Long Beach City Council
September 19, 2023

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-10' Lab Sample ID: 440-152586-2 Date Collected: 07/13/16 07:45 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Hexachlorobutadiene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Isopropylbenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 m,p-Xylene ND 3.4 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Methylene Chloride ND 17 4.2 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Methyl-t-Butyl Ether (MTBE) ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Naphthalene ND 4.2 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 n-Butylbenzene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 N-Propylbenzene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 o-Xylene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 sec-Butylbenzene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Styrene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Tert-amyl-methyl ether (TAME) ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 tert-Butyl alcohol (TBA) ND 85 8.5 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 tert-Butylbenzene ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Tetrachloroethene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Toluene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 trans-1,2-Dichloroethene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 trans-1,3-Dichloropropene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Trichloroethene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Trichlorofluoromethane ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Vinyl chloride ND 4.2 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Xylenes, Total ND 3.4 1.7 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 p-Isopropyltoluene ND 1.7 0.85 ug/Kg 07/14/16 15:46 07/18/16 12:56 1 Toluene-d8 (Surr) 106 79 - 123 07/14/16 15:46 07/18/16 12:56 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 79 - 120 07/14/16 15:46 07/18/16 12:56 1 Dibromofluoromethane (Surr) 95 60 - 120 07/14/16 15:46 07/18/16 12:56 1 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Anthracene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Benzo[a]anthracene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Benzo[a]pyrene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Benzo[b]fluoranthene 9.4 J 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Benzo[g,h,i]perylene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Benzo[k]fluoranthene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Chrysene 20 J 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Dibenz(a,h)anthracene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Fluoranthene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Fluorene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Indeno[1,2,3-cd]pyrene ND 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Naphthalene 14 J 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Phenanthrene 10 J 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 Pyrene 15 J 61 8.1 ug/Kg 07/14/16 09:34 07/15/16 22:09 1 TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-10' Lab Sample ID: 440-152586-2 Date Collected: 07/13/16 07:45 Matrix: Solid
Date Received: 07/13/16 18:30
2-Fluorobiphenyl (Surr) 72 39 - 111 07/14/16 09:34 07/15/16 22:09 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 56 41 - 119 07/14/16 09:34 07/15/16 22:09 1 Terphenyl-d14 104 43 - 150 07/14/16 09:34 07/15/16 22:09 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 3.5 J 5.0 2.5 mg/Kg 07/14/16 09:20 07/15/16 21:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 11 5.0 2.5 mg/Kg 07/14/16 09:20 07/15/16 21:38 1 n-Octacosane 57 40 - 140 07/14/16 09:20 07/15/16 21:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 Aroclor 1232 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 Aroclor 1242 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 Aroclor 1248 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 Aroclor 1254 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 Aroclor 1260 ND 110 36 ug/Kg 07/14/16 09:18 07/15/16 18:46 1 DCB Decachlorobiphenyl (Surr) 51 45 - 120 07/14/16 09:18 07/15/16 18:46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.7 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Barium 140 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Beryllium 0.75 0.30 0.15 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Chromium 32 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Cobalt 11 0.50 0.21 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Copper 34 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Lead 46 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Molybdenum 0.69 J 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 22:58 20 Nickel 40 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Selenium 0.61 J 1.0 0.20 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Vanadium 84 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Zinc 100 10 5.0 mg/Kg 07/14/16 08:13 07/15/16 13:01 20
Antimony 0.34 J 1.0 0.27 mg/Kg 07/14/16 08:13 07/15/16 13:01 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.043 0.020 0.012 mg/Kg 07/14/16 21:26 07/15/16 00:26 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-15' Lab Sample ID: 440-152586-3 Date Collected: 07/13/16 07:50 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
87000 14000 9900 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 94 55 - 140 07/14/16 14:51 07/18/16 12:16 100 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 65 - 140 07/14/16 14:51 07/18/16 12:16 100 Toluene-d8 (Surr) 111 60 - 140 07/14/16 14:51 07/18/16 12:16 100 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,1,2,2-Tetrachloroethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,1,2-Trichloroethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,1-Dichloroethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,1-Dichloroethene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,1-Dichloropropene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2,3-Trichlorobenzene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2,3-Trichloropropane ND 710 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2,4-Trichlorobenzene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2,4-Trimethylbenzene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2-Dibromo-3-Chloropropane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2-Dibromoethane (EDB) ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2-Dichlorobenzene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2-Dichloroethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,2-Dichloropropane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,3,5-Trimethylbenzene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,3-Dichlorobenzene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,3-Dichloropropane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 1,4-Dichlorobenzene 380 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 2,2-Dichloropropane ND 280 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 2-Chlorotoluene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 4-Chlorotoluene ND 350 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Benzene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Bromobenzene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Bromochloromethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Bromodichloromethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Bromoform ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Bromomethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Carbon tetrachloride ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Chlorobenzene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Chloroethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Chloroform ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Chloromethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 cis-1,2-Dichloroethene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 cis-1,3-Dichloropropene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Dibromochloromethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Dibromomethane ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Dichlorodifluoromethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Isopropyl Ether (DIPE) ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-15' Lab Sample ID: 440-152586-3 Date Collected: 07/13/16 07:50 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethanol ND 28000 11000 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethyl-t-butyl ether (ETBE) ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Ethylbenzene 420 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Hexachlorobutadiene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Isopropylbenzene 96 J 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 m,p-Xylene ND 280 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Methylene Chloride ND 1400 710 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Methyl-t-Butyl Ether (MTBE) ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Naphthalene 2300 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 n-Butylbenzene 350 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 N-Propylbenzene 200 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 o-Xylene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 sec-Butylbenzene 180 J 350 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Styrene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Tert-amyl-methyl ether (TAME) ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 tert-Butyl alcohol (TBA) ND 7100 3500 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 tert-Butylbenzene ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Tetrachloroethene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Toluene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 trans-1,2-Dichloroethene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 trans-1,3-Dichloropropene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Trichloroethene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Trichlorofluoromethane ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Vinyl chloride ND 350 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Xylenes, Total ND 280 140 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 p-Isopropyltoluene ND 140 71 ug/Kg 07/14/16 14:51 07/18/16 12:16 100 Toluene-d8 (Surr) 111 60 - 140 07/14/16 14:51 07/18/16 12:16 100 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 65 - 140 07/14/16 14:51 07/18/16 12:16 100 Dibromofluoromethane (Surr) 94 55 - 140 07/14/16 14:51 07/18/16 12:16 100 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene 92 J 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Anthracene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Benzo[a]anthracene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Benzo[a]pyrene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Benzo[b]fluoranthene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Benzo[g,h,i]perylene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Benzo[k]fluoranthene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Chrysene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Dibenz(a,h)anthracene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Fluoranthene 280 J 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Fluorene 150 J 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Indeno[1,2,3-cd]pyrene ND 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Naphthalene 1900 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Phenanthrene 330 J 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 Pyrene 200 J 660 88 ug/Kg 07/14/16 09:34 07/19/16 20:14 5 TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-15' Lab Sample ID: 440-152586-3 Date Collected: 07/13/16 07:50 Matrix: Solid
