Cities Index.
Attachment A - PC Staff Report and Attachments part 4

Long Beach City Council
September 19, 2023

Document
Attachment A - PC Staff Report and Attachments part 4
Meeting
September 19, 2023
Body
Long Beach City Council
Pages
94
Original file
69.7 MB
Text extracted from the city's file for reading and search. Open the original on longbeach.legistar.com. That file is the official record.

TestAmerica Irvine
7/26/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95 1 2
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Lab Sample ID Client Sample ID Matrix Collected Received 440-152462-1 AEC-5-5' Solid 07/12/16 09:00 07/12/16 18:30 440-152462-2 AEC-5-10' Solid 07/12/16 09:05 07/12/16 18:30 440-152462-3 AEC-5-15' Solid 07/12/16 09:08 07/12/16 18:30 440-152462-4 AEC-5-20' Solid 07/12/16 09:12 07/12/16 18:30 440-152462-5 AEC-3-5' Solid 07/12/16 11:05 07/12/16 18:30 440-152462-6 AEC-3-10' Solid 07/12/16 11:10 07/12/16 18:30 440-152462-7 AEC-3-15' Solid 07/12/16 11:14 07/12/16 18:30 440-152462-8 AEC-3-20' Solid 07/12/16 11:21 07/12/16 18:30 440-152462-9 AEC-4-5' Solid 07/12/16 13:15 07/12/16 18:30 440-152462-10 AEC-4-10' Solid 07/12/16 13:19 07/12/16 18:30 440-152462-11 AEC-4-15' Solid 07/12/16 13:25 07/12/16 18:30 440-152462-12 AEC-4-20' Solid 07/12/16 13:30 07/12/16 18:30 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Job ID: 440-152462-1
Laboratory: TestAmerica Irvine
Narrative
Job Narrative
440-152462-1
Comments
No additional comments.

Receipt
The samples were received on 7/12/2016 6:30 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 4.0º C.

Receipt Exceptions
The Field Sampler was not listed on the Chain of Custody.

GC/MS VOA
Method(s) 8260B: The continuing calibration verification (CCV) associated with batch 440-342846 recovered above the upper control limit for Chloroethane and Chloromethane. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following samples are impacted: AEC-4-20' (440-152462-12) and (CCVIS 440-342846/2).

Method(s) 8260B: Internal standard responses were outside of acceptance limits for the following samples: 1,4-Dichlorobenzene-d4 is low AEC-3-5' (440-152462-5) and AEC-3-20' (440-152462-8). The sample(s) shows evidence of matrix interference. Due to limited sample volume no rerun was possible.

Method(s) 8260B: Surrogate recovery for the following samples was outside control limits: 4-Bromofluorobenzene, Dibromofluoromethane and Toluene-d8 are high AEC-3-5' (440-152462-5). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8260B/CA_LUFTMS: Internal standard responses were outside of acceptance limits for the following samples:
1,4-Dichlorobenzene-d4 is low AEC-3-5' (440-152462-5) and AEC-3-20' (440-152462-8). The sample(s) shows evidence of matrix interference. Due to limited sample volume sample could not be reran.

Method(s) 8260B/CA_LUFTMS: Surrogate recovery for the following samples was outside control limits: 4-Bromofluorobenzene, Dibromofluoromethane and Toluene-d8 are high AEC-3-5' (440-152462-5). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. Limited sample volume.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA
Method(s) 8270C SIM: The following sample required a dilution due to the nature of the sample matrix: AEC-3-5' (440-152462-5).

Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8270C SIM: The following sample was diluted due to the nature of the sample matrix: AEC-3-5' (440-152462-5). Elevated reporting limits (RLs) are provided.

Method(s) 8270C SIM: The continuing calibration verification (CCV) associated with batch 440-342622 recovered above the upper control limit for Benzo[g,h,i]perylene. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC Semi VOA
Method(s) 8015B: Surrogate recovery for the following sample was outside control limits: AEC-5-5' (440-152462-1). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Job ID: 440-152462-1 (Continued)
Laboratory: TestAmerica Irvine (Continued)
Method(s) 8015B: The following sample required a dilution due to the nature of the sample matrix: AEC-3-5' (440-152462-5). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8015B: Surrogate recovery for the following sample was outside control limits: AEC-3-10' (440-152462-6). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8082: Surrogate recovery for the following samples was outside control limits: AEC-3-15' (440-152462-7). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8082: The following samples required a copper clean-up to reduce matrix interferences caused by sulfur: AEC-5-5' (440-152462-1), (LCS 440-342185/2-A), (MB 440-342185/1-A), (440-152462-A-1-D MS) and (440-152462-A-1-E MSD).

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep
Method(s) 3546: The following samples was diluted due to the nature of the sample matrix: AEC-5-5' (440-152462-1), AEC-5-10' (440-152462-2), AEC-5-15' (440-152462-3), AEC-5-20' (440-152462-4), AEC-3-5' (440-152462-5), AEC-3-10' (440-152462-6), AEC-3-15' (440-152462-7), AEC-3-20' (440-152462-8), AEC-4-5' (440-152462-9), AEC-4-10' (440-152462-10), AEC-4-15' (440-152462-11), AEC-4-20' (440-152462-12), (440-152462-A-1 MS) and (440-152462-A-1 MSD). Elevated reporting limits (RLs) are provided.

Method(s) 3546: The following samples was diluted due to the nature of the sample matrix: AEC-5-5' (440-152462-1), AEC-5-10' (440-152462-2), AEC-5-15' (440-152462-3), AEC-5-20' (440-152462-4), AEC-3-5' (440-152462-5), AEC-3-10' (440-152462-6), AEC-3-15' (440-152462-7), AEC-3-20' (440-152462-8), AEC-4-5' (440-152462-9), AEC-4-10' (440-152462-10), AEC-4-15' (440-152462-11), AEC-4-20' (440-152462-12), (440-152462-A-1 MS) and (440-152462-A-1 MSD). Elevated reporting limits (RLs) are provided.

Method(s) 3546: Due to the matrix, the following sample could not be concentrated to the final method required volume: AEC-3-5' (440-152462-5). The reporting limits (RLs) are elevated proportionately.

Method(s) 3546: The following samples was diluted due to the nature of the sample matrix: AEC-5-15' (440-152462-3) and AEC-3-15' (440-152462-7). Elevated reporting limits (RLs) are provided.

