetate ND 5.0 2.2 1.00
Vinyl Chloride ND 0.50 0.27 1.00
p/m-Xylene ND 0.50 0.24 1.00
o-Xylene ND 0.50 0.39 1.00
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.29 1.00
t-1,4-Dichloro-2-Butene ND 5.0 3.0 1.00
Tetrahydrofuran ND 5.0 2.2 1.00
Propionitrile ND 10 3.1 1.00
Tert-Butyl Alcohol (TBA) 5.7 10 4.1 1.00 J
Diisopropyl Ether (DIPE) ND 0.50 0.24 1.00
Ethyl-t-Butyl Ether (ETBE) ND 0.50 0.22 1.00
Tert-Amyl-Methyl Ether (TAME) ND 0.50 0.24 1.00
Ethanol ND 50 17 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 91 68-120
Dibromofluoromethane 107 71-135
1,2-Dichloroethane-d4 115 64-139
Toluene-d8 100 72-128
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559-013 Page 3 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-16-446-110 N/A Aqueous GC/MS L 07/14/16 07/14/16 10:28
160714L002
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 10 3.5 1.00
Benzene ND 0.50 0.32 1.00
Bromobenzene ND 0.50 0.33 1.00
Bromochloromethane ND 1.0 0.38 1.00
Bromodichloromethane ND 0.50 0.20 1.00
Bromoform ND 0.50 0.34 1.00
Bromomethane ND 1.0 0.38 1.00
2-Butanone ND 5.0 2.9 1.00
n-Butylbenzene ND 0.50 0.34 1.00
sec-Butylbenzene ND 0.50 0.23 1.00
tert-Butylbenzene ND 0.50 0.38 1.00
Carbon Disulfide ND 1.0 0.44 1.00
Carbon Tetrachloride ND 0.50 0.22 1.00
Chlorobenzene ND 0.50 0.14 1.00
Chloroethane ND 0.50 0.34 1.00
2-Chloroethyl Vinyl Ether ND 5.0 3.1 1.00
Chloroform ND 0.50 0.22 1.00
Chloromethane ND 0.50 0.22 1.00
2-Chlorotoluene ND 0.50 0.34 1.00
4-Chlorotoluene ND 0.50 0.33 1.00
Dibromochloromethane ND 0.50 0.24 1.00
1,2-Dibromo-3-Chloropropane ND 5.0 2.9 1.00
1,2-Dibromoethane ND 0.50 0.34 1.00
Dibromomethane ND 0.50 0.34 1.00
1,2-Dichlorobenzene ND 0.50 0.17 1.00
1,3-Dichlorobenzene ND 0.50 0.17 1.00
1,4-Dichlorobenzene ND 0.50 0.31 1.00
Dichlorodifluoromethane ND 1.0 0.24 1.00
1,1-Dichloroethane ND 0.50 0.19 1.00
1,2-Dichloroethane ND 0.50 0.18 1.00
1,1-Dichloroethene ND 0.50 0.20 1.00
c-1,2-Dichloroethene ND 0.50 0.24 1.00
t-1,2-Dichloroethene ND 0.50 0.26 1.00
Acetonitrile ND 10 2.2 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559-013 Page 4 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
1,2-Dichloropropane ND 0.50 0.24 1.00
Acrolein ND 20 8.8 1.00
Acrylonitrile ND 10 5.2 1.00
1,3-Dichloropropane ND 1.0 0.24 1.00
2,2-Dichloropropane ND 1.0 0.42 1.00
Allyl Chloride ND 1.0 0.36 1.00
1,1-Dichloropropene ND 0.50 0.28 1.00
c-1,3-Dichloropropene ND 0.50 0.18 1.00
t-1,3-Dichloropropene ND 0.50 0.35 1.00
Ethylbenzene ND 0.50 0.32 1.00
2-Hexanone ND 10 2.6 1.00
Isopropylbenzene ND 0.50 0.42 1.00
p-Isopropyltoluene ND 0.50 0.14 1.00
Methylene Chloride ND 1.0 0.38 1.00
4-Methyl-2-Pentanone ND 5.0 2.7 1.00
Naphthalene ND 1.0 0.41 1.00
n-Propylbenzene ND 0.50 0.38 1.00
Styrene ND 0.50 0.32 1.00
Chloroprene ND 0.50 0.24 1.00
1,1,1,2-Tetrachloroethane ND 0.50 0.24 1.00
1,1,2,2-Tetrachloroethane ND 0.50 0.22 1.00
Tetrachloroethene ND 0.50 0.22 1.00
Toluene ND 0.50 0.26 1.00
1,2,3-Trichlorobenzene ND 0.50 0.25 1.00
Ethyl Methacrylate ND 5.0 1.4 1.00
1,2,4-Trichlorobenzene ND 0.50 0.25 1.00
1,1,1-Trichloroethane ND 0.50 0.19 1.00
Hexachloro-1,3-Butadiene ND 2.0 0.48 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 0.50 0.26 1.00 1,1,2-Trichloroethane ND 0.50 0.32 1.00
Iodomethane ND 10 6.8 1.00
Trichloroethene ND 0.50 0.23 1.00
Trichlorofluoromethane ND 0.50 0.25 1.00
Isobutyl Alcohol ND 10 6.7 1.00
1,2,3-Trichloropropane ND 1.0 0.25 1.00
1,2,4-Trimethylbenzene ND 0.50 0.15 1.00
Methacrylonitrile ND 10 2.5 1.00
Methyl Methacrylate ND 5.0 1.3 1.00
1,3,5-Trimethylbenzene ND 0.50 0.33 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559-013 Page 5 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
Vinyl Acetate ND 5.0 2.2 1.00
Vinyl Chloride ND 0.50 0.27 1.00
p/m-Xylene ND 0.50 0.24 1.00
o-Xylene ND 0.50 0.39 1.00
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.29 1.00
t-1,4-Dichloro-2-Butene ND 5.0 3.0 1.00
Tetrahydrofuran ND 5.0 2.2 1.00
Propionitrile ND 10 3.1 1.00
Tert-Butyl Alcohol (TBA) ND 10 4.1 1.00
Diisopropyl Ether (DIPE) ND 0.50 0.24 1.00
Ethyl-t-Butyl Ether (ETBE) ND 0.50 0.22 1.00
Tert-Amyl-Methyl Ether (TAME) ND 0.50 0.24 1.00
Ethanol ND 50 17 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 90 68-120
Dibromofluoromethane 99 71-135
1,2-Dichloroethane-d4 102 64-139
Toluene-d8 96 72-128
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/L
Project: UTAS - Due Diligence / 43559-013 Page 6 of6
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
IDW - Soil 16-07-0873-1-B 07/12/16
13:30
Solid GC/MS Q 07/14/16 07/14/16
11:08
160714L008
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559-013 Page 1 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 96 60-132
Dibromofluoromethane 104 63-141
1,2-Dichloroethane-d4 107 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559-013 Page 2 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Client Sample Number Lab Sample
Number
Date/Time
Collected
Matrix Instrument Date
Prepared
Date/Time
Analyzed
QC Batch ID
Method Blank 099-14-314-583 N/A Solid GC/MS Q 07/14/16 07/14/16 10:15
160714L008
Comment(s): - Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.
Parameter Result RL MDL DF Qualifiers
Acetone ND 120 6.2 1.00
Benzene ND 5.0 0.13 1.00
Bromobenzene ND 5.0 0.21 1.00
Bromochloromethane ND 5.0 0.69 1.00
Bromodichloromethane ND 5.0 0.23 1.00
Bromoform ND 5.0 0.79 1.00
Bromomethane ND 25 9.4 1.00
2-Butanone ND 50 3.8 1.00
n-Butylbenzene ND 5.0 0.16 1.00
sec-Butylbenzene ND 5.0 0.58 1.00
tert-Butylbenzene ND 5.0 0.15 1.00
Carbon Disulfide ND 50 0.31 1.00
Carbon Tetrachloride ND 5.0 0.28 1.00
Chlorobenzene ND 5.0 0.22 1.00
Chloroethane ND 5.0 1.5 1.00
Chloroform ND 5.0 0.24 1.00
Chloromethane ND 25 0.30 1.00
2-Chlorotoluene ND 5.0 0.23 1.00
4-Chlorotoluene ND 5.0 0.21 1.00
Dibromochloromethane ND 5.0 0.57 1.00
1,2-Dibromo-3-Chloropropane ND 10 1.7 1.00
1,2-Dibromoethane ND 5.0 0.26 1.00
Dibromomethane ND 5.0 0.77 1.00
1,2-Dichlorobenzene ND 5.0 0.23 1.00
1,3-Dichlorobenzene ND 5.0 0.18 1.00
1,4-Dichlorobenzene ND 5.0 0.22 1.00
Dichlorodifluoromethane ND 5.0 0.44 1.00
1,1-Dichloroethane ND 5.0 0.21 1.00
1,2-Dichloroethane ND 5.0 0.31 1.00
1,1-Dichloroethene ND 5.0 0.35 1.00
c-1,2-Dichloroethene ND 5.0 0.28 1.00
t-1,2-Dichloroethene ND 5.0 0.51 1.00
1,2-Dichloropropane ND 5.0 0.44 1.00
1,3-Dichloropropane ND 5.0 0.25 1.00
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559-013 Page 3 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Parameter Result RL MDL DF Qualifiers
2,2-Dichloropropane ND 5.0 0.33 1.00
1,1-Dichloropropene ND 5.0 0.33 1.00
c-1,3-Dichloropropene ND 5.0 0.25 1.00
t-1,3-Dichloropropene ND 5.0 0.61 1.00
Ethylbenzene ND 5.0 0.15 1.00
2-Hexanone ND 50 1.8 1.00
Isopropylbenzene ND 5.0 0.55 1.00
p-Isopropyltoluene ND 5.0 0.63 1.00
Methylene Chloride ND 50 1.3 1.00
4-Methyl-2-Pentanone ND 50 4.3 1.00
Naphthalene ND 50 0.81 1.00
n-Propylbenzene ND 5.0 0.50 1.00
Styrene ND 5.0 0.60 1.00
1,1,1,2-Tetrachloroethane ND 5.0 0.24 1.00
1,1,2,2-Tetrachloroethane ND 5.0 0.35 1.00
Tetrachloroethene ND 5.0 0.21 1.00
Toluene ND 5.0 0.52 1.00
1,2,3-Trichlorobenzene ND 10 0.91 1.00
1,2,4-Trichlorobenzene ND 5.0 0.31 1.00
1,1,1-Trichloroethane ND 5.0 0.23 1.00
1,1,2-Trichloroethane ND 5.0 0.35 1.00
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50 0.35 1.00
Trichloroethene ND 5.0 0.30 1.00
1,2,3-Trichloropropane ND 5.0 0.83 1.00
1,2,4-Trimethylbenzene ND 5.0 0.59 1.00
Trichlorofluoromethane ND 50 0.38 1.00
1,3,5-Trimethylbenzene ND 5.0 0.55 1.00
Vinyl Acetate ND 50 4.7 1.00
Vinyl Chloride ND 5.0 0.50 1.00
p/m-Xylene ND 5.0 0.27 1.00
o-Xylene ND 5.0 0.56 1.00
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.30 1.00
Surrogate Rec. (%) Control Limits Qualifiers
1,4-Bromofluorobenzene 99 60-132
Dibromofluoromethane 101 63-141
1,2-Dichloroethane-d4 103 62-146
Toluene-d8 98 70-130
Analytical Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Units: ug/kg
Project: UTAS - Due Diligence / 43559-013 Page 4 of4
RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number IDW - Soil Sample Solid ICP 7300 07/19/16 07/21/16 11:06 160719S03 IDW - Soil Matrix Spike Solid ICP 7300 07/19/16 07/21/16 11:07 160719S03 IDW - Soil Matrix Spike Duplicate Solid ICP 7300 07/19/16 07/21/16 11:08 160719S03 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Antimony ND 25.00 6.108 24 8.447 34 50-115 32 0-20 3,4
Arsenic 1.620 25.00 30.02 114 27.69 104 75-125 8 0-20
Barium 66.91 25.00 110.5 175 93.98 108 75-125 16 0-20 3 Beryllium 0.2706 25.00 28.52 113 25.88 102 75-125 10 0-20 Cadmium ND 25.00 28.39 114 25.70 103 75-125 10 0-20
Chromium 13.62 25.00 43.83 121 39.34 103 75-125 11 0-20 Cobalt 7.342 25.00 37.28 120 32.87 102 75-125 13 0-20
Copper 7.798 25.00 38.47 123 34.28 106 75-125 12 0-20
Lead 3.480 25.00 31.98 114 29.64 105 75-125 8 0-20
Molybdenum 0.3425 25.00 24.78 98 23.42 92 75-125 6 0-20 Nickel 5.560 25.00 34.00 114 31.25 103 75-125 8 0-20
Selenium ND 25.00 26.18 105 24.91 100 75-125 5 0-20
Silver ND 12.50 13.69 110 12.73 102 75-125 7 0-20
Thallium ND 25.00 27.80 111 26.22 105 75-125 6 0-20
Vanadium 46.79 25.00 78.61 127 68.96 89 75-125 13 0-20 3 Zinc 27.20 25.00 59.97 131 54.36 109 75-125 10 0-20 3
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559-013 Page 1 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number IDW - Water Sample Aqueous ICP 7300 07/16/16 07/21/16 10:51 160716SA1 IDW - Water Matrix Spike Aqueous ICP 7300 07/16/16 07/21/16 10:53 160716SA1 IDW - Water Matrix Spike Duplicate Aqueous ICP 7300 07/16/16 07/21/16 10:54 160716SA1 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Antimony ND 0.5000 0.5304 106 0.5317 106 75-125 0 0-20
Arsenic 0.01074 0.5000 0.5593 110 0.5560 109 75-125 1 0-20 Barium 0.02871 0.5000 0.5544 105 0.5507 104 75-125 1 0-20 Beryllium ND 0.5000 0.5287 106 0.5249 105 75-125 1 0-20 Cadmium ND 0.5000 0.5258 105 0.5209 104 75-125 1 0-20
Chromium ND 0.5000 0.5248 105 0.5208 104 75-125 1 0-20
Cobalt ND 0.5000 0.5444 109 0.5479 110 75-125 1 0-20
Copper 0.01651 0.5000 0.5474 106 0.5483 106 75-125 0 0-20 Lead ND 0.5000 0.5148 103 0.5188 104 75-125 1 0-20
Molybdenum 0.06583 0.5000 0.5882 104 0.5939 106 75-125 1 0-20 Nickel 0.01002 0.5000 0.5393 106 0.5417 106 75-125 0 0-20 Selenium ND 0.5000 0.5154 103 0.5375 108 75-125 4 0-20
Silver ND 0.2500 0.2598 104 0.2585 103 75-125 0 0-20
Thallium ND 0.5000 0.5324 106 0.5228 105 75-125 2 0-20
Vanadium 0.02513 0.5000 0.5453 104 0.5439 104 75-125 0 0-20 Zinc 0.02352 0.5000 0.5723 110 0.5746 110 75-125 0 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3010A Total
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559-013 Page 2 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number IDW - Soil Sample Solid Mercury 05 07/20/16 07/20/16 15:29 160720S02 IDW - Soil Matrix Spike Solid Mercury 05 07/20/16 07/20/16 15:31 160720S02 IDW - Soil Matrix Spike Duplicate Solid Mercury 05 07/20/16 07/20/16 15:33 160720S02 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Mercury ND 0.8350 0.8919 107 0.8996 108 75-125 1 0-20
Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559-013 Page 3 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number 16-07-0683-1 Sample Aqueous GC/MS L 07/14/16 07/14/16 11:06 160714S005 16-07-0683-1 Matrix Spike Aqueous GC/MS L 07/14/16 07/14/16 12:01 160714S005 16-07-0683-1 Matrix Spike Duplicate Aqueous GC/MS L 07/14/16 07/14/16 12:28 160714S005 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acetone ND 10.00 9.104 91 9.775 98 51-163 7 0-82
Benzene ND 10.00 10.62 106 10.37 104 77-121 2 0-21
Bromobenzene ND 10.00 10.66 107 10.39 104 78-120 3 0-20 Bromochloromethane ND 10.00 9.394 94 9.760 98 71-135 4 0-28 Bromodichloromethane ND 10.00 10.54 105 10.62 106 72-129 1 0-26 Bromoform ND 10.00 9.599 96 9.918 99 61-140 3 0-22
Bromomethane ND 10.00 6.823 68 6.499 65 63-140 5 0-36
2-Butanone ND 10.00 8.234 82 8.812 88 55-138 7 0-45
n-Butylbenzene ND 10.00 11.16 112 10.98 110 67-127 2 0-26 sec-Butylbenzene ND 10.00 11.20 112 10.99 110 66-122 2 0-26 tert-Butylbenzene ND 10.00 11.13 111 10.96 110 73-120 2 0-26 Carbon Disulfide ND 10.00 10.37 104 10.69 107 27-170 3 0-36 Carbon Tetrachloride ND 10.00 10.82 108 11.43 114 64-135 5 0-31 Chlorobenzene ND 10.00 10.69 107 10.53 105 80-120 2 0-20 Chloroethane ND 10.00 10.62 106 9.576 96 67-131 10 0-35 2-Chloroethyl Vinyl Ether ND 10.00 0 0 0 0 60-139 0 0-90 3 Chloroform ND 10.00 9.551 96 9.687 97 75-126 1 0-20
Chloromethane ND 10.00 7.089 71 6.772 68 54-143 5 0-41
2-Chlorotoluene ND 10.00 11.08 111 10.79 108 64-123 3 0-34 4-Chlorotoluene ND 10.00 10.76 108 10.53 105 67-126 2 0-23 Dibromochloromethane ND 10.00 9.763 98 9.786 98 76-132 0 0-23 1,2-Dibromo-3-Chloropropane ND 10.00 8.926 89 9.720 97 65-125 9 0-31 1,2-Dibromoethane ND 10.00 10.27 103 10.12 101 74-130 1 0-22 Dibromomethane ND 10.00 9.894 99 10.04 100 75-127 1 0-29 1,2-Dichlorobenzene ND 10.00 10.51 105 10.31 103 78-120 2 0-19 1,3-Dichlorobenzene ND 10.00 10.51 105 10.27 103 75-120 2 0-22 1,4-Dichlorobenzene ND 10.00 10.25 103 10.03 100 78-120 2 0-21 Dichlorodifluoromethane ND 10.00 7.802 78 6.993 70 25-168 11 0-41 1,1-Dichloroethane ND 10.00 10.01 100 10.17 102 63-144 2 0-32 1,2-Dichloroethane ND 10.00 10.16 102 10.09 101 72-130 1 0-25 1,1-Dichloroethene ND 10.00 10.00 100 10.41 104 66-130 4 0-32 c-1,2-Dichloroethene ND 10.00 9.355 94 9.587 96 76-123 2 0-32 t-1,2-Dichloroethene ND 10.00 10.06 101 10.20 102 67-129 1 0-35 Acetonitrile ND 20.00 19.69 98 20.38 102 70-130 3 0-35
1,2-Dichloropropane ND 10.00 10.35 103 10.31 103 74-122 0 0-24 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 4 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acrolein ND 20.00 19.04 95 20.65 103 70-130 8 0-35
Acrylonitrile ND 10.00 9.122 91 9.758 98 65-149 7 0-89
1,3-Dichloropropane ND 10.00 10.32 103 10.18 102 74-128 1 0-21 2,2-Dichloropropane ND 10.00 9.898 99 9.948 99 68-125 1 0-40 Allyl Chloride ND 10.00 9.497 95 9.925 99 70-130 4 0-35 1,1-Dichloropropene ND 10.00 10.00 100 10.24 102 68-119 2 0-26 c-1,3-Dichloropropene ND 10.00 9.788 98 9.821 98 76-126 0 0-24 t-1,3-Dichloropropene ND 10.00 9.405 94 9.537 95 71-127 1 0-22 Ethylbenzene ND 10.00 11.10 111 10.96 110 78-120 1 0-23 2-Hexanone ND 10.00 8.681 87 9.252 93 61-137 6 0-36
Isopropylbenzene ND 10.00 11.35 114 11.28 113 71-123 1 0-24 p-Isopropyltoluene ND 10.00 11.24 112 11.03 110 68-122 2 0-25 Methylene Chloride ND 10.00 9.573 96 9.514 95 71-129 1 0-30 4-Methyl-2-Pentanone ND 10.00 8.328 83 9.070 91 60-136 9 0-41 Naphthalene ND 10.00 9.279 93 9.687 97 55-159 4 0-30
n-Propylbenzene ND 10.00 11.44 114 11.29 113 64-125 1 0-35 Styrene ND 10.00 11.07 111 10.68 107 77-120 4 0-23
Chloroprene ND 10.00 10.39 104 10.54 105 70-130 1 0-35
1,1,1,2-Tetrachloroethane ND 10.00 11.14 111 11.14 111 79-123 0 0-20 1,1,2,2-Tetrachloroethane ND 10.00 9.613 96 9.634 96 67-132 0 0-25 Tetrachloroethene ND 10.00 10.70 107 10.63 106 72-119 1 0-24 Toluene ND 10.00 10.65 106 10.58 106 78-120 1 0-25
1,2,3-Trichlorobenzene ND 10.00 9.904 99 9.815 98 70-129 1 0-27 Ethyl Methacrylate ND 10.00 9.242 92 9.774 98 70-130 6 0-35 1,2,4-Trichlorobenzene ND 10.00 9.938 99 9.967 100 71-128 0 0-26 1,1,1-Trichloroethane ND 10.00 9.996 100 10.24 102 66-130 2 0-30 Hexachloro-1,3-Butadiene ND 10.00 10.91 109 10.70 107 52-128 2 0-30 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10.00 10.37 104 10.54 105 52-145 2 0-35 1,1,2-Trichloroethane ND 10.00 10.41 104 10.13 101 77-124 3 0-25 Iodomethane ND 20.00 14.25 71 15.05 75 70-130 5 0-35
Trichloroethene ND 10.00 10.42 104 10.50 105 75-116 1 0-24 Trichlorofluoromethane ND 10.00 10.55 105 9.904 99 62-146 6 0-36 Isobutyl Alcohol ND 20.00 18.52 93 15.68 78 70-130 17 0-35 1,2,3-Trichloropropane ND 10.00 9.874 99 10.25 103 80-120 4 0-20 1,2,4-Trimethylbenzene ND 10.00 10.95 110 10.68 107 70-127 3 0-23 Methacrylonitrile ND 10.00 7.790 78 8.874 89 70-130 13 0-35 Methyl Methacrylate ND 10.00 8.523 85 9.109 91 70-130 7 0-35 1,3,5-Trimethylbenzene ND 10.00 11.37 114 11.40 114 72-124 0 0-23 Vinyl Acetate ND 10.00 5.964 60 8.029 80 45-164 30 0-74 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 5 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Vinyl Chloride ND 10.00 9.972 100 8.664 87 60-141 14 0-34 p/m-Xylene ND 20.00 22.66 113 22.24 111 74-122 2 0-23
o-Xylene ND 10.00 11.16 112 11.01 110 74-122 1 0-24
Methyl-t-Butyl Ether (MTBE) ND 10.00 8.967 90 9.430 94 57-144 5 0-31 t-1,4-Dichloro-2-Butene ND 10.00 10.03 100 10.51 105 70-130 5 0-35 Tetrahydrofuran ND 10.00 7.930 79 8.746 87 70-130 10 0-35 Propionitrile ND 10.00 8.729 87 9.159 92 70-130 5 0-35
Tert-Butyl Alcohol (TBA) ND 50.00 58.38 117 50.29 101 43-170 15 0-38 Diisopropyl Ether (DIPE) ND 10.00 10.26 103 10.33 103 70-130 1 0-35 Ethyl-t-Butyl Ether (ETBE) ND 10.00 8.944 89 9.176 92 70-130 3 0-35 Tert-Amyl-Methyl Ether (TAME) ND 10.00 9.709 97 9.944 99 70-130 2 0-35 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 6 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number IDW - Soil Sample Solid GC/MS Q 07/14/16 07/14/16 11:08 160714S003 IDW - Soil Matrix Spike Solid GC/MS Q 07/14/16 07/14/16 11:34 160714S003 IDW - Soil Matrix Spike Duplicate Solid GC/MS Q 07/14/16 07/14/16 12:00 160714S003 Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Acetone ND 50.00 46.94 94 44.51 89 70-130 5 0-20
Benzene ND 50.00 44.80 90 41.58 83 61-127 7 0-20
Bromobenzene ND 50.00 40.10 80 38.07 76 70-130 5 0-20
Bromochloromethane ND 50.00 47.33 95 38.54 77 70-130 20 0-20 Bromodichloromethane ND 50.00 45.43 91 40.31 81 70-130 12 0-20 Bromoform ND 50.00 42.88 86 44.13 88 70-130 3 0-20
Bromomethane ND 50.00 41.30 83 34.02 68 70-130 19 0-20 3 2-Butanone ND 50.00 45.01 90 46.77 94 70-130 4 0-20
n-Butylbenzene ND 50.00 37.66 75 35.05 70 77-123 7 0-25 3 sec-Butylbenzene ND 50.00 39.93 80 38.25 76 70-130 4 0-20 tert-Butylbenzene ND 50.00 42.06 84 40.47 81 70-130 4 0-20 Carbon Disulfide ND 50.00 47.82 96 38.76 78 70-130 21 0-20 4 Carbon Tetrachloride ND 50.00 46.68 93 41.10 82 51-135 13 0-29 Chlorobenzene ND 50.00 41.41 83 39.48 79 57-123 5 0-20
Chloroethane ND 50.00 48.05 96 39.92 80 70-130 18 0-20
Chloroform ND 50.00 43.57 87 36.87 74 70-130 17 0-20
Chloromethane ND 50.00 47.36 95 39.13 78 70-130 19 0-20 2-Chlorotoluene ND 50.00 39.80 80 37.97 76 70-130 5 0-20 4-Chlorotoluene ND 50.00 39.85 80 37.48 75 70-130 6 0-20 Dibromochloromethane ND 50.00 44.19 88 40.68 81 70-130 8 0-20 1,2-Dibromo-3-Chloropropane ND 50.00 39.91 80 44.59 89 70-130 11 0-20 1,2-Dibromoethane ND 50.00 44.54 89 42.58 85 64-124 5 0-20 Dibromomethane ND 50.00 45.29 91 38.96 78 70-130 15 0-20 1,2-Dichlorobenzene ND 50.00 36.91 74 35.25 70 35-131 5 0-25 1,3-Dichlorobenzene ND 50.00 36.51 73 35.01 70 70-130 4 0-20 1,4-Dichlorobenzene ND 50.00 36.33 73 34.51 69 70-130 5 0-20 3 Dichlorodifluoromethane ND 50.00 43.76 88 35.38 71 70-130 21 0-20 4 1,1-Dichloroethane ND 50.00 46.70 93 38.56 77 70-130 19 0-20 1,2-Dichloroethane ND 50.00 42.34 85 38.08 76 70-130 11 0-20 1,1-Dichloroethene ND 50.00 47.29 95 39.49 79 47-143 18 0-25 c-1,2-Dichloroethene ND 50.00 46.49 93 38.32 77 70-130 19 0-20 t-1,2-Dichloroethene ND 50.00 47.63 95 40.48 81 70-130 16 0-20 1,2-Dichloropropane ND 50.00 45.91 92 42.55 85 79-115 8 0-25 1,3-Dichloropropane ND 50.00 45.04 90 41.94 84 70-130 7 0-20 2,2-Dichloropropane ND 50.00 45.20 90 39.42 79 70-130 14 0-20 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 7 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Sample
Conc.