Date Received: 07/13/16 18:30
2-Fluorobiphenyl (Surr) 60 39 - 111 07/14/16 09:34 07/19/16 20:14 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 147 X 41 - 119 07/14/16 09:34 07/19/16 20:14 5 Terphenyl-d14 78 43 - 150 07/14/16 09:34 07/19/16 20:14 5 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 110 10 5.0 mg/Kg 07/14/16 09:20 07/15/16 22:20 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 700 10 5.0 mg/Kg 07/14/16 09:20 07/15/16 22:20 1 n-Octacosane 77 40 - 140 07/14/16 09:20 07/15/16 22:20 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 Aroclor 1232 ND 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 Aroclor 1242 ND 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 Aroclor 1248 ND 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 Aroclor 1254 ND 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 Aroclor 1260 76 J 99 34 ug/Kg 07/14/16 09:18 07/15/16 19:02 1 DCB Decachlorobiphenyl (Surr) 49 45 - 120 07/14/16 09:18 07/15/16 19:02 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.49 0.099 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 6.9 0.49 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Barium 160 0.49 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Beryllium ND 0.30 0.15 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Cadmium 0.26 J 0.49 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Chromium 18 0.99 0.49 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Cobalt 3.3 0.49 0.21 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Copper 31 0.99 0.49 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Lead 36 0.49 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Molybdenum 1.8 0.99 0.49 mg/Kg 07/14/16 08:13 07/15/16 23:00 20 Nickel 13 0.99 0.49 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Selenium ND 0.99 0.20 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Thallium ND 0.49 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Vanadium 3.5 0.99 0.49 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Zinc 250 9.9 4.9 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Antimony 0.63 J 0.99 0.27 mg/Kg 07/14/16 08:13 07/15/16 13:03 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.82 0.020 0.012 mg/Kg 07/14/16 21:26 07/15/16 00:34 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-20' Lab Sample ID: 440-152586-4 Date Collected: 07/13/16 07:58 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
84000 17000 12000 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 89 55 - 140 07/14/16 14:51 07/18/16 12:45 100 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 65 - 140 07/14/16 14:51 07/18/16 12:45 100 Toluene-d8 (Surr) 112 60 - 140 07/14/16 14:51 07/18/16 12:45 100 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,1,2,2-Tetrachloroethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,1,2-Trichloroethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,1-Dichloroethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,1-Dichloroethene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,1-Dichloropropene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2,3-Trichlorobenzene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2,3-Trichloropropane ND 830 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2,4-Trichlorobenzene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2,4-Trimethylbenzene 1200 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2-Dibromo-3-Chloropropane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2-Dibromoethane (EDB) ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2-Dichlorobenzene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2-Dichloroethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,2-Dichloropropane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,3,5-Trimethylbenzene 260 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,3-Dichlorobenzene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,3-Dichloropropane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 1,4-Dichlorobenzene 260 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 2,2-Dichloropropane ND 330 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 2-Chlorotoluene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 4-Chlorotoluene ND 410 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Benzene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Bromobenzene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Bromochloromethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Bromodichloromethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Bromoform ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Bromomethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Carbon tetrachloride ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Chlorobenzene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Chloroethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Chloroform ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Chloromethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 cis-1,2-Dichloroethene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 cis-1,3-Dichloropropene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Dibromochloromethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Dibromomethane ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Dichlorodifluoromethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Isopropyl Ether (DIPE) ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-20' Lab Sample ID: 440-152586-4 Date Collected: 07/13/16 07:58 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethanol ND 33000 12000 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethyl-t-butyl ether (ETBE) ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Ethylbenzene 450 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Hexachlorobutadiene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Isopropylbenzene 110 J 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 m,p-Xylene 240 J 330 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Methylene Chloride ND 1700 830 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Methyl-t-Butyl Ether (MTBE) ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Naphthalene 2600 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 n-Butylbenzene 280 J 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 N-Propylbenzene 100 J 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 o-Xylene 120 J 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 sec-Butylbenzene 120 J 410 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Styrene 130 J 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Tert-amyl-methyl ether (TAME) ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 tert-Butyl alcohol (TBA) ND 8300 4100 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 tert-Butylbenzene ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Tetrachloroethene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Toluene 620 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 trans-1,2-Dichloroethene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 trans-1,3-Dichloropropene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Trichloroethene ND 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Trichlorofluoromethane ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Vinyl chloride ND 410 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Xylenes, Total 360 330 170 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 p-Isopropyltoluene 700 170 83 ug/Kg 07/14/16 14:51 07/18/16 12:45 100 Toluene-d8 (Surr) 112 60 - 140 07/14/16 14:51 07/18/16 12:45 100 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 65 - 140 07/14/16 14:51 07/18/16 12:45 100 Dibromofluoromethane (Surr) 89 55 - 140 07/14/16 14:51 07/18/16 12:45 100 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Anthracene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Benzo[a]anthracene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Benzo[a]pyrene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Benzo[b]fluoranthene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Benzo[g,h,i]perylene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Benzo[k]fluoranthene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Chrysene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Dibenz(a,h)anthracene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Fluoranthene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Fluorene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Indeno[1,2,3-cd]pyrene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Naphthalene 1300 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Phenanthrene 250 J 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5 Pyrene ND 710 95 ug/Kg 07/14/16 09:34 07/19/16 20:35 5
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-20' Lab Sample ID: 440-152586-4 Date Collected: 07/13/16 07:58 Matrix: Solid
Date Received: 07/13/16 18:30
2-Fluorobiphenyl (Surr) 54 39 - 111 07/14/16 09:34 07/19/16 20:35 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 64 41 - 119 07/14/16 09:34 07/19/16 20:35 5 Terphenyl-d14 65 43 - 150 07/14/16 09:34 07/19/16 20:35 5 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 2000 200 100 mg/Kg 07/14/16 09:20 07/18/16 19:52 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 13000 200 100 mg/Kg 07/14/16 09:20 07/18/16 19:52 10 n-Octacosane 4039 X 40 - 140 07/14/16 09:20 07/18/16 19:52 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 550 230 79 ug/Kg 07/14/16 09:18 07/16/16 11:27 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 230 79 ug/Kg 07/14/16 09:18 07/16/16 11:27 1 Aroclor 1232 ND 230 79 ug/Kg 07/14/16 09:18 07/16/16 11:27 1 Aroclor 1242 ND 230 79 ug/Kg 07/14/16 09:18 07/16/16 11:27 1 Aroclor 1248 ND 230 79 ug/Kg 07/14/16 09:18 07/16/16 11:27 1 Aroclor 1254 340 230 79 ug/Kg 07/14/16 09:18 07/18/16 13:19 1 Aroclor 1260 300 230 79 ug/Kg 07/14/16 09:18 07/16/16 11:27 1 DCB Decachlorobiphenyl (Surr) 54 45 - 120 07/14/16 09:18 07/16/16 11:27 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 2.8 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Barium 39 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Beryllium ND 0.30 0.15 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Cadmium 0.37 J 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Chromium 61 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Cobalt 1.8 0.50 0.21 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Copper 14 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Lead 350 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Molybdenum 1.6 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 23:03 20 Nickel 4.8 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Selenium ND 1.0 0.20 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Vanadium 3.8 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Zinc 200 10 5.0 mg/Kg 07/14/16 08:13 07/15/16 13:06 20