Method(s) 3546: The following sample was diluted due to the nature of the sample matrix: AEC-4-15' (440-152462-11). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-5' Lab Sample ID: 440-152462-1
Date Collected: 07/12/16 09:00 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 0.099 0.069 mg/Kg 07/14/16 16:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 107 60 - 120 07/14/16 16:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 79 - 120 07/14/16 16:53 1 Toluene-d8 (Surr) 104 79 - 123 07/14/16 16:53 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 1,1,2,2-Tetrachloroethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 1,1,2-Trichloroethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 1,1-Dichloroethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,1-Dichloroethene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
1,1-Dichloropropene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,2,3-Trichlorobenzene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 1,2,3-Trichloropropane ND 9.9 0.99 ug/Kg 07/14/16 16:53 1 1,2,4-Trichlorobenzene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 1,2,4-Trimethylbenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/14/16 16:53 1 1,2-Dibromoethane (EDB) ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 1,2-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,2-Dichloroethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,2-Dichloropropane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,3,5-Trimethylbenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 1,3-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,3-Dichloropropane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
1,4-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
2,2-Dichloropropane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
2-Chlorotoluene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
4-Chlorotoluene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Benzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Bromobenzene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Bromochloromethane ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Bromodichloromethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 Bromoform ND 5.0 2.0 ug/Kg 07/14/16 16:53 1
Bromomethane ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Carbon tetrachloride ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 Chlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Chloroethane ND 5.0 2.0 ug/Kg 07/14/16 16:53 1
Chloroform ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Chloromethane ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
cis-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 cis-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 Dibromochloromethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 Dibromomethane ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/14/16 16:53 1 Isopropyl Ether (DIPE) ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 Ethanol ND 300 99 ug/Kg 07/14/16 16:53 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-5' Lab Sample ID: 440-152462-1
Date Collected: 07/12/16 09:00 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Hexachlorobutadiene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Isopropylbenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/14/16 16:53 1
Methylene Chloride ND 20 5.0 ug/Kg 07/14/16 16:53 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 Naphthalene ND 5.0 2.0 ug/Kg 07/14/16 16:53 1
n-Butylbenzene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
N-Propylbenzene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
o-Xylene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
sec-Butylbenzene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Styrene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Tert-amyl-methyl ether (TAME) ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 tert-Butyl alcohol (TBA) ND 99 9.9 ug/Kg 07/14/16 16:53 1 tert-Butylbenzene ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Tetrachloroethene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Toluene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
trans-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 trans-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1 Trichloroethene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Trichlorofluoromethane ND 5.0 0.99 ug/Kg 07/14/16 16:53 1 Vinyl chloride ND 5.0 0.99 ug/Kg 07/14/16 16:53 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/14/16 16:53 1
p-Isopropyltoluene ND 2.0 0.99 ug/Kg 07/14/16 16:53 1
Toluene-d8 (Surr) 104 79 - 123 07/14/16 16:53 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 79 - 120 07/14/16 16:53 1 Dibromofluoromethane (Surr) 107 60 - 120 07/14/16 16:53 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Benzo[a]anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Benzo[a]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Benzo[b]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Benzo[g,h,i]perylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Benzo[k]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Chrysene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Dibenz(a,h)anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Fluorene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Indeno[1,2,3-cd]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Naphthalene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Phenanthrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1 Pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 12:11 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-5' Lab Sample ID: 440-152462-1
Date Collected: 07/12/16 09:00 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 68 39 - 111 07/14/16 09:28 07/15/16 12:11 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 66 41 - 119 07/14/16 09:28 07/15/16 12:11 1 Terphenyl-d14 77 43 - 150 07/14/16 09:28 07/15/16 12:11 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.2 mg/Kg 07/13/16 18:24 07/14/16 11:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 10 5.2 mg/Kg 07/13/16 18:24 07/14/16 11:54 1 n-Octacosane 37 X 40 - 140 07/13/16 18:24 07/14/16 11:54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 Aroclor 1232 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 Aroclor 1242 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 Aroclor 1248 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 Aroclor 1254 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 Aroclor 1260 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:26 1 DCB Decachlorobiphenyl (Surr) 72 45 - 120 07/13/16 18:43 07/15/16 14:26 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 4.5 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Barium 130 F1 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Beryllium 0.46 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Chromium 18 F1 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Cobalt 7.1 F1 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Copper 18 F1 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Lead 5.5 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Molybdenum 0.77 J 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Nickel 13 F1 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Selenium 0.47 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Vanadium 35 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Zinc 49 F1 9.9 5.0 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Antimony 0.40 J F1 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 09:34 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.031 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 20:40 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-10' Lab Sample ID: 440-152462-2 Date Collected: 07/12/16 09:05 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 0.10 0.070 mg/Kg 07/14/16 20:47 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 105 60 - 120 07/14/16 20:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 79 - 120 07/14/16 20:47 1 Toluene-d8 (Surr) 106 79 - 123 07/14/16 20:47 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/14/16 20:47 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/14/16 20:47 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Benzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Bromoform ND 5.0 2.0 ug/Kg 07/14/16 20:47 1
Bromomethane ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Chloroethane ND 5.0 2.0 ug/Kg 07/14/16 20:47 1
Chloroform ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Chloromethane ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/14/16 20:47 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 Ethanol ND 300 100 ug/Kg 07/14/16 20:47 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-10' Lab Sample ID: 440-152462-2 Date Collected: 07/12/16 09:05 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/14/16 20:47 1
Methylene Chloride ND 20 5.0 ug/Kg 07/14/16 20:47 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 Naphthalene ND 5.0 2.0 ug/Kg 07/14/16 20:47 1
n-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
o-Xylene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Styrene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/14/16 20:47 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Toluene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/14/16 20:47 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/14/16 20:47 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/14/16 20:47 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/14/16 20:47 1
Toluene-d8 (Surr) 106 79 - 123 07/14/16 20:47 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 79 - 120 07/14/16 20:47 1 Dibromofluoromethane (Surr) 105 60 - 120 07/14/16 20:47 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Benzo[a]anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Benzo[a]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Benzo[b]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Benzo[g,h,i]perylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Benzo[k]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Chrysene 4.5 J 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Dibenz(a,h)anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Fluoranthene 12 J 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Fluorene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Indeno[1,2,3-cd]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Naphthalene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Phenanthrene 31 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 Pyrene 8.8 J 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 13:13 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-10' Lab Sample ID: 440-152462-2 Date Collected: 07/12/16 09:05 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 67 39 - 111 07/14/16 09:28 07/15/16 13:13 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 66 41 - 119 07/14/16 09:28 07/15/16 13:13 1 Terphenyl-d14 83 43 - 150 07/14/16 09:28 07/15/16 13:13 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 22 11 5.3 mg/Kg 07/13/16 18:24 07/14/16 14:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 45 11 5.3 mg/Kg 07/13/16 18:24 07/14/16 14:39 1 n-Octacosane 52 40 - 140 07/13/16 18:24 07/14/16 14:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 Aroclor 1232 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 Aroclor 1242 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 Aroclor 1248 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 Aroclor 1254 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 Aroclor 1260 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 14:41 1 DCB Decachlorobiphenyl (Surr) 77 45 - 120 07/13/16 18:43 07/15/16 14:41 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 6.2 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Barium 110 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Beryllium 0.58 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Chromium 24 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Cobalt 8.7 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Copper 23 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Lead 10 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Molybdenum 1.3 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Nickel 16 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Selenium 0.84 J 1.0 0.20 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Vanadium 45 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Zinc 67 10 5.0 mg/Kg 07/14/16 08:05 07/15/16 09:46 20
Antimony 0.30 J 1.0 0.27 mg/Kg 07/14/16 08:05 07/15/16 09:46 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.048 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 20:43 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-15' Lab Sample ID: 440-152462-3 Date Collected: 07/12/16 09:08 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 0.099 0.070 mg/Kg 07/14/16 21:15 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 111 60 - 120 07/14/16 21:15 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 79 - 120 07/14/16 21:15 1 Toluene-d8 (Surr) 104 79 - 123 07/14/16 21:15 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 1,1,2,2-Tetrachloroethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 1,1,2-Trichloroethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 1,1-Dichloroethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,1-Dichloroethene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
1,1-Dichloropropene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,2,3-Trichlorobenzene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 1,2,3-Trichloropropane ND 9.9 0.99 ug/Kg 07/14/16 21:15 1 1,2,4-Trichlorobenzene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 1,2,4-Trimethylbenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/14/16 21:15 1 1,2-Dibromoethane (EDB) ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 1,2-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,2-Dichloroethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,2-Dichloropropane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,3,5-Trimethylbenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 1,3-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,3-Dichloropropane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
1,4-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
2,2-Dichloropropane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
2-Chlorotoluene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
4-Chlorotoluene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Benzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Bromobenzene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Bromochloromethane ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Bromodichloromethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 Bromoform ND 5.0 2.0 ug/Kg 07/14/16 21:15 1
Bromomethane ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Carbon tetrachloride ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 Chlorobenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Chloroethane ND 5.0 2.0 ug/Kg 07/14/16 21:15 1
Chloroform ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Chloromethane ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
cis-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 cis-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 Dibromochloromethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 Dibromomethane ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/14/16 21:15 1 Isopropyl Ether (DIPE) ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 Ethanol ND 300 99 ug/Kg 07/14/16 21:15 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-15' Lab Sample ID: 440-152462-3 Date Collected: 07/12/16 09:08 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Hexachlorobutadiene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Isopropylbenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/14/16 21:15 1
Methylene Chloride ND 20 5.0 ug/Kg 07/14/16 21:15 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 Naphthalene ND 5.0 2.0 ug/Kg 07/14/16 21:15 1
n-Butylbenzene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
N-Propylbenzene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
o-Xylene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
sec-Butylbenzene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Styrene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Tert-amyl-methyl ether (TAME) ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 tert-Butyl alcohol (TBA) ND 99 9.9 ug/Kg 07/14/16 21:15 1 tert-Butylbenzene ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Tetrachloroethene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Toluene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
trans-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 trans-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1 Trichloroethene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Trichlorofluoromethane ND 5.0 0.99 ug/Kg 07/14/16 21:15 1 Vinyl chloride ND 5.0 0.99 ug/Kg 07/14/16 21:15 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/14/16 21:15 1
p-Isopropyltoluene ND 2.0 0.99 ug/Kg 07/14/16 21:15 1
Toluene-d8 (Surr) 104 79 - 123 07/14/16 21:15 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 79 - 120 07/14/16 21:15 1 Dibromofluoromethane (Surr) 111 60 - 120 07/14/16 21:15 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Anthracene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Benzo[a]anthracene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Benzo[a]pyrene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Benzo[b]fluoranthene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Benzo[g,h,i]perylene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Benzo[k]fluoranthene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Chrysene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Dibenz(a,h)anthracene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Fluoranthene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Fluorene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Indeno[1,2,3-cd]pyrene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Naphthalene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Phenanthrene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1 Pyrene ND 60 8.0 ug/Kg 07/14/16 09:28 07/15/16 13:34 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-15' Lab Sample ID: 440-152462-3 Date Collected: 07/12/16 09:08 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 64 39 - 111 07/14/16 09:28 07/15/16 13:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 64 41 - 119 07/14/16 09:28 07/15/16 13:34 1 Terphenyl-d14 66 43 - 150 07/14/16 09:28 07/15/16 13:34 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.1 mg/Kg 07/13/16 18:24 07/14/16 13:52 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 10 5.1 mg/Kg 07/13/16 18:24 07/14/16 13:52 1 n-Octacosane 51 40 - 140 07/13/16 18:24 07/14/16 13:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 Aroclor 1232 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 Aroclor 1242 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 Aroclor 1248 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 Aroclor 1254 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 Aroclor 1260 ND 220 76 ug/Kg 07/13/16 18:43 07/15/16 14:56 1 DCB Decachlorobiphenyl (Surr) 76 45 - 120 07/13/16 18:43 07/15/16 14:56 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 8.3 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Barium 76 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Beryllium 0.53 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Chromium 24 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Cobalt 7.8 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Copper 17 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Lead 8.8 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Molybdenum 3.0 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Nickel 16 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Selenium 0.78 J 1.0 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Vanadium 49 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Zinc 61 10 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:29 20
Antimony 0.30 J 1.0 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:29 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.049 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 20:51 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-20' Lab Sample ID: 440-152462-4 Date Collected: 07/12/16 09:12 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 0.10 0.070 mg/Kg 07/14/16 21:44 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 110 60 - 120 07/14/16 21:44 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 79 - 120 07/14/16 21:44 1 Toluene-d8 (Surr) 105 79 - 123 07/14/16 21:44 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/14/16 21:44 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/14/16 21:44 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Benzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Bromoform ND 5.0 2.0 ug/Kg 07/14/16 21:44 1
Bromomethane ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Chloroethane ND 5.0 2.0 ug/Kg 07/14/16 21:44 1
Chloroform ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Chloromethane ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/14/16 21:44 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 Ethanol ND 300 100 ug/Kg 07/14/16 21:44 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-20' Lab Sample ID: 440-152462-4 Date Collected: 07/12/16 09:12 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/14/16 21:44 1
Methylene Chloride ND 20 5.0 ug/Kg 07/14/16 21:44 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 Naphthalene ND 5.0 2.0 ug/Kg 07/14/16 21:44 1
n-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
o-Xylene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Styrene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/14/16 21:44 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Toluene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/14/16 21:44 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/14/16 21:44 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/14/16 21:44 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/14/16 21:44 1
Toluene-d8 (Surr) 105 79 - 123 07/14/16 21:44 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 79 - 120 07/14/16 21:44 1 Dibromofluoromethane (Surr) 110 60 - 120 07/14/16 21:44 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Benzo[a]anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Benzo[a]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Benzo[b]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Benzo[g,h,i]perylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Benzo[k]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Chrysene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Dibenz(a,h)anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Fluorene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Indeno[1,2,3-cd]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Naphthalene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Phenanthrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1 Pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 13:54 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-20' Lab Sample ID: 440-152462-4 Date Collected: 07/12/16 09:12 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 69 39 - 111 07/14/16 09:28 07/15/16 13:54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 68 41 - 119 07/14/16 09:28 07/15/16 13:54 1 Terphenyl-d14 84 43 - 150 07/14/16 09:28 07/15/16 13:54 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.1 mg/Kg 07/13/16 18:24 07/14/16 14:12 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 10 5.1 mg/Kg 07/13/16 18:24 07/14/16 14:12 1 n-Octacosane 51 40 - 140 07/13/16 18:24 07/14/16 14:12 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 Aroclor 1232 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 Aroclor 1242 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 Aroclor 1248 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 Aroclor 1254 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 Aroclor 1260 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:12 1 DCB Decachlorobiphenyl (Surr) 84 45 - 120 07/13/16 18:43 07/15/16 15:12 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 2.6 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Barium 110 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Beryllium 0.37 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Chromium 20 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Cobalt 7.6 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Copper 15 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Lead 3.7 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Molybdenum 0.79 J 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Nickel 15 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Selenium 0.52 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Vanadium 37 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Zinc 54 9.9 5.0 mg/Kg 07/14/16 08:05 07/15/16 09:51 20
Antimony 0.29 J 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 09:51 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.034 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 20:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-5' Lab Sample ID: 440-152462-5
Date Collected: 07/12/16 11:05 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 95 67 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 124 X 60 - 120 07/13/16 11:20 07/15/16 22:54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 149 * X 79 - 120 07/13/16 11:20 07/15/16 22:54 1 Toluene-d8 (Surr) 127 X 79 - 123 07/13/16 11:20 07/15/16 22:54 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,1,2,2-Tetrachloroethane ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,1,2-Trichloroethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,1-Dichloroethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,1-Dichloroethene ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,1-Dichloropropene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2,3-Trichlorobenzene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2,3-Trichloropropane ND * 9.5 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2,4-Trichlorobenzene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2,4-Trimethylbenzene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2-Dibromo-3-Chloropropane ND * 4.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2-Dibromoethane (EDB) ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2-Dichlorobenzene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2-Dichloroethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,2-Dichloropropane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,3,5-Trimethylbenzene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,3-Dichlorobenzene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,3-Dichloropropane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 1,4-Dichlorobenzene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 2,2-Dichloropropane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 2-Chlorotoluene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 4-Chlorotoluene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Benzene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Bromobenzene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Bromochloromethane ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Bromodichloromethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Bromoform ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Bromomethane ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Carbon tetrachloride ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Chlorobenzene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Chloroethane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Chloroform ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Chloromethane ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 cis-1,2-Dichloroethene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 cis-1,3-Dichloropropene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Dibromochloromethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Dibromomethane ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Dichlorodifluoromethane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Isopropyl Ether (DIPE) ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Ethanol ND 290 95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-5' Lab Sample ID: 440-152462-5
Date Collected: 07/12/16 11:05 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Hexachlorobutadiene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Isopropylbenzene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 m,p-Xylene ND 3.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Methylene Chloride ND 19 4.8 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Methyl-t-Butyl Ether (MTBE) ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Naphthalene ND * 4.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 n-Butylbenzene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 N-Propylbenzene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 o-Xylene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 sec-Butylbenzene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Styrene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Tert-amyl-methyl ether (TAME) ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 tert-Butyl alcohol (TBA) ND 95 9.5 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 tert-Butylbenzene ND * 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Tetrachloroethene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Toluene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 trans-1,2-Dichloroethene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 trans-1,3-Dichloropropene ND 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Trichloroethene 1.7 J 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Trichlorofluoromethane ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Vinyl chloride ND 4.8 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Xylenes, Total ND 3.8 1.9 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 p-Isopropyltoluene ND * 1.9 0.95 ug/Kg 07/13/16 11:20 07/15/16 22:54 1 Toluene-d8 (Surr) 127 X 79 - 123 07/13/16 11:20 07/15/16 22:54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 149 * X 79 - 120 07/13/16 11:20 07/15/16 22:54 1 Dibromofluoromethane (Surr) 124 X 60 - 120 07/13/16 11:20 07/15/16 22:54 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Anthracene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Benzo[a]anthracene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Benzo[a]pyrene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Benzo[b]fluoranthene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Benzo[g,h,i]perylene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Benzo[k]fluoranthene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Chrysene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Dibenz(a,h)anthracene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Fluoranthene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Fluorene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Indeno[1,2,3-cd]pyrene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Naphthalene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Phenanthrene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 Pyrene ND 2300 310 ug/Kg 07/14/16 09:28 07/15/16 14:15 40 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-5' Lab Sample ID: 440-152462-5
Date Collected: 07/12/16 11:05 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 60 39 - 111 07/14/16 09:28 07/15/16 14:15 40 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 75 41 - 119 07/14/16 09:28 07/15/16 14:15 40 Terphenyl-d14 88 43 - 150 07/14/16 09:28 07/15/16 14:15 40 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 89 J 100 52 mg/Kg 07/13/16 18:24 07/14/16 15:44 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 1700 100 52 mg/Kg 07/13/16 18:24 07/14/16 15:44 10 n-Octacosane 457 X 40 - 140 07/13/16 18:24 07/14/16 15:44 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 Aroclor 1232 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 Aroclor 1242 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 Aroclor 1248 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 Aroclor 1254 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 Aroclor 1260 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:28 1 DCB Decachlorobiphenyl (Surr) 59 45 - 120 07/13/16 18:43 07/15/16 15:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.49 0.099 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 12 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Barium 79 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Beryllium 0.20 J 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Cadmium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Chromium 14 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Cobalt 4.7 0.49 0.21 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Copper 12 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Lead 14 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Molybdenum 1.2 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Nickel 13 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Selenium 0.50 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Thallium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Vanadium 30 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Zinc 38 9.9 4.9 mg/Kg 07/14/16 08:05 07/15/16 09:59 20
Antimony ND 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 09:59 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.048 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 20:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-10' Lab Sample ID: 440-152462-6 Date Collected: 07/12/16 11:10 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 99 69 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 115 60 - 120 07/13/16 11:20 07/15/16 23:24 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 79 - 120 07/13/16 11:20 07/15/16 23:24 1 Toluene-d8 (Surr) 108 79 - 123 07/13/16 11:20 07/15/16 23:24 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,1,2,2-Tetrachloroethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,1,2-Trichloroethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,1-Dichloroethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,1-Dichloroethene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,1-Dichloropropene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2,3-Trichlorobenzene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2,3-Trichloropropane ND 9.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2,4-Trichlorobenzene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2,4-Trimethylbenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2-Dibromo-3-Chloropropane ND 4.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2-Dibromoethane (EDB) ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2-Dichloroethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,2-Dichloropropane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,3,5-Trimethylbenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,3-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,3-Dichloropropane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 1,4-Dichlorobenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 2,2-Dichloropropane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 2-Chlorotoluene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 4-Chlorotoluene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Benzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Bromobenzene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Bromochloromethane ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Bromodichloromethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Bromoform ND 4.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Bromomethane ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Carbon tetrachloride ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Chlorobenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Chloroethane ND 4.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Chloroform ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Chloromethane ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 cis-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 cis-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Dibromochloromethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Dibromomethane ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Dichlorodifluoromethane ND 4.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Isopropyl Ether (DIPE) ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Ethanol ND 300 99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-10' Lab Sample ID: 440-152462-6 Date Collected: 07/12/16 11:10 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Hexachlorobutadiene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Isopropylbenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 m,p-Xylene ND 3.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Methylene Chloride ND 20 4.9 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Methyl-t-Butyl Ether (MTBE) ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Naphthalene ND 4.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 n-Butylbenzene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 N-Propylbenzene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 o-Xylene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 sec-Butylbenzene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Styrene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Tert-amyl-methyl ether (TAME) ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 tert-Butyl alcohol (TBA) ND 99 9.9 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 tert-Butylbenzene ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Tetrachloroethene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Toluene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 trans-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 trans-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Trichloroethene 1.1 J 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Trichlorofluoromethane ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Vinyl chloride ND 4.9 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Xylenes, Total ND 3.9 2.0 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 p-Isopropyltoluene ND 2.0 0.99 ug/Kg 07/13/16 11:20 07/15/16 23:24 1 Toluene-d8 (Surr) 108 79 - 123 07/13/16 11:20 07/15/16 23:24 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 79 - 120 07/13/16 11:20 07/15/16 23:24 1 Dibromofluoromethane (Surr) 115 60 - 120 07/13/16 11:20 07/15/16 23:24 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Benzo[a]anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Benzo[a]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Benzo[b]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Benzo[g,h,i]perylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Benzo[k]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Chrysene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Dibenz(a,h)anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Fluorene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Indeno[1,2,3-cd]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Naphthalene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Phenanthrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1 Pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 14:36 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-10' Lab Sample ID: 440-152462-6 Date Collected: 07/12/16 11:10 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 67 39 - 111 07/14/16 09:28 07/15/16 14:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 66 41 - 119 07/14/16 09:28 07/15/16 14:36 1 Terphenyl-d14 83 43 - 150 07/14/16 09:28 07/15/16 14:36 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.1 mg/Kg 07/13/16 18:24 07/14/16 15:01 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 8.6 J 10 5.1 mg/Kg 07/13/16 18:24 07/14/16 15:01 1 n-Octacosane 36 X 40 - 140 07/13/16 18:24 07/14/16 15:01 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 Aroclor 1232 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 Aroclor 1242 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 Aroclor 1248 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 Aroclor 1254 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 Aroclor 1260 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 15:43 1 DCB Decachlorobiphenyl (Surr) 68 45 - 120 07/13/16 18:43 07/15/16 15:43 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 3.7 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Barium 100 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Beryllium 0.47 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Chromium 22 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Cobalt 8.2 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Copper 18 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Lead 6.1 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Molybdenum 0.66 J 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Nickel 15 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Selenium 0.68 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Vanadium 42 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Zinc 59 9.9 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:01 20
Antimony ND 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:01 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.013 J 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 20:59 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-15' Lab Sample ID: 440-152462-7 Date Collected: 07/12/16 11:14 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 89 63 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 115 60 - 120 07/13/16 11:20 07/15/16 23:54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 108 79 - 120 07/13/16 11:20 07/15/16 23:54 1 Toluene-d8 (Surr) 109 79 - 123 07/13/16 11:20 07/15/16 23:54 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,1,2,2-Tetrachloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,1,2-Trichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,1-Dichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,1-Dichloroethene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,1-Dichloropropene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2,3-Trichlorobenzene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2,3-Trichloropropane ND 8.9 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2,4-Trichlorobenzene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2,4-Trimethylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2-Dibromo-3-Chloropropane ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2-Dibromoethane (EDB) ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2-Dichlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2-Dichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,2-Dichloropropane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,3,5-Trimethylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,3-Dichlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,3-Dichloropropane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 1,4-Dichlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 2,2-Dichloropropane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 2-Chlorotoluene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 4-Chlorotoluene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Benzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Bromobenzene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Bromochloromethane ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Bromodichloromethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Bromoform ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Bromomethane ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Carbon tetrachloride ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Chlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Chloroethane ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Chloroform ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Chloromethane ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 cis-1,2-Dichloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 cis-1,3-Dichloropropene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Dibromochloromethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Dibromomethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Dichlorodifluoromethane ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Isopropyl Ether (DIPE) ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Ethanol ND 270 89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-15' Lab Sample ID: 440-152462-7 Date Collected: 07/12/16 11:14 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Hexachlorobutadiene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Isopropylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 m,p-Xylene ND 3.6 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Methylene Chloride ND 18 4.5 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Methyl-t-Butyl Ether (MTBE) ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Naphthalene ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 n-Butylbenzene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 N-Propylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 o-Xylene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 sec-Butylbenzene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Styrene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Tert-amyl-methyl ether (TAME) ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 tert-Butyl alcohol (TBA) ND 89 8.9 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 tert-Butylbenzene ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Tetrachloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Toluene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 trans-1,2-Dichloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 trans-1,3-Dichloropropene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Trichloroethene 0.89 J 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Trichlorofluoromethane ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Vinyl chloride ND 4.5 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Xylenes, Total ND 3.6 1.8 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 p-Isopropyltoluene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/15/16 23:54 1 Toluene-d8 (Surr) 109 79 - 123 07/13/16 11:20 07/15/16 23:54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 108 79 - 120 07/13/16 11:20 07/15/16 23:54 1 Dibromofluoromethane (Surr) 115 60 - 120 07/13/16 11:20 07/15/16 23:54 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Anthracene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Benzo[a]anthracene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Benzo[a]pyrene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Benzo[b]fluoranthene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Benzo[g,h,i]perylene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Benzo[k]fluoranthene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Chrysene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Dibenz(a,h)anthracene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Fluoranthene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Fluorene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Indeno[1,2,3-cd]pyrene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Naphthalene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Phenanthrene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1 Pyrene ND 63 8.4 ug/Kg 07/14/16 09:28 07/15/16 14:56 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-15' Lab Sample ID: 440-152462-7 Date Collected: 07/12/16 11:14 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 67 39 - 111 07/14/16 09:28 07/15/16 14:56 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 66 41 - 119 07/14/16 09:28 07/15/16 14:56 1 Terphenyl-d14 74 43 - 150 07/14/16 09:28 07/15/16 14:56 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 11 5.4 mg/Kg 07/13/16 18:24 07/14/16 14:31 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 11 5.4 mg/Kg 07/13/16 18:24 07/14/16 14:31 1 n-Octacosane 59 40 - 140 07/13/16 18:24 07/14/16 14:31 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 Aroclor 1232 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 Aroclor 1242 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 Aroclor 1248 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 Aroclor 1254 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 Aroclor 1260 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 15:58 1 DCB Decachlorobiphenyl (Surr) 44 X 45 - 120 07/13/16 18:43 07/15/16 15:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 23 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Barium 110 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Beryllium 0.51 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Chromium 25 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Cobalt 9.1 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Copper 25 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Lead 11 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Molybdenum 3.7 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Nickel 17 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Selenium 0.84 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Vanadium 63 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Zinc 62 9.9 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:04 20
Antimony 0.54 J 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:04 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.018 J 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 21:02 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-20' Lab Sample ID: 440-152462-8 Date Collected: 07/12/16 11:21 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 91 64 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 113 60 - 120 07/13/16 11:20 07/16/16 00:24 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 113 * 79 - 120 07/13/16 11:20 07/16/16 00:24 1 Toluene-d8 (Surr) 114 79 - 123 07/13/16 11:20 07/16/16 00:24 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,1,2,2-Tetrachloroethane ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,1,2-Trichloroethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,1-Dichloroethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,1-Dichloroethene ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,1-Dichloropropene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2,3-Trichlorobenzene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2,3-Trichloropropane ND * 9.1 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2,4-Trichlorobenzene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2,4-Trimethylbenzene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2-Dibromo-3-Chloropropane ND * 4.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2-Dibromoethane (EDB) ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2-Dichlorobenzene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2-Dichloroethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,2-Dichloropropane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,3,5-Trimethylbenzene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,3-Dichlorobenzene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,3-Dichloropropane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 1,4-Dichlorobenzene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 2,2-Dichloropropane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 2-Chlorotoluene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 4-Chlorotoluene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Benzene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Bromobenzene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Bromochloromethane ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Bromodichloromethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Bromoform ND 4.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Bromomethane ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Carbon tetrachloride ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Chlorobenzene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Chloroethane ND 4.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Chloroform ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Chloromethane ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 cis-1,2-Dichloroethene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 cis-1,3-Dichloropropene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Dibromochloromethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Dibromomethane ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Dichlorodifluoromethane ND 4.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Isopropyl Ether (DIPE) ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Ethanol ND 270 91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-20' Lab Sample ID: 440-152462-8 Date Collected: 07/12/16 11:21 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Hexachlorobutadiene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Isopropylbenzene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 m,p-Xylene ND 3.7 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Methylene Chloride ND 18 4.6 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Methyl-t-Butyl Ether (MTBE) ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Naphthalene ND * 4.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 n-Butylbenzene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 N-Propylbenzene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 o-Xylene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 sec-Butylbenzene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Styrene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Tert-amyl-methyl ether (TAME) ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 tert-Butyl alcohol (TBA) ND 91 9.1 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 tert-Butylbenzene ND * 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Tetrachloroethene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Toluene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 trans-1,2-Dichloroethene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 trans-1,3-Dichloropropene ND 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Trichloroethene 2.4 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Trichlorofluoromethane ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Vinyl chloride ND 4.6 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Xylenes, Total ND 3.7 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 p-Isopropyltoluene ND * 1.8 0.91 ug/Kg 07/13/16 11:20 07/16/16 00:24 1 Toluene-d8 (Surr) 114 79 - 123 07/13/16 11:20 07/16/16 00:24 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 113 * 79 - 120 07/13/16 11:20 07/16/16 00:24 1 Dibromofluoromethane (Surr) 113 60 - 120 07/13/16 11:20 07/16/16 00:24 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Benzo[a]anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Benzo[a]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Benzo[b]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Benzo[g,h,i]perylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Benzo[k]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Chrysene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Dibenz(a,h)anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Fluorene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Indeno[1,2,3-cd]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Naphthalene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Phenanthrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1 Pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:17 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-20' Lab Sample ID: 440-152462-8 Date Collected: 07/12/16 11:21 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 68 39 - 111 07/14/16 09:28 07/15/16 15:17 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 65 41 - 119 07/14/16 09:28 07/15/16 15:17 1 Terphenyl-d14 81 43 - 150 07/14/16 09:28 07/15/16 15:17 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 11 5.3 mg/Kg 07/13/16 18:24 07/14/16 15:30 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 11 5.3 mg/Kg 07/13/16 18:24 07/14/16 15:30 1 n-Octacosane 89 40 - 140 07/13/16 18:24 07/14/16 15:30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 Aroclor 1232 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 Aroclor 1242 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 Aroclor 1248 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 Aroclor 1254 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 Aroclor 1260 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:13 1 DCB Decachlorobiphenyl (Surr) 69 45 - 120 07/13/16 18:43 07/15/16 16:13 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 2.0 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Barium 120 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Beryllium 0.50 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Chromium 26 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Cobalt 8.6 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Copper 17 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Lead 5.4 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Molybdenum 0.61 J 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Nickel 17 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Selenium 0.72 J 1.0 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Vanadium 48 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Zinc 68 10 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:06 20
Antimony ND 1.0 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:06 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury ND 0.020 0.012 mg/Kg 07/14/16 01:08 07/14/16 21:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-5' Lab Sample ID: 440-152462-9
Date Collected: 07/12/16 13:15 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 89 62 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 116 60 - 120 07/13/16 11:20 07/16/16 00:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 109 79 - 120 07/13/16 11:20 07/16/16 00:53 1 Toluene-d8 (Surr) 110 79 - 123 07/13/16 11:20 07/16/16 00:53 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,1,2,2-Tetrachloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,1,2-Trichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,1-Dichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,1-Dichloroethene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,1-Dichloropropene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2,3-Trichlorobenzene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2,3-Trichloropropane ND 8.9 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2,4-Trichlorobenzene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2,4-Trimethylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2-Dibromo-3-Chloropropane ND 4.4 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2-Dibromoethane (EDB) ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2-Dichlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2-Dichloroethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,2-Dichloropropane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,3,5-Trimethylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,3-Dichlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,3-Dichloropropane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 1,4-Dichlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 2,2-Dichloropropane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 2-Chlorotoluene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 4-Chlorotoluene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Benzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Bromobenzene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Bromochloromethane ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Bromodichloromethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Bromoform ND 4.4 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Bromomethane ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Carbon tetrachloride ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Chlorobenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Chloroethane ND 4.4 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Chloroform ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Chloromethane ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 cis-1,2-Dichloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 cis-1,3-Dichloropropene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Dibromochloromethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Dibromomethane ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Dichlorodifluoromethane ND 4.4 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Isopropyl Ether (DIPE) ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Ethanol ND 270 89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-5' Lab Sample ID: 440-152462-9
Date Collected: 07/12/16 13:15 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Hexachlorobutadiene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Isopropylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 m,p-Xylene ND 3.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Methylene Chloride ND 18 4.4 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Methyl-t-Butyl Ether (MTBE) ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Naphthalene ND 4.4 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 n-Butylbenzene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 N-Propylbenzene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 o-Xylene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 sec-Butylbenzene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Styrene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Tert-amyl-methyl ether (TAME) ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 tert-Butyl alcohol (TBA) ND 89 8.9 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 tert-Butylbenzene ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Tetrachloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Toluene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 trans-1,2-Dichloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 trans-1,3-Dichloropropene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Trichloroethene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Trichlorofluoromethane ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Vinyl chloride ND 4.4 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Xylenes, Total ND 3.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 p-Isopropyltoluene ND 1.8 0.89 ug/Kg 07/13/16 11:20 07/16/16 00:53 1 Toluene-d8 (Surr) 110 79 - 123 07/13/16 11:20 07/16/16 00:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 109 79 - 120 07/13/16 11:20 07/16/16 00:53 1 Dibromofluoromethane (Surr) 116 60 - 120 07/13/16 11:20 07/16/16 00:53 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Benzo[a]anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Benzo[a]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Benzo[b]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Benzo[g,h,i]perylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Benzo[k]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Chrysene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Dibenz(a,h)anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Fluorene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Indeno[1,2,3-cd]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Naphthalene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Phenanthrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1 Pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 15:37 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-5' Lab Sample ID: 440-152462-9
Date Collected: 07/12/16 13:15 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 74 39 - 111 07/14/16 09:28 07/15/16 15:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 72 41 - 119 07/14/16 09:28 07/15/16 15:37 1 Terphenyl-d14 87 43 - 150 07/14/16 09:28 07/15/16 15:37 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.0 mg/Kg 07/13/16 18:24 07/14/16 15:49 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 10 5.0 mg/Kg 07/13/16 18:24 07/14/16 15:49 1 n-Octacosane 73 40 - 140 07/13/16 18:24 07/14/16 15:49 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 Aroclor 1232 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 Aroclor 1242 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 Aroclor 1248 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 Aroclor 1254 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 Aroclor 1260 ND 100 34 ug/Kg 07/13/16 18:43 07/15/16 16:29 1 DCB Decachlorobiphenyl (Surr) 66 45 - 120 07/13/16 18:43 07/15/16 16:29 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 3.1 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Barium 47 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Beryllium 0.42 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Chromium 18 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Cobalt 7.0 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Copper 12 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Lead 3.9 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Molybdenum 0.53 J 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Nickel 12 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Selenium 0.46 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Vanadium 36 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Zinc 49 9.9 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:09 20
Antimony ND 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:09 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury ND 0.020 0.012 mg/Kg 07/14/16 01:08 07/14/16 21:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-10' Lab Sample ID: 440-152462-10 Date Collected: 07/12/16 13:19 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 90 63 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 115 60 - 120 07/13/16 11:20 07/16/16 01:23 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 109 79 - 120 07/13/16 11:20 07/16/16 01:23 1 Toluene-d8 (Surr) 112 79 - 123 07/13/16 11:20 07/16/16 01:23 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,1,2,2-Tetrachloroethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,1,2-Trichloroethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,1-Dichloroethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,1-Dichloroethene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,1-Dichloropropene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2,3-Trichlorobenzene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2,3-Trichloropropane ND 9.0 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2,4-Trichlorobenzene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2,4-Trimethylbenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2-Dibromo-3-Chloropropane ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2-Dibromoethane (EDB) ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2-Dichlorobenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2-Dichloroethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,2-Dichloropropane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,3,5-Trimethylbenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,3-Dichlorobenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,3-Dichloropropane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 1,4-Dichlorobenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 2,2-Dichloropropane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 2-Chlorotoluene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 4-Chlorotoluene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Benzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Bromobenzene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Bromochloromethane ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Bromodichloromethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Bromoform ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Bromomethane ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Carbon tetrachloride ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Chlorobenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Chloroethane ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Chloroform ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Chloromethane ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 cis-1,2-Dichloroethene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 cis-1,3-Dichloropropene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Dibromochloromethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Dibromomethane ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Dichlorodifluoromethane ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Isopropyl Ether (DIPE) ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Ethanol ND 270 90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-10' Lab Sample ID: 440-152462-10 Date Collected: 07/12/16 13:19 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Hexachlorobutadiene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Isopropylbenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 m,p-Xylene ND 3.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Methylene Chloride ND 18 4.5 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Methyl-t-Butyl Ether (MTBE) ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Naphthalene ND 4.5 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 n-Butylbenzene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 N-Propylbenzene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 o-Xylene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 sec-Butylbenzene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Styrene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Tert-amyl-methyl ether (TAME) ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 tert-Butyl alcohol (TBA) ND 90 9.0 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 tert-Butylbenzene ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Tetrachloroethene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Toluene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 trans-1,2-Dichloroethene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 trans-1,3-Dichloropropene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Trichloroethene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Trichlorofluoromethane ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Vinyl chloride ND 4.5 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Xylenes, Total ND 3.6 1.8 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 p-Isopropyltoluene ND 1.8 0.90 ug/Kg 07/13/16 11:20 07/16/16 01:23 1 Toluene-d8 (Surr) 112 79 - 123 07/13/16 11:20 07/16/16 01:23 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 109 79 - 120 07/13/16 11:20 07/16/16 01:23 1 Dibromofluoromethane (Surr) 115 60 - 120 07/13/16 11:20 07/16/16 01:23 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Benzo[a]anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Benzo[a]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Benzo[b]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Benzo[g,h,i]perylene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Benzo[k]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Chrysene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Dibenz(a,h)anthracene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Fluorene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Indeno[1,2,3-cd]pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Naphthalene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Phenanthrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1 Pyrene ND 29 3.9 ug/Kg 07/14/16 09:28 07/15/16 15:58 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-10' Lab Sample ID: 440-152462-10 Date Collected: 07/12/16 13:19 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 62 39 - 111 07/14/16 09:28 07/15/16 15:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 61 41 - 119 07/14/16 09:28 07/15/16 15:58 1 Terphenyl-d14 75 43 - 150 07/14/16 09:28 07/15/16 15:58 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.2 mg/Kg 07/13/16 18:24 07/14/16 15:10 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 10 5.2 mg/Kg 07/13/16 18:24 07/14/16 15:10 1 n-Octacosane 76 40 - 140 07/13/16 18:24 07/14/16 15:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 Aroclor 1232 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 Aroclor 1242 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 Aroclor 1248 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 Aroclor 1254 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 Aroclor 1260 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:44 1 DCB Decachlorobiphenyl (Surr) 70 45 - 120 07/13/16 18:43 07/15/16 16:44 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.49 0.099 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 6.0 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Barium 110 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Beryllium 0.31 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Cadmium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Chromium 21 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Cobalt 6.5 0.49 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Copper 18 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Lead 5.4 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Molybdenum 1.8 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Nickel 12 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Selenium 0.40 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Thallium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Vanadium 42 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Zinc 50 9.9 4.9 mg/Kg 07/14/16 08:05 07/15/16 10:11 20
Antimony 0.29 J 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:11 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.027 0.020 0.012 mg/Kg 07/14/16 01:08 07/14/16 21:42 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-15' Lab Sample ID: 440-152462-11 Date Collected: 07/12/16 13:25 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 97 68 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 117 60 - 120 07/13/16 11:20 07/16/16 01:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 106 79 - 120 07/13/16 11:20 07/16/16 01:52 1 Toluene-d8 (Surr) 110 79 - 123 07/13/16 11:20 07/16/16 01:52 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,1,2,2-Tetrachloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,1,2-Trichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,1-Dichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,1-Dichloroethene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,1-Dichloropropene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2,3-Trichlorobenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2,3-Trichloropropane ND 9.7 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2,4-Trichlorobenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2,4-Trimethylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2-Dibromo-3-Chloropropane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2-Dibromoethane (EDB) ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2-Dichlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2-Dichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,2-Dichloropropane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,3,5-Trimethylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,3-Dichlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,3-Dichloropropane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 1,4-Dichlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 2,2-Dichloropropane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 2-Chlorotoluene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 4-Chlorotoluene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Benzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Bromobenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Bromochloromethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Bromodichloromethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Bromoform ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Bromomethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Carbon tetrachloride ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Chlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Chloroethane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Chloroform ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Chloromethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 cis-1,2-Dichloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 cis-1,3-Dichloropropene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Dibromochloromethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Dibromomethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Dichlorodifluoromethane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Isopropyl Ether (DIPE) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Ethanol ND 290 97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-15' Lab Sample ID: 440-152462-11 Date Collected: 07/12/16 13:25 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Hexachlorobutadiene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Isopropylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 m,p-Xylene ND 3.9 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Methylene Chloride ND 19 4.8 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Methyl-t-Butyl Ether (MTBE) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Naphthalene ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 n-Butylbenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 N-Propylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 o-Xylene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 sec-Butylbenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Styrene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Tert-amyl-methyl ether (TAME) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 tert-Butyl alcohol (TBA) ND 97 9.7 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 tert-Butylbenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Tetrachloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Toluene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 trans-1,2-Dichloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 trans-1,3-Dichloropropene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Trichloroethene 2.1 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Trichlorofluoromethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Vinyl chloride ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Xylenes, Total ND 3.9 1.9 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 p-Isopropyltoluene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 01:52 1 Toluene-d8 (Surr) 110 79 - 123 07/13/16 11:20 07/16/16 01:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 106 79 - 120 07/13/16 11:20 07/16/16 01:52 1 Dibromofluoromethane (Surr) 117 60 - 120 07/13/16 11:20 07/16/16 01:52 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Anthracene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Benzo[a]anthracene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Benzo[a]pyrene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Benzo[b]fluoranthene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Benzo[g,h,i]perylene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Benzo[k]fluoranthene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Chrysene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Dibenz(a,h)anthracene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Fluoranthene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Fluorene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Indeno[1,2,3-cd]pyrene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Naphthalene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Phenanthrene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1 Pyrene ND 64 8.5 ug/Kg 07/14/16 09:28 07/15/16 16:19 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-15' Lab Sample ID: 440-152462-11 Date Collected: 07/12/16 13:25 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 67 39 - 111 07/14/16 09:28 07/15/16 16:19 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 67 41 - 119 07/14/16 09:28 07/15/16 16:19 1 Terphenyl-d14 74 43 - 150 07/14/16 09:28 07/15/16 16:19 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 25 13 mg/Kg 07/19/16 08:02 07/19/16 22:51 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 13 J 25 13 mg/Kg 07/19/16 08:02 07/19/16 22:51 1 n-Octacosane 45 40 - 140 07/19/16 08:02 07/19/16 22:51 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 Aroclor 1232 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 Aroclor 1242 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 Aroclor 1248 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 Aroclor 1254 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 Aroclor 1260 ND 100 35 ug/Kg 07/13/16 18:43 07/15/16 16:59 1 DCB Decachlorobiphenyl (Surr) 86 45 - 120 07/13/16 18:43 07/15/16 16:59 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 3.1 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Barium 55 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Beryllium 0.72 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Chromium 29 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Cobalt 8.9 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Copper 19 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Lead 5.7 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Molybdenum 0.96 J 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Nickel 17 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Selenium 0.59 J 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Vanadium 45 0.99 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Zinc 72 9.9 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:14 20
Antimony ND 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:14 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.065 0.020 0.012 mg/Kg 07/14/16 01:08 07/14/16 21:44 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-20' Lab Sample ID: 440-152462-12 Date Collected: 07/12/16 13:30 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 97 68 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 98 60 - 120 07/13/16 11:20 07/16/16 12:46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 79 - 120 07/13/16 11:20 07/16/16 12:46 1 Toluene-d8 (Surr) 109 79 - 123 07/13/16 11:20 07/16/16 12:46 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,1,2,2-Tetrachloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,1,2-Trichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,1-Dichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,1-Dichloroethene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,1-Dichloropropene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2,3-Trichlorobenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2,3-Trichloropropane ND 9.7 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2,4-Trichlorobenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2,4-Trimethylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2-Dibromo-3-Chloropropane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2-Dibromoethane (EDB) ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2-Dichlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2-Dichloroethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,2-Dichloropropane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,3,5-Trimethylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,3-Dichlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,3-Dichloropropane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 1,4-Dichlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 2,2-Dichloropropane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 2-Chlorotoluene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 4-Chlorotoluene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Benzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Bromobenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Bromochloromethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Bromodichloromethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Bromoform ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Bromomethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Carbon tetrachloride ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Chlorobenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Chloroethane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Chloroform ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Chloromethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 cis-1,2-Dichloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 cis-1,3-Dichloropropene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Dibromochloromethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Dibromomethane ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Dichlorodifluoromethane ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Isopropyl Ether (DIPE) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Ethanol ND 290 97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-20' Lab Sample ID: 440-152462-12 Date Collected: 07/12/16 13:30 Matrix: Solid
Date Received: 07/12/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Hexachlorobutadiene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Isopropylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 m,p-Xylene ND 3.9 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Methylene Chloride ND 19 4.8 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Methyl-t-Butyl Ether (MTBE) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Naphthalene ND 4.8 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 n-Butylbenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 N-Propylbenzene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 o-Xylene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 sec-Butylbenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Styrene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Tert-amyl-methyl ether (TAME) ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 tert-Butyl alcohol (TBA) ND 97 9.7 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 tert-Butylbenzene ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Tetrachloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Toluene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 trans-1,2-Dichloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 trans-1,3-Dichloropropene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Trichloroethene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Trichlorofluoromethane ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Vinyl chloride ND 4.8 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Xylenes, Total ND 3.9 1.9 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 p-Isopropyltoluene ND 1.9 0.97 ug/Kg 07/13/16 11:20 07/16/16 12:46 1 Toluene-d8 (Surr) 109 79 - 123 07/13/16 11:20 07/16/16 12:46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 79 - 120 07/13/16 11:20 07/16/16 12:46 1 Dibromofluoromethane (Surr) 98 60 - 120 07/13/16 11:20 07/16/16 12:46 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Anthracene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Benzo[a]anthracene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Benzo[a]pyrene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Benzo[b]fluoranthene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Benzo[g,h,i]perylene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Benzo[k]fluoranthene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Chrysene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Dibenz(a,h)anthracene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Fluoranthene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Fluorene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Indeno[1,2,3-cd]pyrene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Naphthalene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Phenanthrene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1 Pyrene ND 59 7.9 ug/Kg 07/14/16 09:28 07/15/16 16:39 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-20' Lab Sample ID: 440-152462-12 Date Collected: 07/12/16 13:30 Matrix: Solid
Date Received: 07/12/16 18:30
2-Fluorobiphenyl (Surr) 61 39 - 111 07/14/16 09:28 07/15/16 16:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 60 41 - 119 07/14/16 09:28 07/15/16 16:39 1 Terphenyl-d14 71 43 - 150 07/14/16 09:28 07/15/16 16:39 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 10 5.2 mg/Kg 07/13/16 18:24 07/14/16 17:47 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 10 5.2 mg/Kg 07/13/16 18:24 07/14/16 17:47 1 n-Octacosane 51 40 - 140 07/13/16 18:24 07/14/16 17:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 Aroclor 1232 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 Aroclor 1242 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 Aroclor 1248 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 Aroclor 1254 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 Aroclor 1260 ND 110 36 ug/Kg 07/13/16 18:43 07/15/16 17:14 1 DCB Decachlorobiphenyl (Surr) 53 45 - 120 07/13/16 18:43 07/15/16 17:14 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 8.4 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Barium 100 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Beryllium 0.45 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Chromium 24 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Cobalt 11 0.50 0.21 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Copper 21 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Lead 7.7 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Molybdenum 2.6 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Nickel 18 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Selenium 0.67 J 1.0 0.20 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Vanadium 46 1.0 0.50 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Zinc 63 10 5.0 mg/Kg 07/14/16 08:05 07/15/16 10:16 20
Antimony ND 1.0 0.27 mg/Kg 07/14/16 08:05 07/15/16 10:16 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.016 J 0.020 0.012 mg/Kg 07/14/16 01:08 07/14/16 21:47 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL IRV
8260B/CA_LUFTM SW846
S
Volatile Organic Compounds by GC/MS TAL IRV
8270C SIM Semivolatile Organic Compounds (GC/MS SIM) SW846 TAL IRV 8015B Diesel Range Organics (DRO) (GC) SW846 TAL IRV
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL IRV 6020 Metals (ICP/MS) SW846 TAL IRV
7471A Mercury (CVAA) SW846 TAL IRV
Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-5' Lab Sample ID: 440-152462-1
Date Collected: 07/12/16 09:00 Matrix: Solid
Date Received: 07/12/16 18:30
Analysis 8260B 1 342265 07/14/16 16:53 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.05 g 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 5.05 g 10 mL 342266 07/14/16 16:53 ATL TAL IRV Total/NA Prep 3546 15.40 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 12:11 AI TAL IRV Total/NA Prep 3546 7.23 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 11:54 AMH TAL IRV Total/NA Prep 3546 7.13 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 14:26 JM TAL IRV Total/NA Prep 3050B 2.02 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 09:34 EN TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342230 07/13/16 23:32 DB TAL IRV Total/NA Analysis 7471A 1 342524 07/14/16 20:40 DB TAL IRV Client Sample ID: AEC-5-10' Lab Sample ID: 440-152462-2 Date Collected: 07/12/16 09:05 Matrix: Solid
Date Received: 07/12/16 18:30
Analysis 8260B 1 342463 07/14/16 20:47 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.02 g 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 5.02 g 10 mL 342464 07/14/16 20:47 WK TAL IRV Total/NA Prep 3546 15.08 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 13:13 AI TAL IRV Total/NA Prep 3546 7.11 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342361 07/14/16 14:39 AMH TAL IRV Total/NA Prep 3546 7.04 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 14:41 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 09:46 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342230 07/13/16 23:32 DB TAL IRV Total/NA Analysis 7471A 1 342524 07/14/16 20:43 DB TAL IRV Client Sample ID: AEC-5-15' Lab Sample ID: 440-152462-3 Date Collected: 07/12/16 09:08 Matrix: Solid
Date Received: 07/12/16 18:30
Analysis 8260B 1 342463 07/14/16 21:15 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.03 g 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 5.03 g 10 mL 342464 07/14/16 21:15 WK TAL IRV Total/NA Prep 3546 7.47 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 13:34 AI TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-15' Lab Sample ID: 440-152462-3 Date Collected: 07/12/16 09:08 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 3546 342178 07/13/16 18:24 VA TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 7.31 g 1 mL
Total/NA Analysis 8015B 1 342359 07/14/16 13:52 AMH TAL IRV Total/NA Prep 3546 3.37 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 14:56 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:29 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342230 07/13/16 23:32 DB TAL IRV Total/NA Analysis 7471A 1 342524 07/14/16 20:51 DB TAL IRV Client Sample ID: AEC-5-20' Lab Sample ID: 440-152462-4 Date Collected: 07/12/16 09:12 Matrix: Solid
Date Received: 07/12/16 18:30
Analysis 8260B 1 342463 07/14/16 21:44 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.01 g 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 5.01 g 10 mL 342464 07/14/16 21:44 WK TAL IRV Total/NA Prep 3546 15.34 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 13:54 AI TAL IRV Total/NA Prep 3546 7.29 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 14:12 AMH TAL IRV Total/NA Prep 3546 7.24 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 15:12 JM TAL IRV Total/NA Prep 3050B 2.02 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 09:51 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342230 07/13/16 23:32 DB TAL IRV Total/NA Analysis 7471A 1 342524 07/14/16 20:53 DB TAL IRV Client Sample ID: AEC-3-5' Lab Sample ID: 440-152462-5
Date Collected: 07/12/16 11:05 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.26 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/15/16 22:54 AA TAL IRV Total/NA Prep 5035 5.26 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/15/16 22:54 AA TAL IRV Total/NA Prep 3546 15.40 g 2 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 40 342622 07/15/16 14:15 AI TAL IRV Total/NA Prep 3546 7.17 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 10 342361 07/14/16 15:44 AMH TAL IRV Total/NA Prep 3546 7.28 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 15:28 JM TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-5' Lab Sample ID: 440-152462-5
Date Collected: 07/12/16 11:05 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 3050B 342294 07/14/16 08:05 DT TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 2.03 g 50 mL
Total/NA Analysis 6020 20 342656 07/15/16 09:59 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342230 07/13/16 23:32 DB TAL IRV Total/NA Analysis 7471A 1 342524 07/14/16 20:56 DB TAL IRV Client Sample ID: AEC-3-10' Lab Sample ID: 440-152462-6 Date Collected: 07/12/16 11:10 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.07 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/15/16 23:24 AA TAL IRV Total/NA Prep 5035 5.07 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/15/16 23:24 AA TAL IRV Total/NA Prep 3546 15.10 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 14:36 AI TAL IRV Total/NA Prep 3546 7.29 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342361 07/14/16 15:01 AMH TAL IRV Total/NA Prep 3546 7.36 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 15:43 JM TAL IRV Total/NA Prep 3050B 2.02 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:01 EN TAL IRV Total/NA Prep 7471A 0.49 g 50 mL 342230 07/13/16 23:32 DB TAL IRV Total/NA Analysis 7471A 1 342524 07/14/16 20:59 DB TAL IRV Client Sample ID: AEC-3-15' Lab Sample ID: 440-152462-7 Date Collected: 07/12/16 11:14 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.59 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/15/16 23:54 AA TAL IRV Total/NA Prep 5035 5.59 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/15/16 23:54 AA TAL IRV Total/NA Prep 3546 7.12 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 14:56 AI TAL IRV Total/NA Prep 3546 7.00 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 14:31 AMH TAL IRV Total/NA Prep 3546 7.02 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 15:58 JM TAL IRV Total/NA Prep 3050B 2.02 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:04 EN TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-15' Lab Sample ID: 440-152462-7 Date Collected: 07/12/16 11:14 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 7471A 342230 07/13/16 23:32 DB TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 0.50 g 50 mL
Total/NA Analysis 7471A 1 342524 07/14/16 21:02 DB TAL IRV Client Sample ID: AEC-3-20' Lab Sample ID: 440-152462-8 Date Collected: 07/12/16 11:21 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.47 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/16/16 00:24 AA TAL IRV Total/NA Prep 5035 5.47 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/16/16 00:24 AA TAL IRV Total/NA Prep 3546 15.37 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 15:17 AI TAL IRV Total/NA Prep 3546 7.02 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 15:30 AMH TAL IRV Total/NA Prep 3546 7.48 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 16:13 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:06 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342231 07/14/16 01:08 DB TAL IRV Total/NA Analysis 7471A 1 342525 07/14/16 21:36 DB TAL IRV Client Sample ID: AEC-4-5' Lab Sample ID: 440-152462-9
Date Collected: 07/12/16 13:15 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.64 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/16/16 00:53 AA TAL IRV Total/NA Prep 5035 5.64 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/16/16 00:53 AA TAL IRV Total/NA Prep 3546 15.04 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 15:37 AI TAL IRV Total/NA Prep 3546 7.43 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 15:49 AMH TAL IRV Total/NA Prep 3546 7.45 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 16:29 JM TAL IRV Total/NA Prep 3050B 2.02 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:09 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342231 07/14/16 01:08 DB TAL IRV Total/NA Analysis 7471A 1 342525 07/14/16 21:39 DB TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-10' Lab Sample ID: 440-152462-10 Date Collected: 07/12/16 13:19 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.53 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/16/16 01:23 AA TAL IRV Total/NA Prep 5035 5.53 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/16/16 01:23 AA TAL IRV Total/NA Prep 3546 15.38 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 15:58 AI TAL IRV Total/NA Prep 3546 7.16 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 15:10 AMH TAL IRV Total/NA Prep 3546 7.22 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 16:44 JM TAL IRV Total/NA Prep 3050B 2.03 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:11 EN TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342231 07/14/16 01:08 DB TAL IRV Total/NA Analysis 7471A 1 342525 07/14/16 21:42 DB TAL IRV Client Sample ID: AEC-4-15' Lab Sample ID: 440-152462-11 Date Collected: 07/12/16 13:25 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.16 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342769 07/16/16 01:52 AA TAL IRV Total/NA Prep 5035 5.16 g 10 mL 342024 07/13/16 11:20 ATL TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342770 07/16/16 01:52 AA TAL IRV Total/NA Prep 3546 7.03 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 16:19 AI TAL IRV Total/NA Prep 3546 3.00 g 1 mL 343307 07/19/16 08:02 LEG TAL IRV Total/NA Analysis 8015B 1 343451 07/19/16 22:51 JM TAL IRV Total/NA Prep 3546 7.34 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 16:59 JM TAL IRV Total/NA Prep 3050B 2.02 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:14 EN TAL IRV Total/NA Prep 7471A 0.50 g 50 mL 342231 07/14/16 01:08 DB TAL IRV Total/NA Analysis 7471A 1 342525 07/14/16 21:44 DB TAL IRV Client Sample ID: AEC-4-20' Lab Sample ID: 440-152462-12 Date Collected: 07/12/16 13:30 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.17 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 342846 07/16/16 12:46 SHS TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-20' Lab Sample ID: 440-152462-12 Date Collected: 07/12/16 13:30 Matrix: Solid
Date Received: 07/12/16 18:30
Prep 5035 342024 07/13/16 11:20 ATL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.17 g 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 342847 07/16/16 12:46 SHS TAL IRV Total/NA Prep 3546 7.57 g 1 mL 342338 07/14/16 09:28 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 16:39 AI TAL IRV Total/NA Prep 3546 7.16 g 1 mL 342178 07/13/16 18:24 VA TAL IRV Total/NA Analysis 8015B 1 342359 07/14/16 17:47 AMH TAL IRV Total/NA Prep 3546 7.02 g 2 mL 342185 07/13/16 18:43 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 17:14 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342294 07/14/16 08:05 DT TAL IRV Total/NA Analysis 6020 20 342656 07/15/16 10:16 EN TAL IRV Total/NA Prep 7471A 0.49 g 50 mL 342231 07/14/16 01:08 DB TAL IRV Total/NA Analysis 7471A 1 342525 07/14/16 21:47 DB TAL IRV Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 440-342265/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/14/16 08:20 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/14/16 08:20 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Benzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Bromoform ND 5.0 2.0 ug/Kg 07/14/16 08:20 1
Bromomethane ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Chloroethane ND 5.0 2.0 ug/Kg 07/14/16 08:20 1
Chloroform ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Chloromethane ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/14/16 08:20 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 Ethanol ND 300 100 ug/Kg 07/14/16 08:20 1
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 Ethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/14/16 08:20 1
Methylene Chloride ND 20 5.0 ug/Kg 07/14/16 08:20 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342265/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
RL MDL
Naphthalene ND 5.0 2.0 ug/Kg 07/14/16 08:20 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac n-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
o-Xylene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Styrene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/14/16 08:20 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Toluene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/14/16 08:20 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/14/16 08:20 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/14/16 08:20 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/14/16 08:20 1
Toluene-d8 (Surr) 106 79 - 123 07/14/16 08:20 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 79 - 120 07/14/16 08:20 1 Dibromofluoromethane (Surr) 102 60 - 120 07/14/16 08:20 1 Lab Sample ID: LCS 440-342265/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
1,1,1,2-Tetrachloroethane 50.0 51.4 ug/Kg 103 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 50.0 50.1 ug/Kg 100 65 - 135
1,1,2,2-Tetrachloroethane 50.0 52.6 ug/Kg 105 55 - 140
1,1,2-Trichloroethane 50.0 50.4 ug/Kg 101 65 - 135
1,1-Dichloroethane 50.0 47.0 ug/Kg 94 70 - 130
1,1-Dichloroethene 50.0 52.3 ug/Kg 105 70 - 125
1,1-Dichloropropene 50.0 53.7 ug/Kg 107 70 - 130
1,2,3-Trichlorobenzene 50.0 54.5 ug/Kg 109 60 - 130
1,2,3-Trichloropropane 50.0 52.4 ug/Kg 105 60 - 135
1,2,4-Trichlorobenzene 50.0 56.3 ug/Kg 113 70 - 135
1,2,4-Trimethylbenzene 50.0 48.8 ug/Kg 98 70 - 125
1,2-Dibromo-3-Chloropropane 50.0 51.2 ug/Kg 102 50 - 135 1,2-Dibromoethane (EDB) 50.0 56.2 ug/Kg 112 70 - 130
1,2-Dichlorobenzene 50.0 50.6 ug/Kg 101 75 - 120
1,2-Dichloroethane 50.0 52.5 ug/Kg 105 60 - 140
1,2-Dichloropropane 50.0 52.5 ug/Kg 105 70 - 130
1,3,5-Trimethylbenzene 50.0 48.8 ug/Kg 98 70 - 125
1,3-Dichlorobenzene 50.0 49.8 ug/Kg 100 75 - 125
1,3-Dichloropropane 50.0 52.9 ug/Kg 106 70 - 125
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342265/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
1,4-Dichlorobenzene 50.0 48.1 ug/Kg 96 75 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
2,2-Dichloropropane 50.0 52.9 ug/Kg 106 60 - 145
2-Chlorotoluene 50.0 54.4 ug/Kg 109 70 - 125
4-Chlorotoluene 50.0 55.0 ug/Kg 110 75 - 125
Benzene 50.0 49.4 ug/Kg 99 65 - 120
Bromobenzene 50.0 54.8 ug/Kg 110 75 - 120
Bromochloromethane 50.0 55.2 ug/Kg 110 70 - 135
Bromodichloromethane 50.0 53.0 ug/Kg 106 70 - 135
Bromoform 50.0 58.2 ug/Kg 116 55 - 135
Bromomethane 50.0 47.4 ug/Kg 95 60 - 145
Carbon tetrachloride 50.0 51.6 ug/Kg 103 65 - 140
Chlorobenzene 50.0 48.4 ug/Kg 97 75 - 120
Chloroethane 50.0 49.0 ug/Kg 98 60 - 140
Chloroform 50.0 49.3 ug/Kg 99 70 - 130
Chloromethane 50.0 39.8 ug/Kg 80 45 - 145
cis-1,2-Dichloroethene 50.0 54.7 ug/Kg 109 70 - 125
cis-1,3-Dichloropropene 50.0 55.7 ug/Kg 111 75 - 125
Dibromochloromethane 50.0 51.7 ug/Kg 103 65 - 140
Dibromomethane 50.0 54.1 ug/Kg 108 70 - 130
Dichlorodifluoromethane 50.0 41.5 ug/Kg 83 35 - 160
Isopropyl Ether (DIPE) 50.0 59.7 ug/Kg 119 60 - 140
Ethanol 2000 1810 ug/Kg 91 35 - 160
Ethyl-t-butyl ether (ETBE) 50.0 63.2 ug/Kg 126 60 - 140 Ethylbenzene 50.0 54.4 ug/Kg 109 70 - 125
Hexachlorobutadiene 50.0 49.3 ug/Kg 99 60 - 135
Isopropylbenzene 50.0 51.7 ug/Kg 103 75 - 130
m,p-Xylene 50.0 50.0 ug/Kg 100 70 - 125
Methylene Chloride 50.0 51.0 ug/Kg 102 55 - 135
Methyl-t-Butyl Ether (MTBE) 50.0 61.7 ug/Kg 123 60 - 140 Naphthalene 50.0 50.7 ug/Kg 101 55 - 135
n-Butylbenzene 50.0 48.1 ug/Kg 96 70 - 130
N-Propylbenzene 50.0 49.3 ug/Kg 99 70 - 130
o-Xylene 50.0 49.2 ug/Kg 98 70 - 125
sec-Butylbenzene 50.0 51.5 ug/Kg 103 70 - 125
Styrene 50.0 47.4 ug/Kg 95 75 - 130
Tert-amyl-methyl ether (TAME) 50.0 57.0 ug/Kg 114 60 - 145 tert-Butyl alcohol (TBA) 500 513 ug/Kg 103 70 - 135
tert-Butylbenzene 50.0 50.0 ug/Kg 100 70 - 125
Tetrachloroethene 50.0 50.0 ug/Kg 100 70 - 125
Toluene 50.0 54.2 ug/Kg 108 70 - 125
trans-1,2-Dichloroethene 50.0 54.0 ug/Kg 108 70 - 125
trans-1,3-Dichloropropene 50.0 54.4 ug/Kg 109 70 - 135
Trichloroethene 50.0 51.5 ug/Kg 103 70 - 125
Trichlorofluoromethane 50.0 48.4 ug/Kg 97 60 - 145
Vinyl chloride 50.0 42.7 ug/Kg 85 55 - 135
p-Isopropyltoluene 50.0 54.3 ug/Kg 109 75 - 125
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342265/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
Toluene-d8 (Surr) 79 - 123
Surrogate
106