Spike
Added
MS
Conc.
MS
%Rec.
MSD
Conc.
MSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
1,1-Dichloropropene ND 50.00 45.81 92 40.90 82 70-130 11 0-20 c-1,3-Dichloropropene ND 50.00 45.38 91 43.49 87 70-130 4 0-20 t-1,3-Dichloropropene ND 50.00 46.52 93 44.18 88 70-130 5 0-20 Ethylbenzene ND 50.00 43.23 86 41.65 83 57-129 4 0-22
2-Hexanone ND 50.00 44.77 90 53.92 108 70-130 19 0-20
Isopropylbenzene ND 50.00 42.85 86 41.13 82 70-130 4 0-20 p-Isopropyltoluene ND 50.00 39.38 79 37.27 75 70-130 6 0-20 Methylene Chloride ND 50.00 47.11 94 37.03 74 70-130 24 0-20 4 4-Methyl-2-Pentanone ND 50.00 44.92 90 52.30 105 70-130 15 0-20 Naphthalene ND 50.00 32.66 65 30.55 61 70-130 7 0-20 3
n-Propylbenzene ND 50.00 42.01 84 38.56 77 70-130 9 0-20 Styrene ND 50.00 43.49 87 41.07 82 70-130 6 0-20
1,1,1,2-Tetrachloroethane ND 50.00 44.35 89 43.14 86 70-130 3 0-20 1,1,2,2-Tetrachloroethane ND 50.00 41.60 83 45.16 90 70-130 8 0-20 Tetrachloroethene ND 50.00 45.86 92 45.26 91 70-130 1 0-20 Toluene ND 50.00 44.04 88 42.93 86 63-123 3 0-20
1,2,3-Trichlorobenzene ND 50.00 25.63 51 23.19 46 70-130 10 0-20 3 1,2,4-Trichlorobenzene ND 50.00 27.33 55 25.09 50 70-130 9 0-20 3 1,1,1-Trichloroethane ND 50.00 44.00 88 38.22 76 70-130 14 0-20 1,1,2-Trichloroethane ND 50.00 42.56 85 40.99 82 70-130 4 0-20 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 50.00 49.33 99 42.15 84 70-130 16 0-20 Trichloroethene ND 50.00 45.99 92 42.41 85 44-158 8 0-20 1,2,3-Trichloropropane ND 50.00 42.94 86 43.20 86 70-130 1 0-20 1,2,4-Trimethylbenzene ND 50.00 39.26 79 37.86 76 70-130 4 0-20 Trichlorofluoromethane ND 50.00 46.22 92 37.02 74 70-130 22 0-20 4 1,3,5-Trimethylbenzene ND 50.00 41.10 82 38.03 76 70-130 8 0-20 Vinyl Acetate ND 50.00 27.83 56 22.06 44 70-130 23 0-20 3,4 Vinyl Chloride ND 50.00 51.27 103 41.33 83 49-139 21 0-47 p/m-Xylene ND 100.0 84.87 85 81.44 81 70-130 4 0-20
o-Xylene ND 50.00 42.60 85 40.93 82 70-130 4 0-20
Methyl-t-Butyl Ether (MTBE) ND 50.00 45.01 90 43.78 88 57-123 3 0-21 Quality Control - Spike/Spike Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 8 of8
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
IDW - Soil Sample Solid ICP 7300 07/19/16 00:00 07/21/16 11:06 160719S03 IDW - Soil PDS Solid ICP 7300 07/19/16 00:00 07/21/16 11:09 160719S03 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Antimony ND 25.00 25.80 103 75-125
Arsenic 1.620 25.00 28.98 109 75-125
Barium 66.91 25.00 93.31 106 75-125
Beryllium 0.2706 25.00 26.53 105 75-125
Cadmium ND 25.00 26.38 106 75-125
Chromium 13.62 25.00 39.91 105 75-125
Cobalt 7.342 25.00 34.59 109 75-125
Copper 7.798 25.00 34.96 109 75-125
Lead 3.480 25.00 30.22 107 75-125
Molybdenum 0.3425 25.00 26.89 106 75-125
Nickel 5.560 25.00 32.08 106 75-125
Selenium ND 25.00 26.45 106 75-125
Silver ND 12.50 12.92 103 75-125
Thallium ND 25.00 26.64 107 75-125
Vanadium 46.79 25.00 72.10 101 75-125
Zinc 27.20 25.00 53.77 106 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559-013 Page 1 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
IDW - Water Sample Aqueous ICP 7300 07/16/16 00:00 07/21/16 10:51 160716SA1 IDW - Water PDS Aqueous ICP 7300 07/16/16 00:00 07/21/16 10:55 160716SA1 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Antimony ND 0.5000 0.4740 95 75-125
Arsenic 0.01074 0.5000 0.5448 107 75-125
Barium 0.02871 0.5000 0.5335 101 75-125
Beryllium ND 0.5000 0.5080 102 75-125
Cadmium ND 0.5000 0.5075 102 75-125
Chromium ND 0.5000 0.5072 101 75-125
Cobalt ND 0.5000 0.5404 108 75-125
Copper 0.01651 0.5000 0.5328 103 75-125
Lead ND 0.5000 0.5066 101 75-125
Molybdenum 0.06583 0.5000 0.5874 104 75-125
Nickel 0.01002 0.5000 0.5353 105 75-125
Selenium ND 0.5000 0.5183 104 75-125
Silver ND 0.2500 0.2442 98 75-125
Thallium ND 0.5000 0.5235 105 75-125
Vanadium 0.02513 0.5000 0.5263 100 75-125
Zinc 0.02352 0.5000 0.5704 109 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3010A Total
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559-013 Page 2 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
IDW - Water Sample Aqueous Mercury 04 07/20/16 00:00 07/21/16 12:08 160720PSA3 IDW - Water PDS Aqueous Mercury 04 07/20/16 00:00 07/21/16 12:11 160720PSA3 IDW - Water PDSD Aqueous Mercury 04 07/20/16 00:00 07/21/16 12:13 160720PSA3 Parameter Sample
Conc.
Spike
Added
PDS
Conc.
PDS
%Rec.
PDSD
Conc.
PDSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Mercury ND 0.01000 0.009581 96 0.01034 103 75-125 8 0-20 Quality Control - PDS/PDSD
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7470A Total
Method: EPA 7470A
Project: UTAS - Due Diligence / 43559-013 Page 3 of4
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD Batch Number
IDW - Soil Sample Solid Mercury 05 07/20/16 00:00 07/20/16 15:29 160720S02 IDW - Soil PDS Solid Mercury 05 07/20/16 00:00 07/20/16 15:36 160720S02 Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers Mercury ND 0.8350 0.8423 101 75-125
Quality Control - PDS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559-013 Page 4 of4
RPD: Relative Percent Difference. CL: Control Limits
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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Duplicate Batch Number 16-07-0851-1 Sample Solid N/A 07/14/16 00:00 07/15/16 11:00 G0715MOID4 16-07-0851-1 Sample Duplicate Solid N/A 07/14/16 00:00 07/15/16 11:00 G0715MOID4 Parameter Sample Conc. DUP Conc. RPD RPD CL Qualifiers
Moisture 6.900 7.000 1 0-10
Quality Control - Sample Duplicate
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: N/A
Method: ASTM D-2216 (M)
Project: UTAS - Due Diligence / 43559-013 Page 1 of1
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 097-01-002-22971 LCS Solid ICP 7300 07/19/16 07/21/16 11:03 160719L03U Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Antimony 25.00 26.10 104 80-120 73-127
Arsenic 25.00 25.77 103 80-120 73-127
Barium 25.00 26.81 107 80-120 73-127
Beryllium 25.00 25.87 103 80-120 73-127
Cadmium 25.00 25.94 104 80-120 73-127
Chromium 25.00 26.28 105 80-120 73-127
Cobalt 25.00 27.74 111 80-120 73-127
Copper 25.00 26.36 105 80-120 73-127
Lead 25.00 27.48 110 80-120 73-127
Molybdenum 25.00 26.43 106 80-120 73-127
Nickel 25.00 27.25 109 80-120 73-127
Selenium 25.00 25.71 103 80-120 73-127
Silver 12.50 12.93 103 80-120 73-127
Thallium 25.00 27.99 112 80-120 73-127
Vanadium 25.00 25.29 101 80-120 73-127
Zinc 25.00 26.71 107 80-120 73-127
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3050B
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559-013 Page 1 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 16
Total number of ME compounds: 0
Total number of ME compounds allowed: 1
LCS ME CL validation result: Pass
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-458-46 LCS Aqueous ICP 7300 07/16/16 07/21/16 10:58 160716LA1U Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Antimony 0.5000 0.4991 100 80-120 73-127
Arsenic 0.5000 0.4962 99 80-120 73-127
Barium 0.5000 0.5136 103 80-120 73-127
Beryllium 0.5000 0.4827 97 80-120 73-127
Cadmium 0.5000 0.5130 103 80-120 73-127
Chromium 0.5000 0.5170 103 80-120 73-127
Cobalt 0.5000 0.5378 108 80-120 73-127
Copper 0.5000 0.5184 104 80-120 73-127
Lead 0.5000 0.5286 106 80-120 73-127
Molybdenum 0.5000 0.5096 102 80-120 73-127
Nickel 0.5000 0.5373 107 80-120 73-127
Selenium 0.5000 0.4755 95 80-120 73-127
Silver 0.2500 0.2466 99 80-120 73-127
Thallium 0.5000 0.5316 106 80-120 73-127
Vanadium 0.5000 0.4964 99 80-120 73-127
Zinc 0.5000 0.5357 107 80-120 73-127
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 3010A Total
Method: EPA 6010B
Project: UTAS - Due Diligence / 43559-013 Page 2 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS/LCSD Batch Number 099-04-008-7926 LCS Aqueous Mercury 04 07/20/16 07/21/16 12:04 160720LA3 099-04-008-7926 LCSD Aqueous Mercury 04 07/20/16 07/21/16 12:06 160720LA3 Parameter Spike Added LCS Conc. LCS
%Rec.
LCSD Conc. LCSD
%Rec.
%Rec. CL RPD RPD CL Qualifiers
Mercury 0.01000 0.01026 103 0.01023 102 80-120 0 0-20
Quality Control - LCS/LCSD
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7470A Total
Method: EPA 7470A
Project: UTAS - Due Diligence / 43559-013 Page 3 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-16-480-51 LCS Solid Mercury 05 07/20/16 07/20/16 15:27 160720L02U Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers Mercury 0.8350 0.8745 105 80-120
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 7471A Total
Method: EPA 7471A
Project: UTAS - Due Diligence / 43559-013 Page 4 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS/LCSD Batch Number 099-16-446-110 LCS Aqueous GC/MS L 07/14/16 07/14/16 09:20 160714L002 099-16-446-110 LCSD Aqueous GC/MS L 07/14/16 07/14/16 09:47 160714L002 Parameter Spike
Added
LCS Conc. LCS
%Rec.
LCSD
Conc.
LCSD
%Rec.
%Rec. CL ME CL RPD RPD CL Qualifiers
Acetone 10.00 9.206 92 9.423 94 51-163 32-182 2 0-82
Benzene 10.00 10.49 105 10.43 104 77-121 70-128 1 0-21
Bromobenzene 10.00 10.75 108 10.79 108 78-120 71-127 0 0-20 Bromochloromethane 10.00 9.614 96 10.02 100 71-135 60-146 4 0-28 Bromodichloromethane 10.00 10.98 110 11.05 110 72-129 62-138 1 0-26 Bromoform 10.00 11.42 114 10.99 110 61-140 48-153 4 0-22 Bromomethane 10.00 6.080 61 6.508 65 63-140 50-153 7 0-36 ME 2-Butanone 10.00 9.025 90 9.420 94 55-138 41-152 4 0-45 n-Butylbenzene 10.00 11.32 113 10.95 110 67-127 57-137 3 0-26 sec-Butylbenzene 10.00 11.34 113 10.97 110 66-122 57-131 3 0-26 tert-Butylbenzene 10.00 11.35 114 11.00 110 73-120 65-128 3 0-26 Carbon Disulfide 10.00 10.71 107 10.63 106 27-170 3-194 1 0-36 Carbon Tetrachloride 10.00 11.35 114 11.11 111 64-135 52-147 2 0-31 Chlorobenzene 10.00 10.82 108 10.67 107 80-120 73-127 1 0-20 Chloroethane 10.00 9.778 98 10.19 102 67-131 56-142 4 0-35 2-Chloroethyl Vinyl Ether 10.00 5.778 58 7.445 74 60-139 47-152 25 0-90 ME Chloroform 10.00 9.645 96 9.772 98 75-126 66-134 1 0-31 Chloromethane 10.00 6.418 64 6.623 66 54-143 39-158 3 0-41 2-Chlorotoluene 10.00 11.08 111 10.98 110 64-123 54-133 1 0-34 4-Chlorotoluene 10.00 11.01 110 10.64 106 67-126 57-136 3 0-23 Dibromochloromethane 10.00 10.37 104 10.52 105 76-132 67-141 1 0-23 1,2-Dibromo-3-Chloropropane 10.00 10.25 102 11.14 111 65-125 55-135 8 0-31 1,2-Dibromoethane 10.00 10.63 106 10.74 107 74-130 65-139 1 0-22 Dibromomethane 10.00 9.930 99 10.37 104 75-127 66-136 4 0-29 1,2-Dichlorobenzene 10.00 10.69 107 10.68 107 78-120 71-127 0 0-19 1,3-Dichlorobenzene 10.00 10.65 106 10.53 105 75-120 68-128 1 0-22 1,4-Dichlorobenzene 10.00 10.46 105 10.41 104 78-120 71-127 0 0-21 Dichlorodifluoromethane 10.00 9.064 91 9.156 92 25-168 1-192 1 0-41 1,1-Dichloroethane 10.00 10.33 103 10.41 104 63-144 50-158 1 0-32 1,2-Dichloroethane 10.00 9.900 99 10.20 102 72-130 62-140 3 0-25 1,1-Dichloroethene 10.00 10.16 102 10.28 103 66-130 55-141 1 0-32 c-1,2-Dichloroethene 10.00 9.341 93 9.706 97 76-123 68-131 4 0-32 t-1,2-Dichloroethene 10.00 10.11 101 9.337 93 67-129 57-139 8 0-35 Acetonitrile 20.00 19.42 97 16.66 83 70-130 60-140 15 0-35 1,2-Dichloropropane 10.00 10.46 105 10.69 107 74-122 66-130 2 0-24 Acrolein 20.00 23.52 118 25.20 126 70-130 60-140 7 0-35 Quality Control - LCS/LCSD
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 5 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Parameter Spike
Added
LCS Conc. LCS
%Rec.
LCSD
Conc.
LCSD
%Rec.
%Rec. CL ME CL RPD RPD CL Qualifiers
Acrylonitrile 10.00 8.933 89 8.087 81 65-149 51-163 10 0-89 1,3-Dichloropropane 10.00 10.34 103 10.56 106 74-128 65-137 2 0-21 2,2-Dichloropropane 10.00 10.13 101 9.477 95 68-125 58-134 7 0-40 Allyl Chloride 10.00 10.11 101 8.936 89 70-130 60-140 12 0-35 1,1-Dichloropropene 10.00 10.29 103 10.25 103 68-119 60-128 0 0-26 c-1,3-Dichloropropene 10.00 10.48 105 10.74 107 76-126 68-134 3 0-24 t-1,3-Dichloropropene 10.00 10.03 100 10.14 101 71-127 62-136 1 0-22 Ethylbenzene 10.00 11.27 113 10.92 109 78-120 71-127 3 0-23 2-Hexanone 10.00 9.599 96 10.28 103 61-137 48-150 7 0-36 Isopropylbenzene 10.00 11.50 115 11.24 112 71-123 62-132 2 0-24 p-Isopropyltoluene 10.00 11.36 114 11.03 110 68-122 59-131 3 0-25 Methylene Chloride 10.00 9.554 96 8.965 90 71-129 61-139 6 0-30 4-Methyl-2-Pentanone 10.00 9.149 91 9.556 96 60-136 47-149 4 0-41 Naphthalene 10.00 10.07 101 10.34 103 55-159 38-176 3 0-30 n-Propylbenzene 10.00 11.48 115 11.15 111 64-125 54-135 3 0-35 Styrene 10.00 11.21 112 11.21 112 77-120 70-127 0 0-23
Chloroprene 10.00 10.96 110 10.83 108 70-130 60-140 1 0-35 1,1,1,2-Tetrachloroethane 10.00 11.90 119 11.72 117 79-123 72-130 2 0-20 1,1,2,2-Tetrachloroethane 10.00 10.39 104 10.34 103 67-132 56-143 0 0-25 Tetrachloroethene 10.00 11.11 111 10.64 106 72-119 64-127 4 0-24 Toluene 10.00 10.67 107 10.67 107 78-120 71-127 0 0-25
1,2,3-Trichlorobenzene 10.00 10.31 103 10.42 104 70-129 60-139 1 0-27 Ethyl Methacrylate 10.00 9.850 99 10.47 105 70-130 60-140 6 0-35 1,2,4-Trichlorobenzene 10.00 10.40 104 10.54 105 71-128 62-138 1 0-26 1,1,1-Trichloroethane 10.00 10.16 102 9.978 100 66-130 55-141 2 0-30 Hexachloro-1,3-Butadiene 10.00 11.26 113 10.81 108 52-128 39-141 4 0-30 1,1,2-Trichloro-1,2,2-
Trifluoroethane
10.00 10.53 105 10.32 103 52-145 36-160 2 0-35
1,1,2-Trichloroethane 10.00 10.76 108 10.59 106 77-124 69-132 2 0-25 Iodomethane 20.00 15.42 77 16.15 81 70-130 60-140 5 0-35 Trichloroethene 10.00 10.56 106 10.57 106 75-116 68-123 0 0-24 Trichlorofluoromethane 10.00 10.01 100 10.25 103 62-146 48-160 2 0-36 Isobutyl Alcohol 20.00 16.20 81 18.11 91 70-130 60-140 11 0-35 1,2,3-Trichloropropane 10.00 10.50 105 10.76 108 80-120 73-127 2 0-20 1,2,4-Trimethylbenzene 10.00 11.00 110 10.86 109 70-127 60-136 1 0-23 Methacrylonitrile 10.00 8.478 85 8.923 89 70-130 60-140 5 0-35 Methyl Methacrylate 10.00 9.406 94 9.948 99 70-130 60-140 6 0-35 1,3,5-Trimethylbenzene 10.00 11.37 114 11.35 113 72-124 63-133 0 0-23 Vinyl Acetate 10.00 8.467 85 8.718 87 45-164 25-184 3 0-74 Vinyl Chloride 10.00 9.380 94 10.19 102 60-141 46-154 8 0-34 Quality Control - LCS/LCSD
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 6 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 85
Total number of ME compounds: 2
Total number of ME compounds allowed: 4
LCS ME CL validation result: Pass
Parameter Spike
Added
LCS Conc. LCS
%Rec.