Antimony 0.35 J 1.0 0.27 mg/Kg 07/14/16 08:13 07/15/16 13:06 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.38 0.020 0.012 mg/Kg 07/14/16 21:26 07/15/16 00:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-5' Lab Sample ID: 440-152586-5
Date Collected: 07/13/16 09:45 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
300000 27000 19000 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 89 55 - 140 07/14/16 14:51 07/18/16 13:15 200 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 97 65 - 140 07/14/16 14:51 07/18/16 13:15 200 Toluene-d8 (Surr) 113 60 - 140 07/14/16 14:51 07/18/16 13:15 200 Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,1,2,2-Tetrachloroethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,1,2-Trichloroethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,1-Dichloroethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,1-Dichloroethene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,1-Dichloropropene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2,3-Trichlorobenzene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2,3-Trichloropropane ND 1400 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2,4-Trichlorobenzene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2,4-Trimethylbenzene 5000 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2-Dibromo-3-Chloropropane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2-Dibromoethane (EDB) ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2-Dichlorobenzene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2-Dichloroethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,2-Dichloropropane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,3,5-Trimethylbenzene 1700 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,3-Dichlorobenzene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,3-Dichloropropane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 1,4-Dichlorobenzene 1300 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 2,2-Dichloropropane ND 550 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 2-Chlorotoluene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 4-Chlorotoluene ND 680 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Benzene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Bromobenzene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Bromochloromethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Bromodichloromethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Bromoform ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Bromomethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Carbon tetrachloride ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Chlorobenzene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Chloroethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Chloroform ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Chloromethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 cis-1,2-Dichloroethene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 cis-1,3-Dichloropropene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Dibromochloromethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Dibromomethane ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Dichlorodifluoromethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Isopropyl Ether (DIPE) ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-5' Lab Sample ID: 440-152586-5
Date Collected: 07/13/16 09:45 Matrix: Solid
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethanol ND 55000 20000 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethyl-t-butyl ether (ETBE) ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Ethylbenzene 540 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Hexachlorobutadiene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Isopropylbenzene 160 J 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 m,p-Xylene 1800 550 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Methylene Chloride ND 2700 1400 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Methyl-t-Butyl Ether (MTBE) ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Naphthalene 5600 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 n-Butylbenzene 540 J 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 N-Propylbenzene 430 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 o-Xylene 1100 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 sec-Butylbenzene 510 J 680 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Styrene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Tert-amyl-methyl ether (TAME) ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 tert-Butyl alcohol (TBA) ND 14000 6800 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 tert-Butylbenzene ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Tetrachloroethene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Toluene 320 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 trans-1,2-Dichloroethene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 trans-1,3-Dichloropropene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Trichloroethene ND 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Trichlorofluoromethane ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Vinyl chloride ND 680 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Xylenes, Total 2900 550 270 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 p-Isopropyltoluene 1900 270 140 ug/Kg 07/14/16 14:51 07/18/16 13:15 200 Toluene-d8 (Surr) 113 60 - 140 07/14/16 14:51 07/18/16 13:15 200 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 97 65 - 140 07/14/16 14:51 07/18/16 13:15 200 Dibromofluoromethane (Surr) 89 55 - 140 07/14/16 14:51 07/18/16 13:15 200 Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene 210 J 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Anthracene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Benzo[a]anthracene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Benzo[a]pyrene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Benzo[b]fluoranthene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Benzo[g,h,i]perylene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Benzo[k]fluoranthene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Chrysene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Dibenz(a,h)anthracene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Fluoranthene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Fluorene 360 J 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Indeno[1,2,3-cd]pyrene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Naphthalene 400 J 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Phenanthrene 100 J 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 Pyrene ND 590 79 ug/Kg 07/14/16 09:34 07/19/16 20:55 20 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-5' Lab Sample ID: 440-152586-5
Date Collected: 07/13/16 09:45 Matrix: Solid
Date Received: 07/13/16 18:30
2-Fluorobiphenyl (Surr) 48 39 - 111 07/14/16 09:34 07/19/16 20:55 20 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 46 41 - 119 07/14/16 09:34 07/19/16 20:55 20 Terphenyl-d14 29 X 43 - 150 07/14/16 09:34 07/19/16 20:55 20 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 540 50 25 mg/Kg 07/14/16 09:20 07/15/16 17:40 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 850 50 25 mg/Kg 07/14/16 09:20 07/15/16 17:40 10 n-Octacosane 20 X 40 - 140 07/14/16 09:20 07/15/16 17:40 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 Aroclor 1232 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 Aroclor 1242 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 Aroclor 1248 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 Aroclor 1254 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 Aroclor 1260 ND 50 17 ug/Kg 07/14/16 09:18 07/15/16 19:34 1 DCB Decachlorobiphenyl (Surr) 42 X 45 - 120 07/14/16 09:18 07/15/16 19:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 6020 - Metals (ICP/MS)
RL MDL
Silver ND 0.50 0.10 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.5 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Barium 110 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Beryllium 0.51 0.30 0.15 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Chromium 25 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Cobalt 9.1 0.50 0.21 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Copper 23 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Lead 15 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Molybdenum 0.97 J 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 23:05 20 Nickel 19 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Selenium 0.61 J 1.0 0.20 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Vanadium 47 1.0 0.50 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Zinc 69 10 5.0 mg/Kg 07/14/16 08:13 07/15/16 13:08 20
Antimony ND 1.0 0.27 mg/Kg 07/14/16 08:13 07/15/16 13:08 20 Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.064 0.020 0.012 mg/Kg 07/14/16 21:26 07/15/16 00:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-W Lab Sample ID: 440-152586-6
Date Collected: 07/13/16 11:30 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
92 50 35 ug/L 07/19/16 16:43 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 113 76 - 132 07/19/16 16:43 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 80 - 120 07/19/16 16:43 1 Toluene-d8 (Surr) 109 80 - 128 07/19/16 16:43 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 16:43 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/19/16 16:43 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 16:43 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/19/16 16:43 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/19/16 16:43 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 16:43 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/19/16 16:43 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 16:43 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Benzene 1.1 0.50 0.25 ug/L 07/19/16 16:43 1
Bromobenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Bromochloromethane ND 0.50 0.25 ug/L 07/19/16 16:43 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 Bromoform ND 1.0 0.40 ug/L 07/19/16 16:43 1
Bromomethane ND 0.50 0.25 ug/L 07/19/16 16:43 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/19/16 16:43 1 Chlorobenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Chloroethane ND 1.0 0.40 ug/L 07/19/16 16:43 1
Chloroform ND 0.50 0.25 ug/L 07/19/16 16:43 1