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 79 - 120
Dibromofluoromethane (Surr) 103 60 - 120
Lab Sample ID: 440-152537-A-3 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
1,1,1,2-Tetrachloroethane ND 49.8 51.5 ug/Kg 103 65 - 145 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 49.8 48.9 ug/Kg 98 65 - 145
1,1,2,2-Tetrachloroethane ND 49.8 52.5 ug/Kg 105 40 - 160 1,1,2-Trichloroethane ND 49.8 49.7 ug/Kg 100 65 - 140
1,1-Dichloroethane ND 49.8 46.6 ug/Kg 93 65 - 135
1,1-Dichloroethene ND 49.8 49.1 ug/Kg 99 65 - 135
1,1-Dichloropropene ND 49.8 53.2 ug/Kg 107 65 - 135
1,2,3-Trichlorobenzene ND 49.8 54.1 ug/Kg 109 45 - 145
1,2,3-Trichloropropane ND 49.8 51.8 ug/Kg 104 50 - 150
1,2,4-Trichlorobenzene ND 49.8 55.1 ug/Kg 111 50 - 140
1,2,4-Trimethylbenzene ND 49.8 49.0 ug/Kg 98 65 - 140
1,2-Dibromo-3-Chloropropane ND 49.8 46.7 ug/Kg 94 40 - 150 1,2-Dibromoethane (EDB) ND 49.8 56.7 ug/Kg 114 65 - 140 1,2-Dichlorobenzene ND 49.8 50.6 ug/Kg 102 70 - 130
1,2-Dichloroethane ND 49.8 52.5 ug/Kg 105 60 - 150
1,2-Dichloropropane ND 49.8 53.1 ug/Kg 107 65 - 130
1,3,5-Trimethylbenzene ND 49.8 49.2 ug/Kg 99 65 - 135
1,3-Dichlorobenzene ND 49.8 50.3 ug/Kg 101 70 - 130
1,3-Dichloropropane ND 49.8 53.0 ug/Kg 106 65 - 140
1,4-Dichlorobenzene ND 49.8 48.3 ug/Kg 97 70 - 130
2,2-Dichloropropane ND 49.8 52.4 ug/Kg 105 65 - 150
2-Chlorotoluene ND 49.8 54.2 ug/Kg 109 60 - 135
4-Chlorotoluene ND 49.8 54.8 ug/Kg 110 65 - 135
Benzene ND 49.8 48.6 ug/Kg 98 65 - 130
Bromobenzene ND 49.8 55.4 ug/Kg 111 65 - 140
Bromochloromethane ND 49.8 54.2 ug/Kg 109 65 - 145
Bromodichloromethane ND 49.8 52.6 ug/Kg 106 65 - 145
Bromoform ND 49.8 56.3 ug/Kg 113 50 - 145
Bromomethane ND 49.8 45.8 ug/Kg 92 60 - 155
Carbon tetrachloride ND 49.8 50.6 ug/Kg 102 60 - 145
Chlorobenzene ND 49.8 48.5 ug/Kg 97 70 - 130
Chloroethane ND 49.8 46.4 ug/Kg 93 60 - 150
Chloroform ND 49.8 48.5 ug/Kg 97 65 - 135
Chloromethane ND 49.8 39.2 ug/Kg 79 40 - 145
cis-1,2-Dichloroethene ND 49.8 54.5 ug/Kg 109 65 - 135
cis-1,3-Dichloropropene ND 49.8 56.1 ug/Kg 113 70 - 135 Dibromochloromethane ND 49.8 51.9 ug/Kg 104 60 - 145
Dibromomethane ND 49.8 53.8 ug/Kg 108 65 - 140
Dichlorodifluoromethane ND 49.8 40.0 ug/Kg 80 30 - 160
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152537-A-3 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
Isopropyl Ether (DIPE) ND 49.8 58.5 ug/Kg 117 60 - 150
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Ethanol ND 1990 1920 ug/Kg 96 30 - 165
Ethyl-t-butyl ether (ETBE) ND 49.8 60.3 ug/Kg 121 60 - 145 Ethylbenzene ND 49.8 54.4 ug/Kg 109 70 - 135
Hexachlorobutadiene ND 49.8 48.0 ug/Kg 96 50 - 145
Isopropylbenzene ND 49.8 51.8 ug/Kg 104 70 - 145
m,p-Xylene ND 49.8 50.1 ug/Kg 101 70 - 130
Methylene Chloride ND 49.8 49.3 ug/Kg 99 55 - 145
Methyl-t-Butyl Ether (MTBE) ND 49.8 59.5 ug/Kg 120 55 - 155 Naphthalene ND 49.8 49.2 ug/Kg 99 40 - 150
n-Butylbenzene ND 49.8 48.6 ug/Kg 98 55 - 145
N-Propylbenzene ND 49.8 49.1 ug/Kg 99 65 - 140
o-Xylene ND 49.8 49.8 ug/Kg 100 65 - 130
sec-Butylbenzene ND 49.8 51.9 ug/Kg 104 60 - 135
Styrene ND 49.8 48.4 ug/Kg 97 70 - 140
Tert-amyl-methyl ether (TAME) ND 49.8 55.3 ug/Kg 111 60 - 150 tert-Butyl alcohol (TBA) ND 498 520 ug/Kg 104 65 - 145
tert-Butylbenzene ND 49.8 49.9 ug/Kg 100 60 - 140
Tetrachloroethene ND 49.8 51.3 ug/Kg 103 65 - 135
Toluene ND 49.8 54.4 ug/Kg 109 70 - 130
trans-1,2-Dichloroethene ND 49.8 51.2 ug/Kg 103 70 - 135 trans-1,3-Dichloropropene ND 49.8 54.6 ug/Kg 110 60 - 145 Trichloroethene ND 49.8 51.0 ug/Kg 102 65 - 140
Trichlorofluoromethane ND 49.8 46.1 ug/Kg 93 55 - 155
Vinyl chloride ND 49.8 41.9 ug/Kg 84 55 - 140
p-Isopropyltoluene ND 49.8 53.9 ug/Kg 108 60 - 140
Toluene-d8 (Surr) 79 - 123
Surrogate
106
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 79 - 120
Dibromofluoromethane (Surr) 102 60 - 120
Lab Sample ID: 440-152537-A-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
1,1,1,2-Tetrachloroethane ND 49.6 50.0 ug/Kg 101 65 - 145 3 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 49.6 46.6 ug/Kg 94 65 - 145 5 20 1,1,2,2-Tetrachloroethane ND 49.6 51.1 ug/Kg 103 40 - 160 3 30 1,1,2-Trichloroethane ND 49.6 48.6 ug/Kg 98 65 - 140 2 30 1,1-Dichloroethane ND 49.6 43.6 ug/Kg 88 65 - 135 7 25
1,1-Dichloroethene ND 49.6 45.2 ug/Kg 91 65 - 135 8 25
1,1-Dichloropropene ND 49.6 50.0 ug/Kg 101 65 - 135 6 20 1,2,3-Trichlorobenzene ND 49.6 51.5 ug/Kg 104 45 - 145 5 30 1,2,3-Trichloropropane ND 49.6 50.1 ug/Kg 101 50 - 150 3 30 1,2,4-Trichlorobenzene ND 49.6 52.1 ug/Kg 105 50 - 140 6 30 1,2,4-Trimethylbenzene ND 49.6 47.7 ug/Kg 96 65 - 140 3 25 TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152537-A-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
1,2-Dibromo-3-Chloropropane ND 49.6 45.0 ug/Kg 91 40 - 150 4 30 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,2-Dibromoethane (EDB) ND 49.6 54.8 ug/Kg 110 65 - 140 3 25 1,2-Dichlorobenzene ND 49.6 49.8 ug/Kg 100 70 - 130 2 25 1,2-Dichloroethane ND 49.6 51.7 ug/Kg 104 60 - 150 1 25 1,2-Dichloropropane ND 49.6 50.5 ug/Kg 102 65 - 130 5 20 1,3,5-Trimethylbenzene ND 49.6 46.8 ug/Kg 94 65 - 135 5 25 1,3-Dichlorobenzene ND 49.6 49.0 ug/Kg 99 70 - 130 3 25 1,3-Dichloropropane ND 49.6 50.4 ug/Kg 102 65 - 140 5 25 1,4-Dichlorobenzene ND 49.6 47.6 ug/Kg 96 70 - 130 1 25 2,2-Dichloropropane ND 49.6 49.3 ug/Kg 99 65 - 150 6 25 2-Chlorotoluene ND 49.6 53.2 ug/Kg 107 60 - 135 2 25
4-Chlorotoluene ND 49.6 53.6 ug/Kg 108 65 - 135 2 25
Benzene ND 49.6 47.1 ug/Kg 95 65 - 130 3 20
Bromobenzene ND 49.6 54.2 ug/Kg 109 65 - 140 2 25
Bromochloromethane ND 49.6 52.1 ug/Kg 105 65 - 145 4 25 Bromodichloromethane ND 49.6 50.7 ug/Kg 102 65 - 145 4 20 Bromoform ND 49.6 54.8 ug/Kg 111 50 - 145 3 30
Bromomethane ND 49.6 45.3 ug/Kg 91 60 - 155 1 25
Carbon tetrachloride ND 49.6 48.8 ug/Kg 98 60 - 145 4 25 Chlorobenzene ND 49.6 46.3 ug/Kg 93 70 - 130 5 25
Chloroethane ND 49.6 44.7 ug/Kg 90 60 - 150 4 25
Chloroform ND 49.6 47.6 ug/Kg 96 65 - 135 2 20
Chloromethane ND 49.6 39.5 ug/Kg 80 40 - 145 1 25
cis-1,2-Dichloroethene ND 49.6 52.8 ug/Kg 107 65 - 135 3 25 cis-1,3-Dichloropropene ND 49.6 54.4 ug/Kg 110 70 - 135 3 25 Dibromochloromethane ND 49.6 50.5 ug/Kg 102 60 - 145 3 25 Dibromomethane ND 49.6 52.8 ug/Kg 106 65 - 140 2 25
Dichlorodifluoromethane ND 49.6 38.9 ug/Kg 78 30 - 160 3 35 Isopropyl Ether (DIPE) ND 49.6 57.2 ug/Kg 115 60 - 150 2 25 Ethanol ND 1980 1900 ug/Kg 96 30 - 165 1 40
Ethyl-t-butyl ether (ETBE) ND 49.6 59.9 ug/Kg 121 60 - 145 1 30 Ethylbenzene ND 49.6 52.2 ug/Kg 105 70 - 135 4 25
Hexachlorobutadiene ND 49.6 45.4 ug/Kg 92 50 - 145 5 35 Isopropylbenzene ND 49.6 49.0 ug/Kg 99 70 - 145 6 25
m,p-Xylene ND 49.6 47.8 ug/Kg 96 70 - 130 5 25
Methylene Chloride ND 49.6 45.8 ug/Kg 92 55 - 145 7 25
Methyl-t-Butyl Ether (MTBE) ND 49.6 58.4 ug/Kg 118 55 - 155 2 35 Naphthalene ND 49.6 48.1 ug/Kg 97 40 - 150 2 40
n-Butylbenzene ND 49.6 45.8 ug/Kg 92 55 - 145 6 30
N-Propylbenzene ND 49.6 48.2 ug/Kg 97 65 - 140 2 25
o-Xylene ND 49.6 48.6 ug/Kg 98 65 - 130 2 25
sec-Butylbenzene ND 49.6 49.1 ug/Kg 99 60 - 135 5 25
Styrene ND 49.6 46.6 ug/Kg 94 70 - 140 4 25
Tert-amyl-methyl ether (TAME) ND 49.6 54.4 ug/Kg 110 60 - 150 1 25 tert-Butyl alcohol (TBA) ND 496 520 ug/Kg 105 65 - 145 0 30 tert-Butylbenzene ND 49.6 48.0 ug/Kg 97 60 - 140 4 25
Tetrachloroethene ND 49.6 48.0 ug/Kg 97 65 - 135 7 25
Toluene ND 49.6 51.9 ug/Kg 105 70 - 130 5 20
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152537-A-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342265
trans-1,2-Dichloroethene ND 49.6 50.6 ug/Kg 102 70 - 135 1 25 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
trans-1,3-Dichloropropene ND 49.6 52.9 ug/Kg 107 60 - 145 3 25 Trichloroethene ND 49.6 49.0 ug/Kg 99 65 - 140 4 25
Trichlorofluoromethane ND 49.6 44.2 ug/Kg 89 55 - 155 4 25 Vinyl chloride ND 49.6 42.4 ug/Kg 85 55 - 140 1 30
p-Isopropyltoluene ND 49.6 51.7 ug/Kg 104 60 - 140 4 25 Toluene-d8 (Surr) 79 - 123
Surrogate
105