LCSD
Conc.
LCSD
%Rec.
%Rec. CL ME CL RPD RPD CL Qualifiers
p/m-Xylene 20.00 22.73 114 22.28 111 74-122 66-130 2 0-23 o-Xylene 10.00 11.29 113 11.10 111 74-122 66-130 2 0-24 Methyl-t-Butyl Ether (MTBE) 10.00 9.270 93 8.960 90 57-144 42-158 3 0-31 t-1,4-Dichloro-2-Butene 10.00 10.53 105 11.07 111 70-130 60-140 5 0-35 Tetrahydrofuran 10.00 8.726 87 8.822 88 70-130 60-140 1 0-35 Propionitrile 10.00 9.327 93 9.342 93 70-130 60-140 0 0-35 Tert-Butyl Alcohol (TBA) 50.00 53.92 108 51.84 104 43-170 22-191 4 0-38 Diisopropyl Ether (DIPE) 10.00 10.72 107 11.20 112 70-130 60-140 4 0-35 Ethyl-t-Butyl Ether (ETBE) 10.00 9.213 92 9.606 96 70-130 60-140 4 0-35 Tert-Amyl-Methyl Ether (TAME) 10.00 9.902 99 10.34 103 70-130 60-140 4 0-35 Quality Control - LCS/LCSD
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 7 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number 099-14-314-583 LCS Solid GC/MS Q 07/14/16 07/14/16 09:11 160714L008 Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Acetone 50.00 46.73 93 70-130 60-140
Benzene 50.00 45.37 91 78-120 71-127
Bromobenzene 50.00 47.79 96 70-130 60-140
Bromochloromethane 50.00 45.08 90 70-130 60-140
Bromodichloromethane 50.00 45.25 90 70-130 60-140
Bromoform 50.00 48.57 97 70-130 60-140
Bromomethane 50.00 39.77 80 70-130 60-140
2-Butanone 50.00 48.83 98 70-130 60-140
n-Butylbenzene 50.00 47.13 94 77-123 69-131
sec-Butylbenzene 50.00 47.77 96 70-130 60-140
tert-Butylbenzene 50.00 50.40 101 70-130 60-140
Carbon Disulfide 50.00 45.64 91 70-130 60-140
Carbon Tetrachloride 50.00 46.58 93 49-139 34-154
Chlorobenzene 50.00 45.60 91 79-120 72-127
Chloroethane 50.00 46.09 92 70-130 60-140
Chloroform 50.00 43.27 87 70-130 60-140
Chloromethane 50.00 44.36 89 70-130 60-140
2-Chlorotoluene 50.00 47.88 96 70-130 60-140
4-Chlorotoluene 50.00 46.61 93 70-130 60-140
Dibromochloromethane 50.00 45.56 91 70-130 60-140
1,2-Dibromo-3-Chloropropane 50.00 48.91 98 70-130 60-140 1,2-Dibromoethane 50.00 46.27 93 70-130 60-140
Dibromomethane 50.00 44.10 88 70-130 60-140
1,2-Dichlorobenzene 50.00 47.64 95 75-120 68-128
1,3-Dichlorobenzene 50.00 46.77 94 70-130 60-140
1,4-Dichlorobenzene 50.00 45.36 91 70-130 60-140
Dichlorodifluoromethane 50.00 41.16 82 70-130 60-140
1,1-Dichloroethane 50.00 45.02 90 70-130 60-140
1,2-Dichloroethane 50.00 41.53 83 70-130 60-140
1,1-Dichloroethene 50.00 45.33 91 74-122 66-130
c-1,2-Dichloroethene 50.00 44.70 89 70-130 60-140
t-1,2-Dichloroethene 50.00 46.34 93 70-130 60-140
1,2-Dichloropropane 50.00 47.51 95 79-115 73-121
1,3-Dichloropropane 50.00 45.38 91 70-130 60-140
2,2-Dichloropropane 50.00 45.59 91 70-130 60-140
1,1-Dichloropropene 50.00 46.59 93 70-130 60-140
c-1,3-Dichloropropene 50.00 48.49 97 70-130 60-140
t-1,3-Dichloropropene 50.00 49.33 99 70-130 60-140
Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 8 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Total number of LCS compounds: 66
Total number of ME compounds: 0
Total number of ME compounds allowed: 3
LCS ME CL validation result: Pass
Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers Ethylbenzene 50.00 47.99 96 76-120 69-127
2-Hexanone 50.00 55.25 111 70-130 60-140
Isopropylbenzene 50.00 49.15 98 70-130 60-140
p-Isopropyltoluene 50.00 47.69 95 70-130 60-140
Methylene Chloride 50.00 43.93 88 70-130 60-140
4-Methyl-2-Pentanone 50.00 54.50 109 70-130 60-140
Naphthalene 50.00 46.85 94 70-130 60-140
n-Propylbenzene 50.00 48.49 97 70-130 60-140
Styrene 50.00 50.00 100 70-130 60-140
1,1,1,2-Tetrachloroethane 50.00 48.85 98 70-130 60-140
1,1,2,2-Tetrachloroethane 50.00 48.19 96 70-130 60-140
Tetrachloroethene 50.00 44.80 90 70-130 60-140
Toluene 50.00 47.31 95 77-120 70-127
1,2,3-Trichlorobenzene 50.00 46.92 94 70-130 60-140
1,2,4-Trichlorobenzene 50.00 49.67 99 70-130 60-140
1,1,1-Trichloroethane 50.00 43.21 86 70-130 60-140
1,1,2-Trichloroethane 50.00 44.44 89 70-130 60-140
1,1,2-Trichloro-1,2,2-Trifluoroethane 50.00 47.79 96 70-130 60-140 Trichloroethene 50.00 46.97 94 70-130 60-140
1,2,3-Trichloropropane 50.00 48.46 97 70-130 60-140
1,2,4-Trimethylbenzene 50.00 46.75 93 70-130 60-140
Trichlorofluoromethane 50.00 42.69 85 70-130 60-140
1,3,5-Trimethylbenzene 50.00 48.71 97 70-130 60-140
Vinyl Acetate 50.00 41.26 83 70-130 60-140
Vinyl Chloride 50.00 48.03 96 68-122 59-131
p/m-Xylene 100.0 96.25 96 70-130 60-140
o-Xylene 50.00 48.79 98 70-130 60-140
Methyl-t-Butyl Ether (MTBE) 50.00 47.53 95 77-120 70-127 Quality Control - LCS
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Haley & Aldrich, Inc,
5333 Mission Center Rd., Suite 300
San Diego, CA 92108-1350
Date Received: 07/13/16
Work Order: 16-07-0873
Preparation: EPA 5030C
Method: EPA 8260B
Project: UTAS - Due Diligence / 43559-013 Page 9 of9
RPD: Relative Percent Difference. CL: Control Limits
Return to Contents
Method Extraction Chemist ID Instrument Analytical Location ASTM D-2216 (M) N/A 1009 N/A 1
EPA 6010B EPA 3010A Total 935 ICP 7300 1
EPA 6010B EPA 3050B 935 ICP 7300 1
EPA 7470A EPA 7470A Total 868 Mercury 04 1
EPA 7471A EPA 7471A Total 868 Mercury 05 1
EPA 8260B EPA 5030C 316 GC/MS L 2
EPA 8260B EPA 5030C 1055 GC/MS Q 2
Sample Analysis Summary Report
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-07-0873 Page 1 of1
Location 1: 7440 Lincoln Way, Garden Grove, CA 92841
Location 2: 7445 Lampson Avenue, Garden Grove, CA 92841 Return to Contents
Qualifiers Definition
* See applicable analysis comment.
< Less than the indicated value.
> Greater than the indicated value.
1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clarification.
2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefore, the sample data was reported without further clarification. 3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recovery was in control.
4 The MS/MSD RPD was out of control due to suspected matrix interference. 5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference. 6 Surrogate recovery below the acceptance limit.
7 Surrogate recovery above the acceptance limit.
B Analyte was present in the associated method blank.
BU Sample analyzed after holding time expired.
BV Sample received after holding time expired.
CI See case narrative.
E Concentration exceeds the calibration range.
ET Sample was extracted past end of recommended max. holding time.
HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.
HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons were also present (or detected).
HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detected).
J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated.
JA Analyte positively identified but quantitation is an estimate.
ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).
ND Parameter not detected at the indicated reporting limit.
Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a factor of four or greater.
SG The sample extract was subjected to Silica Gel treatment prior to analysis.
X % Recovery and/or RPD out-of-range.
Z Analyte presence was not confirmed by second column or GC/MS analysis.
Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis.
Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time.
A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations.
Glossary of Terms and Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Work Order: 16-07-0873 Page 1 of1
Return to Contents
Return to Contents
Return to Contents
COUNTY OF SAN DIEGO
DEPARTMENT OF ENVIRONMENTAL HEALTH
LAND AND WATER QUALITY DIVISION
MONITORING WELL PROGRAM
MONITORING WELL DESTRUCTION PERMIT
SITE NAME: ROHR, INC, A COLLINS AEROSPACE COMPANY
SITE ADDRESS: 390 BAY BLVD, CHULA VISTA, CA 91910
PERMIT TO: DESTROY MONITORING WELLS (3) & TRANSDUCERS (2) PERMIT APPROVAL DATE: 9/28/2020
PERMIT EXPIRES ON: 1/27/2021
RESPONSIBLE PARTY: ROHR, INC, A COLLINS AEROSPACE COMPANY (RICK SIORDIA) ______________________________________________________________________________ PERMIT CONDITIONS:
1. Due to the wells being constructed with a minimum 20-foot seal, the proposal to destroy wells DB-2, DB-4, and DB-5 by pressure grouting is approved. Ensure that sufficient sealing material is placed in the well casing, filter pack, and all other significant voids within the entire well boring. In the drilling report, provide the volume pre-calculations and the actual amount of sealing material used in each well.
2. Since the transducers are constructed with bentonite filled boreholes, your proposal to destroy transducers OW-1 and OW-2 by removing the traffic cover and filling it with concrete is approved.
3. All water and soil resulting from the activities covered by this permit must be managed, stored and disposed of as specified in the SAM Manual in Section 5, II, D-4. (http://www.sdcounty.ca.gov/deh/lwq/sam/manual_guidelines.html). In addition, drill cuttings must be properly handled and disposed in compliance with the Stormwater Best Management Practices of the local jurisdiction.
4. Within 60 days of completing work, please submit a well destruction report that includes a description of the well destruction method as well as the type and volume of materials used (in cubic feet) to the Monitoring Well Permit Desk. This report must include all items required by the SAM Manual, Section 5, Pages 5-7.
5. This office must be given 24-hour notice of any drilling activity on this site and advanced notification of drilling cancellation. Please contact the Well Permit Desk at (858) 505-6688.
NOTE: This permit does not constitute approval of a work plan as defined in Section 2722 of Article 11 of C.C.R., Title 23. Work plans are required for all unauthorized release investigations in San Diego County.
APPROVED BY: DATE: 9/28/2020
Jon Senaha
PERMIT #: LMWP-004690
A.P.N.: 567-022-30-00
EST #: RWQCB
9/21/2020
1058336
ROHR
BUILDING 1
A@ A@
A@
A@A@
A@ A@
DB-4 OW-4
OW-3 OW-1
DB-2
OW-2
DB-5
G ST
BAY BOULEVARD
H STREET
99 100
29 56702233
57133002
56701007
56701029 56702228
57133030
57133024
56702230
56702231
57133016
57133003
57133029
56726033
NOTES
1. ALL LOCATIONS AND DIMENS IONS AREA APPROXIMATE.
2. AERIAL IMAGERY S OURCE: S AN DIEGO COUNTY, MARCH 2017 LEGEND
S ITE BOUNDARY
PARCEL BOUNDARY AND AS S ES S OR'S PARCEL NUMBER
0 120 240
S CALE IN FEET
ROHR, INC., A COLLINS AEROS PACE COMPANY
NORTH CAMPUS - PARCEL A
CHULA VIS TA, CALIFORNIA
EXIS TING MONITORING
WELL LOCATIONS MAP
S CALE: AS S HOWN
S EPTEMBER 2020
GIS FILE PATH: G:\43559_North Cam pus\000_Global\GIS \Maps\2020_09\127827_019_0001_WELL_LOCATION_MAP.m xd ― US ER: dfm ― LAS T S AVED: 9/15/2020 9:35:24 AM §¨¦5
29 BUILDING NUMBER
56701029
A@ APPROXIMATE MONITORING WELL LOCATION
•
URS Greiner Woodward Clyde
A Division of URS Corporation
February 16, 2000
Ms. Marisue Crystal
San Diego County
Department of Environmental Health
Land and Water Quality Division
P.O. Box 129261
San Diego, CA 9:2112-9261
Subject: Well Log Submittal
Permit No\".}£9827-:ZJ
BFGood1ich Aerostructures Facility
Chula Vista, California
•
1615 Murray Canyon Road, Suite 1000
San Diego, CA 92108
Tel: 619.294.9400
Fax: 619.293.7920
u i l nr AM ·oo Offices Worldwide
j -
URSGWC Project No. 589853067B.00-00400
Dear Ms. Crystal:
of Building 99 at the
BFGoodrich Aerostructure[l'B___EG)JFacility in Chula Vista, California, during June and July 1999. The wells were installed for use during an aquifer test. Base,: on initial results. one additional pumping weU 2 additional observation ·;.·ell(!QYI.=3-,md.-4)rwere installed at the A check foljthe f permit fee for three additior.al wells ($450) is included with this> well log submittal. Drill cuttings from the six well borings were placed in rcll-off bins and were properly dispcsed of by Pacific Treatment Environmental Services (PTES). Wash water generated during well 'nstallation was transferred to the onsite pretreatment facility by BFG personneL
[n accordance with the Site c'\s><:S.<ment and Mitiption Manual (revised 1999), copies of a site plan showing the well locarions, we!l logs and laboratory analy1iQJ report are provided._,Lithologic.logs were not for wei! b01ings OW-3 and OW--'1 because in close proxin!J!Y (within 20 feet) of well completion diagrams for wells OW-3 and OW-4 are provided in Figure 3. If you have: any questions, please gi•.'e tlS a -:alL Very truly yours,
URS GREINER WOODWARD CLYDE
Robert K. Scott, R.G. N
Senior Project Mar,age
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60'
70'
80'
45.2'
54.3'
59.4'
BOTTOM OF BORING
AT 80 FEET
0 10'
20'
SCHEDULE 40
BLANK PVC CASING
30'
CEMENT
ENVIROPLUG
BENTONITE PELLETS
0.020" SLOTTED
PVC SCREEN
LONESTAR
#3 SAND
BOTTOM OF BORING
AT 30.7 FEET
OW-3 MATERIALS
CEMENT
SCHEDULE 40
BLANK PVC CASING
ENVIROPLUG
BENTONITE PELLETS
0.020" SLOTTED
PVC SCREEN
LONESTAR
#3 SAND
7 BAGS LONESTAR #3 SAND
2 BAGS ENVIROPLUG PELLETS
20' PVC 0.020" SCREEN PIPE
1 0' SCHEDULE 40 BLANK CASING
OW-4 MATERIALS
1 0 BAGS LON EST AR //3 SAND
4 BAGS ENVIROPLUG PELLETS
10 BAGS PORTLAND CEMENT II
1 BAG BENTONITE POWDER
20' PVC 0.020" SCREEN PIPE
60' SCHEDULE 40 BLANK CASING
Project: BFGoodrich Key to Log
Project Location: Chula Vista, CA
Sheet 1 of 2 Project Number: 58-98530676.00-00400
-5
CY
o-2:! "'"'
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0 ·;:;
"' >- "'"' _., • w_ "-> ,_
I
.c •
E
z "
MATERIAL DESCRIPTION
Medium dense, moist, brown, silty SAND (SM)
[solid line denotes observed contact between strata]
[dashed line denotes inferred contact between strata
or gradational change in soil type]
Wire-line core barrel sample
c
0 ...
•
= • 0 :S:u
• E "-"-
""-
., -
J:o..
REMARKS
COLUMN DESCRIPTIONS
[}]
0 IIJ
@]
[_[]
Elevation:
Sample Type:
Sample Number:
Sample Blows/foot:
Graphic Log:
Distance On feet) below the ground surface.
Approximate elevation (in feet) referenced from the ground surface.* Type of soil sample collected at depth interval depicted; symbols explained above.
Sample identification number.
Number of blows required to advance driven sampler 1 foot, or distance indicated, using a 140-lb hammer (or as otherwise indicated) with a 30-inch drop. " .... indicates blow count for initial 6-inch seating interval of sampling only.
Graphic depiction of subsurface material encountered; symbology explained on Sheet 2 of Key.
Material Description: Description of subsurface material encountered, including USCS soil designation.
Well Completion log: Graphic depiction of well construction; symbology explained on Sheet 2 of Key.
Headspace:
Remarks:
GENERAL NOTES
Photoionization detector (PI D) field headspace reading (in parts per million).
NO indicates that no organic vapors were detected.
Comments or observations regarding drilling/sampling made by driller or URSGWC's field personnel
1. Soil classifications are based on the Unified Soil Classification System (USCS) or recorded and include consistency/relative density (where standard blow count correlation is possible). moisture, and color.
2. Descriptions on these boring logs apply only to the specific boring locations at the time the borings were advanced. They are not warranted to be representative of subsurface conditions at other locations or for other times.
NR - No Recovery
•Based on available topographic plan
Figure A-1 .... ;;;-;wc,;cu;;;;;;-,:m;; "'"';;;;;;, • .,,,.,w"""".:--URS Greiner Woodward Clyde Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678-00-00400
c:
0 -= ·;::;
-
c.- "' >- .<> • "" "" 0 E o.e -Q) c. w- > , >- z
M
Sand
Clay
s;lt
MATERIAL DESCRIPTION
UNIAEO SOIL CLASSIACATION SYSTEM
SYMBOL AND ROCK TYPE NAME VERSUS
CORRESPONDING GRAPHIC LOG
Silt/Sand
Silt/Clay
SYMBOLS USED IN WELL
COMPLETION LOG
Casing in concrete
Casing in cement/bentonite grout
Casing in bentonite chips or pellets
Casing in bentonite/sand
Slotted casing in f1lter pack
to Log
Sheet 2 of 2
c
0 c.
= 0 0 ":.s
REMARKS
Project: BFGoodrich of Boring::::DB:-4::==
Project Location: Chula Vista, CA --- Project Number: 58-98530678.00-00400 Sheet 1 of 15 Oate(s) 6/16/99 thmugh 6/22/99 Logged A. Greene Checked R. Scott Drilled By By Drilling Mud Rotary Drill Bit 6.25"112.26" tricone Approx. Surface 22 0 Method Size!Type Elevation (feet, MSL) • Drill Rig T -3 lngersoi-Rand Drilled Beylik Drilling Total Depth 555.0 Type By Drilled (feet) Depth to Ground-i First i Completion ! Sampling Number I ! Undisturbed: ·- Sampler water (feet, bg3) i 14 ' I of Samples 1 Disturbed: -- Type Wire-line core barrel '
Diameter of 12.25 1 Diameter of 4 Type of Schedule 80 PVC Screen 0.020" Hole (inches} ! Well (inches) Well Casing Perforation Type of Lonestar #3 Type of Bentonite chips and cement/bentonite grout Filter Pack Seal(s) Boring Location North of Building 99
'"'DI FS
c: .; "- 0
.s::;" ·;; u MATERIAL DESCRIPTION g E
- "' :;: c. c. .,., c.- .,.,
>- .n •c. REMARKS • E c. -co2 -<ll c. me> >- 0 j 0 .... z "'-' I c.. ol '-' Ill i l POINT FORMATION
-w 2" asphalt parking lot over 3" base material over medium dense, moist, reddish brown, silty fine SAND (SM)
20 Becomes less dense
5- -
-
-15
",r- Becomes moist to wet, medium brown, fine to
medium SAND with silt (SM), micaceous
10- lliJIIt -
10 15-
jr Becomes wet
-
-
-5 J
20- .,.__ Interbedded clay layers -
I
1/
0 25- -
-5
30-
URS Greiner Woodward Cl de _l'i!!llre l/1 tl/00 1 WL 1 tiFGOO Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
" 0
.<:: .,
"' "" "" -QJ
w30l
·1 0
35 ·15
40 ·20
45 ·25
50 -30
55 -35
60 -40
' • -" • c. E
>
... z "
MATERIAL DESCRIPTION
Becomes wet, grayish brown,
(SP)
Becomes finer grained
to medium SAND
Dense, wet, grayish brown, silty to clayey fine SAND
ISM/SCI
Slight increase in grain size, fine to medium sand
Becomes poorly graded fine to medium SAND with
little silt (SP)
of Boring DB-4
Sheet 2 of 15
c
0 . .,
• c.
=E
• 0
!!:u
REMARKS
Project: BFGoodrich ..
Project Location:
Project Number:
.!:
.,.,
o2
75 80
85 90
95 100
105
110
·55
-60
-65
-70
-75
-80
-85
Chula Vista, CA
58-9853067B.00-00400
" .c
E
z
MATERIAL DESCRIPTION
r-Increasing reddish brown SILT (SM)
Dense, wet, medium brown, silty fine SAND (SM)
Becomes grayish brown, fine to very fine sand with
silt
of Boring DB-4
Sheet 3 of 15
c
0 "i
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=E
• 0
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.,_ me_
•o
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REMARKS
Project: BFGoodrich log of Boring DB-4
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400 Sheet 4 of 15
115
-95
120
-100
125
-105
130
-110
135
-115
140
-120
145
-125
150
c.
>
....
.c
E
z
MATERIAL DESCRIPTION
Becomes dark gray to olive, fine to very fine sand
with silt
Becomes olive gray, fine to medium SAND with
little silt (SP/SM) and coarse sand
Becomes clayey fine SAND (SC) with shell
fragments
c
0 ·;
Q_
=E oo :S:u
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
155
160
165
c:
0 ·;:;
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UJ-
-130
-135
-140
-145
not""
175
-155
180
-160
185
-165
• c.
• .D
E
z "
MATERIAL DESCRIPTION
&+····················································· Dense, wet, dark olive gray, silty to clayey fine SAND
with trace medium sand {SM/SC)
Increasing Sll T with little fine sand (ML)
Wet, grayish brown to gray, fine to coarse SAND
with subrounded gravels (SP/GP) 3/4" gravels
of Boring DB-4
Sheet 5 of 15
c
0 c.
=E
• 0 :S:u
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
c
0 ·;:;
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w-
• c.
>
...
MATERIAL DESCRIPTION ..0
E
,
z
of Boring DB-4
Sheet 6 of 15
c
0 .,
• c.
=E
• 0 :?:u
REMARKS
1901 --------------------------
J -170
195
-175
200
-180
205
-185
210
-190
215
·195
220
-200
Decreasing gravels
Dense, wet, reddish to grayish brown, silty to clayey fine to medium SAND (SM/SC)
Gravel lanse
oen·s·e-,- ·siitV- SANDsand (SM)
225l
'-===;;;;--,.------URS Greiner Woodward Clyde
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
23 -210
235
I -215
240
-220
245
-225
250
-230
255
-235
260
-240
265
.0
E
z
0 ,g
0 0
ii5
MATERIAL DESCRIPTION
Dense, wet, reddish brown to brown, fine to medium
SAND with silt (SM)
of Boring DB-4
Sheet 7 of 15
·-E
.