Chloromethane ND 0.50 0.25 ug/L 07/19/16 16:43 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 16:43 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 16:43 1 Dibromochloromethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 Dibromomethane ND 0.50 0.25 ug/L 07/19/16 16:43 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/19/16 16:43 1 Ethanol ND 150 75 ug/L 07/19/16 16:43 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-W Lab Sample ID: 440-152586-6
Date Collected: 07/13/16 11:30 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/19/16 16:43 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/19/16 16:43 1 Ethylbenzene 0.57 0.50 0.25 ug/L 07/19/16 16:43 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
m,p-Xylene ND 1.0 0.50 ug/L 07/19/16 16:43 1
Methylene Chloride ND 2.0 0.88 ug/L 07/19/16 16:43 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/19/16 16:43 1 Naphthalene ND 1.0 0.40 ug/L 07/19/16 16:43 1
n-Butylbenzene ND 1.0 0.40 ug/L 07/19/16 16:43 1
N-Propylbenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
o-Xylene ND 0.50 0.25 ug/L 07/19/16 16:43 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/19/16 16:43 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Styrene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/19/16 16:43 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Toluene ND 0.50 0.25 ug/L 07/19/16 16:43 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 16:43 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 16:43 1 Trichloroethene ND 0.50 0.25 ug/L 07/19/16 16:43 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/19/16 16:43 1 Xylenes, Total ND 1.0 0.50 ug/L 07/19/16 16:43 1
Vinyl chloride ND 0.50 0.25 ug/L 07/19/16 16:43 1
tert-Butyl alcohol (TBA) 24 10 5.0 ug/L 07/19/16 16:43 1 4-Bromofluorobenzene (Surr) 103 80 - 120 07/19/16 16:43 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 113 76 - 132 07/19/16 16:43 1 Toluene-d8 (Surr) 109 80 - 128 07/19/16 16:43 1
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Anthracene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Benzo[a]anthracene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Benzo[a]pyrene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Benzo[b]fluoranthene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Benzo[g,h,i]perylene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Benzo[k]fluoranthene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Chrysene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Dibenz(a,h)anthracene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Fluoranthene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Fluorene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Indeno[1,2,3-cd]pyrene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Naphthalene 0.62 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Phenanthrene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 Pyrene ND 0.18 0.091 ug/L 07/16/16 09:00 07/19/16 21:16 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-4-W Lab Sample ID: 440-152586-6
Date Collected: 07/13/16 11:30 Matrix: Water
Date Received: 07/13/16 18:30
2-Fluorobiphenyl (Surr) 55 50 - 104 07/16/16 09:00 07/19/16 21:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 79 46 - 109 07/16/16 09:00 07/19/16 21:16 1 Terphenyl-d14 80 28 - 124 07/16/16 09:00 07/19/16 21:16 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 0.73 0.46 0.092 mg/L 07/18/16 06:55 07/19/16 20:20 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 0.31 J 0.46 0.092 mg/L 07/18/16 06:55 07/19/16 20:20 1 n-Octacosane 61 45 - 120 07/18/16 06:55 07/19/16 20:20 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 Aroclor 1242 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 Aroclor 1254 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:37 1 DCB Decachlorobiphenyl (Surr) 71 26 - 115 07/18/16 12:42 07/22/16 18:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 300.0 - Anions, Ion Chromatography
RL MDL
Chloride 35000 1000 500 mg/L 07/16/16 00:13 2000
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate 2300 1000 500 mg/L 07/16/16 00:13 2000
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable RL MDL
Antimony ND 0.050 0.030 mg/L 07/18/16 09:51 07/20/16 13:03 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Barium 0.15 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Beryllium ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 13:03 5 Cadmium ND 0.025 0.010 mg/L 07/18/16 09:51 07/20/16 13:03 5 Chromium ND 0.025 0.013 mg/L 07/18/16 09:51 07/20/16 13:03 5 Cobalt ND 0.050 0.013 mg/L 07/18/16 09:51 07/20/16 13:03 5 Lead ND 0.025 0.013 mg/L 07/18/16 09:51 07/20/16 13:03 5 Copper 0.026 J 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Molybdenum ND ^ 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:03 5 Nickel ND 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Selenium ND 0.050 0.031 mg/L 07/18/16 09:51 07/20/16 13:03 5 Silver ND 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Thallium ND 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Vanadium 0.030 J 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:03 5 Zinc ND 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:03 5 Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury ND 0.00020 0.00010 mg/L 07/18/16 17:00 07/19/16 16:55 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
General Chemistry
RL MDL
Total Dissolved Solids 59000 2000 1000 mg/L 07/18/16 07:50 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Client Sample ID: AEC-3-W Lab Sample ID: 440-152586-7
Date Collected: 07/13/16 12:50 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
49 J 50 35 ug/L 07/19/16 10:16 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 115 76 - 132 07/19/16 10:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 80 - 120 07/19/16 10:16 1 Toluene-d8 (Surr) 110 80 - 128 07/19/16 10:16 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 10:16 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/19/16 10:16 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 10:16 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/19/16 10:16 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/19/16 10:16 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 10:16 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/19/16 10:16 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 10:16 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Benzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Bromobenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Bromochloromethane ND 0.50 0.25 ug/L 07/19/16 10:16 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 Bromoform ND 1.0 0.40 ug/L 07/19/16 10:16 1
Bromomethane ND 0.50 0.25 ug/L 07/19/16 10:16 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/19/16 10:16 1 Chlorobenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Chloroethane ND 1.0 0.40 ug/L 07/19/16 10:16 1
Chloroform ND 0.50 0.25 ug/L 07/19/16 10:16 1
Chloromethane ND 0.50 0.25 ug/L 07/19/16 10:16 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 10:16 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 10:16 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-W Lab Sample ID: 440-152586-7
Date Collected: 07/13/16 12:50 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Dibromochloromethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromomethane ND 0.50 0.25 ug/L 07/19/16 10:16 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/19/16 10:16 1 Ethanol ND 150 75 ug/L 07/19/16 10:16 1
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/19/16 10:16 1 Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/19/16 10:16 1 Ethylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
m,p-Xylene ND 1.0 0.50 ug/L 07/19/16 10:16 1
Methylene Chloride ND 2.0 0.88 ug/L 07/19/16 10:16 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/19/16 10:16 1 Naphthalene ND 1.0 0.40 ug/L 07/19/16 10:16 1
n-Butylbenzene ND 1.0 0.40 ug/L 07/19/16 10:16 1
N-Propylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
o-Xylene ND 0.50 0.25 ug/L 07/19/16 10:16 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/19/16 10:16 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Styrene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/19/16 10:16 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Toluene ND 0.50 0.25 ug/L 07/19/16 10:16 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 10:16 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 10:16 1 Trichloroethene ND 0.50 0.25 ug/L 07/19/16 10:16 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/19/16 10:16 1 Xylenes, Total ND 1.0 0.50 ug/L 07/19/16 10:16 1
Vinyl chloride ND 0.50 0.25 ug/L 07/19/16 10:16 1
tert-Butyl alcohol (TBA) 11 ID 10 5.0 ug/L 07/19/16 10:16 1 4-Bromofluorobenzene (Surr) 105 80 - 120 07/19/16 10:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 115 76 - 132 07/19/16 10:16 1 Toluene-d8 (Surr) 110 80 - 128 07/19/16 10:16 1
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Anthracene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Benzo[a]anthracene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Benzo[a]pyrene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Benzo[b]fluoranthene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Benzo[g,h,i]perylene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Benzo[k]fluoranthene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Chrysene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Dibenz(a,h)anthracene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Fluoranthene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Fluorene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-W Lab Sample ID: 440-152586-7
Date Collected: 07/13/16 12:50 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) RL MDL
Indeno[1,2,3-cd]pyrene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Naphthalene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Phenanthrene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 Pyrene ND 0.19 0.097 ug/L 07/16/16 09:00 07/19/16 21:37 1 2-Fluorobiphenyl (Surr) 56 50 - 104 07/16/16 09:00 07/19/16 21:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 73 46 - 109 07/16/16 09:00 07/19/16 21:37 1 Terphenyl-d14 90 28 - 124 07/16/16 09:00 07/19/16 21:37 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 2.6 J 9.5 1.9 mg/L 07/18/16 06:55 07/19/16 22:04 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 40 9.5 1.9 mg/L 07/18/16 06:55 07/19/16 22:04 10 n-Octacosane 698 X 45 - 120 07/18/16 06:55 07/19/16 22:04 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 Aroclor 1242 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 Aroclor 1254 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 18:50 1 DCB Decachlorobiphenyl (Surr) 67 26 - 115 07/18/16 12:42 07/22/16 18:50 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 300.0 - Anions, Ion Chromatography
RL MDL
Chloride 36000 5000 2500 mg/L 07/16/16 15:02 10000
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate 4800 1000 500 mg/L 07/16/16 00:33 2000
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable RL MDL