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 79 - 120
Dibromofluoromethane (Surr) 104 60 - 120
Lab Sample ID: MB 440-342463/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/14/16 19:21 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/14/16 19:21 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Benzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Bromoform ND 5.0 2.0 ug/Kg 07/14/16 19:21 1
Bromomethane ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342463/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
RL MDL
Chloroethane ND 5.0 2.0 ug/Kg 07/14/16 19:21 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Chloroform ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Chloromethane ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/14/16 19:21 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 Ethanol ND 300 100 ug/Kg 07/14/16 19:21 1
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 Ethylbenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/14/16 19:21 1
Methylene Chloride ND 20 5.0 ug/Kg 07/14/16 19:21 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 Naphthalene ND 5.0 2.0 ug/Kg 07/14/16 19:21 1
n-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
o-Xylene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Styrene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/14/16 19:21 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Toluene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/14/16 19:21 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/14/16 19:21 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/14/16 19:21 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/14/16 19:21 1
Toluene-d8 (Surr) 102 79 - 123 07/14/16 19:21 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 79 - 120 07/14/16 19:21 1 Dibromofluoromethane (Surr) 108 60 - 120 07/14/16 19:21 1 Lab Sample ID: LCS 440-342463/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
1,1,1,2-Tetrachloroethane 50.0 52.8 ug/Kg 106 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 50.0 48.7 ug/Kg 97 65 - 135
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342463/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
1,1,2,2-Tetrachloroethane 50.0 55.0 ug/Kg 110 55 - 140
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,2-Trichloroethane 50.0 51.2 ug/Kg 102 65 - 135
1,1-Dichloroethane 50.0 48.3 ug/Kg 97 70 - 130
1,1-Dichloroethene 50.0 48.3 ug/Kg 97 70 - 125
1,1-Dichloropropene 50.0 52.6 ug/Kg 105 70 - 130
1,2,3-Trichlorobenzene 50.0 57.8 ug/Kg 116 60 - 130
1,2,3-Trichloropropane 50.0 55.0 ug/Kg 110 60 - 135
1,2,4-Trichlorobenzene 50.0 57.3 ug/Kg 115 70 - 135
1,2,4-Trimethylbenzene 50.0 50.2 ug/Kg 100 70 - 125
1,2-Dibromo-3-Chloropropane 50.0 47.6 ug/Kg 95 50 - 135 1,2-Dibromoethane (EDB) 50.0 56.9 ug/Kg 114 70 - 130
1,2-Dichlorobenzene 50.0 53.6 ug/Kg 107 75 - 120
1,2-Dichloroethane 50.0 55.6 ug/Kg 111 60 - 140
1,2-Dichloropropane 50.0 55.0 ug/Kg 110 70 - 130
1,3,5-Trimethylbenzene 50.0 49.9 ug/Kg 100 70 - 125
1,3-Dichlorobenzene 50.0 52.3 ug/Kg 105 75 - 125
1,3-Dichloropropane 50.0 55.3 ug/Kg 111 70 - 125
1,4-Dichlorobenzene 50.0 51.2 ug/Kg 102 75 - 120
2,2-Dichloropropane 50.0 49.8 ug/Kg 100 60 - 145
2-Chlorotoluene 50.0 56.7 ug/Kg 113 70 - 125
4-Chlorotoluene 50.0 55.9 ug/Kg 112 75 - 125
Benzene 50.0 50.8 ug/Kg 102 65 - 120
Bromobenzene 50.0 57.2 ug/Kg 114 75 - 120
Bromochloromethane 50.0 56.0 ug/Kg 112 70 - 135
Bromodichloromethane 50.0 55.1 ug/Kg 110 70 - 135
Bromoform 50.0 58.9 ug/Kg 118 55 - 135
Bromomethane 50.0 48.3 ug/Kg 97 60 - 145
Carbon tetrachloride 50.0 49.5 ug/Kg 99 65 - 140
Chlorobenzene 50.0 49.6 ug/Kg 99 75 - 120
Chloroethane 50.0 46.4 ug/Kg 93 60 - 140
Chloroform 50.0 51.8 ug/Kg 104 70 - 130
Chloromethane 50.0 42.5 ug/Kg 85 45 - 145
cis-1,2-Dichloroethene 50.0 56.0 ug/Kg 112 70 - 125
cis-1,3-Dichloropropene 50.0 57.3 ug/Kg 115 75 - 125
Dibromochloromethane 50.0 52.6 ug/Kg 105 65 - 140
Dibromomethane 50.0 55.5 ug/Kg 111 70 - 130
Dichlorodifluoromethane 50.0 41.1 ug/Kg 82 35 - 160
Isopropyl Ether (DIPE) 50.0 60.9 ug/Kg 122 60 - 140
Ethanol 2000 2170 ug/Kg 108 35 - 160
Ethyl-t-butyl ether (ETBE) 50.0 60.4 ug/Kg 121 60 - 140 Ethylbenzene 50.0 54.7 ug/Kg 109 70 - 125
Hexachlorobutadiene 50.0 50.0 ug/Kg 100 60 - 135
Isopropylbenzene 50.0 51.7 ug/Kg 103 75 - 130
m,p-Xylene 50.0 49.7 ug/Kg 99 70 - 125
Methylene Chloride 50.0 52.5 ug/Kg 105 55 - 135
Methyl-t-Butyl Ether (MTBE) 50.0 58.5 ug/Kg 117 60 - 140 Naphthalene 50.0 50.9 ug/Kg 102 55 - 135
n-Butylbenzene 50.0 48.9 ug/Kg 98 70 - 130
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342463/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
N-Propylbenzene 50.0 49.6 ug/Kg 99 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
o-Xylene 50.0 51.4 ug/Kg 103 70 - 125
sec-Butylbenzene 50.0 52.2 ug/Kg 104 70 - 125
Styrene 50.0 48.9 ug/Kg 98 75 - 130
Tert-amyl-methyl ether (TAME) 50.0 54.8 ug/Kg 110 60 - 145 tert-Butyl alcohol (TBA) 500 585 ug/Kg 117 70 - 135
tert-Butylbenzene 50.0 50.3 ug/Kg 101 70 - 125
Tetrachloroethene 50.0 50.8 ug/Kg 102 70 - 125
Toluene 50.0 56.5 ug/Kg 113 70 - 125
trans-1,2-Dichloroethene 50.0 50.5 ug/Kg 101 70 - 125
trans-1,3-Dichloropropene 50.0 55.0 ug/Kg 110 70 - 135
Trichloroethene 50.0 52.1 ug/Kg 104 70 - 125
Trichlorofluoromethane 50.0 46.6 ug/Kg 93 60 - 145
Vinyl chloride 50.0 45.0 ug/Kg 90 55 - 135
p-Isopropyltoluene 50.0 55.1 ug/Kg 110 75 - 125
Toluene-d8 (Surr) 79 - 123
Surrogate
107