"-"-"- -o-
•o
J:Q_
·-
REMARKS
Project: BFGoodrich
Project Location:
Project Number:
270
275
280
285
290
295
300
305
c:
0 ·;::;
..
Q)Ql G W2 g:
>-
-250
-255
-260
-265
-270
-275
-280
-285
Chula Vista, CA
58-9853067B.00-00400
0 0
"" • 3
0 iii
MATERIAL DESCRIPTION
Dense, wet, grayish brown, silty to clayey fine SAND
(SM/SC)
Light brown, poorly graded fine to medium SAND
with little silt (SP)
,r-Increasing gravels
of Boring DB-4
Sheet 8 of 15
·-E "-"-
""- -e- Go G_
:I: c.
REMARKS
Project: BFGoodrich Log of Boring DB-4
Project location: Chula Vista, CA
Project Number: 58-98530678.00-00400
,;
0 0
£ :;::; 0; 0
"' "' 0
.r. • :;: .,., .,., • E ;: Q.
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>- z 10 "-' "1 ·290
·295
Run 2
320 Run 3
·300
325
330
·310
1 Run 8
335
·315
340
345
NR
350
MATERIAL DESCRIPTION
oen·s·e·,-We·t: gray· t-0 reddiSh ·very-fine· S&ndysiL T to silty fine SAND (SM/ML) ...__ Becomes dark gray, fine to medium sand with little ...- silt and coarse sand
, ____ ____________________ _
Dense, moist olive gray, silty fine SAND with little clay sand (SM)
Becomes reddish brown, lean CLAY with trace fine
sand (CL) -------------.-------------------------------------- ·.,Dense, wet, grayish brown, poorly graded fine to , .. ______________________ _ :
wet, dark brown, silty fine SAND with few thin
- _,.,.o,;;um sand lenses (SM), micaceous
_____ _ _______ . ___ . ______________ _ Dense, wet, reddish to olive brown, fine sandy SILT to silty fine SAND (SM/ML)
Olive brown SILT (ML)
Sand nodule concretion
,r-- Becomes dark brown, clayey fine SAND (SC) to fine
sandy CLAY ICL}, trace medium sand
,r-- Becomes brownish dark gray, clayey fine SAND
with interbedded fine to medium sand lenses (SC)
r-- Becomes dark gray. fine to medium SAND with silt
.,. ISP/SM)
Dense, wet, dark brown, silty fine SAND ISM)
Becomes dark brown to dark brownish gray
Dense, wet, dark yellowish brown, very fine sandy CLAY
(CLJ
Sheet 9 of 15
c
0 c.
=E
• 0 3:u
REMARKS
#1, 315'-324'
#2, 324.-333'
#3, 333'-345.5'
#4, 345.5'-357.5'
Project: SF Goodrich
Project location: Chula Vista, CA
Project Number: 58-98530678.00-00400
-5
.,.,
a.-
350
355
360
365
370
375
380
385
390
c
0 ·;:;
.,
.,.,
>-
-Ql
w-
-330
·345
·355
-360
• "->
fMATERIAL DESCRIPTION
Becomes dark yellowish brown, silty fine SAND to
fine sandy Sll T ISMIML)
Medium coarse sand lense
Dark grayish brown, fine SAND with silt and
medium sand {SM)
1--1--=-:-cc;o-+---fi"'r'TI-r- Becomes fine sandy silt
Run 24
NA
Grayish brown very fine sandy silt
Concretion
Very dense, wet, brown, fine to coarse SAND with silt
and few gravels (SP/SM), gravel 3/4 ..
-very wet: medfum· t-O (fa-,k-bro;.;n; S1it"Y very -t-ine---- to fine SAND (SM) Becomes brownish gray
Reddish brown, fine sandy SILT lanse (ML)
Interbedded fine to medium SAND with silt and
trace coarse sand (SM)
Reddish brown, fine sandy SILT lanse (ML)
Coarsens to fine to medium sand wtth little silt
Dense, wet, medium brown, silty fine SAND (SM)
Dense, wet, brownish gray, fine SAND with silt (SP/SM), micaceous
Dense, wet, grayish brown, fine to coarse SAND with
silt and few gravels (SM)
-
365 ·ro ve·ry-dense: OliVE;
Run 26 fine sandy SILT to CLAY (ML/CL)
Becomes more sandy (SC), concretion
Concretion
of Boring DB-4
Sheet 1 0 of 1 5
·-
E "-"- REMARKS
:ro..
#5, 357.7'·373.5'
#6, 373.5'·383'
#7. 383'-395'
Project: SF Goodrich
Project Location: Chula Vista, CA
of Boring DB-4
Sheet 11 of 1 5 Project Number: 58-98530678.00-00400
c·
0 .<: ·;:;
.,., .,., "'
o2 -Q) UJ390l
--370
395-
O:AOAPI 0:0:
0 ,g 0
.0 • 0 :c
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> . " " 0 0 .... z iii Cl...J
MATERIAL DESCRIPTION
Run 27
Run 28 I
w ........................................................
Dense, wet, olive brown, silty very fine SAND (SM),
micaceous
- Run 29
- reddis-h ve·ry-fine· sanay· SIL-T ·to- c·cAv----
(MUCL)
ljH: wet, dark brown, silty fine SAND (SM),
micaceous
Reddish brown, sandy SILT (ML) to CLAY (CL)
Redd1sh brown, sandy Sll T to CLAY (ML/CL) to
olive brown to dark brown, s1tty very fme SAND
(SM) to very f1ne sandy SILT (ML) ) ,r-- Becomes more dark brown and SILT (Mll ,r-- Becomes dense, olive brown, silty very fine SAND
(SM), micaceous
Concretion
-
-
.... ·; .................................................... . Hard, wet, reddish brown, fine sandy CLAY with medium coarse (CL) to clayey medium to fine SAND (SC)
,r-- Becomes more clayey (CUSC)
..,._ Concretion
,r-- Becomes greenish brown, silty very fine SAND (SM)
,r-- Dark olive gray, silty fine sand with gravels
- 2.5" gravel
1" gravel
-
-
m' ·········-··············································· c
0 . .,
0 c.
= E. 0 0
5:u-"
= = ::
c::
=
= =
REMARKS
Box #8,
Box #10, 414.25'-428'
!Box #11, 428'-442.25'
Greiner Woodward Clyde -------'-F=i 9UI"e:___-'
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
.s:::
15.-
o.e ""
440
445
450
455
460
465
·425
-430
-435
-440
-445
c -" •
E "-> " ,... z
Run 42
NR
Run 44
0 ,g
•
0 1D
MATERIAL DESCRIPTION
Dense, wet, olive gray, poorly graded fine
little silt (SP), contains trace gravels
Dense, wet, light brown, poorly graded fine SAND (SP),
NR
NR
Run 49
NR
Run 51
NR
Core 53
Run 56
_t_?_ !i!l!!. ____________________ _
Dense to hard, wet, medium brown, fine sandy CLAY to
silty fine SAND (interbedded) (SM/Cl)
Brown, lean CLAY (CL)
- -tine ·sAND ·..:...it-h ·--·- (SCI
Becomes more sandy (SP)
+---Cuttings are light brownish to greenish gray, poorly graded fine SAND with medium sand (SP)
-very· -,i9
-ht- to gray.-SitiY--
fine SAND (SM)
Sandstone concretion 2"x2"
---- Very dense, moist, reddish brown to olive brown, clayey fine to medium SAND with trace coarse sand (SC)
oer;se-.-,;.;o1st: t1ne- SAND (SMi.-----
Becomes brownish gray, fine sandy SILT (ML)
Becomes reddish brown, SILT to CLAY (MUCL)
Reddish brown, fine sandy silt to clay
Silty fine SAND with trace medium sand (SM)
Silty fine SAND with trace medium sand (SM),
coarsens with depth
Reddish brown, fine sandy SILT to fine sandy CLAY
(ML/CL) ----------------------------------------------------- Dense, moist, reddish brown, silty fine to medium SAND
(SM). with trace coarse grains
of Boring DB-4
Sheet 1 2 of 1 5
REMARKS
470
Greiner Woodward
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
r::
0 .r:: ·;;
-.,., c.- .,., "' >-
-Ill
LU470
-450
475
480
-460
485
-465
490
-470
495
-475
500
505
510
• c. • " E
>
... z
NR
NR
0 ,g
•
0 1ii
MATERIAL DESCRIPTION
-oen·s·e·.- ·gr'"a-viSh .. ;;,·,
SAND with gravels and trace silt (SP), angular gravels
- Gray, silty fine SAND lanse (SM)
·gr""a·v-. SAND---
with silt (SP/SM)
NR Very dense, wet, light brown, poorly graded fine to
Run 63
Run 66
NR
NR
Run 67
coarse SAND with few gravels (SP)
Becornes greenish gray, silty to clayey fine SAND
lense (SM/SC)
____ ________________ _ Hard, wet, dark greenish gray, very fine sandy Sll T (ML), iron staining
- Silt-y to tine- to---- coarse SAND (SM/SC)
Becomes grayish brown (mottled)
Coarsens to clayey fine to medium SAND (SC)
(concretion)
Reddish brown to very fine sandy SILT (Ml)
Coarsens
Becomes brown, fine to coarse SAND with little
clay (SP/SC)
DB-4
Sheet 1 3 of 1 5
REMARKS
#15,
Project: BFGoodrich of Boring DB-4
Sheet 14 of 1 5
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
§ 0 c Ill_
g E £ .iii <; ,g MATERIAL DESCRIPTION c. c. REMARKS ! ! 1.9 :.9 ••
NR silt .
I- -490 1 / j Concretions
515-
II "71: ....,__ Dark brown, silty to clayey fine SAND (SM/SC), • •u• • • .... r-interbedded
NR • Becomes fine sandy with trace silt
I.-J-R_u_n_7_6---J---_j•;;:')J .. · · · · · · · · · · · · · · · · ·-· · · · ·-· · ·-· · ·-· ·-· · · · · · · ·--·--·-· · · · .-:
Hard, wet, reddish brown, very fine sandy SILT (MLJ
r- Becomes interbedded, reddish to grayish brown,
· ci"Av· icCi · · · · ·
Very dense, wet, brownish to greenish gray, fine SAND
with little silt (SP/SM)
Dark brown, fine sandy CLAY tCL)
L I····-····-·-··-·-·-·-······--··--·---·--··-·--·-·----·--· Hard, wet, grayish brown, fine sandy SILT (ML),
us
I
-+ Becomes finer, medium brown, very fine sandy
CLAY (CL), micaceous
+ Becomes reddish brown to gray brown
+Strong reddish brown, fine sandy CLAY to clayey
1-....--- fine SAND with medium sand (SCICLI (very dense) I .; Mottled coloring
- -wet: bfOWciiS_h_ gray -to- Oiive-brown.-tine-sandy------ SILT to CLAY (ML/CL)
+ Grades to clayey fine to medium SAND (SCI
-H8-rd: -wet; -tirle -SflT tO-ELAY-fMUCij-
:J.- Brown, clayey fine SAND lense (SC)
+--- Cemented sandstone concretion
- -Qr8_y_iSh -tine -t-0 -sA-ND-With----
little clay(SP/SC)
..................................................................................
Hard, wet, grayish to reddish brown, very fine sandy
CLAY (CL)
+ Brown, silty fine SAND (SM)
Becomes grayish brown, poorly graded fine SAND iii irr- with trace silt (SP) i =:J- Reddish brown, silty fine SAND (SP)
t _ _v_e_r_y_ !i!_"l_e_ '!_ _________ "
Hard, wet, grayish brown, very fine sandy SILT (ML),
mottled coloring ... Concretion (cemented sandstone)
::'-,...-"
'-===::-------URS Greiner Woodward Clyde
Box #1 6, 526'-538'
I sox #17, 538"-555'
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
" 0
.<:: ·;:;
.,., .,., "' • o2 w-
-Ql a.
>
1-
550- I
c--530
555-
f-·535
560-
c--540
565-
--545
570-
-
--550
575-
c--555
580-
--560
585-
-
---565
-
-
590-
SAMPLES
0 • ,g .c • E
0 0
z iii
Run 90
NR
Run 91
NR
u
:;:
.
a. ., - 0 "-'
MATERIAL DESCRIPTION
___)- Reddish brown, very fine sandy CLAY (CL)
Grayish brown, silty very fine SAND (SM)
Concretion (cemented sandstone)
Hard, wet, olive gray, very fine sandy SILT {ML)
.------ Grayish brown, silty fine SAND (SM)
Bottom of boring at 555 feet
Log of Boring DB-4
Sheet 1 5 of 1 5
-
-
-
-
-
-
c
0 ...
• c.
>00
>U-'
REMARKS
-----URS Greiner Woodward Clyde ____ _..:.F..:.=ig:::..:u•.::..e --..J Project: BFGoodrich
Project Location:
Project Number:
Chula Vista, CA
58-98530678.00-00400
Date(s)
Drilled 7/6/99 through 7 n /99
Drilling
Method Mud Rotary
Drill Rig
Type T -3 lngersoi-Rand
Depth to Ground-' First J
1 completion II Sampling
water (feet, bgs) ; 14
Diameter of
Hole (inches) 14.75 ! Diameter of 6 I Well (inches)
Logged
By A. Greene
Bit Size/Type 6.25"/14.75" tricone
Drilled
By Beylik Drilling
Number
of Samples
Type of
Well Casing
I j Disturbed: l Undisturbed: -
Steel with wire wrap screen
of Boring:_QB=:5=::J
Sheet 1 of 6
Checked
By R. Scott
Approx. Surface 22 0 Elevation {feet, MSL) •
Total Depth 202 5 Drilled (feet) •
Sampler
Type
Screen
Perforation
Wire-line core barrel
0.075"
Type of
Filter Pack Lonestar Crs. Aquarium Type of
Seal(s) Bentonite chips and cement/bentonite grout
Boring Location
5 15
10 10
15 6
20 0
25 -5
North of Building 99
r-- Becomes moist to wet, medium brown, fine to medium SAND with silt (SM), micaceous Interbedded clay layers
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-9853067B.00-00400
30 -10
35 -1 5
40 -20
45 -25
50 -30
55 -35
60 -40
65 -45
70 MATERIAL DESCRIPTION
Becomes wet, grayish brown, fine to medium SAND
(SP)
Dense, wet, grayish brown, silty to clayey fine SAND
{SM/SC)
Slight increase in grain size, fine to medium sand
Becomes poorly graded fine to medium SAND with
little silt (SP)
of Boring DB-5
Sheet 2 of 6
c
0 ...
• c.
=E
• 0
;'i:u
• E c. c. •c. -c-
•o
:I:Il.
·-
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Log of Boring
Sheet 3 of 6 Project Number: 58-98530678.00-00400
r::
0 .c ·;:;
-C.1i) "' >1i)
0-"" w70
·50
75 ·55
80 ·60
85 ·65
30 ·70
95 ·75
100
·80
105
·85
110
0;
.D
c. • E >-
... z
0 0
"' w
0 a;
MATERIAL DESCRIPTION
,r-- Increasing reddish brown SILT (SM)
Dense, wet, medium brown, silty fine SAND (SM)
Becomes grayish brown, fine to very fine sand with
silt
DB-5
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
£
o.2: ""
110
1151
120
125
130
135
140
145
150-
·90
·95
·1 00
·1 05
·1 10
·115
·120
·125
.c
E
z "
0 ,g
• 3
0 iii
MATERIAL DESCRIPTION
Becomes dark gray to olive, fine to very fine sand
with silt
Becomes olive gray, fine to medium SAND with
little silt (SP/SMI end coarse sand
Becomes clayey fine SAND {SCI with shell
fragments
of Boring DB-5
Sheet 4 of 6
c
0 Q.
=E
• 0
S:u
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
.c
-.,., c.-
o2
150
155
160
165
170
175
180
185
., 30
·1 35
_, 40
_, 45
_,50
G
c.
>
...
.c
E
z "
Run 2
-155 Run3
MATERIAL DESCRIPTION
Dense, wet, dark olive gray, silty to clayey fine SAND
with trace medium sand (SM/SC)
'Wet; dark ·g;.;y; ;,it-y very -tine ·s.A:No·-
with interbedded very fine, sandy silt layers (SM/ML)
r- Becomes more sandy with trace gravels (SM/SPJ
Dark gray to brown, silty to clayey fine SAND
• (SCISM) '-------------------------------------------------- Dense, wet, yellowish brown, silty fine SAND with ·coarse sand and gravel (SM) , l-4l-=c:-;:-f-----1F H -,iQht poo·,ly ·---• -160 coarse SAND with grovels and cobblea (SPIGPJ, angular to rounded rock fragments
of Boring DB-5
Sheet 5 of 6
REMARKS
190 Greiner Woodward Clyde-
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
of Boring DB-5
Sheet 6 of 6
c .... 0 o ME
£ a; MATERIAL DESCRIPTION a. a.
1i) Q) E ! =- Ql i:::_a. REMARKS
w.& g: ::1 1..::; :_3
__
--170
205-
--185
210-
-f"" .< 15 J
-195
220-
--200
225-
f- -205
230-
1-1-=.,-,--f----lli' t- #
2 •
Run11 tRun 12
••••
Bottom of boring at 202.5 feet
I
b= t-
- I=
I=
I=
I= t:
I= r-
-
-
-
-
-
-
-
-
-
'-;-,="""'"'"w"'";o., ____ URS Greiner Woodward FigUIJr;;..;_e_-----' Project: BFGoodrich of Borina--uw ·•
Project Location: Chula Vista, CA - Project Number: 58-98530678.00-00400 Sheet 1 of 4 Oate(s) 7/1/99 to 7/2/99 Logged A. Greene Checked R.Scott Drilled By By Drilling Mud Rotary Drill Bit s· tricone Approx. Surface 22 0 Method Size/Type Elevation (feet, MSL) • Drill Rig T -3 lngeraoi-Rand Drilled Beylik Drilling Total Depth 160.0 Type By Drilled (feet) Depth to Ground-i First 1 Sampling Number ' Sampler l Disturbed: - j Undisturbed: -- NA w8ter (feet, bgs): 14 I of Samples ' Type Diameter of 8 ! Diameter of 2 Type of Schedule 40 PVC Screen 0.020" hole (inches) ) Well (inches) We/J Casing Perforation Type of Lonestar #8 Type of Bentonite pellets end cement/bentonite grout Filter Pack Seal(s) Boring Location North of Building 99
SAMPLES
c: 0 c ·- 0 0
.£ ., ,g MATERIAL DESCRIPTION ... g E
- "' • "-"- c.- >- -" 0 c. 0 "- REMARKS "" "" c E 3 1.3 =E "0- o2 -Q)
w- "-> 0 ooj ,_ z "' S:u_"" Ill. 0- I .
Claos II base ove< dense, mo;ot, ! bo,i;;;. log brown, fine to medium SAND (SM), OW·2 20 few
BAY POINT FORMATION
Dense, moist, reddish to medium brown, silty to clayey
fine SAND with medium sand and few gravels (SM/SC)
5- -
15 10- -
r-1o
Becomes wet
15- Becomes more sandy (SM/SP) -
1-5 .
.
20- -
r-o -
25-
11 i!i
-
C"-·5
30-
URS Greiner Woodward Cli r/e Figure 2/16/00 1 Wll C I)N.;OO Project: SF Goodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
35 40
45 50
55 60
65 70
_, 0
• 1 5
-20
-25
-30
-35
-40
-45
.c •
E
z "
0 :c
c.
""' 0
MATERIAL DESCRIPTION
Hard, wet, grayish to olive brown, fine sandy CLAY (CL) with few interbedded coarse sand layers
-o;,-n·s·e·.- ·grS-viSh ·to mec:tfum·
fine to medium SAND (SP) with few interbedded coarse
and lenses
Greiner Woodward Clyde
of Boring OW-1
Sheet 2 of 4
REMARKS
Project: BFGoodrich
Project location: Chula Vista, CA
Project Number: 58-98530678.00-00400
-60
75 -55
80 -60
85 -65
90 -70
95 -75
100
-80
105
.c
E
z
0 ,g
0 0
1ii
MATERIAL DESCRIPTION
Becomes more sandy
Dense, wet, brownish gray, poorly graded fine to
medium SAND with few coarse sands (SP)
l of Boring OW-1
Sheet 3 of 4
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
110
115
120
125
135
140
145
-90
-95
-100
-105
. 1 1 0
• 1 1 5
-120
·1 25
0 ..0
E
z
0 ,g
• ;;
0 iii
MATERIAl DESCRIPTION
Becomes finer grained
dense to hard, wet, dark brownish gray, fine fine
(SM) with interbedded CLAY layers (Cl)
Dense, wet, light grayish brown, poorly graded fine to
coarse SAND (SP) few gravels
gray, silty to clayey fine SAND (SM)
of Boring OW-1
Sheet 4 of 4
REMARKS
Project: BFGoodrich of B . on ' .. y- -uvv-£
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400 Sheet 1 of 5
Oate(s) 6/30/99 to 711/99 Logged A. Greene Checked R.Scott Drilled By By Drilling Mud Rotary Drill Bit 8'" trioone Approx. Surface 22 0 Method Size/Type Elevation (feet, MSL) • Drill Rig T -3 lngersoi-Rand Drilled Beylik Drilling Total Depth 168.5 Type By Drilled (feet) Depth to Ground-.! First /Completion / Sampling Number i Disturbed: -- Undisturbed: -- Sampler NA water (feet. bgs) i 14 ' . of Samples Type Diameter of 8 i Diameter of 2 Type of Schedule 40 PVC Screen 0.020" Hole (inches) ! Well (inches) Well Casing Perforation Type of lonestar #8 Type of Bentonite chips and cement/bentonite grout Filter Pack Seal(s) Boring Location North of Building 99
c:" '"" 0 0
.r:;" :;:; :?_ g MATERIAL DESCRIPTION "' c. c. ..c • h .,., .,., •c. REMARKS • E ..,_ o.!!! -Q) c. i.S w- > 0 ,... z Ol :to. 0- over Class II base over dense, moist,
20 1 r to medium SAND (SM),
.... medium brown, silty to clayey
fine SAND with medium sand and few gravels (SM/SC)
5- -
="'
1 5
10- - -
-
l-10
••••
'V
Becomes wet
15- Becomes more sandy (SM/SP) -
5 20-. -
\-0
25- -
l-·5
'
30-
2 '1 6/00 1 Wll C BFGOO URS Greiner Woodward Cl de
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-9853067B.00-00400
30 -10
35 -1 5
40 -20
45 -25
50 -30
55 -35
60 -40
65 t·45
7J
.c
E
z
MATERIAL DESCRIPTION
Hard, wet, grayish to olive brown, fine sandy CLAY (CL) with few interbedded coarse sand layers
Dense, wet, grayish to medium brown, poorly graded
fine to medium SAND (SP) with few interbedded coarse
and lenses
of Boring OW-2
Sheet 2 of 5
c
0 c_
=E e o ;i:u
e E 0.0.
-omo e_
::t:c.