Antimony 0.074 0.050 0.030 mg/L 07/16/16 11:58 07/18/16 18:43 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 0.093 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 Barium 0.70 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 Beryllium ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:43 5 Cadmium ND 0.025 0.010 mg/L 07/16/16 11:58 07/18/16 18:43 5 Chromium 0.15 0.025 0.013 mg/L 07/16/16 11:58 07/18/16 18:43 5 Cobalt 0.054 0.050 0.013 mg/L 07/16/16 11:58 07/18/16 18:43 5 Lead 0.14 0.025 0.013 mg/L 07/16/16 11:58 07/19/16 17:44 5 Copper 0.23 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 Molybdenum 0.053 J 0.10 0.050 mg/L 07/16/16 11:58 07/18/16 18:43 5 Nickel 0.10 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 Selenium ND 0.050 0.031 mg/L 07/16/16 11:58 07/19/16 17:44 5 Silver ND 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-W Lab Sample ID: 440-152586-7
Date Collected: 07/13/16 12:50 Matrix: Water
Date Received: 07/13/16 18:30
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable (Continued) RL MDL
Thallium ND 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Vanadium 0.29 0.050 0.025 mg/L 07/16/16 11:58 07/18/16 18:43 5 Zinc 0.35 0.10 0.050 mg/L 07/16/16 11:58 07/18/16 18:43 5 Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 0.00015 J 0.00020 0.00010 mg/L 07/18/16 17:00 07/19/16 16:58 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac General Chemistry
RL MDL
Total Dissolved Solids 62000 2000 1000 mg/L 07/18/16 07:50 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Client Sample ID: AEC-5-W Lab Sample ID: 440-152586-8
Date Collected: 07/13/16 14:00 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 50 35 ug/L 07/19/16 17:13 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 116 76 - 132 07/19/16 17:13 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 80 - 120 07/19/16 17:13 1 Toluene-d8 (Surr) 110 80 - 128 07/19/16 17:13 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 17:13 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/19/16 17:13 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 17:13 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/19/16 17:13 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/19/16 17:13 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 17:13 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/19/16 17:13 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 17:13 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Benzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-W Lab Sample ID: 440-152586-8
Date Collected: 07/13/16 14:00 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Bromobenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Bromochloromethane ND 0.50 0.25 ug/L 07/19/16 17:13 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 Bromoform ND 1.0 0.40 ug/L 07/19/16 17:13 1
Bromomethane ND 0.50 0.25 ug/L 07/19/16 17:13 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/19/16 17:13 1 Chlorobenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Chloroethane ND 1.0 0.40 ug/L 07/19/16 17:13 1
Chloroform ND 0.50 0.25 ug/L 07/19/16 17:13 1
Chloromethane ND 0.50 0.25 ug/L 07/19/16 17:13 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 17:13 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 17:13 1 Dibromochloromethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 Dibromomethane ND 0.50 0.25 ug/L 07/19/16 17:13 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/19/16 17:13 1 Ethanol ND * 150 75 ug/L 07/19/16 17:13 1
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/19/16 17:13 1 Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/19/16 17:13 1 Ethylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
m,p-Xylene ND 1.0 0.50 ug/L 07/19/16 17:13 1
Methylene Chloride ND 2.0 0.88 ug/L 07/19/16 17:13 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/19/16 17:13 1 Naphthalene ND 1.0 0.40 ug/L 07/19/16 17:13 1
n-Butylbenzene ND 1.0 0.40 ug/L 07/19/16 17:13 1
N-Propylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
o-Xylene ND 0.50 0.25 ug/L 07/19/16 17:13 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/19/16 17:13 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Styrene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/19/16 17:13 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Toluene ND 0.50 0.25 ug/L 07/19/16 17:13 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 17:13 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 17:13 1 Trichloroethene ND 0.50 0.25 ug/L 07/19/16 17:13 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/19/16 17:13 1 Xylenes, Total ND 1.0 0.50 ug/L 07/19/16 17:13 1
Vinyl chloride ND 0.50 0.25 ug/L 07/19/16 17:13 1
tert-Butyl alcohol (TBA) ND * 10 5.0 ug/L 07/19/16 17:13 1 4-Bromofluorobenzene (Surr) 103 80 - 120 07/19/16 17:13 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 116 76 - 132 07/19/16 17:13 1 Toluene-d8 (Surr) 110 80 - 128 07/19/16 17:13 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-W Lab Sample ID: 440-152586-8
Date Collected: 07/13/16 14:00 Matrix: Water
Date Received: 07/13/16 18:30
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Anthracene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Benzo[a]anthracene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Benzo[a]pyrene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Benzo[b]fluoranthene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Benzo[g,h,i]perylene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Benzo[k]fluoranthene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Chrysene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Dibenz(a,h)anthracene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Fluoranthene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Fluorene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Indeno[1,2,3-cd]pyrene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Naphthalene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Phenanthrene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 Pyrene ND 0.17 0.087 ug/L 07/16/16 09:00 07/19/16 21:57 1 2-Fluorobiphenyl (Surr) 59 50 - 104 07/16/16 09:00 07/19/16 21:57 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 61 46 - 109 07/16/16 09:00 07/19/16 21:57 1 Terphenyl-d14 64 28 - 124 07/16/16 09:00 07/19/16 21:57 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 0.44 0.088 mg/L 07/18/16 06:55 07/19/16 17:58 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 0.44 0.088 mg/L 07/18/16 06:55 07/19/16 17:58 1 n-Octacosane 77 45 - 120 07/18/16 06:55 07/19/16 17:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 Aroclor 1242 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 Aroclor 1254 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:03 1 DCB Decachlorobiphenyl (Surr) 58 26 - 115 07/18/16 12:42 07/22/16 19:03 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 300.0 - Anions, Ion Chromatography
RL MDL
Chloride 62000 10000 5000 mg/L 07/16/16 15:14 20000
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate 7100 1000 500 mg/L 07/16/16 00:52 2000
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable RL MDL
Antimony ND 0.10 0.060 mg/L 07/18/16 09:51 07/20/16 13:05 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-5-W Lab Sample ID: 440-152586-8
Date Collected: 07/13/16 14:00 Matrix: Water
Date Received: 07/13/16 18:30
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable (Continued) RL MDL
Arsenic ND 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Barium 0.29 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Beryllium ND 0.020 0.010 mg/L 07/18/16 09:51 07/20/16 13:05 10 Cadmium ND 0.050 0.020 mg/L 07/18/16 09:51 07/20/16 13:05 10 Chromium 0.047 J 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:05 10 Cobalt ND 0.10 0.025 mg/L 07/18/16 09:51 07/20/16 13:05 10 Lead ND 0.050 0.025 mg/L 07/18/16 09:51 07/20/16 13:05 10 Copper 0.096 J 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Molybdenum ND ^ 0.20 0.10 mg/L 07/18/16 09:51 07/20/16 13:05 10 Nickel ND 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Selenium ND 0.10 0.061 mg/L 07/18/16 09:51 07/20/16 13:05 10 Silver ND 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Thallium ND 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Vanadium 0.11 0.10 0.050 mg/L 07/18/16 09:51 07/20/16 13:05 10 Zinc ND 0.20 0.10 mg/L 07/18/16 09:51 07/20/16 13:05 10 Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury ND 0.00020 0.00010 mg/L 07/18/16 17:00 07/19/16 17:01 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac General Chemistry
RL MDL
Total Dissolved Solids 100000 2000 1000 mg/L 07/18/16 07:50 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL IRV
8260B/CA_LUFTM SW846
S
Volatile Organic Compounds by GC/MS TAL IRV
8270C SIM Semivolatile Organic Compounds (GC/MS SIM) SW846 TAL IRV 8015B Diesel Range Organics (DRO) (GC) SW846 TAL IRV
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL IRV 300.0 Anions, Ion Chromatography MCAWW TAL IRV
200.7 Rev 4.4 Metals (ICP) EPA TAL IRV
245.1 Mercury (CVAA) EPA TAL IRV
6020 Metals (ICP/MS) SW846 TAL IRV
7471A Mercury (CVAA) SW846 TAL IRV
SM 2540C Solids, Total Dissolved (TDS) SM TAL IRV
Protocol References:

EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater", SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-5' Lab Sample ID: 440-152586-1
Date Collected: 07/13/16 07:40 Matrix: Solid
Date Received: 07/13/16 18:30
Prep 5035 342449 07/14/16 15:46 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.69 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 343001 07/18/16 12:25 HR TAL IRV Total/NA Prep 5035 5.69 g 10 mL 342449 07/14/16 15:46 WK TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 343002 07/18/16 12:25 HR TAL IRV Total/NA Prep 3546 15.47 g 1 mL 342341 07/14/16 09:34 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 20:47 AI TAL IRV Total/NA Prep 3546 15.01 g 1 mL 342333 07/14/16 09:20 LEG TAL IRV Total/NA Analysis 8015B 1 342644 07/15/16 21:59 VS TAL IRV Total/NA Prep 3546 15.18 g 2 mL 342185 07/14/16 09:18 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 18:31 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 342802 07/15/16 12:58 TK TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 343028 07/15/16 22:55 RC TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342507 07/14/16 21:26 DB TAL IRV Total/NA Analysis 7471A 1 342536 07/15/16 00:23 DB TAL IRV Client Sample ID: AEC-2-10' Lab Sample ID: 440-152586-2 Date Collected: 07/13/16 07:45 Matrix: Solid
Date Received: 07/13/16 18:30
Prep 5035 342449 07/14/16 15:46 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 5.91 g 10 mL
Total/NA Analysis 8260B 1 10 mL 10 mL 343001 07/18/16 12:56 HR TAL IRV Total/NA Prep 5035 5.91 g 10 mL 342449 07/14/16 15:46 WK TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 343002 07/18/16 12:56 HR TAL IRV Total/NA Prep 3546 7.41 g 1 mL 342341 07/14/16 09:34 LEG TAL IRV Total/NA Analysis 8270C SIM 1 342622 07/15/16 22:09 AI TAL IRV Total/NA Prep 3546 15.05 g 1 mL 342333 07/14/16 09:20 LEG TAL IRV Total/NA Analysis 8015B 1 342644 07/15/16 21:38 VS TAL IRV Total/NA Prep 3546 7.07 g 2 mL 342185 07/14/16 09:18 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 18:46 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 342802 07/15/16 13:01 TK TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 343028 07/15/16 22:58 RC TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342507 07/14/16 21:26 DB TAL IRV Total/NA Analysis 7471A 1 342536 07/15/16 00:26 DB TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-15' Lab Sample ID: 440-152586-3 Date Collected: 07/13/16 07:50 Matrix: Solid