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 79 - 120
Dibromofluoromethane (Surr) 107 60 - 120
Lab Sample ID: 440-152462-2 MS Client Sample ID: AEC-5-10' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
1,1,1,2-Tetrachloroethane ND 50.2 53.9 ug/Kg 107 65 - 145 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 50.2 50.3 ug/Kg 100 65 - 145
1,1,2,2-Tetrachloroethane ND 50.2 54.1 ug/Kg 108 40 - 160 1,1,2-Trichloroethane ND 50.2 53.8 ug/Kg 107 65 - 140
1,1-Dichloroethane ND 50.2 48.2 ug/Kg 96 65 - 135
1,1-Dichloroethene ND 50.2 49.7 ug/Kg 99 65 - 135
1,1-Dichloropropene ND 50.2 52.1 ug/Kg 104 65 - 135
1,2,3-Trichlorobenzene ND 50.2 53.9 ug/Kg 107 45 - 145
1,2,3-Trichloropropane ND 50.2 55.7 ug/Kg 111 50 - 150
1,2,4-Trichlorobenzene ND 50.2 56.1 ug/Kg 112 50 - 140
1,2,4-Trimethylbenzene ND 50.2 47.4 ug/Kg 94 65 - 140
1,2-Dibromo-3-Chloropropane ND 50.2 50.6 ug/Kg 101 40 - 150 1,2-Dibromoethane (EDB) ND 50.2 61.1 ug/Kg 122 65 - 140 1,2-Dichlorobenzene ND 50.2 51.2 ug/Kg 102 70 - 130
1,2-Dichloroethane ND 50.2 57.4 ug/Kg 114 60 - 150
1,2-Dichloropropane ND 50.2 53.8 ug/Kg 107 65 - 130
1,3,5-Trimethylbenzene ND 50.2 47.4 ug/Kg 94 65 - 135
1,3-Dichlorobenzene ND 50.2 50.0 ug/Kg 100 70 - 130
1,3-Dichloropropane ND 50.2 58.2 ug/Kg 116 65 - 140
1,4-Dichlorobenzene ND 50.2 49.3 ug/Kg 98 70 - 130
2,2-Dichloropropane ND 50.2 54.1 ug/Kg 108 65 - 150
2-Chlorotoluene ND 50.2 52.8 ug/Kg 105 60 - 135
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152462-2 MS Client Sample ID: AEC-5-10' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
4-Chlorotoluene ND 50.2 54.0 ug/Kg 108 65 - 135
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Benzene ND 50.2 50.3 ug/Kg 100 65 - 130
Bromobenzene ND 50.2 53.0 ug/Kg 106 65 - 140
Bromochloromethane ND 50.2 56.0 ug/Kg 112 65 - 145
Bromodichloromethane ND 50.2 54.2 ug/Kg 108 65 - 145
Bromoform ND 50.2 63.1 ug/Kg 126 50 - 145
Bromomethane ND 50.2 44.5 ug/Kg 89 60 - 155
Carbon tetrachloride ND 50.2 51.9 ug/Kg 103 60 - 145
Chlorobenzene ND 50.2 49.5 ug/Kg 99 70 - 130
Chloroethane ND 50.2 46.6 ug/Kg 93 60 - 150
Chloroform ND 50.2 50.8 ug/Kg 101 65 - 135
Chloromethane ND 50.2 39.0 ug/Kg 78 40 - 145
cis-1,2-Dichloroethene ND 50.2 54.2 ug/Kg 108 65 - 135
cis-1,3-Dichloropropene ND 50.2 57.2 ug/Kg 114 70 - 135 Dibromochloromethane ND 50.2 55.6 ug/Kg 111 60 - 145
Dibromomethane ND 50.2 58.0 ug/Kg 116 65 - 140
Dichlorodifluoromethane ND 50.2 40.1 ug/Kg 80 30 - 160
Isopropyl Ether (DIPE) ND 50.2 61.5 ug/Kg 123 60 - 150
Ethanol ND 2010 1970 ug/Kg 98 30 - 165
Ethyl-t-butyl ether (ETBE) ND 50.2 62.7 ug/Kg 125 60 - 145 Ethylbenzene ND 50.2 55.3 ug/Kg 110 70 - 135
Hexachlorobutadiene ND 50.2 47.4 ug/Kg 94 50 - 145
Isopropylbenzene ND 50.2 52.8 ug/Kg 105 70 - 145
m,p-Xylene ND 50.2 50.7 ug/Kg 101 70 - 130
Methylene Chloride ND 50.2 52.4 ug/Kg 104 55 - 145
Methyl-t-Butyl Ether (MTBE) ND 50.2 62.1 ug/Kg 124 55 - 155 Naphthalene ND 50.2 50.4 ug/Kg 100 40 - 150
n-Butylbenzene ND 50.2 48.4 ug/Kg 96 55 - 145
N-Propylbenzene ND 50.2 47.7 ug/Kg 95 65 - 140
o-Xylene ND 50.2 51.8 ug/Kg 103 65 - 130
sec-Butylbenzene ND 50.2 49.8 ug/Kg 99 60 - 135
Styrene ND 50.2 48.9 ug/Kg 97 70 - 140
Tert-amyl-methyl ether (TAME) ND 50.2 56.8 ug/Kg 113 60 - 150 tert-Butyl alcohol (TBA) ND 502 533 ug/Kg 106 65 - 145
tert-Butylbenzene ND 50.2 47.3 ug/Kg 94 60 - 140
Tetrachloroethene ND 50.2 50.9 ug/Kg 101 65 - 135
Toluene ND 50.2 55.4 ug/Kg 110 70 - 130
trans-1,2-Dichloroethene ND 50.2 51.4 ug/Kg 102 70 - 135 trans-1,3-Dichloropropene ND 50.2 56.4 ug/Kg 112 60 - 145 Trichloroethene ND 50.2 52.5 ug/Kg 104 65 - 140
Trichlorofluoromethane ND 50.2 45.9 ug/Kg 91 55 - 155
Vinyl chloride ND 50.2 43.3 ug/Kg 86 55 - 140
p-Isopropyltoluene ND 50.2 52.9 ug/Kg 105 60 - 140
Toluene-d8 (Surr) 79 - 123
Surrogate
107
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 79 - 120
Dibromofluoromethane (Surr) 106 60 - 120
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Lab Sample ID: 440-152462-2 MSD Client Sample ID: AEC-5-10' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
1,1,1,2-Tetrachloroethane ND 50.1 53.7 ug/Kg 107 65 - 145 0 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 50.1 51.4 ug/Kg 103 65 - 145 2 20 1,1,2,2-Tetrachloroethane ND 50.1 56.1 ug/Kg 112 40 - 160 4 30 1,1,2-Trichloroethane ND 50.1 54.9 ug/Kg 110 65 - 140 2 30 1,1-Dichloroethane ND 50.1 49.4 ug/Kg 99 65 - 135 3 25
1,1-Dichloroethene ND 50.1 48.9 ug/Kg 98 65 - 135 2 25
1,1-Dichloropropene ND 50.1 54.0 ug/Kg 108 65 - 135 4 20 1,2,3-Trichlorobenzene ND 50.1 56.1 ug/Kg 112 45 - 145 4 30 1,2,3-Trichloropropane ND 50.1 56.7 ug/Kg 113 50 - 150 2 30 1,2,4-Trichlorobenzene ND 50.1 56.3 ug/Kg 112 50 - 140 0 30 1,2,4-Trimethylbenzene ND 50.1 47.9 ug/Kg 96 65 - 140 1 25 1,2-Dibromo-3-Chloropropane ND 50.1 51.7 ug/Kg 103 40 - 150 2 30 1,2-Dibromoethane (EDB) ND 50.1 61.9 ug/Kg 123 65 - 140 1 25 1,2-Dichlorobenzene ND 50.1 52.0 ug/Kg 104 70 - 130 2 25 1,2-Dichloroethane ND 50.1 60.0 ug/Kg 120 60 - 150 5 25 1,2-Dichloropropane ND 50.1 56.5 ug/Kg 113 65 - 130 5 20 1,3,5-Trimethylbenzene ND 50.1 48.2 ug/Kg 96 65 - 135 2 25 1,3-Dichlorobenzene ND 50.1 50.7 ug/Kg 101 70 - 130 1 25 1,3-Dichloropropane ND 50.1 58.8 ug/Kg 117 65 - 140 1 25 1,4-Dichlorobenzene ND 50.1 50.3 ug/Kg 100 70 - 130 2 25 2,2-Dichloropropane ND 50.1 54.3 ug/Kg 108 65 - 150 0 25 2-Chlorotoluene ND 50.1 53.7 ug/Kg 107 60 - 135 2 25
4-Chlorotoluene ND 50.1 54.7 ug/Kg 109 65 - 135 1 25
Benzene ND 50.1 51.1 ug/Kg 102 65 - 130 2 20
Bromobenzene ND 50.1 55.3 ug/Kg 110 65 - 140 4 25
Bromochloromethane ND 50.1 58.2 ug/Kg 116 65 - 145 4 25 Bromodichloromethane ND 50.1 57.5 ug/Kg 115 65 - 145 6 20 Bromoform ND 50.1 63.7 ug/Kg 127 50 - 145 1 30
Bromomethane ND 50.1 46.6 ug/Kg 93 60 - 155 4 25
Carbon tetrachloride ND 50.1 53.3 ug/Kg 106 60 - 145 3 25 Chlorobenzene ND 50.1 49.8 ug/Kg 99 70 - 130 0 25
Chloroethane ND 50.1 46.4 ug/Kg 93 60 - 150 0 25
Chloroform ND 50.1 52.8 ug/Kg 105 65 - 135 4 20
Chloromethane ND 50.1 39.0 ug/Kg 78 40 - 145 0 25
cis-1,2-Dichloroethene ND 50.1 57.0 ug/Kg 114 65 - 135 5 25 cis-1,3-Dichloropropene ND 50.1 58.2 ug/Kg 116 70 - 135 2 25 Dibromochloromethane ND 50.1 56.5 ug/Kg 113 60 - 145 2 25 Dibromomethane ND 50.1 61.0 ug/Kg 122 65 - 140 5 25
Dichlorodifluoromethane ND 50.1 40.2 ug/Kg 80 30 - 160 0 35 Isopropyl Ether (DIPE) ND 50.1 63.4 ug/Kg 126 60 - 150 3 25 Ethanol ND 2000 2010 ug/Kg 100 30 - 165 2 40
Ethyl-t-butyl ether (ETBE) ND 50.1 65.8 ug/Kg 131 60 - 145 5 30 Ethylbenzene ND 50.1 55.4 ug/Kg 111 70 - 135 0 25
Hexachlorobutadiene ND 50.1 45.4 ug/Kg 91 50 - 145 4 35 Isopropylbenzene ND 50.1 52.0 ug/Kg 104 70 - 145 2 25
m,p-Xylene ND 50.1 49.7 ug/Kg 99 70 - 130 2 25
Methylene Chloride ND 50.1 54.1 ug/Kg 108 55 - 145 3 25 Methyl-t-Butyl Ether (MTBE) ND 50.1 65.7 ug/Kg 131 55 - 155 6 35 Naphthalene ND 50.1 53.0 ug/Kg 106 40 - 150 5 40
n-Butylbenzene ND 50.1 47.9 ug/Kg 96 55 - 145 1 30
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152462-2 MSD Client Sample ID: AEC-5-10' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342463
N-Propylbenzene ND 50.1 48.4 ug/Kg 97 65 - 140 1 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
o-Xylene ND 50.1 51.7 ug/Kg 103 65 - 130 0 25
sec-Butylbenzene ND 50.1 49.3 ug/Kg 98 60 - 135 1 25
Styrene ND 50.1 49.8 ug/Kg 99 70 - 140 2 25
Tert-amyl-methyl ether (TAME) ND 50.1 59.8 ug/Kg 119 60 - 150 5 25 tert-Butyl alcohol (TBA) ND 501 541 ug/Kg 108 65 - 145 1 30 tert-Butylbenzene ND 50.1 46.9 ug/Kg 94 60 - 140 1 25
Tetrachloroethene ND 50.1 50.1 ug/Kg 100 65 - 135 2 25
Toluene ND 50.1 55.3 ug/Kg 110 70 - 130 0 20
trans-1,2-Dichloroethene ND 50.1 53.7 ug/Kg 107 70 - 135 4 25 trans-1,3-Dichloropropene ND 50.1 57.0 ug/Kg 114 60 - 145 1 25 Trichloroethene ND 50.1 53.5 ug/Kg 107 65 - 140 2 25
Trichlorofluoromethane ND 50.1 47.1 ug/Kg 94 55 - 155 2 25 Vinyl chloride ND 50.1 43.2 ug/Kg 86 55 - 140 0 30
p-Isopropyltoluene ND 50.1 53.5 ug/Kg 107 60 - 140 1 25 Toluene-d8 (Surr) 79 - 123
Surrogate
105

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 100 79 - 120
Dibromofluoromethane (Surr) 109 60 - 120
Lab Sample ID: MB 440-342769/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/15/16 18:55 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/15/16 18:55 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342769/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769
RL MDL
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Benzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Bromoform ND 5.0 2.0 ug/Kg 07/15/16 18:55 1
Bromomethane ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Chloroethane ND 5.0 2.0 ug/Kg 07/15/16 18:55 1
Chloroform ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Chloromethane ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/15/16 18:55 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 Ethanol ND 300 100 ug/Kg 07/15/16 18:55 1
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 Ethylbenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/15/16 18:55 1
Methylene Chloride ND 20 5.0 ug/Kg 07/15/16 18:55 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 Naphthalene ND 5.0 2.0 ug/Kg 07/15/16 18:55 1
n-Butylbenzene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
o-Xylene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Styrene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/15/16 18:55 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Toluene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/15/16 18:55 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/15/16 18:55 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/15/16 18:55 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/15/16 18:55 1
Toluene-d8 (Surr) 110 79 - 123 07/15/16 18:55 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 79 - 120 07/15/16 18:55 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342769/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769
Dibromofluoromethane (Surr) 112 60 - 120 07/15/16 18:55 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-342769/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769
1,1,1,2-Tetrachloroethane 50.0 51.3 ug/Kg 103 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 50.0 46.6 ug/Kg 93 65 - 135
1,1,2,2-Tetrachloroethane 50.0 45.4 ug/Kg 91 55 - 140
1,1,2-Trichloroethane 50.0 47.4 ug/Kg 95 65 - 135
1,1-Dichloroethane 50.0 47.7 ug/Kg 95 70 - 130
1,1-Dichloroethene 50.0 47.1 ug/Kg 94 70 - 125
1,1-Dichloropropene 50.0 45.2 ug/Kg 90 70 - 130
1,2,3-Trichlorobenzene 50.0 48.2 ug/Kg 96 60 - 130
1,2,3-Trichloropropane 50.0 42.0 ug/Kg 84 60 - 135
1,2,4-Trichlorobenzene 50.0 49.6 ug/Kg 99 70 - 135
1,2,4-Trimethylbenzene 50.0 45.7 ug/Kg 91 70 - 125
1,2-Dibromo-3-Chloropropane 50.0 37.6 ug/Kg 75 50 - 135 1,2-Dibromoethane (EDB) 50.0 50.6 ug/Kg 101 70 - 130
1,2-Dichlorobenzene 50.0 49.6 ug/Kg 99 75 - 120
1,2-Dichloroethane 50.0 49.1 ug/Kg 98 60 - 140
1,2-Dichloropropane 50.0 52.9 ug/Kg 106 70 - 130
1,3,5-Trimethylbenzene 50.0 44.9 ug/Kg 90 70 - 125
1,3-Dichlorobenzene 50.0 47.6 ug/Kg 95 75 - 125
1,3-Dichloropropane 50.0 44.7 ug/Kg 89 70 - 125
1,4-Dichlorobenzene 50.0 48.2 ug/Kg 96 75 - 120
2,2-Dichloropropane 50.0 42.6 ug/Kg 85 60 - 145
2-Chlorotoluene 50.0 45.5 ug/Kg 91 70 - 125
4-Chlorotoluene 50.0 48.0 ug/Kg 96 75 - 125
Benzene 50.0 49.2 ug/Kg 98 65 - 120
Bromobenzene 50.0 51.1 ug/Kg 102 75 - 120
Bromochloromethane 50.0 49.2 ug/Kg 98 70 - 135
Bromodichloromethane 50.0 52.0 ug/Kg 104 70 - 135
Bromoform 50.0 51.1 ug/Kg 102 55 - 135
Bromomethane 50.0 42.0 ug/Kg 84 60 - 145
Carbon tetrachloride 50.0 46.4 ug/Kg 93 65 - 140
Chlorobenzene 50.0 48.7 ug/Kg 97 75 - 120
Chloroethane 50.0 42.7 ug/Kg 85 60 - 140
Chloroform 50.0 50.5 ug/Kg 101 70 - 130
Chloromethane 50.0 42.8 ug/Kg 86 45 - 145
cis-1,2-Dichloroethene 50.0 47.3 ug/Kg 95 70 - 125
cis-1,3-Dichloropropene 50.0 53.4 ug/Kg 107 75 - 125
Dibromochloromethane 50.0 50.9 ug/Kg 102 65 - 140
Dibromomethane 50.0 47.2 ug/Kg 94 70 - 130
Dichlorodifluoromethane 50.0 33.9 ug/Kg 68 35 - 160
Isopropyl Ether (DIPE) 50.0 55.7 ug/Kg 111 60 - 140
Ethanol 2000 1910 ug/Kg 96 35 - 160
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342769/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769
Ethyl-t-butyl ether (ETBE) 50.0 54.7 ug/Kg 109 60 - 140 Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Ethylbenzene 50.0 46.1 ug/Kg 92 70 - 125
Hexachlorobutadiene 50.0 34.9 ug/Kg 70 60 - 135
Isopropylbenzene 50.0 45.6 ug/Kg 91 75 - 130
m,p-Xylene 50.0 49.5 ug/Kg 99 70 - 125
Methylene Chloride 50.0 50.4 ug/Kg 101 55 - 135
Methyl-t-Butyl Ether (MTBE) 50.0 52.0 ug/Kg 104 60 - 140 Naphthalene 50.0 46.2 ug/Kg 92 55 - 135
n-Butylbenzene 50.0 39.6 ug/Kg 79 70 - 130
N-Propylbenzene 50.0 42.7 ug/Kg 85 70 - 130
o-Xylene 50.0 49.5 ug/Kg 99 70 - 125
sec-Butylbenzene 50.0 40.2 ug/Kg 80 70 - 125
Styrene 50.0 52.6 ug/Kg 105 75 - 130
Tert-amyl-methyl ether (TAME) 50.0 55.2 ug/Kg 110 60 - 145 tert-Butyl alcohol (TBA) 500 513 ug/Kg 103 70 - 135
tert-Butylbenzene 50.0 42.6 ug/Kg 85 70 - 125
Tetrachloroethene 50.0 47.5 ug/Kg 95 70 - 125
Toluene 50.0 47.4 ug/Kg 95 70 - 125
trans-1,2-Dichloroethene 50.0 48.6 ug/Kg 97 70 - 125
trans-1,3-Dichloropropene 50.0 52.5 ug/Kg 105 70 - 135
Trichloroethene 50.0 42.9 ug/Kg 86 70 - 125
Trichlorofluoromethane 50.0 41.4 ug/Kg 83 60 - 145
Vinyl chloride 50.0 41.6 ug/Kg 83 55 - 135
p-Isopropyltoluene 50.0 41.1 ug/Kg 82 75 - 125
Toluene-d8 (Surr) 79 - 123
Surrogate
108

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 105 79 - 120
Dibromofluoromethane (Surr) 111 60 - 120
Lab Sample ID: 440-152557-B-2-B MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769 Prep Batch: 342782
1,1,1,2-Tetrachloroethane ND 41.2 40.7 ug/Kg 99 65 - 145 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 41.2 38.8 ug/Kg 94 65 - 145
1,1,2,2-Tetrachloroethane ND 41.2 39.1 ug/Kg 95 40 - 160 1,1,2-Trichloroethane ND 41.2 39.4 ug/Kg 96 65 - 140
1,1-Dichloroethane ND 41.2 39.3 ug/Kg 95 65 - 135
1,1-Dichloroethene ND 41.2 38.2 ug/Kg 93 65 - 135
1,1-Dichloropropene ND 41.2 37.6 ug/Kg 91 65 - 135
1,2,3-Trichlorobenzene ND 41.2 40.8 ug/Kg 99 45 - 145
1,2,3-Trichloropropane ND 41.2 38.5 ug/Kg 93 50 - 150
1,2,4-Trichlorobenzene ND 41.2 42.6 ug/Kg 103 50 - 140
1,2,4-Trimethylbenzene ND 41.2 37.2 ug/Kg 90 65 - 140
1,2-Dibromo-3-Chloropropane ND 41.2 33.8 ug/Kg 82 40 - 150 1,2-Dibromoethane (EDB) ND 41.2 43.0 ug/Kg 105 65 - 140 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152557-B-2-B MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769 Prep Batch: 342782
1,2-Dichlorobenzene ND 41.2 40.2 ug/Kg 98 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,2-Dichloroethane ND 41.2 41.7 ug/Kg 101 60 - 150
1,2-Dichloropropane ND 41.2 43.1 ug/Kg 105 65 - 130
1,3,5-Trimethylbenzene ND 41.2 37.1 ug/Kg 90 65 - 135
1,3-Dichlorobenzene ND 41.2 39.2 ug/Kg 95 70 - 130
1,3-Dichloropropane ND 41.2 37.3 ug/Kg 90 65 - 140
1,4-Dichlorobenzene ND 41.2 39.2 ug/Kg 95 70 - 130
2,2-Dichloropropane ND 41.2 35.5 ug/Kg 86 65 - 150
2-Chlorotoluene ND 41.2 36.5 ug/Kg 89 60 - 135
4-Chlorotoluene ND 41.2 38.9 ug/Kg 94 65 - 135
Benzene ND 41.2 40.5 ug/Kg 98 65 - 130
Bromobenzene ND 41.2 40.4 ug/Kg 98 65 - 140
Bromochloromethane ND 41.2 42.2 ug/Kg 102 65 - 145
Bromodichloromethane ND 41.2 43.7 ug/Kg 106 65 - 145
Bromoform ND 41.2 44.9 ug/Kg 109 50 - 145
Bromomethane ND 41.2 34.4 ug/Kg 83 60 - 155
Carbon tetrachloride ND 41.2 38.3 ug/Kg 93 60 - 145
Chlorobenzene ND 41.2 39.2 ug/Kg 95 70 - 130
Chloroethane ND 41.2 35.3 ug/Kg 86 60 - 150
Chloroform ND 41.2 41.6 ug/Kg 101 65 - 135
Chloromethane ND 41.2 35.4 ug/Kg 86 40 - 145
cis-1,2-Dichloroethene ND 41.2 39.2 ug/Kg 95 65 - 135
cis-1,3-Dichloropropene ND 41.2 43.9 ug/Kg 107 70 - 135 Dibromochloromethane ND 41.2 42.0 ug/Kg 102 60 - 145
Dibromomethane ND 41.2 40.9 ug/Kg 99 65 - 140
Dichlorodifluoromethane ND 41.2 29.4 ug/Kg 71 30 - 160
Isopropyl Ether (DIPE) ND 41.2 46.5 ug/Kg 113 60 - 150
Ethanol ND 1650 1370 ug/Kg 83 30 - 165
Ethyl-t-butyl ether (ETBE) ND 41.2 46.4 ug/Kg 113 60 - 145 Ethylbenzene ND 41.2 37.4 ug/Kg 91 70 - 135
Hexachlorobutadiene ND 41.2 35.4 ug/Kg 86 50 - 145
Isopropylbenzene ND 41.2 37.3 ug/Kg 91 70 - 145
m,p-Xylene ND 41.2 40.5 ug/Kg 98 70 - 130
Methylene Chloride ND 41.2 41.7 ug/Kg 101 55 - 145
Methyl-t-Butyl Ether (MTBE) ND 41.2 45.0 ug/Kg 109 55 - 155 Naphthalene ND 41.2 40.3 ug/Kg 98 40 - 150
n-Butylbenzene ND 41.2 35.4 ug/Kg 86 55 - 145
N-Propylbenzene ND 41.2 35.1 ug/Kg 85 65 - 140
o-Xylene ND 41.2 40.5 ug/Kg 98 65 - 130
sec-Butylbenzene ND 41.2 34.7 ug/Kg 84 60 - 135
Styrene ND 41.2 42.7 ug/Kg 104 70 - 140
Tert-amyl-methyl ether (TAME) ND 41.2 47.0 ug/Kg 114 60 - 150 tert-Butyl alcohol (TBA) ND 412 405 ug/Kg 98 65 - 145
tert-Butylbenzene ND 41.2 35.9 ug/Kg 87 60 - 140
Tetrachloroethene ND 41.2 38.4 ug/Kg 93 65 - 135
Toluene ND 41.2 38.0 ug/Kg 92 70 - 130
trans-1,2-Dichloroethene ND 41.2 39.4 ug/Kg 96 70 - 135 trans-1,3-Dichloropropene ND 41.2 44.0 ug/Kg 107 60 - 145 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152557-B-2-B MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769 Prep Batch: 342782
Trichloroethene ND 41.2 36.2 ug/Kg 88 65 - 140
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Trichlorofluoromethane ND 41.2 35.0 ug/Kg 85 55 - 155
Vinyl chloride ND 41.2 33.3 ug/Kg 81 55 - 140
p-Isopropyltoluene ND 41.2 35.8 ug/Kg 87 60 - 140
Toluene-d8 (Surr) 79 - 123
Surrogate
105
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 103 79 - 120
Dibromofluoromethane (Surr) 113 60 - 120
Lab Sample ID: 440-152557-D-2-A MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769 Prep Batch: 342782
1,1,1,2-Tetrachloroethane ND 45.0 47.6 ug/Kg 106 65 - 145 16 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 45.0 42.9 ug/Kg 95 65 - 145 10 20 1,1,2,2-Tetrachloroethane ND 45.0 43.8 ug/Kg 97 40 - 160 11 30 1,1,2-Trichloroethane ND 45.0 45.0 ug/Kg 100 65 - 140 13 30 1,1-Dichloroethane ND 45.0 43.6 ug/Kg 97 65 - 135 10 25 1,1-Dichloroethene ND 45.0 43.3 ug/Kg 96 65 - 135 13 25 1,1-Dichloropropene ND 45.0 42.0 ug/Kg 94 65 - 135 11 20 1,2,3-Trichlorobenzene ND 45.0 47.2 ug/Kg 105 45 - 145 14 30 1,2,3-Trichloropropane ND 45.0 42.4 ug/Kg 94 50 - 150 10 30 1,2,4-Trichlorobenzene ND 45.0 48.2 ug/Kg 107 50 - 140 12 30 1,2,4-Trimethylbenzene ND 45.0 42.1 ug/Kg 94 65 - 140 12 25 1,2-Dibromo-3-Chloropropane ND 45.0 37.6 ug/Kg 84 40 - 150 11 30 1,2-Dibromoethane (EDB) ND 45.0 49.8 ug/Kg 111 65 - 140 15 25 1,2-Dichlorobenzene ND 45.0 46.0 ug/Kg 102 70 - 130 13 25 1,2-Dichloroethane ND 45.0 47.0 ug/Kg 104 60 - 150 12 25 1,2-Dichloropropane ND 45.0 48.4 ug/Kg 108 65 - 130 12 20 1,3,5-Trimethylbenzene ND 45.0 41.2 ug/Kg 92 65 - 135 10 25 1,3-Dichlorobenzene ND 45.0 44.3 ug/Kg 99 70 - 130 12 25 1,3-Dichloropropane ND 45.0 43.1 ug/Kg 96 65 - 140 14 25 1,4-Dichlorobenzene ND 45.0 44.6 ug/Kg 99 70 - 130 13 25 2,2-Dichloropropane ND 45.0 40.2 ug/Kg 89 65 - 150 13 25 2-Chlorotoluene ND 45.0 41.3 ug/Kg 92 60 - 135 12 25
4-Chlorotoluene ND 45.0 43.7 ug/Kg 97 65 - 135 12 25
Benzene ND 45.0 44.8 ug/Kg 100 65 - 130 10 20
Bromobenzene ND 45.0 46.9 ug/Kg 104 65 - 140 15 25
Bromochloromethane ND 45.0 47.4 ug/Kg 105 65 - 145 12 25 Bromodichloromethane ND 45.0 48.2 ug/Kg 107 65 - 145 10 20 Bromoform ND 45.0 51.0 ug/Kg 113 50 - 145 13 30
Bromomethane ND 45.0 37.2 ug/Kg 83 60 - 155 8 25
Carbon tetrachloride ND 45.0 42.3 ug/Kg 94 60 - 145 10 25 Chlorobenzene ND 45.0 44.7 ug/Kg 99 70 - 130 13 25
Chloroethane ND 45.0 38.0 ug/Kg 84 60 - 150 7 25
Chloroform ND 45.0 46.5 ug/Kg 103 65 - 135 11 20
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152557-D-2-A MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342769 Prep Batch: 342782
Chloromethane ND 45.0 37.4 ug/Kg 83 40 - 145 6 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
cis-1,2-Dichloroethene ND 45.0 44.5 ug/Kg 99 65 - 135 13 25 cis-1,3-Dichloropropene ND 45.0 50.8 ug/Kg 113 70 - 135 15 25 Dibromochloromethane ND 45.0 48.2 ug/Kg 107 60 - 145 14 25 Dibromomethane ND 45.0 46.2 ug/Kg 103 65 - 140 12 25
Dichlorodifluoromethane ND 45.0 32.2 ug/Kg 72 30 - 160 9 35 Isopropyl Ether (DIPE) ND 45.0 52.0 ug/Kg 116 60 - 150 11 25 Ethanol ND 1800 1680 ug/Kg 94 30 - 165 21 40
Ethyl-t-butyl ether (ETBE) ND 45.0 52.2 ug/Kg 116 60 - 145 12 30 Ethylbenzene ND 45.0 42.1 ug/Kg 94 70 - 135 12 25
Hexachlorobutadiene ND 45.0 40.8 ug/Kg 91 50 - 145 14 35 Isopropylbenzene ND 45.0 42.2 ug/Kg 94 70 - 145 12 25
m,p-Xylene ND 45.0 45.1 ug/Kg 100 70 - 130 11 25
Methylene Chloride ND 45.0 47.1 ug/Kg 105 55 - 145 12 25 Methyl-t-Butyl Ether (MTBE) ND 45.0 50.6 ug/Kg 113 55 - 155 12 35 Naphthalene ND 45.0 46.0 ug/Kg 102 40 - 150 13 40
n-Butylbenzene ND 45.0 39.5 ug/Kg 88 55 - 145 11 30
N-Propylbenzene ND 45.0 39.6 ug/Kg 88 65 - 140 12 25
o-Xylene ND 45.0 45.8 ug/Kg 102 65 - 130 12 25
sec-Butylbenzene ND 45.0 38.7 ug/Kg 86 60 - 135 11 25
Styrene ND 45.0 48.5 ug/Kg 108 70 - 140 13 25
Tert-amyl-methyl ether (TAME) ND 45.0 53.2 ug/Kg 118 60 - 150 12 25 tert-Butyl alcohol (TBA) ND 450 428 ug/Kg 95 65 - 145 6 30 tert-Butylbenzene ND 45.0 40.5 ug/Kg 90 60 - 140 12 25
Tetrachloroethene ND 45.0 43.8 ug/Kg 97 65 - 135 13 25
Toluene ND 45.0 43.2 ug/Kg 96 70 - 130 13 20
trans-1,2-Dichloroethene ND 45.0 44.8 ug/Kg 100 70 - 135 13 25 trans-1,3-Dichloropropene ND 45.0 50.4 ug/Kg 112 60 - 145 14 25 Trichloroethene ND 45.0 40.2 ug/Kg 89 65 - 140 11 25
Trichlorofluoromethane ND 45.0 38.8 ug/Kg 86 55 - 155 10 25 Vinyl chloride ND 45.0 36.9 ug/Kg 82 55 - 140 10 30
p-Isopropyltoluene ND 45.0 39.6 ug/Kg 88 60 - 140 10 25 Toluene-d8 (Surr) 79 - 123
Surrogate
107