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
75 -65
80 -60
85 -66
90 -r-70
95 -75
100
-80
105
-85
..c
E
z "
MATERIAL DESCRIPTION
Dense, wet, reddish brown, silty fine
clay (SM/SC)
Becomes more sa.ndy
Dense, wet, brownish gray, poorly graded fine to
medium SAND with few coarse sands (SP)
of Boring OW-2
Sheet 3 of 5
E "-"-
-cJ:o. ·-
REMARKS
Project: BFGoodrich
Project Location:
Project Number:
110
115
120
125
130
135
140
145
c:
0 ·;:;
"' >-
w.e "" . g:
,__
-90
-95
-100
-105
-110
·115
-120
-125
Chula Vista, CA
58-98530678.00-00400
..c • E
z "
MATERIAL DESCRIPTION
Very dense to hard, wet, dark brownish gray, fine fine
SAND (SM) with interbedded CLAY layers (Cl)
Dense, wet, light grayish brown, poorly graded fine to
coarse SAND (SP) few gravels
Very dense to hard, wet, brownish dark gray to olive
gray, silty to clayey fine SAND (SM)
of Boring OW-2
Sheet 4 of 5
REMARKS
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 58-98530678.00-00400
0::
0 0
.c: ,g 10 G
-" 0 .,., .,., G -Q) c. E
w- > 0
... z a;
MATERIAL DESCRIPTION
150
-130 lnterbeded CLAY lenses (CL)
155
t"'
1601
-140
165
-145
Bottom of boring at 1 68.5 feet
170
-150
175
t·155
I -16o
185
-1 66
L of Boring OW-2
Sheet 5 of 5
REMARKS
. -
Pacific Treatment •
Analytical Services, Inc.
September 24, 1999
URS Greiner/Woodward-Clyde
Attn: Bob Scott
1615 Murray Canyon Road, Suite 1000
San Diego, California 92108
4340 Viewridge Avenue, Suite A • San Diego, CA 92123
(858) 560-7717 • Fax (858) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: BFG-South Campus
Laboratory Log No.: 1815-99
Date Received: 09/20/99
Sample Matrix: One water sample
PO No.: 589853045B.01-FI001
Please find the following enclosures for the above referenced project identified:
I) Analytical Report
2) QNQC Report
3) Chain of Custody Form
......•................................................ Certificate of Analysis ....................•.................................
Samples were analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. Date of extraction, date of analysis, detection limits and dilution factor are reported for each compound analyzed. All samples were analyzed within the method required holding time from sample collection ..
Data for each analytical method was evaluated by assessing the following QNQC functions, as applicable to the methodology:
• Quality Control Standard
• Surrogate Percent Recovery
• Laboratory Control Sample (LCS) percent recoveries for all analyses • Matrix Spike Recovery/Matrix Spike Duplicate Recovery (MSR & MSDR) and/or • Relative Percent Difference (RPD from MSR & MSDR)
I certify that this data report is in compliance both technically and for completeness. Release of the data contained in this hardcopy data report has been authorized by the following signature. ice President/Laboratory Director
Water • Soil • Waste • Wastewater • Marine Sediment & Tissues • Elutriate Analyses That Produce Results!
• •
ANALYSIS RESULTS
CLIENT: URS GREINER/WOODWARD-CLYDE DATE SAMPLED: 09/20/99 DATE RECEIVED: 09120199
PROJECT NAME/No.: BFG-SOUTII CAMPUS DATE DIGESTED: 09/20/99* PTASLOG#: 1815-99-1 DATE ANALYZED: 09/20-22/99
SAMPLE ID: DB-5 MATRIX: WATER
ANALYTE PREP./ ANALYSIS REPORTING LIMITS DF RESULTS UNITS
METIIODS
ALKALINITY SMEWW2320B 5 I 96 MGCaC031L
CONDUCTIVITY SMEWW2510B I I 4,710 UMHOS/CM
MBAS SMEWW5540C 1.0 I ND MGIL
TDS SMEWW2540C 20 I 3,130 MGIL
pH EPA 150.1 0.1 I 7.2 pH UNITS
CHLORIDE SMEWW 4500 Cl C 0.05 I 1,450 MGIL
SULFATE SMEWW 4500 S04 E 10 I 181 MGIL
CALCIUM EPA 3010/6010 20 10 254 MGIL
COPPER EPA 3010/6010 0.05 I ND MGIL
IRON EPA 3010/6010 0.1 I ND MGIL
MAGNESIUM EPA 3010/6010 10 10 144 MGIL
MANGANESE EPA 3010/6010 0.03 I 1.14 MGIL
SODIUM EPA 3010/6010 5 1 466 MGIL
ZINC EPA 3010/6010 0.05 1 8.61 MGIL
HARDNESS SMEWW2340B 10 1 1,230 MGCaC03/L
POTASSIUM EPA 3010/6010 5 I 6 MGIL·
DF G DILUTION FACTOR
ND m ANAL YTE NOT DETECTED AT OR ABOVE TifE INDICATED REPORTING UMIT REPORTING UMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR. ' NOTE: APPUES TO METALS ONLY.
PTAS DCN 300-027 (Rev4/99) ® Pacific Treatment Analytical Services, Inc. 4340 Viewndge Ave., sune A • San Diego, CA 92123 (858) seo-n17 FAX (858) 560-n63 •
ANALYSIS RESULTS
CLIENT: URS GREINER/WOODWARD-CLYDE DATE SAMPLED: 09h0!99 DATE RECEIVED: 09/20/99
PROJECT NAME/No.: BFG-SOUTII CAMPUS DATE DIGESTED: 09/20/99* PTASLOG#: 1815-99-1 (DUPLICATE) DATE ANALYZED: 09/20-22/99 SAMPLE ID: DB-5 (DUPLICATE) MATRIX: WATER
ANALYTE PREP./ANAL YSIS REPORTING LIMITS DF RESULTS UNITS METI!ODS
ALKALINITY SMEWW2320B 5 1 97 MGCaC03/L
CONDUCTIVITY SMEWW 2510 B 1 1 (730 UMHOS/CM
TDS SMEWW2540C 20 1 3,130 MG/L
pH EPA 150.1 0.1 1 7.1 pH UNITS
CALCIUM EPA 3010/6010 20 10 251 MG/L
COPPER EPA 3010/6010 0.05 1 ND MG/L
IRON EPA 3010/6010 0.1 1 ND MG/L
MAGNESIUM EPA 3010/6010 10 10 145 MGIL
·MANGANESE EPA 3010/6010 0.03 1 1.14. MG/L
SODIUM EPA 3010/6010 5 1 481 MG/L
ZINC · EPA 3010/6010 0.05. 1 8.30 MG/L
HARDNESS SMEWW2340B 10 1 1,230 MGCaC03/L
POTASSIUM EPA 3010/6010 5 1 6 MG/L
DF • DILUITON FACTOR
ND =ANAL YTE NOT DETECTED AT OR ABOVE THE INDICATED REPORTING LIMIT REPORTING LIMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR. ' NOTE: APPLIES TO METALS ONLY.
PT AS DCN 300.027 (Rov 4/99) ® Pacific Treatment Analytical Services, Inc. 4340 Ave., Suite A • Sen Diego, CA 92123 (858) 560-7717 FAX (858) 560-7763 • . QA/QC REPORT
QA/QC SAMPLE: ERA9983
DATE ANALYZED: 09/20/99
SPIKED ANAL YTE I TV DV AR
pH I 9.02 8.87 8.82-9.22
QA/QC REPORT
QA/QC SAMPLE: ERA 9983
DATE ANALYZED: 09/22/99
SPIKED ANAL YTE TV DV %R
ALKALINITY 118 120 102
CONDUCTIVITY 758 736 97
TDS 583 540 93
QA!QC REPORT
DATE ANALYZED:
SPIKED ANAL YTE
MBAS
. CHLORIDE
SULFATE
CALCIUM
COPPER
IRON
MAGNESIUM
MANGANESE
SODIUM
ZINC·
POTASSTIUM
TV= TRUE VALUE
DV =DETERMINED VALUE
AR • ACCEPTABLE RANGE
% R =PERCENT RECOVERY
09/21-22/99
LCS%R
96 98
96 89
90 88
87 87
94 89
85 MS%R MSD%R
91 93
103 . 101
101 94
• •
90 88
84 86
• •
81 82
65** 76
67** 64**
75 86
LCS% R =LABORATORY CONTROL SAMPLE PERCENT RECOVERY
MS% R =MATRIX SPIKE PERCENT RECOVERY
MSD % R • MATRIX SPIKE DUPUCATE PERCENT RECOVERY
RPD = RELATIVE PERCENT DIFFERENCE
ACCEPTABLE ACCEPTABLE
LCS,MSIMSD RPD
CRITERIA CRITERIA
RPD % %
2 80-120 <20
2 80-120 < 20
7 80-120 < 20
• 75-125 <20
2 75-125 <20
2 . 75-125 <20
• 75-125 < 20
I 75-125 < 20
16 75-125 < 20
5 75-125 <20
14 75-125 <20
• NOTE: NO RECOVERY REPORT ABLE DUE TO NECESSARY DILUTION OF SAMPLE SPIKED. ALL OTHER QC DATA INDICATES METHOD IS IN CONTROL. LCSD % R FOR CALCIUM = 97%. LCSD % R FOR MAGNESIUM • "NOTE: POOR RECOVERY ATTRIBUTABLE TO HIGH DISSOLVED SOUDS CONTENT OF SAMPLE SPIKED. ALL OTHER QC DATA INDICATES METHOD IS IN CONTROL. LCSD% R FOR ZINC • 96o/o. LCSD% R FOR SOD ruM= 96%.
PTAS DCN 300-027 (Rov 4/99)
':t::J Pacific Treatment Analytical Services, Inc. 4340 Viewridge Ave., A· San Diego, CA 92123 (858) 560-n17 FAX (858) 560-n63 PTAS
JDN
.2
• y 1 A>) reserves
...:..
: . ....;;
the right to return samp I cs that do not match our waste p•uu•"'· . . .
·,
..:.
I.
.
.
•.
.
.
. \, '··
• • o71 - :130 - 17
APN 5Cn1 - 02..2.. - .30
PERMIT #W 7'6 0
EST. #H ::3 7 \ Co5
MONITORING WELL COMPLIANCE/DRILLING INSPECTION REPORT
SITE ADDRESS 850 \....c,'jooo .\)<' .. ZIP 1::\\0..\.0 T.B. _..:..!_ PROPERTY OWNER 1)'f CZocxir\c't;l / R..oh C ' .
MAILING ADDRESS <i3 50 'Dr. STATE C.t>, ZIP C\\<>,\0
0DRILLING
I
MW I v I 8 I 0 I AS I TYPE OF INSPECTION:. MONITORING WELL DATE: OS- 17-00 COMPLIANCE
WI = Well D = Destruction
V = Vadose Well AS = Air Sparglng
WELL LOCATION NUMBER II)ll,- 2,
COVER CONDITION ·er
PERIMETER SEAL CONDITION G
STRUCTURE DRAINAGE
SECURED '(
TYPE OF SEAL c.
INNER VAULT INTEGRITY r:.
CASING TYPE BZ.c.
LOCKED CAP '(
SEALED CAP y
LIQUIDS PRESENT ). ')''
G=Good
F =Fair
P = Poor B = Bentonite
C = Concrete S = Soil
B =Boring
Y=Yes
N =No
M =Missing
U = Unable to Locate
V = Visual Inspection Only
*=Other
CONSULTANT: Wocdwc;,rd -C\_.\jde. GEOLOGIST:------------ DRILLER: Tci- C ¢1 o+.j .1).-".\.l:o0 LIC. #: ----------------- SOIL BORINGS PROPERLY CONTAINED AND LABELED 0 YES 0 NO
HEAL THISAFETY: BOOTS HARD HATS TRAFFIC OTHER-------
REMARKS: (Dl)-:l.."j Wo...le.c/\i\:,;d ')lrnc.o± ;a i once VA-u\"""\-
RECEIVED BY
Ext.2223 1 Warina Veronica Garm
DEPARTMENT OF ENVIRON:T: HEAL TH11NSPECTOR
Land and Water Quality Division, Site Assessment & Mitigation Program, P.O. Box 129261, San Diego, CA 92112-9261; (619) 338-2222 DEH:SAM-9217 (Rev. 3199)
County of San Diego
Department of Environmental Health
• •
@ouuty- of
GARY ERBECK
DIRECTOR
February lO, 2000
Woodward-C!)de
Attn: Robert k. Scott
1615 MUITayCyn. Rd, Ste 1000
San Diego, CA 92!08
Dear Mr. k. Scott :
EXPIRED WELL PERMIT
DEPARTMENT OF ENVIRONMENTAL HEALTH
P.O. BOX 129261, SAN DIEGO, CA 92112-9261
(619) 338-2222 FAX (619) 338-2377
LAND AND WATER QUALITY DIVISION
OFFICIAL NOTICE
Bfgoodrich Aerostructures Group, 850 Lagoon Dr, Chula Vista, CA, 919!0 AP.N. 571-330-17 + 567-022-30 PERMIT #W97850 EST. #H37165
RICHARD HAAS
ASSISTANT DIRECTOR
As of February 10, 2000, the Department of Environmental Health (D EH), Site A=nent & Mitigllion Program (SAM) has not received information regarding the above-referenced permit issued on l 0/ 29/ 98 for the drilling of weDs and/ or borings.
Within 30 days, please submit the following information:
I. Provide a detailed site plan giving accurate locations of all weDs and borings. The site plan should be dnl\\n to scale.
2. Provide complete well logs, \\hich include \\ell construction details, lithologic log, static water level including date of measurement, and, if available, the surveyed casing elevation.
3. Provide all laboratory analysis data if there was/ is no site assessment case.
A failure to provide information regarding this permit is a misdemeanor violation of Section 67.447 of the San Diego County Code, \mich will result in further action, including, but not limited to, an Administrative Office Hearing and a complaint being fded by this department with the State Contractors Liocnsing Board. Thank you for your cooperation.
Should )OU have any questions, please contact me at (619) 338-2339.
Sinocrely,
Marisue Crystal, Monitoring Well Permit Clerk
Site Assessment and Mitigation Program (SAM)
Enclosure (Permit Summary from TWIST)
''Errviromm!al llluipubliclnJth tlroti_/1 [al(ir.hip, JX811ur.ltip and.<riaKC'' . :--
;
\.
!
•
URS Greiner Woodward Clyde
A Division of URS Corporation
February 29, 2000
9 32 M\ ·nn
Ms. Marisue Crystal
San Diego County
Department of Environmental Health
Land and Water Quality Division
P.O. Box 129261
San Diego, CA 92112-9261
Subject: Well Log Submittal
Permit No.
-.:.
BFGoodrich Aerostructures Facility
Chula Vista, California
URSGWC Project No. 5898530678.00-00400
Dear l'v!s. Crystal:
·:·.cts
•
1615 Murray Canyon Road, Suite 1000
San Diego, CA 92108
Tel: 619.294.9400
Fax: 619.293.7920
Offices Worldwide
Two deep test boringS1IJ.B-:;:!'ancrDB=3) and one deep installed at the BFGoodrich Aerostructures (BFG) Facility in Chula Vista, California, during November and December 1998. The borings and wells were installed to monitor general water quality (TDS and general minerals). The original permit application dated October 20,1998, which included one boring, was approved by the DEH on October 29, 1998. URS Greiner Woodward Clyde (1JR.SGWC) submitted two modifications to the permit for one additional well and one additional boring on November 4 and 18, 1998.
In accordance with the Site Assessment and Mitigation Manual (revised 1999), copies of a site plan showing the boring and well locations, well logs, 3nd laboratory analy1ical reports are provided. Drill cuttings from the three boreholes were placed in roll-off bins and were properly disposed of by Pacific Treatment Environmental Services (PTES). Wash water generated during well installation was transferred to the onsite pretreatment facility by BFG personnel. If you have any questions, please give us a cal!.
Very truly yours,
Senior Project Manager
RKS:kvs
Ill
Ill
........ --
)
•
·-_.:))
L&G£rJD
f-----·------- )
MARINA PARKWAY
..._
t;:;
w
c:::
1-
C/l
Project: BFGoodrich
Project Location: Chula Vista, GA
Project Number: 98530678-0100
Key to Log
Sheet 1 of 2
• 0.
>
,_
-" •
E
0 z
0 ,g
•
0 aJ
COLUMN DESCRIPTIONS
Elevation:
Sample Type:
Sample Number:
Sample Blows/foot:
Grephic log:
MATERIAL DESCRIPTION
Medium dense, moist, brown, silty SAND (SM)
[solid line denotes observed contact between strata]
[dashed line denotes inferred contact between strata
or gradational change in soil type]
Samples obtained by using a wire-line core sampler
Distance lin feet) below the ground surface.
11-
Q E 0.0.
• 0. -uI a.
Approximate elevation {in feet) referenced from the ground surface. •
REMARKS
Type of soil sample collected at depth interval depicted; symbols explained above.
Semple identification number.
Number of blows required to advance driven sampler 1 foot, or distance indicated, using a 1 40-lb hammer (or as otherwise indicetcd) with a 30-inch drop. "•" indicates blow count for initial 6-inch seating interval of sempling only.
Graphic depiction of subsurface materiel encountered; symbology explained on Sheet 2 of Key.
Material Description: Description of subsurface materiel encountered, including USCS soil designation.
Well Completion log: Graphic depiction of well construction; symbology explained on Sheet 2 of Key.
He&dspace:
Remarks:
GENERAL NOTES
Photoionization detector (PIDl field headspece reeding (in parts per million).
NO indicates that no organic vapors were detected.
Comments or observations regarding drilling/sampling mad" by driller or Woodward-Clyde's field personnel
1. Soil clessifications ere baaed on the Unified Soil Clessificetion System (USCS) or recorded end include consistency/relative density (where standerd blow count correlation is possible). moisture, end color.
2. Descriptions on these boring logs apply only to the specific boring locations et the time the borings were advenced. They are not werrented to be representative of subsurface conditions et other Jocetions or for other times.
ATD = At time of drilling
NO = Organic vapors not detected
NR = Negligible to no recovery
.. Based on availeble topographic plen
Greiner Woodward Clyde ____ _ _j
Project: . BFGoodrich Key to Log
Project Location: Chula Vista, CA
Sheet 2 of 2 Project Number: 98530678-0100
SAMPLES
c 0 c
·- 0 0
.c' ·;; ' ,g MATERIAL DESCRIPTION ·;; E
- "' • ] • 0.0.
c.- >- .c • a. • 0. REMARKS
"" "" • E 3 0. =1j ., - o.e w-
-OJ 0. • C>
" :> 0 ' 0
• 0
>-- z "' (!)__, :S:u J:O..
UNIAEO SOIL CLASSIACATION SYSTEM
SYMBOL AND ROCK TYPE NAME VERSUS
CORRESPONDING GRAPHIC LOG
Sand
Clay
Silt
Silt/Sand
Sand/Clay
Gravel
Sand with cobbles·
SYMBOlS USED IN WE:U
COMPlETION tOG
Casing in cement grout
Casing in bentonite grout
Casing in Lones tar # 1/20 aand I\ I}
··'··'
Casing in Lonestar #3 sand
'ii
f:
! Slotted casing in fitter pack t::
c•. B-1
,,.,.,,_;,;o'-<•• URS Greiner Woodward G e
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 98530678-0100
og of Boring DB-1
Sheet 1 of '9
Date(s)
Drilled 1 1/2/98 through 1 1/1 2/98 Logged
By KS, VW, RKS Checked By RKS
Drilling
Method Mud Rotary
Drill Rig
Type CME 75, Canterra 550
Groundwater 3
levef (feet)
Location: South of BuiJding 61
._.
C:UJ 0
£ . g:2 ,g "' >.; .0 • "" "" • E 3 o.e _.,
w- a.
> 0 ,_ z 1ii
0 5
5 0
J NR
15 -10
20 -15
I
25 Drill Bit 94-mm wireline core.
SizefType 5 7/8" tricone
Total Depth
Drilled (feet) 30Z.O
Drilled
By
Date
Measured
Tri-County Drilling
1 1/2/98
Hammer Weight/
Drop (lbs/in.) ••
Approx. Surface
Elevation (feet, MSLJ 5.0
Borehole
Backfill Bentonite grout
MATERIAL DESCRIPTION
and other remarks
Asphalt over rock base and silt
olive brown, silty CLAY (Cl)
.- Becomes wet, dark gray to black, clay
,r-- Becomes reddish brown, silty CLAY {Cl) with trace send Wet, olive brown, clayey SILT {Ml)
- CLAY "(CU.- Wfth-
·-'t.io·t: ·a,JVe ·brown: ·siLt- ·y,;ith ·some ·cfa·v ·------·-· · ·-------- -- ·ci.Av· iCU--------------------------
-- W"e·t: .... s·AND-iSMi .. -
· V../o·t: tin;,· SAND ·,spr,· · ·--·---· ·-· ·-·---· ·--·- ...,_._ With trace of sand at 26.5 feet
·-wet·.· Oiive; browr;.-;fit¥ -tine; SAf..fD · fSMf sencf at·-- ·. 27.6' ·ciA y· iC:Lr---------------.----------.------------. .... u
0. c ·c .... : -. :o-" ·- 0>
- c >'- • 0 -. :!:u o:!:
Other Tests/
Comments
2'
ents at
end
GM
Project: SF Goodrich of Boring DB-1
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 2 of 9
_ __,
C:(f)
-5 .g:2
"'
>..;
"'""
o.!!' """"
_,
UJ30T -25
35 -30
40 -35
-40
50 -45
60 65 -60
D -" •
E "-> 0
>- z
MATERIAL DESCRIPTION
and other remarks
,r- Becomes silty at 33'
Wet, olive brown, Sll T (Mll
.. SAND -(SMY
·- 37.5-38.5' 1-.._-+--¥<8'<'+ ·,wet.- b·ro·wn.· Sf1tV ·cl.A'l tcu ·,;. .-itli- ·tine· · OiiV_e_ SAND- (SMi------------.----------------. -. i.i.fc·t: tO SAr'lD "iSWC
shells
.. iS Pi ·.;.:ith
shells
-- -iS Pi .. -----.... -------.--------.
-- SAND. iSCf--------------------------------
---r-+--biZit: ,-- "SAND- (SMi "CiA 'l (Ci..i.------
-.
'',With coarse szmd, shells and cley lenses from 52'-52.8' , ·to SiltY. c·LA Y 1CU .. -...... -........... . -Vl,;t: ·g;ayfsh ·to mediUn;-SAND ·,gpj ..... -......... -.. -- W"e·t: "s"iitY- iSM)
- t;ra·wr;,· sar;dy ·cLAY. tO "SANti iC-LtSCi--------
..,.
c
-·-
". c • 0
0 "- .<::: - Other c-
>"ii Comments
iB
, GS
,GM
Greiner Woodward Clyde ___
Project: BFGoodrich of Boring DB-1
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 3 of 9
MATERIAL DESCRIPTION *
c ' . and other remarks -·-c • 0 $:u
-_J
ccn
.<::
.,., .,.,
"' - o2 -Q)
I
1 I
70+ -65
T
75 -70
85 -80 - SANti (SM)-------------------------------
NR
95 -- S1i-f -fMU----------------------------
100 - -(5\M- -s-ilt-----------
0 a. ·'§ ...: Other
:J-li, Comments ·o
a$:
Project: BFGoodrich of Boring DB-1
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 4 of 9
-..J
C:.CJ)
.!::
-a.- "'
>.;
o2 "" ""
_,
wSAMPLES
0 • ,g .Q • c. • E ,. , 0
f- 2: a;
.<;
c.