Date Received: 07/13/16 18:30
Prep 5035 342437 07/14/16 14:51 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 3.53 g 5 mL
Total/NA Analysis 8260B 100 10 mL 10 mL 342991 07/18/16 12:16 ATL TAL IRV Total/NA Prep 5035 3.53 g 5 mL 342437 07/14/16 14:51 WK TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 100 10 mL 10 mL 342992 07/18/16 12:16 ATL TAL IRV Total/NA Prep 3546 3.39 g 1 mL 342341 07/14/16 09:34 LEG TAL IRV Total/NA Analysis 8270C SIM 5 343497 07/19/16 20:14 AI TAL IRV Total/NA Prep 3546 7.52 g 1 mL 342333 07/14/16 09:20 LEG TAL IRV Total/NA Analysis 8015B 1 342644 07/15/16 22:20 VS TAL IRV Total/NA Prep 3546 7.57 g 2 mL 342185 07/14/16 09:18 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 19:02 JM TAL IRV Total/NA Prep 3050B 2.03 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 342802 07/15/16 13:03 TK TAL IRV Total/NA Prep 3050B 2.03 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 343028 07/15/16 23:00 RC TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342507 07/14/16 21:26 DB TAL IRV Total/NA Analysis 7471A 1 342536 07/15/16 00:34 DB TAL IRV Client Sample ID: AEC-2-20' Lab Sample ID: 440-152586-4 Date Collected: 07/13/16 07:58 Matrix: Solid
Date Received: 07/13/16 18:30
Prep 5035 342437 07/14/16 14:51 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 3.03 g 5 mL
Total/NA Analysis 8260B 100 10 mL 10 mL 342991 07/18/16 12:45 ATL TAL IRV Total/NA Prep 5035 3.03 g 5 mL 342437 07/14/16 14:51 WK TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 100 10 mL 10 mL 342992 07/18/16 12:45 ATL TAL IRV Total/NA Prep 3546 3.15 g 1 mL 342341 07/14/16 09:34 LEG TAL IRV Total/NA Analysis 8270C SIM 5 343497 07/19/16 20:35 AI TAL IRV Total/NA Prep 3546 7.52 g 2 mL 342333 07/14/16 09:20 LEG TAL IRV Total/NA Analysis 8015B 10 343077 07/18/16 19:52 JM TAL IRV Total/NA Prep 3546 3.22 g 2 mL 342185 07/14/16 09:18 VA TAL IRV Total/NA Analysis 8082 1 342640 07/16/16 11:27 JM TAL IRV Total/NA Prep 3546 3.22 g 2 mL 342185 07/14/16 09:18 VA TAL IRV Total/NA Analysis 8082 1 343048 07/18/16 13:19 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 342802 07/15/16 13:06 TK TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 343028 07/15/16 23:03 RC TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342507 07/14/16 21:26 DB TAL IRV Total/NA Analysis 7471A 1 342536 07/15/16 00:36 DB TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-5' Lab Sample ID: 440-152586-5
Date Collected: 07/13/16 09:45 Matrix: Solid
Date Received: 07/13/16 18:30
Prep 5035 342437 07/14/16 14:51 WK TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 3.66 g 5 mL
Total/NA Analysis 8260B 200 10 mL 10 mL 342991 07/18/16 13:15 ATL TAL IRV Total/NA Prep 5035 3.66 g 5 mL 342437 07/14/16 14:51 WK TAL IRV Analysis 8260B/CA_LUFTM
S
Total/NA 200 10 mL 10 mL 342992 07/18/16 13:15 ATL TAL IRV Total/NA Prep 3546 15.19 g 1 mL 342341 07/14/16 09:34 LEG TAL IRV Total/NA Analysis 8270C SIM 20 343497 07/19/16 20:55 AI TAL IRV Total/NA Prep 3546 15.00 g 1 mL 342333 07/14/16 09:20 LEG TAL IRV Total/NA Analysis 8015B 10 342375 07/15/16 17:40 JM TAL IRV Total/NA Prep 3546 15.01 g 2 mL 342185 07/14/16 09:18 VA TAL IRV Total/NA Analysis 8082 1 342640 07/15/16 19:34 JM TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 342802 07/15/16 13:08 TK TAL IRV Total/NA Prep 3050B 2.01 g 50 mL 342296 07/14/16 08:13 DT TAL IRV Total/NA Analysis 6020 20 343028 07/15/16 23:05 RC TAL IRV Total/NA Prep 7471A 0.51 g 50 mL 342507 07/14/16 21:26 DB TAL IRV Total/NA Analysis 7471A 1 342536 07/15/16 00:39 DB TAL IRV Client Sample ID: AEC-4-W Lab Sample ID: 440-152586-6
Date Collected: 07/13/16 11:30 Matrix: Water
Date Received: 07/13/16 18:30
Analysis 8260B 1 343275 07/19/16 16:43 MM1 TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 10 mL 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 343276 07/19/16 16:43 AYL TAL IRV Total/NA Prep 3520C 1100 mL 1 mL 342864 07/16/16 09:00 FTD TAL IRV Total/NA Analysis 8270C SIM 1 343497 07/19/16 21:16 AI TAL IRV Total/NA Prep 3510C 1090 mL 1 mL 343009 07/18/16 06:55 L2A TAL IRV Total/NA Analysis 8015B 1 343351 07/19/16 20:20 EI TAL IRV Total/NA Prep 3510C 125 mL 2 mL 343105 07/18/16 12:42 L2A TAL IRV Total/NA Analysis 8082 1 344252 07/22/16 18:37 JM TAL IRV Total/NA Analysis 300.0 2000 342634 07/16/16 00:13 NTN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343049 07/18/16 09:51 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 5 343712 07/20/16 13:03 EN TAL IRV Total/NA Prep 245.1 20 mL 20 mL 343189 07/18/16 17:00 DB TAL IRV Total/NA Analysis 245.1 1 343504 07/19/16 16:55 DB TAL IRV Total/NA Analysis SM 2540C 1 0.5 mL 100 mL 343021 07/18/16 07:50 XL TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-3-W Lab Sample ID: 440-152586-7
Date Collected: 07/13/16 12:50 Matrix: Water
Date Received: 07/13/16 18:30
Analysis 8260B 1 343275 07/19/16 10:16 MM1 TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 10 mL 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 343276 07/19/16 10:16 AYL TAL IRV Total/NA Prep 3520C 1030 mL 1 mL 342864 07/16/16 09:00 FTD TAL IRV Total/NA Analysis 8270C SIM 1 343497 07/19/16 21:37 AI TAL IRV Total/NA Prep 3510C 1050 mL 2 mL 343009 07/18/16 06:55 L2A TAL IRV Total/NA Analysis 8015B 10 343351 07/19/16 22:04 EI TAL IRV Total/NA Prep 3510C 125 mL 2 mL 343105 07/18/16 12:42 L2A TAL IRV Total/NA Analysis 8082 1 344252 07/22/16 18:50 JM TAL IRV Total/NA Analysis 300.0 10000 342822 07/16/16 15:02 NTN TAL IRV Total/NA Analysis 300.0 2000 342634 07/16/16 00:33 NTN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 342888 07/16/16 11:58 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 5 343234 07/18/16 18:43 EN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 342888 07/16/16 11:58 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 5 343507 07/19/16 17:44 EN TAL IRV Total/NA Prep 245.1 20 mL 20 mL 343189 07/18/16 17:00 DB TAL IRV Total/NA Analysis 245.1 1 343504 07/19/16 16:58 DB TAL IRV Total/NA Analysis SM 2540C 1 0.5 mL 100 mL 343021 07/18/16 07:50 XL TAL IRV Client Sample ID: AEC-5-W Lab Sample ID: 440-152586-8
Date Collected: 07/13/16 14:00 Matrix: Water
Date Received: 07/13/16 18:30
Analysis 8260B 1 343275 07/19/16 17:13 MM1 TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 10 mL 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 343276 07/19/16 17:13 AYL TAL IRV Total/NA Prep 3520C 1145 mL 1 mL 342864 07/16/16 09:00 FTD TAL IRV Total/NA Analysis 8270C SIM 1 343497 07/19/16 21:57 AI TAL IRV Total/NA Prep 3510C 1135 mL 1 mL 343009 07/18/16 06:55 L2A TAL IRV Total/NA Analysis 8015B 1 343351 07/19/16 17:58 EI TAL IRV Total/NA Prep 3510C 125 mL 2 mL 343105 07/18/16 12:42 L2A TAL IRV Total/NA Analysis 8082 1 344252 07/22/16 19:03 JM TAL IRV Total/NA Analysis 300.0 20000 342822 07/16/16 15:14 NTN TAL IRV Total/NA Analysis 300.0 2000 342634 07/16/16 00:52 NTN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343049 07/18/16 09:51 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 10 343712 07/20/16 13:05 EN TAL IRV Total/NA Prep 245.1 20 mL 20 mL 343189 07/18/16 17:00 DB TAL IRV Total/NA Analysis 245.1 1 343504 07/19/16 17:01 DB TAL IRV Total/NA Analysis SM 2540C 1 0.5 mL 100 mL 343021 07/18/16 07:50 XL TAL IRV Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 440-342991/6 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
RL MDL
1,1,1,2-Tetrachloroethane ND 250 100 ug/Kg 07/18/16 09:48 100 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 100 50 ug/Kg 07/18/16 09:48 100 1,1,2,2-Tetrachloroethane ND 100 50 ug/Kg 07/18/16 09:48 100 1,1,2-Trichloroethane ND 100 50 ug/Kg 07/18/16 09:48 100 1,1-Dichloroethane ND 100 50 ug/Kg 07/18/16 09:48 100
1,1-Dichloroethene ND 250 100 ug/Kg 07/18/16 09:48 100
1,1-Dichloropropene ND 100 50 ug/Kg 07/18/16 09:48 100
1,2,3-Trichlorobenzene ND 250 100 ug/Kg 07/18/16 09:48 100 1,2,3-Trichloropropane ND 500 100 ug/Kg 07/18/16 09:48 100 1,2,4-Trichlorobenzene ND 250 100 ug/Kg 07/18/16 09:48 100 1,2,4-Trimethylbenzene ND 100 50 ug/Kg 07/18/16 09:48 100 1,2-Dibromo-3-Chloropropane ND 250 100 ug/Kg 07/18/16 09:48 100 1,2-Dibromoethane (EDB) ND 100 50 ug/Kg 07/18/16 09:48 100 1,2-Dichlorobenzene ND 100 50 ug/Kg 07/18/16 09:48 100
1,2-Dichloroethane ND 100 50 ug/Kg 07/18/16 09:48 100
1,2-Dichloropropane ND 100 50 ug/Kg 07/18/16 09:48 100
1,3,5-Trimethylbenzene ND 100 50 ug/Kg 07/18/16 09:48 100 1,3-Dichlorobenzene ND 100 50 ug/Kg 07/18/16 09:48 100
1,3-Dichloropropane ND 100 50 ug/Kg 07/18/16 09:48 100
1,4-Dichlorobenzene ND 100 50 ug/Kg 07/18/16 09:48 100
2,2-Dichloropropane ND 200 100 ug/Kg 07/18/16 09:48 100 2-Chlorotoluene ND 250 100 ug/Kg 07/18/16 09:48 100
4-Chlorotoluene ND 250 50 ug/Kg 07/18/16 09:48 100
Benzene ND 100 50 ug/Kg 07/18/16 09:48 100
Bromobenzene ND 250 100 ug/Kg 07/18/16 09:48 100
Bromochloromethane ND 250 100 ug/Kg 07/18/16 09:48 100
Bromodichloromethane ND 100 50 ug/Kg 07/18/16 09:48 100 Bromoform ND 250 100 ug/Kg 07/18/16 09:48 100
Bromomethane ND 250 100 ug/Kg 07/18/16 09:48 100
Carbon tetrachloride ND 250 100 ug/Kg 07/18/16 09:48 100 Chlorobenzene ND 100 50 ug/Kg 07/18/16 09:48 100
Chloroethane ND 250 100 ug/Kg 07/18/16 09:48 100
Chloroform ND 100 50 ug/Kg 07/18/16 09:48 100
Chloromethane ND 250 100 ug/Kg 07/18/16 09:48 100
cis-1,2-Dichloroethene ND 100 50 ug/Kg 07/18/16 09:48 100 cis-1,3-Dichloropropene ND 100 50 ug/Kg 07/18/16 09:48 100 Dibromochloromethane ND 100 50 ug/Kg 07/18/16 09:48 100 Dibromomethane ND 100 50 ug/Kg 07/18/16 09:48 100
Dichlorodifluoromethane ND 250 100 ug/Kg 07/18/16 09:48 100 Isopropyl Ether (DIPE) ND 250 100 ug/Kg 07/18/16 09:48 100 Ethanol ND 20000 7500 ug/Kg 07/18/16 09:48 100
Ethyl-t-butyl ether (ETBE) ND 250 100 ug/Kg 07/18/16 09:48 100 Ethylbenzene ND 100 50 ug/Kg 07/18/16 09:48 100
Hexachlorobutadiene ND 250 100 ug/Kg 07/18/16 09:48 100 Isopropylbenzene ND 100 50 ug/Kg 07/18/16 09:48 100
m,p-Xylene ND 200 100 ug/Kg 07/18/16 09:48 100
Methylene Chloride ND 1000 500 ug/Kg 07/18/16 09:48 100 Methyl-t-Butyl Ether (MTBE) ND 250 100 ug/Kg 07/18/16 09:48 100 TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-342991/6 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
RL MDL
Naphthalene ND 250 100 ug/Kg 07/18/16 09:48 100
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac n-Butylbenzene ND 250 100 ug/Kg 07/18/16 09:48 100
N-Propylbenzene ND 100 50 ug/Kg 07/18/16 09:48 100
o-Xylene ND 100 50 ug/Kg 07/18/16 09:48 100
sec-Butylbenzene ND 250 50 ug/Kg 07/18/16 09:48 100
Styrene ND 100 50 ug/Kg 07/18/16 09:48 100
Tert-amyl-methyl ether (TAME) ND 250 100 ug/Kg 07/18/16 09:48 100 tert-Butyl alcohol (TBA) ND 5000 2500 ug/Kg 07/18/16 09:48 100 tert-Butylbenzene ND 250 100 ug/Kg 07/18/16 09:48 100
Tetrachloroethene ND 100 50 ug/Kg 07/18/16 09:48 100
Toluene ND 100 50 ug/Kg 07/18/16 09:48 100
trans-1,2-Dichloroethene ND 100 50 ug/Kg 07/18/16 09:48 100 trans-1,3-Dichloropropene ND 100 50 ug/Kg 07/18/16 09:48 100 Trichloroethene ND 100 50 ug/Kg 07/18/16 09:48 100