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 106 79 - 120
Dibromofluoromethane (Surr) 114 60 - 120
Lab Sample ID: MB 440-342846/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342846/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
RL MDL
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/16/16 09:55 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/16/16 09:55 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Benzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Bromoform ND 5.0 2.0 ug/Kg 07/16/16 09:55 1
Bromomethane ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Chloroethane ND 5.0 2.0 ug/Kg 07/16/16 09:55 1
Chloroform ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Chloromethane ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/16/16 09:55 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 Ethanol ND 300 100 ug/Kg 07/16/16 09:55 1
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 Ethylbenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/16/16 09:55 1
Methylene Chloride ND 20 5.0 ug/Kg 07/16/16 09:55 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 Naphthalene ND 5.0 2.0 ug/Kg 07/16/16 09:55 1
n-Butylbenzene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
o-Xylene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342846/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
RL MDL
Styrene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/16/16 09:55 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Toluene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/16/16 09:55 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/16/16 09:55 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/16/16 09:55 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/16/16 09:55 1
Toluene-d8 (Surr) 108 79 - 123 07/16/16 09:55 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 79 - 120 07/16/16 09:55 1 Dibromofluoromethane (Surr) 104 60 - 120 07/16/16 09:55 1 Lab Sample ID: LCS 440-342846/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
1,1,1,2-Tetrachloroethane 50.0 46.0 ug/Kg 92 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 50.0 41.6 ug/Kg 83 65 - 135
1,1,2,2-Tetrachloroethane 50.0 45.2 ug/Kg 90 55 - 140
1,1,2-Trichloroethane 50.0 43.8 ug/Kg 88 65 - 135
1,1-Dichloroethane 50.0 41.8 ug/Kg 84 70 - 130
1,1-Dichloroethene 50.0 45.3 ug/Kg 91 70 - 125
1,1-Dichloropropene 50.0 45.2 ug/Kg 90 70 - 130
1,2,3-Trichlorobenzene 50.0 51.3 ug/Kg 103 60 - 130
1,2,3-Trichloropropane 50.0 44.4 ug/Kg 89 60 - 135
1,2,4-Trichlorobenzene 50.0 52.4 ug/Kg 105 70 - 135
1,2,4-Trimethylbenzene 50.0 45.4 ug/Kg 91 70 - 125
1,2-Dibromo-3-Chloropropane 50.0 44.5 ug/Kg 89 50 - 135 1,2-Dibromoethane (EDB) 50.0 44.2 ug/Kg 88 70 - 130
1,2-Dichlorobenzene 50.0 46.7 ug/Kg 93 75 - 120
1,2-Dichloroethane 50.0 42.2 ug/Kg 84 60 - 140
1,2-Dichloropropane 50.0 47.6 ug/Kg 95 70 - 130
1,3,5-Trimethylbenzene 50.0 44.9 ug/Kg 90 70 - 125
1,3-Dichlorobenzene 50.0 45.4 ug/Kg 91 75 - 125
1,3-Dichloropropane 50.0 45.0 ug/Kg 90 70 - 125
1,4-Dichlorobenzene 50.0 46.9 ug/Kg 94 75 - 120
2,2-Dichloropropane 50.0 50.4 ug/Kg 101 60 - 145
2-Chlorotoluene 50.0 41.4 ug/Kg 83 70 - 125
4-Chlorotoluene 50.0 43.4 ug/Kg 87 75 - 125
Benzene 50.0 44.5 ug/Kg 89 65 - 120
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342846/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
Bromobenzene 50.0 46.7 ug/Kg 93 75 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Bromochloromethane 50.0 48.7 ug/Kg 97 70 - 135
Bromodichloromethane 50.0 42.1 ug/Kg 84 70 - 135
Bromoform 50.0 44.9 ug/Kg 90 55 - 135
Bromomethane 50.0 56.0 ug/Kg 112 60 - 145
Carbon tetrachloride 50.0 43.9 ug/Kg 88 65 - 140
Chlorobenzene 50.0 43.2 ug/Kg 86 75 - 120
Chloroethane 50.0 60.0 ug/Kg 120 60 - 140
Chloroform 50.0 45.4 ug/Kg 91 70 - 130
Chloromethane 50.0 52.5 ug/Kg 105 45 - 145
cis-1,2-Dichloroethene 50.0 47.7 ug/Kg 95 70 - 125
cis-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 75 - 125
Dibromochloromethane 50.0 46.4 ug/Kg 93 65 - 140
Dibromomethane 50.0 45.2 ug/Kg 90 70 - 130
Dichlorodifluoromethane 50.0 34.6 ug/Kg 69 35 - 160
Isopropyl Ether (DIPE) 50.0 46.1 ug/Kg 92 60 - 140
Ethanol 2000 2490 ug/Kg 125 35 - 160
Ethyl-t-butyl ether (ETBE) 50.0 46.4 ug/Kg 93 60 - 140
Ethylbenzene 50.0 42.4 ug/Kg 85 70 - 125
Hexachlorobutadiene 50.0 47.0 ug/Kg 94 60 - 135
Isopropylbenzene 50.0 45.0 ug/Kg 90 75 - 130
m,p-Xylene 50.0 46.7 ug/Kg 93 70 - 125
Methylene Chloride 50.0 44.4 ug/Kg 89 55 - 135
Methyl-t-Butyl Ether (MTBE) 50.0 47.0 ug/Kg 94 60 - 140 Naphthalene 50.0 52.3 ug/Kg 105 55 - 135
n-Butylbenzene 50.0 46.1 ug/Kg 92 70 - 130
N-Propylbenzene 50.0 44.0 ug/Kg 88 70 - 130
o-Xylene 50.0 44.8 ug/Kg 90 70 - 125
sec-Butylbenzene 50.0 44.0 ug/Kg 88 70 - 125
Styrene 50.0 46.1 ug/Kg 92 75 - 130
Tert-amyl-methyl ether (TAME) 50.0 48.1 ug/Kg 96 60 - 145 tert-Butyl alcohol (TBA) 500 480 ug/Kg 96 70 - 135
tert-Butylbenzene 50.0 46.4 ug/Kg 93 70 - 125
Tetrachloroethene 50.0 49.1 ug/Kg 98 70 - 125
Toluene 50.0 44.1 ug/Kg 88 70 - 125
trans-1,2-Dichloroethene 50.0 44.9 ug/Kg 90 70 - 125
trans-1,3-Dichloropropene 50.0 46.8 ug/Kg 94 70 - 135
Trichloroethene 50.0 45.9 ug/Kg 92 70 - 125
Trichlorofluoromethane 50.0 36.3 ug/Kg 73 60 - 145
Vinyl chloride 50.0 43.7 ug/Kg 87 55 - 135
p-Isopropyltoluene 50.0 45.2 ug/Kg 90 75 - 125
Toluene-d8 (Surr) 79 - 123
Surrogate
102

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 92 79 - 120
Dibromofluoromethane (Surr) 99 60 - 120
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-342846/7 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
1,1,1,2-Tetrachloroethane 50.0 47.9 ug/Kg 96 70 - 130 4 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane 50.0 45.0 ug/Kg 90 65 - 135 8 20
1,1,2,2-Tetrachloroethane 50.0 46.0 ug/Kg 92 55 - 140 2 30 1,1,2-Trichloroethane 50.0 44.9 ug/Kg 90 65 - 135 2 20
1,1-Dichloroethane 50.0 44.5 ug/Kg 89 70 - 130 6 20
1,1-Dichloroethene 50.0 50.2 ug/Kg 100 70 - 125 10 20
1,1-Dichloropropene 50.0 50.4 ug/Kg 101 70 - 130 11 20
1,2,3-Trichlorobenzene 50.0 50.8 ug/Kg 102 60 - 130 1 20 1,2,3-Trichloropropane 50.0 46.0 ug/Kg 92 60 - 135 4 25 1,2,4-Trichlorobenzene 50.0 53.7 ug/Kg 107 70 - 135 2 20 1,2,4-Trimethylbenzene 50.0 48.2 ug/Kg 96 70 - 125 6 20 1,2-Dibromo-3-Chloropropane 50.0 47.9 ug/Kg 96 50 - 135 7 30 1,2-Dibromoethane (EDB) 50.0 44.5 ug/Kg 89 70 - 130 1 20 1,2-Dichlorobenzene 50.0 45.8 ug/Kg 92 75 - 120 2 20
1,2-Dichloroethane 50.0 40.8 ug/Kg 82 60 - 140 3 20
1,2-Dichloropropane 50.0 47.6 ug/Kg 95 70 - 130 0 20
1,3,5-Trimethylbenzene 50.0 48.5 ug/Kg 97 70 - 125 8 20 1,3-Dichlorobenzene 50.0 46.8 ug/Kg 94 75 - 125 3 20
1,3-Dichloropropane 50.0 44.6 ug/Kg 89 70 - 125 1 20
1,4-Dichlorobenzene 50.0 48.1 ug/Kg 96 75 - 120 3 20
2,2-Dichloropropane 50.0 55.1 ug/Kg 110 60 - 145 9 20
2-Chlorotoluene 50.0 43.8 ug/Kg 88 70 - 125 6 20
4-Chlorotoluene 50.0 45.5 ug/Kg 91 75 - 125 5 20
Benzene 50.0 47.1 ug/Kg 94 65 - 120 6 20
Bromobenzene 50.0 48.0 ug/Kg 96 75 - 120 3 20
Bromochloromethane 50.0 47.9 ug/Kg 96 70 - 135 2 20
Bromodichloromethane 50.0 42.5 ug/Kg 85 70 - 135 1 20
Bromoform 50.0 46.0 ug/Kg 92 55 - 135 2 25
Bromomethane 50.0 56.8 ug/Kg 114 60 - 145 1 20
Carbon tetrachloride 50.0 48.3 ug/Kg 97 65 - 140 10 20
Chlorobenzene 50.0 46.2 ug/Kg 92 75 - 120 7 20
Chloroethane 50.0 60.4 ug/Kg 121 60 - 140 1 25
Chloroform 50.0 45.2 ug/Kg 90 70 - 130 1 20
Chloromethane 50.0 57.7 ug/Kg 115 45 - 145 10 25
cis-1,2-Dichloroethene 50.0 47.8 ug/Kg 96 70 - 125 0 20 cis-1,3-Dichloropropene 50.0 50.7 ug/Kg 101 75 - 125 0 20 Dibromochloromethane 50.0 46.3 ug/Kg 93 65 - 140 0 20
Dibromomethane 50.0 43.0 ug/Kg 86 70 - 130 5 20
Dichlorodifluoromethane 50.0 36.3 ug/Kg 73 35 - 160 5 30 Isopropyl Ether (DIPE) 50.0 45.9 ug/Kg 92 60 - 140 1 20 Ethanol 2000 2070 ug/Kg 104 35 - 160 18 30
Ethyl-t-butyl ether (ETBE) 50.0 45.9 ug/Kg 92 60 - 140 1 20 Ethylbenzene 50.0 47.1 ug/Kg 94 70 - 125 11 20
Hexachlorobutadiene 50.0 50.0 ug/Kg 100 60 - 135 6 20
Isopropylbenzene 50.0 49.4 ug/Kg 99 75 - 130 9 20
m,p-Xylene 50.0 52.6 ug/Kg 105 70 - 125 12 20
Methylene Chloride 50.0 46.4 ug/Kg 93 55 - 135 4 20
Methyl-t-Butyl Ether (MTBE) 50.0 46.8 ug/Kg 94 60 - 140 0 25 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-342846/7 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342846
Naphthalene 50.0 53.7 ug/Kg 107 55 - 135 3 25
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
n-Butylbenzene 50.0 48.7 ug/Kg 97 70 - 130 6 20
N-Propylbenzene 50.0 47.9 ug/Kg 96 70 - 130 8 20
o-Xylene 50.0 47.7 ug/Kg 95 70 - 125 6 20
sec-Butylbenzene 50.0 47.8 ug/Kg 96 70 - 125 8 20
Styrene 50.0 48.7 ug/Kg 97 75 - 130 6 20
Tert-amyl-methyl ether (TAME) 50.0 48.1 ug/Kg 96 60 - 145 0 20 tert-Butyl alcohol (TBA) 500 503 ug/Kg 101 70 - 135 5 20 tert-Butylbenzene 50.0 49.9 ug/Kg 100 70 - 125 7 20
Tetrachloroethene 50.0 54.3 ug/Kg 109 70 - 125 10 20
Toluene 50.0 47.6 ug/Kg 95 70 - 125 8 20
trans-1,2-Dichloroethene 50.0 49.8 ug/Kg 100 70 - 125 10 20 trans-1,3-Dichloropropene 50.0 48.6 ug/Kg 97 70 - 135 4 20 Trichloroethene 50.0 48.1 ug/Kg 96 70 - 125 5 20
Trichlorofluoromethane 50.0 39.6 ug/Kg 79 60 - 145 9 25 Vinyl chloride 50.0 46.4 ug/Kg 93 55 - 135 6 25
p-Isopropyltoluene 50.0 48.4 ug/Kg 97 75 - 125 7 20
Toluene-d8 (Surr) 79 - 123
Surrogate
105

LCSD LCSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 93 79 - 120
Dibromofluoromethane (Surr) 95 60 - 120
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS Lab Sample ID: MB 440-342266/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342266
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 0.10 0.070 mg/Kg 07/14/16 08:20 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 102 60 - 120 07/14/16 08:20 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 79 - 120 07/14/16 08:20 1 Toluene-d8 (Surr) 106 79 - 123 07/14/16 08:20 1
Lab Sample ID: LCS 440-342266/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342266
Volatile Fuel Hydrocarbons
(C4-C12)

1.00 0.768 mg/Kg 77 60 - 135
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
101

LCS LCS
%Recovery Qualifier Limits
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCS 440-342266/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342266
4-Bromofluorobenzene (Surr) 79 - 120
Surrogate
101

LCS LCS
%Recovery Qualifier Limits
Toluene-d8 (Surr) 106 79 - 123
Lab Sample ID: 440-152537-A-3 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342266
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3.44 3.41 mg/Kg 99 55 - 140
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
102
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 79 - 120
Toluene-d8 (Surr) 106 79 - 123
Lab Sample ID: 440-152537-A-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342266
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3.42 3.29 mg/Kg 96 55 - 140 4 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 60 - 120
Surrogate
104

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 79 - 120
Toluene-d8 (Surr) 105 79 - 123
Lab Sample ID: MB 440-342464/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342464
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 0.10 0.070 mg/Kg 07/14/16 19:21 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 108 60 - 120 07/14/16 19:21 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 79 - 120 07/14/16 19:21 1 Toluene-d8 (Surr) 102 79 - 123 07/14/16 19:21 1
Lab Sample ID: LCS 440-342464/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342464
Volatile Fuel Hydrocarbons
(C4-C12)

1.00 0.763 mg/Kg 76 60 - 135
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
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Dibromofluoromethane (Surr) 60 - 120
Surrogate
105

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 101 79 - 120
Toluene-d8 (Surr) 105 79 - 123
Lab Sample ID: 440-152462-2 MS Client Sample ID: AEC-5-10' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342464
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3.46 3.60 mg/Kg 104 55 - 140
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
106
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 79 - 120
Toluene-d8 (Surr) 107 79 - 123
Lab Sample ID: 440-152462-2 MSD Client Sample ID: AEC-5-10' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342464
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3.46 3.73 mg/Kg 108 55 - 140 3 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 60 - 120
Surrogate
109

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 100 79 - 120
Toluene-d8 (Surr) 105 79 - 123
Lab Sample ID: MB 440-342770/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342770
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 100 70 ug/Kg 07/15/16 18:55 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 112 60 - 120 07/15/16 18:55 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 79 - 120 07/15/16 18:55 1 Toluene-d8 (Surr) 110 79 - 123 07/15/16 18:55 1
Lab Sample ID: LCS 440-342770/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342770
Volatile Fuel Hydrocarbons
(C4-C12)
1000 808 ug/Kg 81 60 - 135
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
111

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 107 79 - 120
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCS 440-342770/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342770
Toluene-d8 (Surr) 79 - 123
Surrogate
108

LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 440-152557-B-2-B MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342770 Prep Batch: 342782
Volatile Fuel Hydrocarbons
(C4-C12)
ND 2840 2500 ug/Kg 88 55 - 140
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
113
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 103 79 - 120
Toluene-d8 (Surr) 105 79 - 123
Lab Sample ID: 440-152557-D-2-A MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342770 Prep Batch: 342782
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3100 2760 ug/Kg 89 55 - 140 10 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 60 - 120
Surrogate
114