""' 0 '-!l...J
MATERIAL DESCRIPTION
and other remarks
f · · ·ciA y· · ;{rt · · · · ·· · · · · · · · · · · · · ·- 1 05
TI _, 00
· · -,.; ·s.ANo· · · · --=
. .. . · · s".A.i·io · isF>i · · .. · · · ·---
I '.--J-'n"'-R·-.Lj-'--l::<<r
, J '" 1 : '""
_ .. "SiLT "{MiY With-
---.. --------------.---
· i.fiie·t: ·bray;.;: -tin;,-t·o ·me·dilim· s·ANo · fSPi ·with ·some ·silt- an·d · · · · · · ·- clay 1-·············································--···········-·········- Wet, olive brown, silty ClAY to c/4yey SILT (CL/MU ····························-·-········-···-·····-·················- Wet, reddish brown, fine silty SAND (SM}. with cll!y, micaceous
Becomes coarser grained
1.. /{ ·cLA•iiSC·,cu · · · · ·--· -·-
1'-+c=+--J · · ;;,<fd';;.t.· b·,;,;,v;;: · si\J\io ·.,:;;iti ·g;o,;;,r · · · --··································--····-·······-··················- Wet, brown, clayey SILT (Mll. with trace of very fine sand and gravel at 133' ·
r- - Becomes more clayey
............ -....................................................... - Wet, grayish brown, silty, fine to medium SAND (SM) SOIL !TIES
-·-c • 0
su
·'§ Other Tests/
:o-" ·if Comments
as
ITDs, GM
IP, GS
and
Greiner Woodward Figure B-2 Clyde ___
Project: BFGoodrich g of Boring DB-1
Project Location: Chula Vista. CA
Project Number: 98530678-0100 Sheet 5 of 9
150 -145
NR
155 -150
160
NR
65 -160
170 -165
MATERIAL DESCRIPTION
and other remarks
Becomes olive brown
Becomes dark gray with orange mottling
.. W""e·t: ·g;,;y: CLA-Y -tCLI-
. mottling ---------------.-----------....
With silt
;:_w;,-, cf.A-v -!CIT-------------------------------------- ,. Becomes silty
-W""e·t: C:L.A Y -(CLJ- SAf,fD (SMi
minor sm811 shells
-·vi,;t: "d8fk ·g;,;y: Cieyey· SAN[) (SC">- Sf1t------------------------ a ark· grey: ·cLAv· fCi.i ·witti ·some ·arT;eli · · ·------· · · · With troco silt
;j1
c
.
--. - c • 0
$u
0 0.
·c Other
:;:,-"
>'Iii "'Comments
as
is very
L,-,==,------URS Greiner Woodward Clyde ___
Project: BFGoodrich of Boring DB-1
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 6 of 9
_ _,
ccn .g:2
"' - "'"'
-<1>
w175+ -170
t
180 -175
185 -180 '.--J----,1-----1
MATERIAL DESCRIPTION
and other remarks
- ·dark ·brown: ·dayey-lftLT -<MLi: Wit-h sancJ an·d · · · -it.agments
__} With gravel
.._ With some silty fine sand
190 -1 8 5 .................................................................. . Wet, dark olive brown, ClAY {Cl) with trace silt -- W""e·t: -<SWf---.----------.--------
200 -195
<f.
c ' .
-·-c • 0 'i::u
0 "-
.. : Other T
=>-E.
>"C Comments
oi::
Project: BFGoodrich og of Boring DB-1
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 7 of 9
•...J
C(/J
-3::?:
"' - "'"
-Q)
210T -205
t
215+ -210 .-.1-+---i
T
I
225 -220
23o I -225
235 -230
240 -235
245 -240
u
Wet, gray.
MATERIAL DESCRIPTION
and other remarks
trace gravel
- -t-O -d·a,·k ·g;,;y .- san·dy-sicr· · · ·- dark gray, silty CLAY {ML-CL) with z:ones of iron staining ·wet·.-g;ay: ·to· san·dy "GR-AVEL"fGMI-------.----------.---- -- - "(SP) GRAVE-L---
(GPI
;!!
c
-·-'. c • 0 i:u
0 0.
·c....:
::>-" "'
oi:
Comments
at
with
bit.
by
Project: BFGoodrich
Project Location: . Chula Vista. CA
Project Number: 98530678-0100
260 -255
' •
J>
E ,.. , ,_ z
og of Boring DB-1
MATERIAL DESCRIPTION
and other remarks
Becomes sandy
Sheet 8 of 9
Comments
275 -270 . Wit: "biOWO "SAND -,s·pj------------------------------.---------- -275
Greiner Woodward Clyde ___
Project: BFGoodrich
Project Location:
Project Number:
_ _,
C:U)
£ "' "" ""
-Q) • w- "->
f-
-285
29 -290
3001-+-- -295
I 3Cl -l- -300
31 -305
31 -310
Chula Vista, CA
98530678-0100
0 • ,g ..0 •
E
, 0
z iii
u
.c
"-• "
0 "-'
J Clay
MATERIAL DESCRIPTION
and other remarks
Bottom of boring at 302 feet
Boring backfilled with bentonite grout
of Boring DB-1
Sheet 9 of 9
c " .
-·-c • 0 su
Other
Comments
Project: BFGoodrich
Project Location:
Project Number:
Chula Vista, CA
98530678-0100
Date(s)
Drilled 11/1 9/98 through 12/22/98 Logged
By K. Shirley
Drilling
Method
Drill Rig
Type
Mud Rotary
Failing F-8
Drill Bit 2" ID wireline core,
Size/Type 5" coring drag bit
Drilled
By THF Drilling
I Disturbed: NA i Undisturbed: NA Depth to Ground-1 Fi(st I Completion 1 Sampling 14 ! •• 1 14.14
Number
of Samples
Diameter of 12&S· 718 1 of 6 Hole {inches} ) Well {Jnches) Type of Lonestar #3 and 111/20
Fitter Pack.
Boring Location North of Building 99
c' 0 .Q .c <; ,g "' -" • "'" "'"' D E o2 -<> c. w- > 0
>-- z a;
0 20
5 15
10 10
15 5
20 0
Type of
Well Casing
Type of
Seal{sl
Schedule 80 PVC
Bentonite grout
MATERIAL DESCRIPTION
BAY POINT FORMATION
Asphalt over moist, brown, silty fine SAND (SM)
. ·sAND ·<s·p,· ·oi---.
silt
Moist, brown, silty SAND (SM) with trace of clay
.. b;o.;.,;n-.- SAND iSC-,-;,.it-h -siti -<Mli .•. --.
Becomes finer grained with trace of silt
Becomes coarser grained
.f= Becomes finer grained with trace of silt
,. Becomes coarser grained
Silt or clay? (confirm with E·log)
W---1----hd-·-·-······---------·-·-·········----·-------····-··-- wet, brown, fine SAND (SP) 25 wet: 01iV8 fine· to ·mediu,;.; s·AND iSMi-- · · ·--
of Well DB-2
Sheet 1 of 10
Checked
By R. Scott
Approx. Surface 22 0 Elevation (feet, MSL) •
Total Depth
Drilled (feet)
Sampler
Type
Screen
Perforation
• E c. c. .,_ • c.
:co..
380.0
Wire-line core barrel
0.020"
REMARKS
Greiner Woodward Clyde ___
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 98530678-0100
c
.c.· .Q
"' "" ""
-Q)
30l
-10
35 -1 5
40 -20
45 -25
50 -30
55 -35
60 -40
65 -46
70 •
0. >
>-
NR
NR
MATERIAL DESCRIPTION
Wet, brown, fine SAND (SP) with trace of medium sand
-b,-a·wn: SAND-(SM)----------.-- ------
With coarse sand and fine and medium gravel at 32'
_______________________ _
OiiVe- tine· to s·ANil ·(sM; With--·-
trace of clay
-t-O SAND- coarse sand (SW)
- "SilT -{Mli------------------
;eddiSh -,ittV ·cLAY ·<c·c,· ·o;
- s·,i. ;.· ·sA:No· cSPl
- SiltY ·cL.A·v ·(ci->----------------
Ci8Y8Y ·siLT {ML) With Oi _s_a_n_d--------
- -tO SA-Nti (SPi,-pc",Orl;;-.-.----
graded
of Well DB-2
Sheet 2 of 10
c
0 .,
•
0. =E
• 0
su
• E 0.0.
• 0. -oIO:
REMARKS
discarded
[b•,ca,usa it contained
mud.
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 98530678-0100
.c
-
a.-
""
70l
75 80
85 90
95 100
105
110
-50
-55
-60
-65
-70
-76
-80
-85
•
a.
>
,_
NA
u
:c
a.
""' 0
"'-'
MATERIAL DESCRIPTION
olive brown, silty fine SAND (SM)
.. iSP1- -t·race· Of -si1t--------
---------.----.----------------.---------------.------
Wet, brown to olive brown, silty fine SAND (SM) with
trace of clay
wer.· very -,inS to· SAND-(SPI.-With ;;ace ·or---·
sitt
Wet: S"ANO ·(sc,· .;..;iih
-Wet·; SA"Nfi iSP,- ----------------------.----.
+---- With some medium and coarse sand
Wet, olive brown, very fine SAND to silty SAND (SMJ
Greiner Woodward Clyde
of Well DB-2
Sheet 3 of 10
c
0 . .,
•
a. =E
• 0 su
• E a. a. • a. ., -
I"-
REMARKS
Hydropunch sample
DB-2-HP77 obtained
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 98530676-0100
£
"'"'
110l
115
120
125
130
135
140
145
c::
.g
"'
"" 0 -<I> a_
w- >
....
·90
·95
NR
·1 00
·1 05
·11 0
MATERIAL DESCRIPTION
-wer.: iS Pi·--------·-··---·······-----
·siity· SANO-(Srii>-----.-- ---.--------.-.-
r-- Becomes silty with shells
•
--------------------------------------·---------------- Wet, dark gray, silty SAND {SM) with shells
- cSV.i)- ·o;---
silt and fine gravel
of Well DB-2
Sheet 4 of 10
o_
E "-"- • a_ "-
o_ oo
I a.
REMARKS
IC obtained
Project: BFGoodrich g of Well DB-2 Project Location: Chula Vista, CA Project Number: 98530678-0100
.<::
a.-
o!
"""
150
155
160
165
170
175
180
185
c:-
0 0
·;; t ,g "' .0 • """"
_., •
0. E w- ,. 0 0
>- z a;
.130 I NR
:.-.1---+---
. 1 3 5 ,Ll.,__-:c::c-+---1 NR
MATERIAL DESCRIPTION
1'-+---:-::::--f---l+S+lNA
. -.................. -......... -............. -........ . Wet, gray, silty tine SAND (SM) .r--- Becomes silty clay with light gray mudstone clasts -145
With light gray mudstone nodules, with iron staining
Viet: iii:,-ht Sil ;-· (-Mi.i
layers
-150
-155
- ;i;,:y SAND (SMf With
NR - ;iit·v· GRAVEL----
IGMJ
-160
NR
-165
--------------.--.----------------.-.-------.---------
Sheet 5 of 10
REMARKS
\ C<>btoleo at 1 80'
to obtain core
samples; drilling
bi-cone
181' to 210',
logged using drill
!cutti<lgo
Project: BFGoodrich og of Well DB-2
Project Location: Chula Vista, CA
Project Number: 98530678-0100
190
-170
195
-175
... ----.---------------------------------------------- Wet, brown, CLAY {CL), with silt 200
-180
205
-185
210
------------------------------------------------------- Wet, brown, silty fine SAND (SM)
215
------------------------------------------------------ -195 Wet, brown, fine to coarse SAND (SWJ 220 -wet; SftiY ·cLAY (Ci.i---------------.-.--
-200
225
.._ Becomes corarsar grained
--- G-RAVEL -<GCi---------------
NR
230
Sheet 6 of 10
REMARKS
Project: BFGoodrich Log of Well DB-2
Project Location: Chula Vista, CA
Project Number: 98530678-0100
2301
·210
235
·215
240.
·220
245
-225
250
·230
255
260
265
·246
a. •
>
....
NR
NR
MATERIAL DESCRIPTION
Dry to moist, brown, fine SAND (SP) with some silt and
trace gravels
tO SAND (SWi
lenses
Sheet 7 of 10
c
.Q
;;
c.
=E
• 0 :S:u
·-
lj E 0.0.
• 0. ., -
:I: a.
REMARKS
\Mate•ialvery dense;
unable to obtain core
barrel samples;
II with bi-cone bit
3to241'
Project: BFGoodrich
Project Location: Chula Vista, CA
Project Number: 98530678-0100
c
0 .c . .,
"'
o!:! """"
_.,
270
-250
275
-255
280
-260
285
-265
290
-270
295
-275
300
-280
305
-286
310
•
c.
>
>--
MATERIAL DESCRIPTION
--- .. ------.--.-----------.-------.------ ..... - Wet, olive brown, silty CLAY (CL) ·wee.· ·b,"c;;..n·. ·siitY-very ·sAi-iO ·wrt;,·
clay lenses
-ory ·ro morst: brown: (SPl v;ith· r·,ace· ot- · ·
'.sitt
-;;;.;;-i
GRAVEL (GW)
------------------------------------------------·····-
Moist, reddish brown, silty CLAY (Cl)
------------------------------------------------------- of Well DB-2
Sheet 8 of 10
• E c. c. • c. -,-
Iii:
REMARKS
I to obtain core
samples; drilling
bi-cone
295.5' to 306'
Project: BFGoodrich g of Well DB-2
Project Location: Chula Vista, CA
Project Number: 98530678-0100
J::
o.e ""
310
315
320
325
330
335
340
345
,:
0 ·;:;
"'
"" 0 -aJ o_ w- >
I-
-290
-295
-300
NR
-305 'r-.1-----t------1
-310
-315
-320
MATERIAL DESCRIPTION
Moist, reddish brown, silty fine SAND (SM)
gravel and silt
. w;t: ;;tty s·AND (SMi
- .. SAND-(SP)---------------------------
Sheet 9 of 10
c
-E
0 c_
=E
0 0 3:u
0 E o_o_
,_
oo_
•o
o_
J:O.
REMARKS
dense sand
to cor&);
!co•nellate with E-log
,,,JI"''i ..
Greiner Woodward Clyde
Project: BFGoodrich og of Well DB-2
Project Location: Chula Vista, CA
Project Number: 98530678-0100
<:AMPI <=<:
c:'
0 0 .c ·;:; ,g MATERIAL DESCRIPTION "' • 0
.c :c • w" "" • E c. -w ,..
c. 0 0 . "' "0
>- z "' "--' 350-
Wet, brown, SILT (Ml), with clay
f- -330
355-
--335
360-
f--340
-wet: brown.· SittY sAND -,sM5- ·------·--·-·-· · · ·--· · · · · · 365-
f--345
370-
f--350
375-
---355
380-
Bottom of boring at 380 feet
+·-360
385-
---385
390-
w"m_,c= .,.,-----URS Greiner Woodward Clyde
Sheet 10 of 10
c
0 . ., • E • c. c. c. • c. REMARKS -ES -o-
• 0
SU...J Io..
- ttttttt1
.
-1
-
Project: BFGoodrich of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 1 of 9
Date(s) 12/17/98 thmugh 12/22/98 I Logged L. Jacobs Checked R. Scott Drilled By By Drilling Mud Rotary, steel conductor Drill Bit 6'" core bit Total Depth 306.0 Method Sizeffype Drilled (feet) Drill Rig Ingersoll Rand TH-100 Drilled Beylik Drilling Hammer Weight/ NA Type By Drop {lbs(in.)
Groundwater 6 Date Surface
Level (feet) Measured Elevation (feet)
Location: Northeatct corner of former Building 56 Borehole Cement-bentonite grout BackfiJJ _ _, '<dMPt FS SOIL
ccn 0 ;j!. <:;
£ .g2 ,g 0.
Other Tests/ ' MATERIAL DESCRIPTION .'!:::: • "' • 0 c c- "' • :c -. :::>-§, "" "" • 0 0. and other remarks ·- Comments o2 -Q) 0. . "' w- - c >'4i > , 0 • 0 >- 2: "' - 0 S:u iSS:
0- "'-'
NR AN 11FICIAL FILL 1; 5 · with
0.2' asphalt over subangular sandy gravel
BAY POINT d d Moist, redd1sh brown, Wit me 1um to coarse san leasing to 1 5'
5- _,r-- Trace of gravel - ...................................................................... - ·Moist to wet, brown, clayey SAND (SC) - i••7ple
10- r- - ,..,Q 0 U010) I .......................................................... ............
Wet, dark brown, silty SAND to sandy SILT (SM/ML)
••
••••• 15- •• r- - •••••• coring .................................................................... - 5" Wet, brown, fine SAND (SP) with trace of silt
Nt<
20- -· .................................................................. ·- Wet, olive, CLAY {CH) with trace of silt
r· .................................................................... - Wet, olive, silty fine SAND (SM), with iron staining 25- I 1- -
.............................................................. ' .... - Wet, olive brown, fine SAND (SPl. with iron staining ,...- With trace of silt •
30-
URS Greiner Woodward Cl de Figure 8-4 2/19199 IGLGIO 5J051 Project: BFGoodrich og of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 2 of 9
30-
35-
40-
45-
50-
55-
60-
65-
•
0. >
>-
.0 •
E
,
z
NR
NR
0 l!h MATERIAL DESCRIPTION
and other remarks
,r- With trace of clay
--------------------------.--·--. -- ·---------------------------------- reddish brown, silty fine SAND (SM) with trace of clay !l@!l\l:l _] With trace of coarse sand from 37.5 to 39 feet k-----------·--------------.------------------.-------------------- Wet, reddish brown, clayey SILT (Ml). with trace of fine sand =:J- Silty SAND (SMI
ri,Y,t+--- fSMi ------------------------------.. ----- . - W'"e·t-. ·sAND -<SPf-------------.----------------------- NR
NR -------------------------------.------------------------ Wet, .. ----.... - brown, SILT (Ml)
I
I NR =:J- Light brown, silty sand layer
1'--'1-=NR+--l'rlll"'l is Mi ..
$Q DDt"" :s
# 'E Other Tests/
::I.e
iii § Comments
su os
'-7,;;;;,, , .,.,,""'oc••""''·"='·" • _____ URS Greiner Woodward Clyde ____ Project: BFGoodrich og of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 3 of 9
--J
CCI)
.c "'
>..;
"" ""'
-<u •
c.
>
,._
70 75
80 85
90 95
100
-" •
E
z
MATERIAL DESCRIPTION
and other remarks
Wet, brown, SILT (Mll
· ·siLT ·(Mii ·w-ith· · · · · ·
fine sand
Becomes finer grained and silty
- SANii iSC}---------------------------------
-- c·LA y·<c-LJ----------.----.-----------------
-- SAND ·<g·p;
......_ With some medium send
--- .......... -- ...... -... ··-.... ·----· ...... --.---------.... --- ... . Wet, light gray to brown, sandy CLAY (Cll :::J-.- ------.------------------.----.---------
*
c
-
.
-. -
c • 0 3:u
0 c.
·i§ -· Other
:>-§,
>"ii Comments
c;:;::
"--<===:;------URS Greiner Woodward Clyde ___
Project: BFGoodrich •
Log of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 4 of 9
•...I
""'
.c .g:E t >-' "' -" "" "" • E o.!'! -Q) c. w- >
f- z
105
1 10
1 15
120
125
130
135
0 ,g
0 0
a;
MATERIAL DESCRIPTION
and other remarks
Wet, olive brown to brown, fine SAND (SP} with iron staining -- SAND -(SPi
Light gray, fine to medium SAND (SW)
With clay
· g·rav·.-SiitY ·etA v· fCi.i ·iron·
· v .. grey: "tine· SAr'fD "fSPf With -t·race· Sltt · · · · · ·-------------· -- g;;y· SIL. f (Mlf--------------------------------------- - ·sAND-iSMi--.-----------------------------
With CLAY (Cll layers
"tfQht ·t·r;; "dtiV;, ·
With shelf fragments
With trace of coarse sand and more shell fragments
Becomes yellowish brown with trace of silt
c
-·-
". c • 0 $:u
Comments
Project: BFGoodrich Log of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 5 of 9
._J
CU)
.c "'
>..;
CJ-1: "" w-
-OJ ""
140-
145-
150-
155-
160-
165-
170-
• MATERIAL DESCRIPTION .Q
•
c. E >
f- z
and other remarks
- .- ·da;k SrLT -1MU ·v,;;th 'o"f ... --------------
162 1··------------------------------------------------------------------- f- Wet, d8rk brown, clayey coarse GRAVEL end cobbles {GC) _ V'1 with trace of sand · NR
-
l-l--+----fH"#---V..i,;t·. ·siLT -<M -<
-
--------------------------------- 1-1--+----f'ff"ft---W"e·t: "CiaVOV SA]\.iQ ·csci: ..... - end aome medium send NR
--------------------------------------------------------------------- Wet, brown, fine to medium SAND (SW) with trace of gravel SOIL !TIES
*- u
0. ·2..: Other Tests/
::J-" c >"C " Comments • 0 3:u a:::
fori/1 chatter
URS Greiner Woodward Clyde ___
Project: BFGoodrich Log of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 6 of 9
-5
""'
175-
180-
185-
190-
195-
200-
205-
210-
0 ,g
•
0 ii'i
,4-,-;;;---+----t f- NR
MATERIAL DESCRIPTION
and other remarks
-
With some clay and cobbles · --------.. --.----------. - - L--.l---1-_...j Wet, brown, SILT (MLI with of clay
-
(Coarse gravel and cobbles)
NR
-·· ........ .... ... ... ........
NR
.. ... ................. ........... ......... ...... Wet, brown, fine to medium AND (SPI SOIL
* 0 c.
C ·c:.; Other Tests/
:J.J: ... c; Comments
as
bit lost
in borehole
,,.,.,,= '"'",.,,=0.,-----URS Greiner Woodward Clyde
Project: BFGoodrich of Boring DB-3
Project Location: Chula Vista, CA
Project Number: 98530678-0100 Sheet 7 of 9
_ _,
C(J)
.c
>..: "'
a2 "" ""
-<>
w210
215
220
225
230
235.
240
245
' • .0
•
c. E
>
>-- z
0 ,g
•
0 a;
MATERIAL DESCRIPTION
and other remarks
· ·(s·w,- ·tine··-···--- .. gravel ·cLAY-fCU ---.--------- .... -----.---------.------. 1--1---+---ffLI"Tt--- "SiLY {rjfLI: ·.;;ith ·c,-aV fi'n·e ra-.;ers---.-.
Becomes coarser grained
=:J- With coarse sand and fine gnwel
.