Trichlorofluoromethane ND 250 100 ug/Kg 07/18/16 09:48 100 Vinyl chloride ND 250 100 ug/Kg 07/18/16 09:48 100
Xylenes, Total ND 200 100 ug/Kg 07/18/16 09:48 100
p-Isopropyltoluene ND 100 50 ug/Kg 07/18/16 09:48 100
Toluene-d8 (Surr) 109 60 - 140 07/18/16 09:48 100
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 107 65 - 140 07/18/16 09:48 100 Dibromofluoromethane (Surr) 101 55 - 140 07/18/16 09:48 100 Lab Sample ID: LCS 440-342991/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
1,1,1,2-Tetrachloroethane 2500 2580 ug/Kg 103 70 - 140
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 2500 2850 ug/Kg 114 65 - 140
1,1,2,2-Tetrachloroethane 2500 2640 ug/Kg 106 55 - 135
1,1,2-Trichloroethane 2500 2540 ug/Kg 102 65 - 130
1,1-Dichloroethane 2500 2630 ug/Kg 105 65 - 130
1,1-Dichloroethene 2500 2920 ug/Kg 117 75 - 140
1,1-Dichloropropene 2500 2940 ug/Kg 118 70 - 130
1,2,3-Trichlorobenzene 2500 2750 ug/Kg 110 60 - 135
1,2,3-Trichloropropane 2500 2590 ug/Kg 103 55 - 130
1,2,4-Trichlorobenzene 2500 2960 ug/Kg 119 65 - 135
1,2,4-Trimethylbenzene 2500 2780 ug/Kg 111 70 - 125
1,2-Dibromo-3-Chloropropane 2500 2500 ug/Kg 100 45 - 135 1,2-Dibromoethane (EDB) 2500 2650 ug/Kg 106 70 - 130
1,2-Dichlorobenzene 2500 2690 ug/Kg 108 70 - 120
1,2-Dichloroethane 2500 2650 ug/Kg 106 60 - 145
1,2-Dichloropropane 2500 2680 ug/Kg 107 75 - 125
1,3,5-Trimethylbenzene 2500 2840 ug/Kg 114 70 - 125
1,3-Dichlorobenzene 2500 2730 ug/Kg 109 70 - 125
1,3-Dichloropropane 2500 2540 ug/Kg 102 65 - 130
TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342991/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
1,4-Dichlorobenzene 2500 2630 ug/Kg 105 70 - 125
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
2,2-Dichloropropane 2500 2790 ug/Kg 112 60 - 145
2-Chlorotoluene 2500 2690 ug/Kg 108 70 - 125
4-Chlorotoluene 2500 2740 ug/Kg 110 70 - 125
Benzene 2500 2690 ug/Kg 108 65 - 120
Bromobenzene 2500 2690 ug/Kg 108 70 - 120
Bromochloromethane 2500 2650 ug/Kg 106 65 - 125
Bromodichloromethane 2500 2690 ug/Kg 108 65 - 135
Bromoform 2500 2770 ug/Kg 111 50 - 130
Bromomethane 2500 1760 ug/Kg 70 30 - 140
Carbon tetrachloride 2500 2970 ug/Kg 119 65 - 145
Chlorobenzene 2500 2560 ug/Kg 102 70 - 125
Chloroethane 2500 2340 ug/Kg 94 40 - 140
Chloroform 2500 2660 ug/Kg 106 75 - 130
Chloromethane 2500 1830 ug/Kg 73 30 - 140
cis-1,2-Dichloroethene 2500 2820 ug/Kg 113 65 - 130
cis-1,3-Dichloropropene 2500 2710 ug/Kg 108 70 - 130
Dibromochloromethane 2500 2620 ug/Kg 105 65 - 140
Dibromomethane 2500 2700 ug/Kg 108 65 - 130
Dichlorodifluoromethane 2500 1510 ug/Kg 60 10 - 155
Isopropyl Ether (DIPE) 2500 2720 ug/Kg 109 60 - 140
Ethanol 100000 119000 ug/Kg 119 35 - 160
Ethyl-t-butyl ether (ETBE) 2500 2680 ug/Kg 107 60 - 140 Ethylbenzene 2500 2630 ug/Kg 105 80 - 120
Hexachlorobutadiene 2500 3080 ug/Kg 123 60 - 135
Isopropylbenzene 2500 2790 ug/Kg 111 70 - 125
m,p-Xylene 2500 2680 ug/Kg 107 70 - 125
Methylene Chloride 2500 2700 ug/Kg 108 60 - 140
Methyl-t-Butyl Ether (MTBE) 2500 2610 ug/Kg 105 55 - 145 Naphthalene 2500 2700 ug/Kg 108 50 - 140
n-Butylbenzene 2500 3050 ug/Kg 122 70 - 130
N-Propylbenzene 2500 2880 ug/Kg 115 70 - 130
o-Xylene 2500 2630 ug/Kg 105 70 - 125
sec-Butylbenzene 2500 2920 ug/Kg 117 70 - 125
Styrene 2500 2670 ug/Kg 107 70 - 135
Tert-amyl-methyl ether (TAME) 2500 2770 ug/Kg 111 60 - 145 tert-Butyl alcohol (TBA) 25000 25100 ug/Kg 101 65 - 140 tert-Butylbenzene 2500 2880 ug/Kg 115 70 - 125
Tetrachloroethene 2500 2780 ug/Kg 111 65 - 125
Toluene 2500 2620 ug/Kg 105 80 - 120
trans-1,2-Dichloroethene 2500 3010 ug/Kg 120 65 - 130
trans-1,3-Dichloropropene 2500 2640 ug/Kg 106 65 - 135
Trichloroethene 2500 2740 ug/Kg 110 70 - 130
Trichlorofluoromethane 2500 2560 ug/Kg 102 50 - 145
Vinyl chloride 2500 1240 ug/Kg 50 10 - 120
p-Isopropyltoluene 2500 2920 ug/Kg 117 70 - 125
TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-342991/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
Toluene-d8 (Surr) 60 - 140
Surrogate
100

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 65 - 140
Dibromofluoromethane (Surr) 102 55 - 140
Lab Sample ID: LCSD 440-342991/9 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
1,1,1,2-Tetrachloroethane 2500 2760 ug/Kg 111 70 - 140 7 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane 2500 2800 ug/Kg 112 65 - 140 2 20 1,1,2,2-Tetrachloroethane 2500 2630 ug/Kg 105 55 - 135 0 25 1,1,2-Trichloroethane 2500 2770 ug/Kg 111 65 - 130 9 20 1,1-Dichloroethane 2500 2670 ug/Kg 107 65 - 130 2 20
1,1-Dichloroethene 2500 2890 ug/Kg 116 75 - 140 1 20
1,1-Dichloropropene 2500 2880 ug/Kg 115 70 - 130 2 20
1,2,3-Trichlorobenzene 2500 2780 ug/Kg 111 60 - 135 1 20 1,2,3-Trichloropropane 2500 2580 ug/Kg 103 55 - 130 0 25 1,2,4-Trichlorobenzene 2500 2930 ug/Kg 117 65 - 135 1 20 1,2,4-Trimethylbenzene 2500 2790 ug/Kg 112 70 - 125 1 20 1,2-Dibromo-3-Chloropropane 2500 2340 ug/Kg 94 45 - 135 6 25 1,2-Dibromoethane (EDB) 2500 2810 ug/Kg 113 70 - 130 6 20 1,2-Dichlorobenzene 2500 2740 ug/Kg 110 70 - 120 2 20
1,2-Dichloroethane 2500 2580 ug/Kg 103 60 - 145 3 20
1,2-Dichloropropane 2500 2690 ug/Kg 108 75 - 125 0 20
1,3,5-Trimethylbenzene 2500 2850 ug/Kg 114 70 - 125 0 20 1,3-Dichlorobenzene 2500 2720 ug/Kg 109 70 - 125 0 20
1,3-Dichloropropane 2500 2720 ug/Kg 109 65 - 130 7 20
1,4-Dichlorobenzene 2500 2680 ug/Kg 107 70 - 125 2 20
2,2-Dichloropropane 2500 2720 ug/Kg 109 60 - 145 3 25
2-Chlorotoluene 2500 2700 ug/Kg 108 70 - 125 0 20
4-Chlorotoluene 2500 2710 ug/Kg 108 70 - 125 1 20
Benzene 2500 2700 ug/Kg 108 65 - 120 0 20
Bromobenzene 2500 2690 ug/Kg 108 70 - 120 0 20
Bromochloromethane 2500 2640 ug/Kg 106 65 - 125 0 20
Bromodichloromethane 2500 2670 ug/Kg 107 65 - 135 1 20
Bromoform 2500 2940 ug/Kg 118 50 - 130 6 25
Bromomethane 2500 1730 ug/Kg 69 30 - 140 2 30
Carbon tetrachloride 2500 2860 ug/Kg 114 65 - 145 4 20
Chlorobenzene 2500 2720 ug/Kg 109 70 - 125 6 20
Chloroethane 2500 2350 ug/Kg 94 40 - 140 1 25
Chloroform 2500 2620 ug/Kg 105 75 - 130 2 20
Chloromethane 2500 1930 ug/Kg 77 30 - 140 6 25
cis-1,2-Dichloroethene 2500 2780 ug/Kg 111 65 - 130 1 20 cis-1,3-Dichloropropene 2500 2980 ug/Kg 119 70 - 130 9 20 Dibromochloromethane 2500 2780 ug/Kg 111 65 - 140 6 20
Dibromomethane 2500 2620 ug/Kg 105 65 - 130 3 20
Dichlorodifluoromethane 2500 1510 ug/Kg 60 10 - 155 0 30 TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-342991/9 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342991
Isopropyl Ether (DIPE) 2500 2750 ug/Kg 110 60 - 140 1 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Ethanol 100000 120000 ug/Kg 120 35 - 160 1 30
Ethyl-t-butyl ether (ETBE) 2500 2630 ug/Kg 105 60 - 140 2 20 Ethylbenzene 2500 2840 ug/Kg 114 80 - 120 7 20
Hexachlorobutadiene 2500 3040 ug/Kg 121 60 - 135 2 20
Isopropylbenzene 2500 3010 ug/Kg 120 70 - 125 8 20
m,p-Xylene 2500 2880 ug/Kg 115 70 - 125 7 20
Methylene Chloride 2500 2700 ug/Kg 108 60 - 140 0 20
Methyl-t-Butyl Ether (MTBE) 2500 2630 ug/Kg 105 55 - 145 1 25 Naphthalene 2500 2700 ug/Kg 108 50 - 140 0 25
n-Butylbenzene 2500 3100 ug/Kg 124 70 - 130 2 20
N-Propylbenzene 2500 2850 ug/Kg 114 70 - 130 1 20
o-Xylene 2500 2810 ug/Kg 112 70 - 125 6 20
sec-Butylbenzene 2500 2880 ug/Kg 115 70 - 125 1 20
Styrene 2500 2920 ug/Kg 117 70 - 135 9 20
Tert-amyl-methyl ether (TAME) 2500 2720 ug/Kg 109 60 - 145 2 25 tert-Butyl alcohol (TBA) 25000 25500 ug/Kg 102 65 - 140 1 20 tert-Butylbenzene 2500 2910 ug/Kg 117 70 - 125 1 20
Tetrachloroethene 2500 2980 ug/Kg 119 65 - 125 7 20
Toluene 2500 2840 ug/Kg 114 80 - 120 8 20
trans-1,2-Dichloroethene 2500 3040 ug/Kg 122 65 - 130 1 20 trans-1,3-Dichloropropene 2500 2900 ug/Kg 116 65 - 135 9 20 Trichloroethene 2500 2670 ug/Kg 107 70 - 130 3 20
Trichlorofluoromethane 2500 2510 ug/Kg 100 50 - 145 2 25 Vinyl chloride 2500 1200 ug/Kg 48 10 - 120 3 30
p-Isopropyltoluene 2500 2920 ug/Kg 117 70 - 125 0 20
Toluene-d8 (Surr) 60 - 140
Surrogate
108

LCSD LCSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 101 65 - 140
Dibromofluoromethane (Surr) 98 55 - 140
Lab Sample ID: MB 440-343001/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
RL MDL
1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 1,1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,1-Dichloroethene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
1,1-Dichloropropene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 07/18/16 08:35 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-343001/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
RL MDL
1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 07/18/16 08:35 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,2-Dichloroethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,3-Dichloropropane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
2,2-Dichloropropane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
2-Chlorotoluene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
4-Chlorotoluene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Benzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Bromobenzene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Bromochloromethane ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Bromodichloromethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Bromoform ND 5.0 2.0 ug/Kg 07/18/16 08:35 1
Bromomethane ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Carbon tetrachloride ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Chlorobenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Chloroethane ND 5.0 2.0 ug/Kg 07/18/16 08:35 1
Chloroform ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Chloromethane ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Dibromomethane ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 07/18/16 08:35 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 Ethanol ND 300 100 ug/Kg 07/18/16 08:35 1
Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 Ethylbenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Hexachlorobutadiene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Isopropylbenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
m,p-Xylene ND 4.0 2.0 ug/Kg 07/18/16 08:35 1
Methylene Chloride ND 20 5.0 ug/Kg 07/18/16 08:35 1
Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 Naphthalene ND 5.0 2.0 ug/Kg 07/18/16 08:35 1
n-Butylbenzene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
N-Propylbenzene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
o-Xylene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
sec-Butylbenzene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Styrene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 07/18/16 08:35 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Tetrachloroethene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Toluene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-343001/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
RL MDL
trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1 Trichloroethene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Trichlorofluoromethane ND 5.0 1.0 ug/Kg 07/18/16 08:35 1 Vinyl chloride ND 5.0 1.0 ug/Kg 07/18/16 08:35 1
Xylenes, Total ND 4.0 2.0 ug/Kg 07/18/16 08:35 1
p-Isopropyltoluene ND 2.0 1.0 ug/Kg 07/18/16 08:35 1