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 106 79 - 120
Toluene-d8 (Surr) 107 79 - 123
Lab Sample ID: MB 440-342847/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342847
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 100 70 ug/Kg 07/16/16 09:55 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 104 60 - 120 07/16/16 09:55 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 79 - 120 07/16/16 09:55 1 Toluene-d8 (Surr) 108 79 - 123 07/16/16 09:55 1
Lab Sample ID: LCS 440-342847/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342847
Volatile Fuel Hydrocarbons
(C4-C12)
1000 899 ug/Kg 90 60 - 135
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCS 440-342847/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342847
Dibromofluoromethane (Surr) 60 - 120
Surrogate
97 LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 95 79 - 120
Toluene-d8 (Surr) 104 79 - 123
Lab Sample ID: LCSD 440-342847/8 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342847
Volatile Fuel Hydrocarbons
(C4-C12)
1000 882 ug/Kg 88 60 - 135 2 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 60 - 120
Surrogate
95 LCSD LCSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 93 79 - 120
Toluene-d8 (Surr) 105 79 - 123
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) Lab Sample ID: MB 440-342338/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342338
RL MDL
Acenaphthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Benzo[a]anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Benzo[a]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Benzo[b]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Benzo[g,h,i]perylene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Benzo[k]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Chrysene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Dibenz(a,h)anthracene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Fluorene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Indeno[1,2,3-cd]pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Naphthalene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Phenanthrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1 Pyrene ND 30 4.0 ug/Kg 07/14/16 09:28 07/15/16 11:30 1
2-Fluorobiphenyl (Surr) 62 39 - 111 07/15/16 11:30 1
MB MB
Surrogate
07/14/16 09:28
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Nitrobenzene-d5 60 41 - 119 07/14/16 09:28 07/15/16 11:30 1 Terphenyl-d14 74 43 - 150 07/14/16 09:28 07/15/16 11:30 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Lab Sample ID: LCS 440-342338/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342338
Acenaphthene 66.7 49.8 ug/Kg 75 53 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acenaphthylene 66.7 50.3 ug/Kg 75 54 - 120
Anthracene 66.7 48.0 ug/Kg 72 53 - 120
Benzo[a]anthracene 66.7 53.3 ug/Kg 80 56 - 120
Benzo[a]pyrene 66.7 52.1 ug/Kg 78 53 - 120
Benzo[b]fluoranthene 66.7 53.5 ug/Kg 80 53 - 120
Benzo[g,h,i]perylene 66.7 76.5 ug/Kg 115 51 - 150
Benzo[k]fluoranthene 66.7 54.3 ug/Kg 81 53 - 124
Chrysene 66.7 53.5 ug/Kg 80 56 - 120
Dibenz(a,h)anthracene 66.7 55.7 ug/Kg 84 51 - 131
Fluoranthene 66.7 50.5 ug/Kg 76 57 - 120
Fluorene 66.7 50.5 ug/Kg 76 54 - 120
Indeno[1,2,3-cd]pyrene 66.7 58.2 ug/Kg 87 50 - 137
Naphthalene 66.7 49.0 ug/Kg 74 49 - 120
Phenanthrene 66.7 49.2 ug/Kg 74 55 - 120
Pyrene 66.7 51.0 ug/Kg 76 56 - 121
2-Fluorobiphenyl (Surr) 39 - 111
Surrogate
72 LCS LCS
%Recovery Qualifier Limits
Nitrobenzene-d5 70 41 - 119
Terphenyl-d14 83 43 - 150
Lab Sample ID: 440-152462-1 MS Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342338
Acenaphthene ND 66.0 43.5 ug/Kg 66 45 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Acenaphthylene ND 66.0 43.6 ug/Kg 66 45 - 120
Anthracene ND 66.0 41.5 ug/Kg 63 55 - 120
Benzo[a]anthracene ND 66.0 43.2 ug/Kg 65 50 - 120
Benzo[a]pyrene ND 66.0 40.8 ug/Kg 62 45 - 125
Benzo[b]fluoranthene ND 66.0 44.1 ug/Kg 67 45 - 125
Benzo[g,h,i]perylene ND 66.0 54.4 ug/Kg 82 25 - 130
Benzo[k]fluoranthene ND 66.0 42.3 ug/Kg 64 45 - 125
Chrysene ND 66.0 43.5 ug/Kg 66 55 - 120
Dibenz(a,h)anthracene ND 66.0 40.7 ug/Kg 62 25 - 135
Fluoranthene ND 66.0 44.4 ug/Kg 67 45 - 120
Fluorene ND 66.0 44.7 ug/Kg 68 50 - 120
Indeno[1,2,3-cd]pyrene ND 66.0 42.7 ug/Kg 65 20 - 130
Naphthalene ND 66.0 43.2 ug/Kg 65 40 - 120
Phenanthrene ND 66.0 43.4 ug/Kg 66 50 - 120
Pyrene ND 66.0 43.8 ug/Kg 66 40 - 125
2-Fluorobiphenyl (Surr) 39 - 111
Surrogate
63 MS MS
%Recovery Qualifier Limits
Nitrobenzene-d5 63 41 - 119
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Lab Sample ID: 440-152462-1 MS Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342338
Terphenyl-d14 43 - 150
Surrogate
68 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 440-152462-1 MSD Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342338
Acenaphthene ND 65.7 44.8 ug/Kg 68 45 - 120 3 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Acenaphthylene ND 65.7 44.8 ug/Kg 68 45 - 120 3 20
Anthracene ND 65.7 43.2 ug/Kg 66 55 - 120 4 25
Benzo[a]anthracene ND 65.7 45.0 ug/Kg 68 50 - 120 4 25
Benzo[a]pyrene ND 65.7 43.5 ug/Kg 66 45 - 125 6 25
Benzo[b]fluoranthene ND 65.7 45.3 ug/Kg 69 45 - 125 3 30 Benzo[g,h,i]perylene ND 65.7 58.1 ug/Kg 89 25 - 130 7 30 Benzo[k]fluoranthene ND 65.7 46.2 ug/Kg 70 45 - 125 9 30 Chrysene ND 65.7 45.5 ug/Kg 69 55 - 120 4 25
Dibenz(a,h)anthracene ND 65.7 43.0 ug/Kg 65 25 - 135 5 30 Fluoranthene ND 65.7 46.2 ug/Kg 70 45 - 120 4 25
Fluorene ND 65.7 46.8 ug/Kg 71 50 - 120 5 25
Indeno[1,2,3-cd]pyrene ND 65.7 45.0 ug/Kg 68 20 - 130 5 30 Naphthalene ND 65.7 43.8 ug/Kg 67 40 - 120 1 25
Phenanthrene ND 65.7 45.1 ug/Kg 69 50 - 120 4 25
Pyrene ND 65.7 46.1 ug/Kg 70 40 - 125 5 30
2-Fluorobiphenyl (Surr) 39 - 111
Surrogate
63 MSD MSD
%Recovery Qualifier Limits
Nitrobenzene-d5 63 41 - 119
Terphenyl-d14 72 43 - 150
Method: 8015B - Diesel Range Organics (DRO) (GC)
Lab Sample ID: MB 440-342178/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342359 Prep Batch: 342178
RL MDL
C13-C22 ND 5.0 2.5 mg/Kg 07/13/16 18:24 07/14/16 10:35 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 5.0 2.5 mg/Kg 07/13/16 18:24 07/14/16 10:35 1 n-Octacosane 90 40 - 140 07/14/16 10:35 1
MB MB
Surrogate
07/13/16 18:24
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued) Lab Sample ID: LCS 440-342178/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342359 Prep Batch: 342178
C10-C28 66.7 52.3 mg/Kg 78 45 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
n-Octacosane 40 - 140
Surrogate
90 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 440-152462-1 MS Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342359 Prep Batch: 342178
C10-C28 ND 139 64.7 mg/Kg 47 40 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
n-Octacosane 40 - 140
Surrogate
45 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 440-152462-1 MSD Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342359 Prep Batch: 342178
C10-C28 ND 134 61.2 mg/Kg 46 40 - 120 6 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
n-Octacosane 40 - 140
Surrogate
42 MSD MSD
%Recovery Qualifier Limits
Lab Sample ID: MB 440-343307/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343350 Prep Batch: 343307
RL MDL
C13-C22 ND 5.0 2.5 mg/Kg 07/19/16 08:02 07/19/16 20:20 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 5.0 2.5 mg/Kg 07/19/16 08:02 07/19/16 20:20 1 n-Octacosane 81 40 - 140 07/19/16 20:20 1
MB MB
Surrogate
07/19/16 08:02
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Lab Sample ID: LCS 440-343307/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343350 Prep Batch: 343307
C10-C28 66.7 48.2 mg/Kg 72 45 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
n-Octacosane 40 - 140
Surrogate
79 LCS LCS
%Recovery Qualifier Limits
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued) Lab Sample ID: 440-152753-A-1-C MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343450 Prep Batch: 343307
C10-C28 38 F1 66.5 54.9 F1 mg/Kg 26 40 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
n-Octacosane 40 - 140
Surrogate
76 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 440-152753-A-1-D MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343450 Prep Batch: 343307
C10-C28 38 F1 66.6 53.4 F1 mg/Kg 24 40 - 120 3 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
n-Octacosane 40 - 140
Surrogate
79 MSD MSD
%Recovery Qualifier Limits
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Lab Sample ID: MB 440-342185/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
RL MDL
Aroclor 1016 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1232 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1242 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1248 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1254 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1260 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 DCB Decachlorobiphenyl (Surr) 88 45 - 120 07/15/16 13:26 1 MB MB
Surrogate
07/13/16 18:43
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Lab Sample ID: LCS 440-342185/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
Aroclor 1016 267 237 ug/Kg 89 65 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Aroclor 1260 267 240 ug/Kg 90 65 - 115
DCB Decachlorobiphenyl (Surr) 45 - 120
Surrogate
92 LCS LCS
%Recovery Qualifier Limits
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) Lab Sample ID: 440-152462-1 MS Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
Aroclor 1016 ND 539 448 ug/Kg 83 50 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Aroclor 1260 ND 539 453 ug/Kg 84 50 - 125
DCB Decachlorobiphenyl (Surr) 45 - 120
Surrogate
82 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 440-152462-1 MSD Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
Aroclor 1016 ND 556 460 ug/Kg 83 50 - 120 3 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Aroclor 1260 ND 556 467 ug/Kg 84 50 - 125 3 30
DCB Decachlorobiphenyl (Surr) 45 - 120
Surrogate
82 MSD MSD
%Recovery Qualifier Limits
Method: 6020 - Metals (ICP/MS)
Lab Sample ID: MB 440-342294/1-A ^20 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342656 Prep Batch: 342294
RL MDL
Silver ND 0.49 0.099 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Barium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Beryllium ND 0.30 0.15 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Cadmium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Chromium ND 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Cobalt ND 0.49 0.21 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Copper ND 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Lead ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Molybdenum ND 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Nickel ND 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Selenium ND 0.99 0.20 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Thallium ND 0.49 0.25 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Vanadium ND 0.99 0.49 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Zinc ND 9.9 4.9 mg/Kg 07/14/16 08:05 07/15/16 09:29 20
Antimony ND 0.99 0.27 mg/Kg 07/14/16 08:05 07/15/16 09:29 20 Lab Sample ID: LCS 440-342294/2-A ^20 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342656 Prep Batch: 342294
Silver 24.8 23.7 mg/Kg 96 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 6020 - Metals (ICP/MS) (Continued)
Lab Sample ID: LCS 440-342294/2-A ^20 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342656 Prep Batch: 342294
Arsenic 49.5 46.9 mg/Kg 95 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Barium 49.5 48.4 mg/Kg 98 80 - 120
Beryllium 49.5 45.1 mg/Kg 91 80 - 120
Cadmium 49.5 47.2 mg/Kg 95 80 - 120
Chromium 49.5 47.4 mg/Kg 96 80 - 120
Cobalt 49.5 46.6 mg/Kg 94 80 - 120
Copper 49.5 46.6 mg/Kg 94 80 - 120
Lead 49.5 48.2 mg/Kg 97 80 - 120
Molybdenum 49.5 49.1 mg/Kg 99 80 - 120
Nickel 49.5 45.9 mg/Kg 93 80 - 120
Selenium 49.5 48.2 mg/Kg 97 80 - 120
Thallium 49.5 46.9 mg/Kg 95 80 - 120
Vanadium 49.5 46.9 mg/Kg 95 80 - 120
Zinc 49.5 46.5 mg/Kg 94 80 - 120
Antimony 49.5 49.3 mg/Kg 100 80 - 120
Lab Sample ID: 440-152462-1 MS Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342656 Prep Batch: 342294
Silver ND 24.9 24.0 mg/Kg 96 80 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic 4.5 49.8 51.8 mg/Kg 95 80 - 120
Barium 130 F1 49.8 169 mg/Kg 89 80 - 120
Beryllium 0.46 49.8 43.2 mg/Kg 86 80 - 120
Cadmium ND 49.8 48.2 mg/Kg 97 80 - 120
Chromium 18 F1 49.8 62.7 mg/Kg 90 80 - 120
Cobalt 7.1 F1 49.8 52.2 mg/Kg 91 80 - 120
Copper 18 F1 49.8 58.2 mg/Kg 80 80 - 120
Lead 5.5 49.8 55.4 mg/Kg 100 80 - 120
Molybdenum 0.77 J 49.8 50.8 mg/Kg 101 80 - 120
Nickel 13 F1 49.8 54.5 mg/Kg 83 80 - 120
Selenium 0.47 J 49.8 48.4 mg/Kg 96 80 - 120
Thallium ND 49.8 46.8 mg/Kg 94 80 - 120
Vanadium 35 49.8 84.3 mg/Kg 99 80 - 120
Zinc 49 F1 49.8 92.2 mg/Kg 86 80 - 120
Antimony 0.40 J F1 49.8 32.4 F1 mg/Kg 64 80 - 120
Lab Sample ID: 440-152462-1 MSD Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342656 Prep Batch: 342294
Silver ND 24.6 22.4 mg/Kg 91 80 - 120 7 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic 4.5 49.3 48.0 mg/Kg 88 80 - 120 8 20
Barium 130 F1 49.3 150 F1 mg/Kg 50 80 - 120 12 20
Beryllium 0.46 49.3 40.3 mg/Kg 81 80 - 120 7 20
Cadmium ND 49.3 44.9 mg/Kg 91 80 - 120 7 20
Chromium 18 F1 49.3 57.1 F1 mg/Kg 79 80 - 120 9 20
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 6020 - Metals (ICP/MS) (Continued)
Lab Sample ID: 440-152462-1 MSD Client Sample ID: AEC-5-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342656 Prep Batch: 342294
Cobalt 7.1 F1 49.3 45.8 F1 mg/Kg 79 80 - 120 13 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Copper 18 F1 49.3 53.0 F1 mg/Kg 70 80 - 120 9 20
Lead 5.5 49.3 50.5 mg/Kg 91 80 - 120 9 20
Molybdenum 0.77 J 49.3 47.2 mg/Kg 94 80 - 120 7 20
Nickel 13 F1 49.3 50.0 F1 mg/Kg 75 80 - 120 9 20
Selenium 0.47 J 49.3 45.1 mg/Kg 91 80 - 120 7 20
Thallium ND 49.3 43.3 mg/Kg 88 80 - 120 8 20
Vanadium 35 49.3 79.3 mg/Kg 90 80 - 120 6 20
Zinc 49 F1 49.3 83.9 F1 mg/Kg 70 80 - 120 9 20
Antimony 0.40 J F1 49.3 31.0 F1 mg/Kg 62 80 - 120 4 20
Method: 7471A - Mercury (CVAA)
Lab Sample ID: MB 440-342230/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342524 Prep Batch: 342230
RL MDL
Mercury ND 0.020 0.012 mg/Kg 07/13/16 23:32 07/14/16 19:49 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-342230/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342524 Prep Batch: 342230
Mercury 0.800 0.807 mg/Kg 101 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: 440-152165-G-1-F MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342524 Prep Batch: 342230
Mercury 0.015 J 0.784 0.798 mg/Kg 100 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 440-152165-G-1-G MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342524 Prep Batch: 342230
Mercury 0.015 J 0.800 0.820 mg/Kg 101 70 - 130 3 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Lab Sample ID: MB 440-342231/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342525 Prep Batch: 342231
RL MDL
Mercury ND 0.020 0.012 mg/Kg 07/13/16 23:38 07/14/16 21:04 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Method: 7471A - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 440-342231/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342525 Prep Batch: 342231
Mercury 0.800 0.865 mg/Kg 108 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: 440-152307-A-1-C MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342525 Prep Batch: 342231
Mercury ND 0.784 0.805 mg/Kg 103 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 440-152307-A-1-D MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342525 Prep Batch: 342231
Mercury ND 0.800 0.802 mg/Kg 100 70 - 130 0 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch

GC/MS VOA
Prep Batch: 342024
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-5 AEC-3-5' Total/NA Solid 5035
440-152462-6 AEC-3-10' Total/NA Solid 5035
440-152462-7 AEC-3-15' Total/NA Solid 5035
440-152462-8 AEC-3-20' Total/NA Solid 5035
440-152462-9 AEC-4-5' Total/NA Solid 5035
440-152462-10 AEC-4-10' Total/NA Solid 5035
440-152462-11 AEC-4-15' Total/NA Solid 5035
440-152462-12 AEC-4-20' Total/NA Solid 5035
Analysis Batch: 342265
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 8260B
MB 440-342265/4 Method Blank Total/NA Solid 8260B
LCS 440-342265/5 Lab Control Sample Total/NA Solid 8260B 440-152537-A-3 MS Matrix Spike Total/NA Solid 8260B
440-152537-A-3 MSD Matrix Spike Duplicate Total/NA Solid 8260B Analysis Batch: 342266
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152462-1 AEC-5-5' Total/NA
Solid 8260B/CA_LUFT
MS
MB 440-342266/4 Method Blank Total/NA
Solid 8260B/CA_LUFT
MS
LCS 440-342266/6 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
440-152537-A-3 MS Matrix Spike Total/NA
Solid 8260B/CA_LUFT
MS
440-152537-A-3 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 342463
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-2 AEC-5-10' Total/NA Solid 8260B
440-152462-3 AEC-5-15' Total/NA Solid 8260B
440-152462-4 AEC-5-20' Total/NA Solid 8260B
MB 440-342463/4 Method Blank Total/NA Solid 8260B
LCS 440-342463/5 Lab Control Sample Total/NA Solid 8260B 440-152462-2 MS AEC-5-10' Total/NA Solid 8260B
440-152462-2 MSD AEC-5-10' Total/NA Solid 8260B
Analysis Batch: 342464
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152462-2 AEC-5-10' Total/NA
Solid 8260B/CA_LUFT
MS
440-152462-3 AEC-5-15' Total/NA
Solid 8260B/CA_LUFT
MS
440-152462-4 AEC-5-20' Total/NA
Solid 8260B/CA_LUFT
MS
MB 440-342464/4 Method Blank Total/NA
Solid 8260B/CA_LUFT
MS
LCS 440-342464/6 Lab Control Sample Total/NA
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
GC/MS VOA (Continued)
Analysis Batch: 342464 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152462-2 MS AEC-5-10' Total/NA
Solid 8260B/CA_LUFT
MS
440-152462-2 MSD AEC-5-10' Total/NA
Analysis Batch: 342769
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-5 AEC-3-5' Total/NA Solid 8260B 342024
440-152462-6 AEC-3-10' Total/NA Solid 8260B 342024
440-152462-7 AEC-3-15' Total/NA Solid 8260B 342024
440-152462-8 AEC-3-20' Total/NA Solid 8260B 342024
440-152462-9 AEC-4-5' Total/NA Solid 8260B 342024
440-152462-10 AEC-4-10' Total/NA Solid 8260B 342024
440-152462-11 AEC-4-15' Total/NA Solid 8260B 342024
MB 440-342769/4 Method Blank Total/NA Solid 8260B
LCS 440-342769/5 Lab Control Sample Total/NA Solid 8260B 440-152557-B-2-B MS Matrix Spike Total/NA Solid 8260B 342782 440-152557-D-2-A MSD Matrix Spike Duplicate Total/NA Solid 8260B 342782 Analysis Batch: 342770
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152462-5 AEC-3-5' Total/NA 342024
Solid 8260B/CA_LUFT
MS
440-152462-6 AEC-3-10' Total/NA 342024
Solid 8260B/CA_LUFT
MS
440-152462-7 AEC-3-15' Total/NA 342024
Solid 8260B/CA_LUFT
MS
440-152462-8 AEC-3-20' Total/NA 342024
Solid 8260B/CA_LUFT
MS
440-152462-9 AEC-4-5' Total/NA 342024
Solid 8260B/CA_LUFT
MS
440-152462-10 AEC-4-10' Total/NA 342024
Solid 8260B/CA_LUFT
MS
440-152462-11 AEC-4-15' Total/NA 342024
Solid 8260B/CA_LUFT
MS
MB 440-342770/4 Method Blank Total/NA
Solid 8260B/CA_LUFT
MS
LCS 440-342770/6 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
440-152557-B-2-B MS Matrix Spike Total/NA 342782
Solid 8260B/CA_LUFT
MS
440-152557-D-2-A MSD Matrix Spike Duplicate Total/NA 342782 Prep Batch: 342782
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152557-B-2-B MS Matrix Spike Total/NA Solid 5035
440-152557-D-2-A MSD Matrix Spike Duplicate Total/NA Solid 5035 Analysis Batch: 342846
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-12 AEC-4-20' Total/NA Solid 8260B 342024
MB 440-342846/4 Method Blank Total/NA Solid 8260B
LCS 440-342846/5 Lab Control Sample Total/NA Solid 8260B TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
GC/MS VOA (Continued)
Analysis Batch: 342846 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCSD 440-342846/7 Lab Control Sample Dup Total/NA Solid 8260B Analysis Batch: 342847
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152462-12 AEC-4-20' Total/NA 342024
Solid 8260B/CA_LUFT
MS
MB 440-342847/4 Method Blank Total/NA
Solid 8260B/CA_LUFT
MS
LCS 440-342847/6 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
LCSD 440-342847/8 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 342338
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 3546
440-152462-2 AEC-5-10' Total/NA Solid 3546
440-152462-3 AEC-5-15' Total/NA Solid 3546
440-152462-4 AEC-5-20' Total/NA Solid 3546
440-152462-5 AEC-3-5' Total/NA Solid 3546
440-152462-6 AEC-3-10' Total/NA Solid 3546
440-152462-7 AEC-3-15' Total/NA Solid 3546
440-152462-8 AEC-3-20' Total/NA Solid 3546
440-152462-9 AEC-4-5' Total/NA Solid 3546
440-152462-10 AEC-4-10' Total/NA Solid 3546
440-152462-11 AEC-4-15' Total/NA Solid 3546
440-152462-12 AEC-4-20' Total/NA Solid 3546
MB 440-342338/1-A Method Blank Total/NA Solid 3546
LCS 440-342338/2-A Lab Control Sample Total/NA Solid 3546 440-152462-1 MS AEC-5-5' Total/NA Solid 3546
440-152462-1 MSD AEC-5-5' Total/NA Solid 3546
Analysis Batch: 342622
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 8270C SIM 342338
440-152462-2 AEC-5-10' Total/NA Solid 8270C SIM 342338
440-152462-3 AEC-5-15' Total/NA Solid 8270C SIM 342338
440-152462-4 AEC-5-20' Total/NA Solid 8270C SIM 342338
440-152462-5 AEC-3-5' Total/NA Solid 8270C SIM 342338
440-152462-6 AEC-3-10' Total/NA Solid 8270C SIM 342338
440-152462-7 AEC-3-15' Total/NA Solid 8270C SIM 342338
440-152462-8 AEC-3-20' Total/NA Solid 8270C SIM 342338
440-152462-9 AEC-4-5' Total/NA Solid 8270C SIM 342338
440-152462-10 AEC-4-10' Total/NA Solid 8270C SIM 342338 440-152462-11 AEC-4-15' Total/NA Solid 8270C SIM 342338 440-152462-12 AEC-4-20' Total/NA Solid 8270C SIM 342338 MB 440-342338/1-A Method Blank Total/NA Solid 8270C SIM 342338 LCS 440-342338/2-A Lab Control Sample Total/NA Solid 8270C SIM 342338 440-152462-1 MS AEC-5-5' Total/NA Solid 8270C SIM 342338 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
GC/MS Semi VOA (Continued)
Analysis Batch: 342622 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 MSD AEC-5-5' Total/NA Solid 8270C SIM 342338 GC Semi VOA
Prep Batch: 342178
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 3546
440-152462-2 AEC-5-10' Total/NA Solid 3546
440-152462-3 AEC-5-15' Total/NA Solid 3546
440-152462-4 AEC-5-20' Total/NA Solid 3546
440-152462-5 AEC-3-5' Total/NA Solid 3546
440-152462-6 AEC-3-10' Total/NA Solid 3546
440-152462-7 AEC-3-15' Total/NA Solid 3546
440-152462-8 AEC-3-20' Total/NA Solid 3546
440-152462-9 AEC-4-5' Total/NA Solid 3546
440-152462-10 AEC-4-10' Total/NA Solid 3546
440-152462-12 AEC-4-20' Total/NA Solid 3546
MB 440-342178/1-A Method Blank Total/NA Solid 3546
LCS 440-342178/2-A Lab Control Sample Total/NA Solid 3546 440-152462-1 MS AEC-5-5' Total/NA Solid 3546
440-152462-1 MSD AEC-5-5' Total/NA Solid 3546
Prep Batch: 342185
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 3546
440-152462-2 AEC-5-10' Total/NA Solid 3546
440-152462-3 AEC-5-15' Total/NA Solid 3546
440-152462-4 AEC-5-20' Total/NA Solid 3546
440-152462-5 AEC-3-5' Total/NA Solid 3546
440-152462-6 AEC-3-10' Total/NA Solid 3546
440-152462-7 AEC-3-15' Total/NA Solid 3546
440-152462-8 AEC-3-20' Total/NA Solid 3546
440-152462-9 AEC-4-5' Total/NA Solid 3546
440-152462-10 AEC-4-10' Total/NA Solid 3546
440-152462-11 AEC-4-15' Total/NA Solid 3546
440-152462-12 AEC-4-20' Total/NA Solid 3546
MB 440-342185/1-A Method Blank Total/NA Solid 3546
LCS 440-342185/2-A Lab Control Sample Total/NA Solid 3546 440-152462-1 MS AEC-5-5' Total/NA Solid 3546
440-152462-1 MSD AEC-5-5' Total/NA Solid 3546
Analysis Batch: 342359
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 8015B 342178
440-152462-3 AEC-5-15' Total/NA Solid 8015B 342178
440-152462-4 AEC-5-20' Total/NA Solid 8015B 342178
440-152462-7 AEC-3-15' Total/NA Solid 8015B 342178
440-152462-8 AEC-3-20' Total/NA Solid 8015B 342178
440-152462-9 AEC-4-5' Total/NA Solid 8015B 342178
440-152462-10 AEC-4-10' Total/NA Solid 8015B 342178
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
GC Semi VOA (Continued)
Analysis Batch: 342359 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-12 AEC-4-20' Total/NA Solid 8015B 342178
MB 440-342178/1-A Method Blank Total/NA Solid 8015B 342178 LCS 440-342178/2-A Lab Control Sample Total/NA Solid 8015B 342178 440-152462-1 MS AEC-5-5' Total/NA Solid 8015B 342178
440-152462-1 MSD AEC-5-5' Total/NA Solid 8015B 342178
Analysis Batch: 342361
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-2 AEC-5-10' Total/NA Solid 8015B 342178
440-152462-5 AEC-3-5' Total/NA Solid 8015B 342178
440-152462-6 AEC-3-10' Total/NA Solid 8015B 342178
Analysis Batch: 342640
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 8082 342185
440-152462-2 AEC-5-10' Total/NA Solid 8082 342185
440-152462-3 AEC-5-15' Total/NA Solid 8082 342185
440-152462-4 AEC-5-20' Total/NA Solid 8082 342185
440-152462-5 AEC-3-5' Total/NA Solid 8082 342185
440-152462-6 AEC-3-10' Total/NA Solid 8082 342185
440-152462-7 AEC-3-15' Total/NA Solid 8082 342185
440-152462-8 AEC-3-20' Total/NA Solid 8082 342185
440-152462-9 AEC-4-5' Total/NA Solid 8082 342185
440-152462-10 AEC-4-10' Total/NA Solid 8082 342185
440-152462-11 AEC-4-15' Total/NA Solid 8082 342185
440-152462-12 AEC-4-20' Total/NA Solid 8082 342185
MB 440-342185/1-A Method Blank Total/NA Solid 8082 342185 LCS 440-342185/2-A Lab Control Sample Total/NA Solid 8082 342185 440-152462-1 MS AEC-5-5' Total/NA Solid 8082 342185
440-152462-1 MSD AEC-5-5' Total/NA Solid 8082 342185
Prep Batch: 343307
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-11 AEC-4-15' Total/NA Solid 3546
MB 440-343307/1-A Method Blank Total/NA Solid 3546
LCS 440-343307/2-A Lab Control Sample Total/NA Solid 3546 440-152753-A-1-C MS Matrix Spike Total/NA Solid 3546
440-152753-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 3546 Analysis Batch: 343350
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch MB 440-343307/1-A Method Blank Total/NA Solid 8015B 343307 LCS 440-343307/2-A Lab Control Sample Total/NA Solid 8015B 343307 Analysis Batch: 343450
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152753-A-1-C MS Matrix Spike Total/NA Solid 8015B 343307 440-152753-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 8015B 343307 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
GC Semi VOA (Continued)
Analysis Batch: 343451
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-11 AEC-4-15' Total/NA Solid 8015B 343307
Metals
Prep Batch: 342230
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 7471A
440-152462-2 AEC-5-10' Total/NA Solid 7471A
440-152462-3 AEC-5-15' Total/NA Solid 7471A
440-152462-4 AEC-5-20' Total/NA Solid 7471A
440-152462-5 AEC-3-5' Total/NA Solid 7471A
440-152462-6 AEC-3-10' Total/NA Solid 7471A
440-152462-7 AEC-3-15' Total/NA Solid 7471A
MB 440-342230/1-A Method Blank Total/NA Solid 7471A
LCS 440-342230/2-A Lab Control Sample Total/NA Solid 7471A 440-152165-G-1-F MS Matrix Spike Total/NA Solid 7471A
440-152165-G-1-G MSD Matrix Spike Duplicate Total/NA Solid 7471A Prep Batch: 342231
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-8 AEC-3-20' Total/NA Solid 7471A
440-152462-9 AEC-4-5' Total/NA Solid 7471A
440-152462-10 AEC-4-10' Total/NA Solid 7471A
440-152462-11 AEC-4-15' Total/NA Solid 7471A
440-152462-12 AEC-4-20' Total/NA Solid 7471A
MB 440-342231/1-A Method Blank Total/NA Solid 7471A
LCS 440-342231/2-A Lab Control Sample Total/NA Solid 7471A 440-152307-A-1-C MS Matrix Spike Total/NA Solid 7471A
440-152307-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 7471A Prep Batch: 342294
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 3050B
440-152462-2 AEC-5-10' Total/NA Solid 3050B
440-152462-3 AEC-5-15' Total/NA Solid 3050B
440-152462-4 AEC-5-20' Total/NA Solid 3050B
440-152462-5 AEC-3-5' Total/NA Solid 3050B
440-152462-6 AEC-3-10' Total/NA Solid 3050B
440-152462-7 AEC-3-15' Total/NA Solid 3050B
440-152462-8 AEC-3-20' Total/NA Solid 3050B
440-152462-9 AEC-4-5' Total/NA Solid 3050B
440-152462-10 AEC-4-10' Total/NA Solid 3050B
440-152462-11 AEC-4-15' Total/NA Solid 3050B
440-152462-12 AEC-4-20' Total/NA Solid 3050B
MB 440-342294/1-A ^20 Method Blank Total/NA Solid 3050B LCS 440-342294/2-A ^20 Lab Control Sample Total/NA Solid 3050B 440-152462-1 MS AEC-5-5' Total/NA Solid 3050B
440-152462-1 MSD AEC-5-5' Total/NA Solid 3050B
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Metals (Continued)
Analysis Batch: 342524
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 7471A 342230
440-152462-2 AEC-5-10' Total/NA Solid 7471A 342230
440-152462-3 AEC-5-15' Total/NA Solid 7471A 342230
440-152462-4 AEC-5-20' Total/NA Solid 7471A 342230
440-152462-5 AEC-3-5' Total/NA Solid 7471A 342230
440-152462-6 AEC-3-10' Total/NA Solid 7471A 342230
440-152462-7 AEC-3-15' Total/NA Solid 7471A 342230
MB 440-342230/1-A Method Blank Total/NA Solid 7471A 342230 LCS 440-342230/2-A Lab Control Sample Total/NA Solid 7471A 342230 440-152165-G-1-F MS Matrix Spike Total/NA Solid 7471A 342230 440-152165-G-1-G MSD Matrix Spike Duplicate Total/NA Solid 7471A 342230 Analysis Batch: 342525
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-8 AEC-3-20' Total/NA Solid 7471A 342231
440-152462-9 AEC-4-5' Total/NA Solid 7471A 342231
440-152462-10 AEC-4-10' Total/NA Solid 7471A 342231
440-152462-11 AEC-4-15' Total/NA Solid 7471A 342231
440-152462-12 AEC-4-20' Total/NA Solid 7471A 342231
MB 440-342231/1-A Method Blank Total/NA Solid 7471A 342231 LCS 440-342231/2-A Lab Control Sample Total/NA Solid 7471A 342231 440-152307-A-1-C MS Matrix Spike Total/NA Solid 7471A 342231 440-152307-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 7471A 342231 Analysis Batch: 342656
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152462-1 AEC-5-5' Total/NA Solid 6020 342294
440-152462-2 AEC-5-10' Total/NA Solid 6020 342294
440-152462-3 AEC-5-15' Total/NA Solid 6020 342294
440-152462-4 AEC-5-20' Total/NA Solid 6020 342294
440-152462-5 AEC-3-5' Total/NA Solid 6020 342294
440-152462-6 AEC-3-10' Total/NA Solid 6020 342294
440-152462-7 AEC-3-15' Total/NA Solid 6020 342294
440-152462-8 AEC-3-20' Total/NA Solid 6020 342294
440-152462-9 AEC-4-5' Total/NA Solid 6020 342294
440-152462-10 AEC-4-10' Total/NA Solid 6020 342294
440-152462-11 AEC-4-15' Total/NA Solid 6020 342294
440-152462-12 AEC-4-20' Total/NA Solid 6020 342294
MB 440-342294/1-A ^20 Method Blank Total/NA Solid 6020 342294 LCS 440-342294/2-A ^20 Lab Control Sample Total/NA Solid 6020 342294 440-152462-1 MS AEC-5-5' Total/NA Solid 6020 342294
440-152462-1 MSD AEC-5-5' Total/NA Solid 6020 342294
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13 Definitions/Glossary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Qualifiers