Wet, brown, fine to coerse SAND (SW} with trece of silt ------------------------------------------------------------------- " ;:
-·-'. c • 0
;;:u
u
c. :'::: - c- ::>-"' " Comments
o;;:
Greiner Woodward Clyde ___
Project: SF Goodrich of Boring DB-3
Project Location: Chula Vista, CA
Sheet 8 of 9 Project Number: 98530678-0100
•...J
r:Ul
-5 "' - o2 ""' "'"
_,
250-
255-
260-
265-
270-
275-
280-
'" I O'C:
0 :; ,g .0 • E
0 0
z a;
'NR
0 :c
c.
""
"0 <!J..J
MATERIAL DESCRIPTION
and other remarks
--------................................ ·-.-.. ---.--- .. -.. -... -- .. -- .. - Wet, brown, fine to coarse SAND (SW) r -
- "tSP) -- ·--.---.----------.-------
l r--- Becomes coarser greined t-"'- Wet, -_-- --.-------------------------------.-----------------------.. - olive brown, CLAY (CL) ---------------------------------------------------------------------- '1- Wet, olive brown, silty SAND ISM) _
v: _. olive brown, SILT (ML)
Becomes reddish brown and clayey with trece sand
"' -
r- Becomes brown
Becomes 8<1!1ndier
11rl Wet, brown, SILT (Ml) with trace cl8y
---
Wet,
-- ---- ----- -------- ---- -- -. --- -- -. -- ----. ----- --------- ----. ---- --. brown to olive brown, silty fine to medium SAND (SM) r- S8od becomes co8rser gr8ined
SOIL riES
c -. -·-c • 0 S:u
u
·;§ Other Tests/
=>"'
Comments
as:
L,=, .. ,G,Gio,=.,o,,------URS Greiner Woodward Clyde
Project: BFGoodrich og of Boring DB-3
Project location: Chula Vista. CA
Project Number: 98530678-0100 Sheet 9 of 9
285-
••••
290-
295-
NR
305- . NR
310- -
315- -
MATERIAL DESCRIPTION
and other remarks
=::r Brown, silty clay
-- ·sANtY iSMi--- ·-
Becomes medium to coarse sand
Becomes silt
Sand becomes coarser grained
·························-
-
-
.................................................................... - Wet, olive brown, SILT (Ml) Become sandy
Becomes clayey
:=J-- Becomes silty sand
Bottom of boring at 306 feet
-
-
-
-
-
SOIL
c
.
-. - -
c 0 0 3:u
y
0. ·1§ _. f Other Tests/
::>"' Comments
o3:
. .""'?'P.i•. lcollccted dut
to
.. URS Greiner Woodward Clyde ___ ---=.F.:a.::.:.igurre::...:B=-- 4 :__.....J
Pacific Treatment •
Analytical Services, Inc.
January 7, 1999
BF Goodrich
Attn: Rick Siordia
850 Lagoon Drive
Chula Vista, California 91910
4340 Viewridge • Avenue, Suite A • San Diego, CA 92123
(619) 560-7717 • Fax (619) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: 9853067B
Laboratory Log No.: 2168-98
Date Received: 11103/98
Sample Matrix: Two water samples
PO No.: 9853067B
Please find the following enclosures for the above referenced project identified:
1) Analytical Report
2) QA/QC Report
4) Chain of Custody Form
....................................................... Certificate of Analysis ..................................................... .
Samples were analyzed pursuant to client request utilizing EPA or other ELAP approved · methodologies. Date of extraction, date of analysis, detection limits and dilution factor are reported for each compound analyzed. All samples were analyzed within the method required holding time from sample collection.
Data for each analytical method was evaluated by assessing the following QA/QC functions, as applicable to the methodology:
•
•
•
•
•
Quality Control Standard
Surrogate Percent Recovery
Laboratory Control Sample (LCS) percent recoveries for all analyses Matrix Spike Recovery/Matrix Spike Duplicate Recovery (MSR & MSDR) and/or Relative Percent Difference (RPD from MSR & MSDR)
I certify that this data report is in compliance both technically and for completeness. Release of the data contained in this hardcopy data report has been authorized by the following signature.
Vice President/Laboratory Director
Water • Soil • Waste • Wastewater • Marine Sediment & Tissues • Elutriate Analyses That Produce Results!
• ANALYSIS RESULTS •
CLIENT: BF GOODRICH DATE SAMPLED: ll/03/98
DATE RECEIVED: 11/03/98
PROJECT NAME/No.: 98530678 DATE DIGESTED: 11/04-11/98•
PTAS LOG#: 2168-98-1 DATE ANALYZED:. 11/04-12/98
SAMPLE ID: DB-1-HPIO MATRIX: LIQUID
ANALYTE PREP./ANAL YSIS REPORTING LIMIT DF RESULTS UNITS
METHODS
CONDUCTIVITY SMEWW 2510 B 19,900 UMHOS/CM
TDS SMEWW2540C 400 20 7,400 •• MGIL
pH EPA 150.1 0.1 7.2 pH UNITS
CHLORIDE SMEWW 4500 Cl C 0.25 5 5,700 MGIL
SULFATE SMEWW 4500 S04 E 50 10 488 MGIL
CALCIUM EPA 3010/6010 2 91 MGIL
COPPER EPA 3010/6010 0.05 0.11 MGIL
IRON EPA 3010/6010 1.0 10 73.2 MGIL
MAGNESIUM EPA 3010/6010 10 10 284 MGIL
MANGANESE EPA 3010/6010 0.03 I 1.18 MGIL
SODIUM EPA 3010/6010 50 10 4,060 MGIL
ZINC EPA 3010/6010 0.05 0.15 MGIL
HARDNESS SMEWW2340B 10 1,400 MGCaC03/L
POTASSIUM EPA 3010/6010 50 100 214 MGIL
BORON EPA 3010/6010 0.3 5.7 MGIL
OF= DILUTION FACTOR
NO= ANALYTE NOT DETECT AT OR ABOVE THE INDICATED REPORTING LIMIT LIMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR. ' NOTE: APPLIES TO METALS ONLY.
''NOTE: UNABLE TO OBTAIN AN ACCURATE MEASUREMENT FOR IDS DUE TO ffiGH TOTAL SOLIDS OF SAMPLE. ® Pacific Treatment Analytical Services, Inc. 4340 Vlewridge Ave., sune A • San Diego, CA 92123 (619) 560-7717 FAX (619) 560-7763 • ANALYSIS RESULTS •
CLIENT: BF GOODRICH DATE SAMPLED: Il/03/98
DATE RECEIVED: ll/03/98
PROJECf NAME/No.: 9853067B DATE DIGESTED: Il/04-II/98*
PTAS LOG#: 2I68-98-2 DATE ANALYZED: ll/04-I2/98
SAMPLE ID: DB-I-HP24 MATRIX: LIQUID
ANALYTE PREP ./ANALYSIS REPORTING LIMIT DF RESULTS UNITS
METHODS
MBAS SMEWW5540C 0.5 ND MGIL
CONDUCITVITY SMEWW25IOB 6,460 UMHOS/CM
TDS SMEWW2540C 80 4 3,460 •• MGIL
CHLORIDE SMEWW 4500 CI C 0.25 5 I,760 MGIL
SULFATE SMEWW 4500 S04 E 25 5 354 MGIL
N!TRITEASN SMEWW 4500 N02 B 0.05 ND MGIL
NITRITE AS N (DUP.) SMEWW 4500 N02 B 0.05 I ND MGIL
NITRATEASN SMEWW 4500 N03 E 1.0 IO I0.9 MGIL
FLUORIDE SMEWW 4500 E C O.I 5.I MGIL
ALKALINITY SMEWW2320B 5 I,960 MGCaC03/L
CALCIUM EPA 30I0/60IO 2 97 MGIL
COPPER EPA 30I0/60IO 0.05 I 0.08 MGIL.
IRON EPA 30I0/60IO 1.0 IO 25.2 MGIL
MAGNESIUM EPA 30I0/60IO IO IO I7I MGIL
MANGANESE EPA 30I0/60IO 0.03 0.59 MGIL
SODIUM EPA 30I0/60IO 50 .10 I,070 MGIL
ZINC EPA 30I0/60IO 0.05 I 0.05 ... MG/L
HARDNESS SMEWW2340B 10 I 946 '·MGCaC03/L
POTASSIUM EPA 30I0/60IO . 5 IO I63 MGIL
BORON EPA 30I0/60IO 0.3 •• 0.7 MGIL
DF'= DILUTION FACTOR
ND =ANAL Y1E NOT DETECT AT OR ABOVE THE !NDICA TED REPORTING LIMIT ..
REPORTING UMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDiNGLY TO ACCOUNT FOR DILUTION FACTOR. 'NOTE: APPLIES TO METALS ONLY.
"NOTE: UNABLE TO OBTAIN AN ACCURATE MEASUREMENT FOR IDS DUE TO illGH TOTAL SOUDS OF SAMPLE. ®Pacific Treatment Analytical Services, Inc. 4340 Vlewndge Ave .• Suite A• san Diego. CA 92123 (619) 560-7717 FAX (619) 560-7763 QA/QC SAMPLE:
QA/QC REPORT
QA/QC SAMPLE: ERA 9980, 9981
DATE ANALYZED: 11104-06/98
SPIRED ANAL YTE TV DV 0/oR
TDS 1080 985 91
CONDUCTIVITY 733 723 99
QAJQC REPORT
DATE ANALYZED:
SPIRED ANALYTE
MBAS
SULFATE
NITRITEASN
NITRATEASN
FLUORIDE
CHLORIDE
CALCIUM
COPPER
IRON
MAGNESIUM
MANGANESE
SODIUM
ZINC
POTASSIUM
BORON
TV-TRUEVALUE
DV- DETERMINED VALUE
AR-ACCEPTABLE RANGE
% R- PERCENT RECOVERY
11/04-12/98
LCS%R
110
91 101
91 105
99 93
97 99
. 91
99 101
87 89
83 MS%R MSD%R
95 107
93 94
99 101
92 98
90 90
95 95
88 88
96 93
99 97
87 86
98 95
• •
81 80
• •
89 88
LCS% R- LABORATORY CONTROL SAMPLE PERCENT RECOVERY
RPD
14 I
2 6
0 0
0 3
2 I
3 I
•
I
LCSD% R =LABOR TORY CONTROL SAMPLE DUPL!CA TE PERCENT RECOVERY MS% R =MATRIX SPIKE PERCENT RECOVERY
MSD% R =MATRIX SPIKE DUPL!CA TE PERCENT RECOVERY
RPD PERCENT DIFFERENCE
LCS,MS/MSD
CRITERIA
%
80-120
80-120
80-120
80-120
80-120
80-120
75,125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
•
ACCEPTABLE
RPD
CRITERIA
%
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
• NOTE: NO RECOVERY REPORTABLE DUE TO NECESSARY DILUTION OF SAMPLE SPIKED. A DUPLICATE LCS S
WITH THE SAMPLE BATCH AND THE RESULTING RECOVERY AND RPD MET OR EXCEEDED ACCEPT AN LCSD% R FOR SODIUM·= !01%, AND LCSD% RFOR POTASSIUM= 89% ®Pacific Treatment Analytical Services, Inc. 4340 Vlewrldge Ave., Suite A· san Diego, CA 92123 (619) 560·7717 FAX (619) 560-7763 ® . _(f+Sif' 1· .
.j) Pacific Treatment Analytical Services, Inc. ,
CHAIN-OF-CUSTODY RECORD -•! c . 4340 Vicwridgc: Avenue, Suite A San Diego, CA 92123 Phone {619)560-7717 Fax (619P60-776J 1 PTASLOG# Pq:' ,: "
RFOT lh YSIS ·
'·
lsampledby: k__. 'Dhv£-v Fax: {pq[-
IX
I ·)
4 5
6 R FT .TNOT IJ<:I-rFn BY DA'1 tt fiME RECEIVED BY
Intact: Yes No a;;; Corre ... 'l Containers: {vJ:) No
(cold) Ambicno Warn• VOAsw/ZHS: Y.:s_ Prinl
<II s, nl• , Prop«ly . No N/ A
I Disoosal: • PT AS r"'« R"um
JTim.c:_ · 24 hr 48 hr 3 day 4 day / Nonnal
• PT AS resc:rves lhe right to n:tum that Jon't mat.;h our prolile. ///.,/>t-
"7SI
jPrinl
White- l'TAS Canary- Ac..:ounting Pink- Client,, ... y ,.1 Goldenrod- Client, ..
;·.
(Rev. 5/97)
Pacific Treatment •
Analytical Services, Inc.
January 7, 1999
BF Goodrich
Attn.: Rick Siordia
850 Lagoon Drive
Chula Vista, California 91910-2098
4340 Viewridge • Avenue, Suite A • San Diego, CA 92123
(619) 560-7717 • Fax (619) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: 9853067B
Laboratory Log No.: 2175-98
Date Received: 11/04/98
Sample Matrix: One water sample
PO No.: 9853067B
Please find the following enclosures for the above referenced project identified:
1) Analytical Report
2) QA/QC Report
3) Chain of Custody Form
Note: Insufficient sample size provided. Unable to perform nitrite and fluoride analysis . ....................................................... Certificate of Analysis ..................................................... .
Samples were analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. Date of extraction, date of analysis, detection limits and dilution factor are reported for each compound analyzed. All samples were analyzed within the method required holding time from sample collection.
Data for each analytical method was evaluated by assessing the following QA/QC functions, as -applicable to the methodology: ·.··} .
• Quality Control Standard
• Surrogate Percent Recovery
• Laboratory Control Sample (LCS) percent recoveries for all analyses • Matrix Spike Recovery/Matrix Spike Duplicate Recovery (MSR & MSDR) and/or • Relative Percent Difference (RPD from MSR & MSDR)
I certify that this data report is in compliance both technically and for completeness. Release of the data contained in this hardcopy data report has been authorized by the following signature.
Second Original
anis · .
UVice President/Laboratory Director
Water • Soil • Waste • Wastewater • Marine Sediment & Tissues • Elutriate Analyses That Produce Results!
• ANALYSIS RESULTS •
CLIENT: BF GOODRICH DATE SAMPLED: 11104/98
DATE RECEIVED: 11104/98
PROJECf NAME/No.: 9853067B DATE DIGESTED: 11/09/98*
PTAS LOG#: 2175-98-1 DATE ANALYZED: 11/04-12/98
SAMPLE ID: DB-1-HP60 MATRIX: WATER
ANALYTE PREP./ANAL YSIS REPORTING LIMIT DF RESULTS UNITS
METHODS
AL.KALJNITY SMEWW1320B 5 5,280 MGCaC03/L
CONDUCTIVITY SMEWW2510B 2,350 UMHOS/CM
TDS SMEWW2540C 134 7 1,460 •• MGIL
pH EPA 150.1 0.1 8.5 pH UNITS
CHLORIDE SMEWW 4500 Cl C 0.25 5 560 -MGIL
SULFATE SMEWW 4500 S04 E 25 5 359 MGIL
MBAS SMEWW5540C 2.0 4 ••• ND MGIL
N!TR.ATEASN SMEWW 4500 N03 E 0.5 5 4.9 MGIL
CALCIUM EPA 3010/6010 100 50 2,910 MGIL
COPPER EPA 3010/6010 0.05 I 8.31 MGIL
IRON EPA 3010/6010 500 5,000 5,580 MGIL
MAGNESIUM EPA 3010/6010 50 50 2,960 MGIL
MANGANESE EPA 3010/6010 O.o3 l 54 MGIL
SODIUM EPA 3010/6010 5 5 570 MGIL·
ZINC EPA 3010/6010 0.05 12 MGIL
HARDNESS SMEWW2340B 10 I 19,500 MGCaC03/L
POTASSIUM EPA 3010/6010 50 100 896 MGIL
BORON EPA 3010/6010 0.2 5 4.0 MGIL
DILUTION FACTOR
NO= ANALYTE NOT DETECTED AT OR ABOVE THE INDICATED REPORTING LIMIT REPORTING LIMITS AND RESULTS HAVE BEEN ADNSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR. 'NOTE: APPLIES TO METALS ONLY.
"NOTE: UNABLE TO OBTAIN AN ACCURATE MEASUREMENT FOR IDS DUE TO HIGH TOTAL SOLIDS OF SAMPLE. "'NOTE: INCREASED DILUTION FACTOR DUE TO LIMITED SAMPLE VOLUME PROVIDED. ® Pacific Treatment Analytical Services, Inc. 4340 Vlewrtdge Ave., Suitto A • San Diogo, CA 92123 (619) 560-7717 FAX (619) 560·7763 ERA 9980
QA/QC REPORT
QNQC SAMPLE: ERA 9981, 9980
DATE ANALYZED: 11/06-09/98
SPIKED ANAL YTE TV DV 0/oR
ALKALINITY 126 134 105
CONDUCTIVITY 1380 1375 100
IDS 583 535 92
QA/QC REPORT
DATE ANALYZED: 11106/98
SPIKED ANAL YTE LCS%R
MilAS
TV= TRUE VALUE
DV =DETERMINED VALUE
AR =ACCEPTABLE RANGE
% Q. =PERCENT RECOVERY
103
LCSD%R RPD
99 4
LCS% R- LABORATORY CONTROL SAMPLE PERCENT RECOVERY
ACCEPTABLE
LCS,MSiMSD
CRITERIA
%
80-120
LCSD% R =LABORATORY CONTROL SAMPLE DUPLICATE PERCENT RECOVERY RPO = RELATIVE PERCENT DIFFERENCE
•
ACCEPTABLE ..
RPD
CRITERIA
%
<20
® Pacific Treatment Analytical Services, Inc. 4340 Vlewrfdgo Ave., A· san Diogo, CA 92123 (619) 560-1717 FAX (619) 560·7763 LCS 'Yo R = LABORATORY CONTROL SAMPLE PERCENT RECOVERY
MS% R =MATRIX SPIKE PERCENT RECOVERY
MSD % R = MATRIX SPIKE DUPLICATE PERCENT RECOVERY
RPD RELATIVE PERCENT DIFFERENCE
ACCEPTABLE ACCEPTABLE
LCS,MS/MSD RPD
'NOTE: NO RECOVERY REPORTABLE DUE TO NECESSARY D!LlfiTON OF SAMPLE SPIKED. A DUPL!CA TE LCS SAMPLE WA
WITH THE SAMPLE BATCH AND THE RESULTING RECOVERY AND RPD MET OR EXCEEDED ACCEPTANCE CRITER LCSD% R FOR CALCIUM== 87%, LCSD% R FOR IRON""' 118%, LCSD% R FOR MAGNESIUM= 86%, LCSD% R FOR S LCSD% RFOR POTASSIUM
®Pacific Treatment Analytical Services, Inc. 4340 Vlewridge Ave., Suite A. san Diego, CA 92123 (619) 560-7717 FAX (519) 560-7763 ® 0i::_ ...-rr:1 " i- v - -1'\Tr>'\f'0•'1__T4tVT '?>c6- A' w_._L l:? .;.Jn 0'--'1 Pacific Treatment Analytical Services, Inc. - /);'-r J
CHAIN-OF-CUSTODY RECORD
Phon< (619) 560-7717 F.x(619) 560-7763
21/ 5'- '7.8 PTAS LOG# PTAS DATErriME 1
4340 Viewridge Avenue, Suite A San Diego, CA 92123
P I I
!client: ..I VJc..h Jn:;nrrP<;TED ANALYSIS
' ' J
'
. 6
7 Types: B•BrassTot>:;.V•VOA; "·"'' .c. :\ RF!IN(Irrrc;:HFn BY DATEfnMb RECEIVtDBY ffAs
dT'i;;;" 2411< 4811< Jot.y 4ot.y ', ;t::/. , . .r./s
: AI• r.O LoAn J._) ), fo/ .....-..-,-"
"' J 1dLliJ t. .f£ lL • L _<;',. .•
I u - Print *' uf:-f; \\ ,{' ltQu\_ J
i; '
.-'
.
• PT AS reserves the right to sampla that don'\ waste profile. While - PT AS Canary - Pink- Client I J- Cli<nl 1 Sampl<s) (R<v, S/97) Pacific Treatment •
Analytical Services, Inc.
January 7, 1999
BF Goodrich
Attn.: Rick Siordia
850 Lagoon Drive
Chula Vista, California 91910-2098
4340 Viewridge • Avenue, Suite A • San Diego, CA 92123
(619) 560-7717 • Fax (619) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: 9853067B-0100
Laboratory Log No.: 2186-98
Date Received: 11105/98
Sample Matrix: One water sample
PO No.: 9853067B
Please find the following enclosures for the above referenced project identified:
1) Analytical Report
2) QA/QC Report
3) Chain of Custody Form
....................................................... Certificate of Analysis ..................................................... .
Samples were analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. Date of extraction, date of analysis, detection limits and dilution factor are reported for each compound analyzed. All samples were analyzed within the method required holding time from sample collection.
Data for each analytical method was evaluated by assessing the following QA/QC functions, as applicable to the methodology:
•
•
•
•
•
Quality Control Standard
Surrogate Percent Recovery
Laboratory Control Sample (LCS) percent recoveries for all analyses Matrix Spike Recovery/Matrix Spike Duplicate Recovery (MSR & MSDR) and/or Relative Percent Difference (RPD from MSR & MSDR)
I certify that this data report is in compliance both technically and for completeness. Release of the data contained in this hardcopy data report has been authorized by the following signature.
Vice President/Laboratory Director
Water • Soil • Waste • Wastewater • Marine Sediment & Tissues • Elutriate Analyses That Produce Results!
•
CLIENT: BF GOODRICH
PROJECTNAME/No.: 9853067B-OIOO
PTAS LOG#: 2186-98-1
SAMPLE ID: DB-1-HPI08.5
ANALYSIS RESULTS
ANALYTE PREP./ ANALYSIS
METHODS
REPORTING LrMIT DF
MBAS SMEWW 5540C 0.5 I
CONDUCTMTY SMEWW2510B I I
SULFATE SMEWW 4500 S04 E 25 5
CHLORIDE SMEWW 4500 Cl C 0.05 I
CHLORIDE (DUP.) SMEWW 4500 Cl C 0.05 I
IDS SMEWW2540C 80 4
ALKALINITY SMEWW2320B 5 I
ALKALINITY (DUP.) SMEWW2320B 5
pH EPA 150.1 0.1 I
NITRITEASN SMEWW 4500 N02 B 0.25 5
NITRITE AS N (DUP.) SMEWW 4500 N02 B 0.25 5
NITRATEASN SMEWW 4500 N03 E 2.0 20
NITRATE AS N (DUP.) SMEWW 4500 N03 E 2.0 20
FLUORIDE SMEWW 4500 F C 0.1 I
CALCIUM EPA 3010/6010· 20 10
COPPER EPA 3010/6010 0.05
IRON EPA 3010/6010 10 100
MAGNESIUM EPA 3010/6010 10 10
MANGANESE EPA 3010/6010 0.03 I
SODIUM EPA 3010/6010 50 10
ZINC EPA 3010/6010 . 0.05 I
HARDNESS SMEWW2340B 10 l
POTASSIUM EPA 3010/6010 5 10
BORON EPA 3010/6010 0.2
OF- DILUTION FACTOR
DUP. =DUPLICATE
NO- ANAL YTE NOT DETECTED AT OR ABOVE THE INDICA TED REPORTING LIMIT •
DATE SAMPLED:
DATE RECEIVED:
DATE DIGESTED:
DATE ANALYZED:
MATRIX:
RESULTS
ND
6,050
356
1,750
1,760
2,790 ••
192
191
7.7 0.18
0.18 1.1
1.1 0.9
328
0.90 422
468
4.17 1,140
215
2,750
89 1.0
REPORTING LIMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR. 'NOTE: APPLIES TO METALS ONLY.
"NOTE: UNABLE TO OBTAIN AN ACCURATE MEASUREMENT FOR TDS DUE TO HIGH TOTAL SOLIDS OF SAMPLE. 11/05/98
11/05/98
11/09/98*
11/05-12/98
WATER
UNITS
MGIL
UMHOS/CM
MGIL
MGIL
MGIL
MGIL
MGCaC03/L
MGCaC03/L
pH UNITS
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGCaC03/L
MGIL
MGIL
®Pacific Treatment Analytical Services, Inc. 4340 l/lewrldoe Ave., Suite A. san Diego. CA 92123 (619) 560-7717 FAX (619) 560-7763 '"''"V'- SAMPLE: ERA 9980
ANALYZED: 11105/98
QA/QC REPORT
QAJQC SAMPLE: ERA 9981, 9980
DATE ANALYZED: 11106-09/98
SPIKED ANALYTE TV DV o/oR
ALKALINITY 126 134 105
CONDUCTIVITY 1380 1375 100
IDS 583 535 92
QA/QC REPORT
DATE ANALYZED: 11106/98
SPIKED ANALYTE LCS%R
Ml3AS
TRUE VALUE
DV VALUE
AR= ACCEPTABLE RANGE
% R RECOVERY
103
LCSD%R RPD
99 4
LCS% R = LABORATORY CONTROL SAMPLE PERCENT RECOVERY
ACCEPTABLE
LCS,MS/MSD
CRITERIA
%
80-120
LCSD% R =LABORATORY CONTROL SAMPLE DUPL!CA TE PERCENT RECOVERY RPD =RELATIVE PERCENT DIFFERENCE
•
ACCEPTABLE
RPD
CRITERIA
%
<20
®Pacific Treatment Analytical Services, Inc. 4340 Vlewridge Ave .• Suite A ·San Diego. CA 92123 (619) 560-7717 FAX (619) 560-7763 LCS% R =LABORATORY CONTROL SAMPLE PERCENT RECOVERY
MS% R = MA TRJX SPIKE PERCENT RECOVERY
MSD% R =MATRIX SPIKE DUPLICATE PERCENT RECOVERY
RPD = RELA T!VE PERCENT DIFFERENCE
ACCEPTABLE ACCEPTABLE
LCS,MS/MSD RPD
'NOTE: NO RECOVERY REPORTABLE DUE TO NECESSARY DILUTION OF SAMPLE SPIKED. A DUPLICATE LCS SAMPLE WA
WITH THE SAMPLE BATCH AND THE RESULTING RECOVERY AND RPD MET OR EXCEEDED ACCEPTANCE CRJTER LCSD% RFORCALCIUM = 87%, LCSD% RFORIRON= 118%, LCSD% RFORMAGNESIUM= 86%, LCSD% RFORS LCSD% R FOR POTASSIUM= 87%
®Pacific Treatment Analytical Services, Inc. 4340 Vlewrldge Ave., Suite A • San Diego, CA 92123 (619) 560-7717 . FAX (619) 560-7763 ' I
-
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Pacific Inc.
1 tl,l!n \
4340 Vicwridgc Avenue, Suite A San Diego, CA 92123 Phone (619) 560-7717 Fax (619) 560-7763 um PTASLOG# PTAS DATE!TIME ..
REOUESTED ANALYS:rs
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Print
White- PTAS Canary- Ac..:ounting Pink- .. , ,_,
Pacific Treatment •
Analytical Services, Inc.
January 7, 1999
BFGoodrich
Attn.: Rick Siordia
850 Lagoon Drive
Chula Vista, California 91910-2098
4340 Viewridge • Avenue, Suite A • San Diego, CA 92123
(619) 560-7717 • Fax (619) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: 9853067B-0100
Laboratory Log No.: 2186-98 (Revision)
Date Received: 11105/98
Sample Matrix: One water sample
PO No.: 9853067B
Please find the revised report for the above referenced project. This report was revised due to a typographical error. We apologize for any inconvenience.
Second Original
Water • Soil • Waste • WasteWater • Marine Sediment & Tissues • Elutriate Analyses That Produce Results!
•
CLIENT: BF GOODRICH
PROIECf NAME/No.: 9853067B-OIOO
PTAS LOG#: 2186-98-1
SAMPLE ID: DB-1-HPI08.5
ANALYSIS RESULTS
ANALYTE PREP./ ANALYSIS
METHODS
REPORTING LIMIT DF
MBAS SMEWW5540C 0.5
CONDUCTIVITY SMEWW2510B
SULFATE SMEWW 4500 S04 E 25 5
CHLORIDE SMEWW 4500 Cl C 0.05
CHLORIDE (DUP.) SMEWW 4500 Cl C 0.05
TDS SMEWW2540C 80 4
ALKALINITY SMEWW2320B 5 I
ALKALINITY (DUP.) SMEWW2320B 5
pH EPA 150.1 0.1 I
NITRITEASN SMEWW 4500 N02 B 0.25 5
NITRITE AS N (DUP.) SMEWW 4500 N02 B 0.25 5
NITRATEASN SMEWW 4500 N03 E 2.0 20
NITRATE AS N (DUP.) SMEWW 4500 N03 E 2.0 20
FLUORIDE SMEWW 4500 F C 0.1 I
CALCIUM EPA 3010/6010 20 10
COPPER EPA 3010/6010 0.05 I
IRON EPA 3010/6010 10 100
MAGNESIUM EPA 3010/6010 10 10
MANGANESE EPA 3010/6010 0.03 I
SODIUM · EPA 3010/6010 50 10
ZINC EPA 3010/6010 0.05 I
HARDNESS SMEWW2340B 10 I
POTASSIUM EPA 3010/6010 5 10
BORON EPA 3010/6010 0.2 l
DF FACTOR
DUI'. = DUI'L!CA TE
NO= ANAL YTE NOT DETECTED AT OR ABOVE THE iNDICA TED REPORTING LIMIT •
DATE SAMPLED:
DATE RECEIVED:
DATE DIGESTED:
DATE ANALYZED:
MATRIX:
RESULTS
ND
6,050
356
1,750
1,760
2,790 ••
192
191
7.7 0.18
0.18 1.1
1.1 0.9
328
0.90 422
468
4.17 1,140
2.15 2,750
·89
1.0 REPORTING LIMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR ' NOTE: APPLIES TO METALS ONLY.
"NOTE: UNABLE TO OBTAIN AN ACCURATE MEASUREMENT FOR TDS DUE TO lllGH TOTAL SOLIDS OF SAMPLE. 11/05/98
11/05/98
11109/98*
11105-12/98
WATER
UNITS
MGIL
UMHOS/CM
MGIL
MGIL
MGIL
MGIL
MGCaC03/L
MGCaC03/L
pH UNITS
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MGIL
MOIL
MGCaC03/L.
MGIL
MGIL
® Pacific Treatment Analytical Services, Inc- 4340 Vlewrldge Ave., sune A· san Diego, CA 92123 (519) S5Q-7717 FAX (519) 560-7763 ERA 9980
QAJQC REPORT
QA/QC SAMPLE: ERA 9981, 9980
DATE ANALYZED: 11106-09/98
SPIKED ANAL YTE TV DV 0
/oR
ALKALINITY 126 134 105
CONDUCTIVITY 1380 1375 100
TDS 583 535 92
QAJQC REPORT
DATE ANALYZED: 11106/98
SPIKED ANALYTE LCS%R
MBAS
TV= TRUE VALUE
DV =DETERMINED VALUE
AR=ACCEPTABLE RANGE
% R =PERCENT RECOVERY
103
LCSD%R RPD
·99 4
LCS% R =LABORATORY CONTROL SAMPLE PERCENT RECOVERY
ACCEPTABLE
LCS,MS/MSD
CRITERIA
%
80-120
LCSD% R =LABORATORY CONTROL SAMPLE DUPLICATE PERCENT RECOVERY RPO = RELATIVE PERCENT DIFFERENCE .
•
ACCEPTABLE
RPD
CRITERIA
%
<20
®Pacific Treatment Anslyt/cs/ Services, Inc. 4340 IJiewndge Ave., Sui1e A. san Diego, CA 92123 (619) 550-7717 FAX (619) 560-7763 LCS% R =LABORATORY CONTROL SAMPLE PERCENT RECOVERY
MS% R =MATRIX SPIKE PERCENT RECOVERY
MSD% R =MATRIX SPIKE DUPL!CA TE PERCENT RECOVERY
RPD =RELATIVE PERCENT DIFFERENCE
ACCEPTABLE ACCEPTABLE
LCS,MS/MSD RPD
'NOTE: NO RECOVERY REPORTABLE DUE TO NECESSARY D!LliT!ON OF SAMPLE SPIKED. A DUPLICATE LCS SAMPLE WA WITH THE SAMPLE BATCH AND THE RESULTING RECOVERY AND RPD MET OR EXCEEDED ACCEPTANCE CR!TER LCSD% RFORCALCIUM = 87%, LCSD% RFOR IRON= ll&%, LCSD% RFORMAGNESIUM = 86%, LCSD% RFORS LCSD% R FOR POTASSIUM= 87%
®Pacific Treatment Analytical Services, Inc. 4340 'llewridge Ave., A • San Diego, CA 92123 (619) 560-7717 FAX (619) 560-7763 • -Jf Ar. ',· Pacific Treatment Analytical Services, inc.
CHAIN-OF-CUSTODY RECORD . · . 4340 Viewridgc Avenue, Suite A San Diego, CA 92123 Phone (619)560-7717 F"" (619)560-7763 ._ ::- · 1PTASLOG# p = ·
REQUES'wu ANALY5:YS .,
X . I • 2
. J
4 5
6 7
. Print
·• · '·' • '·'''"" lh:11 don, out wast.: Jnulilc. Pink- Client! G -Client · • (Rev. 5197 Pacific Treatment •
Analytical Services, Inc.
January 7, 1999
BF Goodrich
Attn: Rick Siordia
850 Lagoon Drive
Chula Vista, California 91910
4340 Viewridge • Avenue, Suite A • San Diego, CA 92123
(619) 560-7717 • Fax (619) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: 9853067B-0200
Laboratory Log No.: 2284-98
Date Received: 11123/98
Sample Matrix: One water sample
PO No.: 9853067B-0200
Please find the following enclosures for the above referenced project identified:
1) Analytical Report
2) QNQC Report
4) Chain of Custody Form
....................................................... Certificate of Analysis ..................................................... .
Samples were analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. Date of extraction, date of analysis, detection limits and dilution factor are reported for each compound analyzed.
Data for each analytical method was evaluated by assessing the following QNQC functions, as applicable to the methodology:
•
•
•
•
•
Quality Control Standard ·
Surrogate Percent Recovery
Laboratory Control Sample (LCS) percent recoveries for all analyses Matrix Spike Recovery/Matrix Spike Duplicate Recovery (MSR & MSDR) and/or Relative Percent Difference (RPD from MSR & MSDR)
I certify that this data report is in compliance both technically and for completeness. Release of the data contained in this hardcopy data report has been authorized by the following signature.
Second Original
Vice President/Laboratory Director
Water • Soil • Waste • Wastewater • Marine Sediment & TlSSues • Elutriate Analyses That Produce Results!
• ANALYSIS RESULTS •
CLIENT: B F GOODRICH DATE SAMPLED: 11122/98
DATE RECEIVED: 11/23/98
PROJECT NAME/No.: 9853067B-0200 DATE DIGESTED: 11/23/98' PTAS LOG#: 2284-98-1 DATE ANALYZED: 11/23-12/02/98
SAMPLE ID: DB-2-HP77 MATRIX: LIQUID
ANALYTE PREP .I ANALYSIS REPORTING LIMITS DF RESULTS UNITS
METHODS
ALKALINITY SMEWW2320B 5 234 MGCaC031L
CONDUCTIVITY SMEWW2510B 5,720 UMHOS/CM
MBAS SMEWW5540C 0.5 0.5 MGIL
IDS SMEWW2540C 20 3,700 MGIL
pH EPA 150.1 0.1 7.2 pH UNITS
CHLORIDE SMEWW 4500 Cl C 0.05 1,690 MGIL
SULFATE SMEWW 4500 S04 E 25 5 350 MOIL
CALCIUM EPA 3010/6010 . 20 10 342 MOIL
COPPER EPA 3010/6010 0.05 ND MOIL
IRON EPA 3010/6010 0.1 3.0 MGIL
MAGNESIUM EPA 3010/6010 10 10 168 MGIL
MANGANESE EPA 3010/6010 0.03 0.16 MOIL
SODIUM EPA 3010/6010 50 10 694 MGIL
ZINC EPA 3010/6010 0.05 ND MOIL
HARDNESS SMEWW 2340 B . 10 1,550 MGCaC03/L
POTASSIUM EPA 3010/6010 0.5 I 7.7 MOIL
BORON EPA 3010/6010 0.5 .I ND MOIL
FLUORIDE SMEWW 4500 F C 0.1 I 0.3 MOIL
FLUORIDE (DUP.) SMEWW 4500 F C 0.1 0.3 MOIL
NITRA 1"E AS N SMEWW 4500 N03 0.1 21.0 MOIL
NITRI1"E AS N SMEWW 4500 N02 0.05 ND MOIL
DF =DILUTION FACTOR
DUP. = DIJPLICA TE
ND =ANAL YTE NOT DETECTED AT OR ABOVE THE INDICATED REPORTING LIMIT REPORTING LIMITS AND RESULTS HAVE BEEN ADJUSTED ACCORDINGLY TO ACCOUNT FOR DILUTION FACTOR. 'NOTE: APPLIES TO METALS ONLY.
®Pacific Treatment Analytical Services, Inc. 4340 vreWridge Ave .. Suite A ·San Diego, CA 92123 (619) 560-7717 FAX (619) 560-7763 QAIQC SAMPLE: ERA 9981
ANALYZED:
QA/QC REPORT
QAIQC SAMPLE: ERA 9981, 9979
DATE ANALYZED: 11123/98
SPIKED ANALYTE TV DV %R
IDS 583 600 103
ALKALINITY 157 161 99
CONDUCTIVITY 733 724 99
QA/QC REPORT
DATE ANALYZED: 11124/98
SPIKED ANAL YTE I LCS% R ILCSD %
MilAS I
TRUE VALUE
DV =DETERMINED VALUE
AR =ACCEPTABLE RANGE
% R =PERCENT RECOVERY
99 I 101
RPD
2 LCS% R =LADORA TORY CONTROL SAMPLE PERCENT RECOVERY
ACCEPTABLE
LCSILCSD
CRITERIA
%
80-120
LCSD% R =LADORA TORY CONTROL SAMPLE DUPLICATE PERCENT RECOVERY •
ACCEPTABLE
RPD
CRITERIA
%
<20
®Pacific Treatment Analytical Services, Inc. 4340 Vlewndge Ave., Surte A •San Diego, CA 92123 (619) 560-7717 FAX (619) 560-7763 '
OA/Or REPORT
DATE ANALYZED:
ANAT.VTE
FTTTOllmJ'
rHTQRIDR
m ltuUi AS N
INITRA TE AS N
\TE
C:AT.C:n TM
:IRON
jMAC '!Vl
\fA NC:A
JM
ZINC
POTASSI TM
OVKVN
DV VALUE
AR RANGE
% R- PERCENT RECOVERY
11/23-30/98
LCS%R
99 100
103
94 92
93 98
98 90
97_
101
97 86
85 MS%R IMSD%R
88 88
99 99
9_5_ 96
89 87
95 93
• •
95 92
85 82
• •
90 88
• •
92 91
87 86
80 80
LCS% R CONTROL SAMPLE PERCENT RECOVERY
MS % R MATRIX SPIKE PERCENT RECOVERY
MSD% R SPIKE DUPLICATE PERCENT RECOVERY
RPD TNE PERCENT DIFFERENCE
RPD
0 0
I
2 2
•
3 4
•
2 •
I
I
0 ACCEPTABLE ACCEPTABLE
LCS,MS/MSD RPD
CRITERIA CRITERIA
% %
80-120 <20
80-120 <20
80-120 <20
80-120 <20
80-120 <20
75-125 <_20
75-125 <20
75-125 <20
75-125 <20
75-125 . <(_20
75-125 <20
75-125 <20
75-125 <20
75-125 <20 .
• NOTE: NO llECOVERY REPORTABLE DUE TO NECESSARY DILUTION OF SAMPLE SPIKED. A DUPLICATE LCS SAMPLE WAS ANALYZED WITH THE SAMPLE BATCH AND THE RESULTING RECOVERY AND RPD MET OR EXCEEDED ACCEPTANCE CRITERIA.
LCSD %R FOR CALCIUM- 89"/o, LCSD% R FOR 88%, AND LCSD% R FOR SODIUM- 99%. ®Pacific Ti'eatment Analytical Services, Inc. 4340 Vlewridge Avo., Suite A· san Diego, CA 92123 (619) 560-7717 FAX (619) 560-7763 ® • Analytical Services, Inc.
•) Pacific TreatmeonFt CHAIN- CUSTODY RECoRD,, 9D NOV 2. 3. - Phone (619) 560· SanDiego,CA92123 PTAS DATEffiME STAMP ....;:
. "d Avenue, Suite A
.,.,_. IPTAs LOG. , "' , +,.- ,
.
'
_'
\
\
\
.\\
A9! 21
I I
. '-'''"'' ' ' - (Rev. 5/97)
Pacific Treatment •
Analytical Services, Inc.
January 7, 1999
BF Goodrich/ROHR
Attn: Rick Siordia
850 Lagoon Drive
Chula Vista, California 91910
4340 Viewridge • Avenue, Suite A • San Diego, CA 92123
(619) 560-7717 • Fax (619) 560-7763
Analytical Chemistry Laboratory
Project Name/No.: 9853067B-0200
Laboratory Log No.: 2290-98
Date Received: 11123/98
Sample Matrix: One water sample
PO No.: S45575
Please find the following enclosures for the above referenced project identified:
I) Analytical Report
2) QNQC Report
4) Chain of Custody Form
....................................................... Certificate of Analysis ..................................................... .
Samples were analyzed pursuant to client request utilizing EPA or other ELAP approved methodologies. Date of extraction, date of analysis, detection limits and dilution factor are reported for each compound analyzed. All samples were analyzed within the method required holding tim·e from sample collection.
Data for each analytical method was evaluated by assessing the following QNQC functions, as applicable to the methodology:
• Quality Centro I Standard
• Surrogate Percent Recovery
• Laboratory Control Sample (LCS) percent recoveries for all analyses • Matrix Spike Recovery/Matrix Spike Duplicate Recovery (MSR & MSDR) and/or • Relative Percent Difference (RPD from MSR & MSDR)
I certifY that this data report is in compliance both technically and for completeness. Release of the data contained in this hardcopy data report has been authorized by the following signature.
Second Original
Vice President/Laboratory Director
Water • Soil • Waste • Wastewater • Marine Sediment & Tissues • Elutriate Analyses That Produce Results!
www.haleyaldrich.com
BORING COMPLETION REPORT
ROHR, INC., A COLLINS AEROSPACE COMPANY
ASSESSOR PARCEL NO. 567-022-30-00
PERMIT NO. LMWP-004690
by
Haley & Aldrich, Inc.
San Diego, California
for
Rohr, Inc., a Collins Aerospace Company
Chula Vista, California
File No. 127827-022
January 2021
HALEY & ALDRICH, INC.
5333 Mission Center Road
Suite 300
San Diego, CA 92108
619.280.9210
www.haleyaldrich.com
January 6, 2021
File No. 127827-022
County of San Diego
Department of Environmental Health
P.O. Box 129261
San Diego, California 92112-9261
Attention: Well Permit Clerk
Subject: Well Destruction Report
Rohr, Inc., a Collins Aerospace Company
390 Bay Boulevard
Chula Vista, California
Assessor’s Parcel No. 567-022-30-00
Permit No. LMWP-004690
Dear Well Permit Clerk:
Haley & Aldrich, Inc., is submitting this well destruction report to the County of San Diego Department of Environmental Health (DEH) for three monitoring wells (DB-2, DB-4, and DB-5) and two pressure transducers (OW-1 and OW-2) on the property associated with Assessor’s Parcel Number 567-022-30- 00, located at 390 Bay Boulevard at the Rohr, Inc., a Collins Aerospace Company, facility located in Chula Vista, California (Site; Figure 1). The wells and transducers were destroyed under Permit No. LMWP004690, approved by the DEH on September 28, 2020.
Cascade Drilling, Inc., a C-57 licensed drilling company located in Upland, California, completed the destruction of the monitoring wells and pressure transducers. Wells DB-2 and DB-5 and the pressure transducers OW-1 and OW-2 were destroyed on October 19 and October 20, 2020. Well DB-5 was destroyed on November 16 and 17, 2020.
Prior to destruction, the total depth of each well was measured to identify whether the well was free of obstructions. No obstructions were observed. The monitoring wells were abandoned by pressure grouting. Each boring was backfilled from the bottom up to within approximately 5 feet below the ground surface (bgs) with cement-bentonite grout (with 5 percent bentonite by weight) mixed at a ratio of approximately 100 pounds of solids to 35 to 40 gallons of water and then pumped through a tremie pipe. The grout was placed within the screen interval and held at 30 pounds per square inch of pressure for 20 minutes.
A hollow-stem auger rig was used to overdrill the two wells with polyvinyl chloride casings (DB-2 and DB-4) so that the casings could be removed. An 8.5-inch-diameter cutting head was used to destroy and remove the upper 5 feet of casing. The upper 5 feet of well DB-5 was removed by excavating around it County of San Diego Department of Environmental Health
January 6, 2021
to approximately 4 feet bgs and cutting the steel casing off at 5 feet bgs using an arc welder. The upper 5 feet of the DB-2 and DB-5 boreholes were filled with bentonite chips hydrated during placement. The surface at each location was finished in concrete. Table I provides a backfill material summary for each well.
The traffic covers for the pressure transducers (OW-1 and OW-2) were removed and filled with concrete to the surface grade to abandon them. The traffic covers for monitoring wells OW-3 and OW-4, which remain on Site, were replaced in accordance with DEH guidelines. If you have any questions regarding the well destructions, please contact us.
Sincerely yours,
HALEY & ALDRICH, INC.
Robert K. Scott, P.G., C.Hg.
Senior Associate Hydrogeologist
c: Raytheon Technologies Corporation; Attn: John Baron
Rohr, Inc., a Collins Aerospace Company; Attn: Rick Siordia Rohr, Inc., a Collins Aerospace Company; Attn: Tyler Adkins PSIP Wohl Properties; Attn: Emil Wohl
Attachments:
Table I – Backfill Material Summary
Figure 1 – Well Location Map
G:\127827_North Campus\022_Parcel A Well Destruction\60 Day report\2021_0106_HAI_BoringCmpltnRpt_F.docx TABLE
TABLE I
BACKFILL MATERIAL SUMMARY
ROHR, INC., A COLLINS AEROSPACE COMPANY
390 BAY BOULEVARD
CHULA VISTA, CALIFORNIA