GC/MS VOA
Qualifier Description
* ISTD response or retention time outside acceptable limits Qualifier
X Surrogate is outside control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier
GC Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

F1 MS and/or MSD Recovery is outside acceptance limits.

Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary
These commonly used abbreviations may or may not be present in this report. ¤ Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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13 Certification Summary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152462-1 Project/Site: Pumpkin Patch
Laboratory: TestAmerica Irvine
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date Alaska State Program 10 CA01531 06-30-17
Arizona State Program 9 AZ0671 10-13-16
California LA Cty Sanitation Districts 9 10256 01-31-17 * California State Program 9 CA ELAP 2706 06-30-18
Guam State Program 9 Cert. No. 12.002r 01-23-17
Hawaii State Program 9 N/A 01-29-17
Kansas NELAP Secondary AB 7 E-10420 07-31-16 *
Nevada State Program 9 CA015312016-2 07-31-16 *
New Mexico State Program 6 N/A 01-29-17
Northern Mariana Islands State Program 9 MP0002 01-29-17 Oregon NELAP 10 4028 01-29-17
USDA Federal P330-09-00080 07-08-18
Washington State Program 10 C900 09-03-16
TestAmerica Irvine
* Certification renewal pending - certification considered valid.

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13 Login Sample Receipt Checklist
Client: Advanced Environmental Concepts Inc Job Number: 440-152462-1 Login Number: 152462
Question Answer Comment
Creator: Soderblom, Tim
List Source: TestAmerica Irvine
List Number: 1
Radioactivity wasn't checked or is </= background as measured by a survey True meter.

The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? False Refer to Job Narrative for details.

There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4").

Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
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13 ANALYTICAL REPORT
TestAmerica Laboratories, Inc.

TestAmerica Irvine
17461 Derian Ave
Suite 100
Irvine, CA 92614-5817
Tel: (949)261-1022
TestAmerica Job ID: 440-152586-1
Client Project/Site: Pumpkin Patch
For:

Advanced Environmental Concepts Inc
220 E. Truxtun Ave.

Bakersfield, California 93305
Attn: Jonathan Buck
Authorized for release by:
7/25/2016 12:34:29 PM
Danielle Roberts, Senior Project Manager
(949)261-1022
[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2
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Client: Advanced Environmental Concepts Inc
Project/Site: Pumpkin Patch
TestAmerica Job ID: 440-152586-1

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TestAmerica Irvine
7/25/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 84 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85 1 2
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Lab Sample ID Client Sample ID Matrix Collected Received 440-152586-1 AEC-2-5' Solid 07/13/16 07:40 07/13/16 18:30 440-152586-2 AEC-2-10' Solid 07/13/16 07:45 07/13/16 18:30 440-152586-3 AEC-2-15' Solid 07/13/16 07:50 07/13/16 18:30 440-152586-4 AEC-2-20' Solid 07/13/16 07:58 07/13/16 18:30 440-152586-5 AEC-1-5' Solid 07/13/16 09:45 07/13/16 18:30 440-152586-6 AEC-4-W Water 07/13/16 11:30 07/13/16 18:30 440-152586-7 AEC-3-W Water 07/13/16 12:50 07/13/16 18:30 440-152586-8 AEC-5-W Water 07/13/16 14:00 07/13/16 18:30 TestAmerica Irvine

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13 Case Narrative
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Job ID: 440-152586-1
Laboratory: TestAmerica Irvine
Narrative
Job Narrative
440-152586-1
Comments
No additional comments.

Receipt
The samples were received on 7/13/2016 6:30 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperatures of the 2 coolers at receipt time were 2.6º C and 3.2º C.

Receipt Exceptions
The Field Sampler was not listed on the Chain of Custody.

GC/MS VOA
Method(s) 8260B/CA_LUFTMS: The following samples were collected in properly preserved vials for analysis of volatile organic compounds (VOCs). However, the pH of 6 was outside the required criteria when verified by the laboratory, and corrective action was not possible: AEC-4-W (440-152586-6).

The sample was analyzed within 7 days per EPA recommendation.

Method(s) 8260B/CA_LUFTMS: TBA-d9 internal standard (ISTD) response for the following sample was above control limits: AEC-5-W (440-152586-8). The sample was re-analyzed with concurring results, and the re-analysis been reported.

Method(s) 8260B: Internal standard (ISTD) response for the following sample(s) was outside of acceptance limits fro TBA-d9. This internal standard is associated with Ethanol and tert-Butyl alcohol (TBA): (440-152586-A-7 MSD). All recoveries were within limits for the MSD.

Method(s) 8260B: Internal standard (ISTD) response for the following sample was outside control limit: TBA-d9 is high AEC-5-W (440-152586-8). The sample was re-analyzed with concurring results. Matrix interference was confirmed.

Method(s) 8260B: The following samples were collected in properly preserved vials for analysis of volatile organic compounds (VOCs).

However, the pH of 6 was outside the required criteria when verified by the laboratory, and corrective action was not possible: AEC-4-W (440-152586-6).

The sample was analyzed within 7 days per EPA recommendation.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA
Method(s) 8270C SIM: The continuing calibration verification (CCV) associated with batch 440-342622 recovered above the upper control limit for Benzo[g,h,i]perylene. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

Method(s) 8270C SIM: The following sample required a dilution due to the nature of the sample matrix: AEC-1-5' (440-152586-5).

Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8270C SIM: Surrogate recovery for the following sample was outside control limits: AEC-2-15' (440-152586-3). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8270C SIM: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-342864 and analytical batch 440-343497. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Job ID: 440-152586-1 (Continued)
Laboratory: TestAmerica Irvine (Continued)
Method(s) 8270C SIM: The following sample was diluted due to the abundance of non-target analytes: AEC-1-5' (440-152586-5). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

HPLC/IC
Method(s) 300.0: Due to the high concentration of Sulfate, the matrix spike / matrix spike duplicate (MS/MSD) for analytical batch 440-342634 could not be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC Semi VOA
Method(s) 8015B: The following sample required a dilution due to the nature of the sample matrix: AEC-1-5' (440-152586-5). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8015B: The following sample required a dilution due to the nature of the sample matrix: AEC-2-20' (440-152586-4). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8015B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-343009 and analytical batch 440-343351. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.

Method(s) 8015B: The following sample required a dilution due to the nature of the sample matrix: AEC-3-W (440-152586-7). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8082: Surrogate recovery for the following samples was outside control limits: AEC-1-5' (440-152586-5). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8082: The following samples required a copper clean-up to reduce matrix interferences caused by sulfur: AEC-2-20' (440-152586-4), (LCS 440-342185/2-A), (MB 440-342185/1-A), (440-152462-A-1-F), (440-152462-A-1-D MS) and (440-152462-A-1-E MSD).

Method(s) 8082: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-343105 and analytical batch 440-344252.The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.(LCS 440-343105/4-A) No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals
Method(s) 200.7 Rev 4.4: The following sample was diluted due to the nature of the sample matrix: AEC-3-W (440-152586-7). Elevated reporting limits (RLs) are provided.

Method(s) 200.7 Rev 4.4: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision of Vanadium for preparation batch 440-342888 and analytical batch 440-343234 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) was within acceptance limits.

Method(s) 200.7 Rev 4.4: The initial calibration verification (ICV) result for batch 440-343712 was above the upper control limit for Molybdenum. Sample results were non-detects, and have been reported as qualified data.AEC-4-W (440-152586-6) and AEC-5-W TestAmerica Irvine Page 5 of 85 7/25/2016
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Job ID: 440-152586-1 (Continued)
Laboratory: TestAmerica Irvine (Continued)
(440-152586-8)
Method(s) 200.7 Rev 4.4: The following samples was diluted due to the nature of the sample matrix: AEC-4-W (440-152586-6) and AEC-5-W (440-152586-8). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep
Method(s) 3510C: Due to the matrix, the following sample could not be concentrated to the final method required volume: 2AEC-3-W (440-152586-7). The reporting limits (RLs) are elevated proportionately.

Method(s) 3546: The following samples was diluted due to the nature of the sample matrix: AEC-2-15' (440-152586-3) and AEC-2-20' (440-152586-4). Elevated reporting limits (RLs) are provided.

Method(s) 3546: AEC-2-20' (440-152586-4) Due to the matrix, the following sample could not be concentrated to the final method required volume: AEC-2-20' (440-152586-4). The reporting limits (RLs) are elevated proportionately.

Method(s) 3546: The following samples was diluted due to the nature of the sample matrix: AEC-2-10' (440-152586-2), AEC-2-15' (440-152586-3) and AEC-2-20' (440-152586-4). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-5' Lab Sample ID: 440-152586-1
Date Collected: 07/13/16 07:40 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 88 62 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 99 60 - 120 07/14/16 15:46 07/18/16 12:25 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 98 79 - 120 07/14/16 15:46 07/18/16 12:25 1 Toluene-d8 (Surr) 103 79 - 123 07/14/16 15:46 07/18/16 12:25 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,1,2,2-Tetrachloroethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,1,2-Trichloroethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,1-Dichloroethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,1-Dichloroethene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,1-Dichloropropene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2,3-Trichlorobenzene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2,3-Trichloropropane ND 8.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2,4-Trichlorobenzene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2,4-Trimethylbenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2-Dibromo-3-Chloropropane ND 4.4 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2-Dibromoethane (EDB) ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2-Dichlorobenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2-Dichloroethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,2-Dichloropropane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,3,5-Trimethylbenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,3-Dichlorobenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,3-Dichloropropane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 1,4-Dichlorobenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 2,2-Dichloropropane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 2-Chlorotoluene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 4-Chlorotoluene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Benzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Bromobenzene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Bromochloromethane ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Bromodichloromethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Bromoform ND 4.4 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Bromomethane ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Carbon tetrachloride ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Chlorobenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Chloroethane ND 4.4 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Chloroform ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Chloromethane ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 cis-1,2-Dichloroethene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 cis-1,3-Dichloropropene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Dibromochloromethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Dibromomethane ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Dichlorodifluoromethane ND 4.4 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Isopropyl Ether (DIPE) ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Ethanol ND 260 88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-5' Lab Sample ID: 440-152586-1
Date Collected: 07/13/16 07:40 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Hexachlorobutadiene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Isopropylbenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 m,p-Xylene ND 3.5 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Methylene Chloride ND 18 4.4 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Methyl-t-Butyl Ether (MTBE) ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Naphthalene ND 4.4 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 n-Butylbenzene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 N-Propylbenzene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 o-Xylene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 sec-Butylbenzene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Styrene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Tert-amyl-methyl ether (TAME) ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 tert-Butyl alcohol (TBA) ND 88 8.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 tert-Butylbenzene ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Tetrachloroethene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Toluene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 trans-1,2-Dichloroethene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 trans-1,3-Dichloropropene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Trichloroethene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Trichlorofluoromethane ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Vinyl chloride ND 4.4 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Xylenes, Total ND 3.5 1.8 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 p-Isopropyltoluene ND 1.8 0.88 ug/Kg 07/14/16 15:46 07/18/16 12:25 1 Toluene-d8 (Surr) 103 79 - 123 07/14/16 15:46 07/18/16 12:25 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 98 79 - 120 07/14/16 15:46 07/18/16 12:25 1 Dibromofluoromethane (Surr) 99 60 - 120 07/14/16 15:46 07/18/16 12:25 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Anthracene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Benzo[a]anthracene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Benzo[a]pyrene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Benzo[b]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Benzo[g,h,i]perylene ND F2 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Benzo[k]fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Chrysene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Dibenz(a,h)anthracene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Fluoranthene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Fluorene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Indeno[1,2,3-cd]pyrene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Naphthalene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Phenanthrene ND 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 Pyrene 5.5 J 29 3.9 ug/Kg 07/14/16 09:34 07/15/16 20:47 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-5' Lab Sample ID: 440-152586-1
Date Collected: 07/13/16 07:40 Matrix: Solid
Date Received: 07/13/16 18:30
2-Fluorobiphenyl (Surr) 66 39 - 111 07/14/16 09:34 07/15/16 20:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 61 41 - 119 07/14/16 09:34 07/15/16 20:47 1 Terphenyl-d14 98 43 - 150 07/14/16 09:34 07/15/16 20:47 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 3.0 J 5.0 2.5 mg/Kg 07/14/16 09:20 07/15/16 21:59 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 11 5.0 2.5 mg/Kg 07/14/16 09:20 07/15/16 21:59 1 n-Octacosane 84 40 - 140 07/14/16 09:20 07/15/16 21:59 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 Aroclor 1232 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 Aroclor 1242 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 Aroclor 1248 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 Aroclor 1254 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 Aroclor 1260 ND 49 17 ug/Kg 07/14/16 09:18 07/15/16 18:31 1 DCB Decachlorobiphenyl (Surr) 52 45 - 120 07/14/16 09:18 07/15/16 18:31 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 15 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Barium 90 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Beryllium 0.37 0.30 0.15 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Chromium 20 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Cobalt 7.4 0.50 0.21 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Copper 16 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Lead 6.4 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Molybdenum 0.64 J 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 22:55 20 Nickel 14 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Selenium 0.31 J 1.0 0.20 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Vanadium 36 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Zinc 53 10 5.0 mg/Kg 07/14/16 08:13 07/15/16 12:58 20
Antimony 0.30 J 1.0 0.27 mg/Kg 07/14/16 08:13 07/15/16 12:58 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.050 0.020 0.012 mg/Kg 07/14/16 21:26 07/15/16 00:23 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-10' Lab Sample ID: 440-152586-2 Date Collected: 07/13/16 07:45 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 85 59 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 95 60 - 120 07/14/16 15:46 07/18/16 12:56 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 79 - 120 07/14/16 15:46 07/18/16 12:56 1 Toluene-d8 (Surr) 106 79 - 123 07/14/16 15:46 07/18/16 12:56 1 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,1,2,2-Tetrachloroethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,1,2-Trichloroethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,1-Dichloroethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,1-Dichloroethene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,1-Dichloropropene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2,3-Trichlorobenzene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2,3-Trichloropropane ND 8.5 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2,4-Trichlorobenzene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2,4-Trimethylbenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2-Dibromo-3-Chloropropane ND 4.2 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2-Dibromoethane (EDB) ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2-Dichlorobenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2-Dichloroethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,2-Dichloropropane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,3,5-Trimethylbenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,3-Dichlorobenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,3-Dichloropropane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 1,4-Dichlorobenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 2,2-Dichloropropane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 2-Chlorotoluene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 4-Chlorotoluene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Benzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Bromobenzene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Bromochloromethane ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Bromodichloromethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Bromoform ND 4.2 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Bromomethane ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Carbon tetrachloride ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Chlorobenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Chloroethane ND 4.2 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Chloroform ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Chloromethane ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 cis-1,2-Dichloroethene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 cis-1,3-Dichloropropene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Dibromochloromethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Dibromomethane ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Dichlorodifluoromethane ND 4.2 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Isopropyl Ether (DIPE) ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Ethanol ND 250 85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 TestAmerica Irvine

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