Toluene-d8 (Surr) 103 79 - 123 07/18/16 08:35 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 98 79 - 120 07/18/16 08:35 1 Dibromofluoromethane (Surr) 96 60 - 120 07/18/16 08:35 1 Lab Sample ID: LCS 440-343001/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
1,1,1,2-Tetrachloroethane 50.0 46.5 ug/Kg 93 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 50.0 45.6 ug/Kg 91 65 - 135
1,1,2,2-Tetrachloroethane 50.0 53.1 ug/Kg 106 55 - 140
1,1,2-Trichloroethane 50.0 49.5 ug/Kg 99 65 - 135
1,1-Dichloroethane 50.0 46.3 ug/Kg 93 70 - 130
1,1-Dichloroethene 50.0 48.8 ug/Kg 98 70 - 125
1,1-Dichloropropene 50.0 54.0 ug/Kg 108 70 - 130
1,2,3-Trichlorobenzene 50.0 52.4 ug/Kg 105 60 - 130
1,2,3-Trichloropropane 50.0 46.4 ug/Kg 93 60 - 135
1,2,4-Trichlorobenzene 50.0 54.9 ug/Kg 110 70 - 135
1,2,4-Trimethylbenzene 50.0 50.8 ug/Kg 102 70 - 125
1,2-Dibromo-3-Chloropropane 50.0 46.3 ug/Kg 93 50 - 135 1,2-Dibromoethane (EDB) 50.0 53.6 ug/Kg 107 70 - 130
1,2-Dichlorobenzene 50.0 48.7 ug/Kg 97 75 - 120
1,2-Dichloroethane 50.0 43.0 ug/Kg 86 60 - 140
1,2-Dichloropropane 50.0 50.0 ug/Kg 100 70 - 130
1,3,5-Trimethylbenzene 50.0 50.7 ug/Kg 101 70 - 125
1,3-Dichlorobenzene 50.0 48.0 ug/Kg 96 75 - 125
1,3-Dichloropropane 50.0 49.2 ug/Kg 98 70 - 125
1,4-Dichlorobenzene 50.0 44.4 ug/Kg 89 75 - 120
2,2-Dichloropropane 50.0 45.1 ug/Kg 90 60 - 145
2-Chlorotoluene 50.0 48.5 ug/Kg 97 70 - 125
4-Chlorotoluene 50.0 48.3 ug/Kg 97 75 - 125
Benzene 50.0 50.1 ug/Kg 100 65 - 120
Bromobenzene 50.0 53.2 ug/Kg 106 75 - 120
Bromochloromethane 50.0 49.2 ug/Kg 98 70 - 135
Bromodichloromethane 50.0 48.2 ug/Kg 96 70 - 135
Bromoform 50.0 48.1 ug/Kg 96 55 - 135
Bromomethane 50.0 42.9 ug/Kg 86 60 - 145
Carbon tetrachloride 50.0 48.3 ug/Kg 97 65 - 140
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343001/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
Chlorobenzene 50.0 45.8 ug/Kg 92 75 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Chloroethane 50.0 44.4 ug/Kg 89 60 - 140
Chloroform 50.0 46.3 ug/Kg 93 70 - 130
Chloromethane 50.0 39.2 ug/Kg 78 45 - 145
cis-1,2-Dichloroethene 50.0 51.4 ug/Kg 103 70 - 125
cis-1,3-Dichloropropene 50.0 50.4 ug/Kg 101 75 - 125
Dibromochloromethane 50.0 47.3 ug/Kg 95 65 - 140
Dibromomethane 50.0 47.0 ug/Kg 94 70 - 130
Dichlorodifluoromethane 50.0 38.4 ug/Kg 77 35 - 160
Isopropyl Ether (DIPE) 50.0 53.0 ug/Kg 106 60 - 140
Ethanol 2000 1720 ug/Kg 86 35 - 160
Ethyl-t-butyl ether (ETBE) 50.0 51.0 ug/Kg 102 60 - 140 Ethylbenzene 50.0 53.5 ug/Kg 107 70 - 125
Hexachlorobutadiene 50.0 46.4 ug/Kg 93 60 - 135
Isopropylbenzene 50.0 50.8 ug/Kg 102 75 - 130
m,p-Xylene 50.0 51.4 ug/Kg 103 70 - 125
Methylene Chloride 50.0 46.2 ug/Kg 92 55 - 135
Methyl-t-Butyl Ether (MTBE) 50.0 53.7 ug/Kg 107 60 - 140 Naphthalene 50.0 51.7 ug/Kg 103 55 - 135
n-Butylbenzene 50.0 51.4 ug/Kg 103 70 - 130
N-Propylbenzene 50.0 51.6 ug/Kg 103 70 - 130
o-Xylene 50.0 47.4 ug/Kg 95 70 - 125
sec-Butylbenzene 50.0 50.6 ug/Kg 101 70 - 125
Styrene 50.0 47.0 ug/Kg 94 75 - 130
Tert-amyl-methyl ether (TAME) 50.0 54.4 ug/Kg 109 60 - 145 tert-Butyl alcohol (TBA) 500 470 ug/Kg 94 70 - 135
tert-Butylbenzene 50.0 50.6 ug/Kg 101 70 - 125
Tetrachloroethene 50.0 49.4 ug/Kg 99 70 - 125
Toluene 50.0 51.5 ug/Kg 103 70 - 125
trans-1,2-Dichloroethene 50.0 53.3 ug/Kg 107 70 - 125
trans-1,3-Dichloropropene 50.0 47.3 ug/Kg 95 70 - 135
Trichloroethene 50.0 49.8 ug/Kg 100 70 - 125
Trichlorofluoromethane 50.0 40.8 ug/Kg 82 60 - 145
Vinyl chloride 50.0 41.3 ug/Kg 83 55 - 135
p-Isopropyltoluene 50.0 53.4 ug/Kg 107 75 - 125
Toluene-d8 (Surr) 79 - 123
Surrogate
103

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 79 - 120
Dibromofluoromethane (Surr) 96 60 - 120
Lab Sample ID: 440-152882-A-2 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
1,1,1,2-Tetrachloroethane ND 49.9 45.1 ug/Kg 90 65 - 145 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 49.9 45.6 ug/Kg 91 65 - 145
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152882-A-2 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
1,1,2,2-Tetrachloroethane ND 49.9 54.0 ug/Kg 108 40 - 160 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,2-Trichloroethane ND 49.9 47.8 ug/Kg 96 65 - 140
1,1-Dichloroethane ND 49.9 45.5 ug/Kg 91 65 - 135
1,1-Dichloroethene ND 49.9 48.9 ug/Kg 98 65 - 135
1,1-Dichloropropene ND 49.9 53.5 ug/Kg 107 65 - 135
1,2,3-Trichlorobenzene ND 49.9 50.3 ug/Kg 101 45 - 145
1,2,3-Trichloropropane ND 49.9 48.1 ug/Kg 96 50 - 150
1,2,4-Trichlorobenzene ND 49.9 50.4 ug/Kg 101 50 - 140
1,2,4-Trimethylbenzene ND 49.9 49.0 ug/Kg 98 65 - 140
1,2-Dibromo-3-Chloropropane ND 49.9 47.5 ug/Kg 95 40 - 150 1,2-Dibromoethane (EDB) ND 49.9 52.6 ug/Kg 105 65 - 140 1,2-Dichlorobenzene ND 49.9 47.8 ug/Kg 96 70 - 130
1,2-Dichloroethane ND 49.9 42.8 ug/Kg 86 60 - 150
1,2-Dichloropropane ND 49.9 48.6 ug/Kg 97 65 - 130
1,3,5-Trimethylbenzene ND 49.9 49.7 ug/Kg 100 65 - 135
1,3-Dichlorobenzene ND 49.9 46.7 ug/Kg 94 70 - 130
1,3-Dichloropropane ND 49.9 49.5 ug/Kg 99 65 - 140
1,4-Dichlorobenzene ND 49.9 44.6 ug/Kg 89 70 - 130
2,2-Dichloropropane ND 49.9 46.9 ug/Kg 94 65 - 150
2-Chlorotoluene ND 49.9 47.8 ug/Kg 96 60 - 135
4-Chlorotoluene ND 49.9 47.3 ug/Kg 95 65 - 135
Benzene ND 49.9 49.4 ug/Kg 99 65 - 130
Bromobenzene ND 49.9 51.1 ug/Kg 102 65 - 140
Bromochloromethane ND 49.9 47.4 ug/Kg 95 65 - 145
Bromodichloromethane ND 49.9 47.1 ug/Kg 94 65 - 145
Bromoform ND 49.9 48.4 ug/Kg 97 50 - 145
Bromomethane ND 49.9 42.5 ug/Kg 85 60 - 155
Carbon tetrachloride ND 49.9 48.4 ug/Kg 97 60 - 145
Chlorobenzene ND 49.9 45.6 ug/Kg 91 70 - 130
Chloroethane ND 49.9 44.9 ug/Kg 90 60 - 150
Chloroform ND 49.9 44.7 ug/Kg 90 65 - 135
Chloromethane ND 49.9 39.4 ug/Kg 79 40 - 145
cis-1,2-Dichloroethene ND 49.9 49.3 ug/Kg 99 65 - 135
cis-1,3-Dichloropropene ND 49.9 49.5 ug/Kg 99 70 - 135
Dibromochloromethane ND 49.9 46.6 ug/Kg 93 60 - 145
Dibromomethane ND 49.9 47.4 ug/Kg 95 65 - 140
Dichlorodifluoromethane ND 49.9 38.7 ug/Kg 78 30 - 160
Isopropyl Ether (DIPE) ND 49.9 50.9 ug/Kg 102 60 - 150
Ethanol ND 2000 1660 ug/Kg 83 30 - 165
Ethyl-t-butyl ether (ETBE) ND 49.9 49.0 ug/Kg 98 60 - 145 Ethylbenzene ND 49.9 54.1 ug/Kg 108 70 - 135
Hexachlorobutadiene ND 49.9 44.3 ug/Kg 89 50 - 145
Isopropylbenzene ND 49.9 52.3 ug/Kg 105 70 - 145
m,p-Xylene ND 49.9 51.8 ug/Kg 104 70 - 130
Methylene Chloride ND 49.9 45.2 ug/Kg 91 55 - 145
Methyl-t-Butyl Ether (MTBE) ND 49.9 52.2 ug/Kg 105 55 - 155 Naphthalene ND 49.9 50.9 ug/Kg 102 40 - 150
n-Butylbenzene ND 49.9 50.7 ug/Kg 102 55 - 145
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152882-A-2 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
N-Propylbenzene ND 49.9 50.8 ug/Kg 102 65 - 140
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
o-Xylene ND 49.9 47.1 ug/Kg 94 65 - 130
sec-Butylbenzene ND 49.9 49.6 ug/Kg 99 60 - 135
Styrene ND 49.9 47.3 ug/Kg 95 70 - 140
Tert-amyl-methyl ether (TAME) ND 49.9 50.9 ug/Kg 102 60 - 150 tert-Butyl alcohol (TBA) ND 499 480 ug/Kg 96 65 - 145
tert-Butylbenzene ND 49.9 49.4 ug/Kg 99 60 - 140
Tetrachloroethene ND 49.9 50.1 ug/Kg 100 65 - 135
Toluene ND 49.9 50.9 ug/Kg 102 70 - 130
trans-1,2-Dichloroethene ND 49.9 52.4 ug/Kg 105 70 - 135 trans-1,3-Dichloropropene ND 49.9 47.4 ug/Kg 95 60 - 145 Trichloroethene ND 49.9 49.5 ug/Kg 99 65 - 140
Trichlorofluoromethane ND 49.9 42.3 ug/Kg 85 55 - 155
Vinyl chloride ND 49.9 41.3 ug/Kg 83 55 - 140
p-Isopropyltoluene ND 49.9 53.0 ug/Kg 106 60 - 140
Toluene-d8 (Surr) 79 - 123
Surrogate
103
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 79 - 120
Dibromofluoromethane (Surr) 94 60 - 120
Lab Sample ID: 440-152882-A-2 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
1,1,1,2-Tetrachloroethane ND 49.7 46.8 ug/Kg 94 65 - 145 4 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 49.7 45.8 ug/Kg 92 65 - 145 0 20 1,1,2,2-Tetrachloroethane ND 49.7 56.5 ug/Kg 114 40 - 160 5 30 1,1,2-Trichloroethane ND 49.7 49.5 ug/Kg 100 65 - 140 3 30 1,1-Dichloroethane ND 49.7 46.3 ug/Kg 93 65 - 135 2 25
1,1-Dichloroethene ND 49.7 51.0 ug/Kg 103 65 - 135 4 25 1,1-Dichloropropene ND 49.7 53.8 ug/Kg 108 65 - 135 1 20 1,2,3-Trichlorobenzene ND 49.7 52.6 ug/Kg 106 45 - 145 4 30 1,2,3-Trichloropropane ND 49.7 49.5 ug/Kg 100 50 - 150 3 30 1,2,4-Trichlorobenzene ND 49.7 52.4 ug/Kg 105 50 - 140 4 30 1,2,4-Trimethylbenzene ND 49.7 50.1 ug/Kg 101 65 - 140 2 25 1,2-Dibromo-3-Chloropropane ND 49.7 50.5 ug/Kg 102 40 - 150 6 30 1,2-Dibromoethane (EDB) ND 49.7 54.8 ug/Kg 110 65 - 140 4 25 1,2-Dichlorobenzene ND 49.7 48.9 ug/Kg 98 70 - 130 2 25 1,2-Dichloroethane ND 49.7 43.7 ug/Kg 88 60 - 150 2 25
1,2-Dichloropropane ND 49.7 50.5 ug/Kg 102 65 - 130 4 20 1,3,5-Trimethylbenzene ND 49.7 49.7 ug/Kg 100 65 - 135 0 25 1,3-Dichlorobenzene ND 49.7 47.8 ug/Kg 96 70 - 130 2 25 1,3-Dichloropropane ND 49.7 49.5 ug/Kg 100 65 - 140 0 25 1,4-Dichlorobenzene ND 49.7 44.6 ug/Kg 90 70 - 130 0 25 2,2-Dichloropropane ND 49.7 46.9 ug/Kg 94 65 - 150 0 25 2-Chlorotoluene ND 49.7 47.2 ug/Kg 95 60 - 135 1 25
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152882-A-2 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343001
4-Chlorotoluene ND 49.7 46.9 ug/Kg 94 65 - 135 1 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Benzene ND 49.7 49.7 ug/Kg 100 65 - 130 1 20
Bromobenzene ND 49.7 50.5 ug/Kg 102 65 - 140 1 25
Bromochloromethane ND 49.7 50.9 ug/Kg 103 65 - 145 7 25 Bromodichloromethane ND 49.7 48.7 ug/Kg 98 65 - 145 3 20 Bromoform ND 49.7 50.4 ug/Kg 101 50 - 145 4 30
Bromomethane ND 49.7 44.7 ug/Kg 90 60 - 155 5 25
Carbon tetrachloride ND 49.7 49.0 ug/Kg 99 60 - 145 1 25 Chlorobenzene ND 49.7 45.2 ug/Kg 91 70 - 130 1 25
Chloroethane ND 49.7 46.0 ug/Kg 93 60 - 150 2 25
Chloroform ND 49.7 45.6 ug/Kg 92 65 - 135 2 20
Chloromethane ND 49.7 41.4 ug/Kg 83 40 - 145 5 25
cis-1,2-Dichloroethene ND 49.7 50.4 ug/Kg 101 65 - 135 2 25 cis-1,3-Dichloropropene ND 49.7 50.3 ug/Kg 101 70 - 135 2 25 Dibromochloromethane ND 49.7 47.3 ug/Kg 95 60 - 145 2 25 Dibromomethane ND 49.7 48.5 ug/Kg 98 65 - 140 2 25
Dichlorodifluoromethane ND 49.7 39.1 ug/Kg 79 30 - 160 1 35 Isopropyl Ether (DIPE) ND 49.7 52.8 ug/Kg 106 60 - 150 4 25 Ethanol ND 1990 1670 ug/Kg 84 30 - 165 1 40
Ethyl-t-butyl ether (ETBE) ND 49.7 51.5 ug/Kg 104 60 - 145 5 30 Ethylbenzene ND 49.7 53.4 ug/Kg 107 70 - 135 1 25
Hexachlorobutadiene ND 49.7 45.6 ug/Kg 92 50 - 145 3 35 Isopropylbenzene ND 49.7 52.2 ug/Kg 105 70 - 145 0 25
m,p-Xylene ND 49.7 52.4 ug/Kg 105 70 - 130 1 25
Methylene Chloride ND 49.7 46.6 ug/Kg 94 55 - 145 3 25
Methyl-t-Butyl Ether (MTBE) ND 49.7 56.4 ug/Kg 114 55 - 155 8 35 Naphthalene ND 49.7 53.1 ug/Kg 107 40 - 150 4 40
n-Butylbenzene ND 49.7 51.7 ug/Kg 104 55 - 145 2 30
N-Propylbenzene ND 49.7 50.1 ug/Kg 101 65 - 140 1 25
o-Xylene ND 49.7 47.6 ug/Kg 96 65 - 130 1 25
sec-Butylbenzene ND 49.7 49.8 ug/Kg 100 60 - 135 0 25
Styrene ND 49.7 46.8 ug/Kg 94 70 - 140 1 25
Tert-amyl-methyl ether (TAME) ND 49.7 55.5 ug/Kg 112 60 - 150 8 25 tert-Butyl alcohol (TBA) ND 497 468 ug/Kg 94 65 - 145 2 30 tert-Butylbenzene ND 49.7 49.4 ug/Kg 99 60 - 140 0 25
Tetrachloroethene ND 49.7 50.0 ug/Kg 101 65 - 135 0 25
Toluene ND 49.7 51.1 ug/Kg 103 70 - 130 0 20
trans-1,2-Dichloroethene ND 49.7 53.0 ug/Kg 107 70 - 135 1 25 trans-1,3-Dichloropropene ND 49.7 48.4 ug/Kg 97 60 - 145 2 25 Trichloroethene ND 49.7 49.1 ug/Kg 99 65 - 140 1 25
Trichlorofluoromethane ND 49.7 43.2 ug/Kg 87 55 - 155 2 25 Vinyl chloride ND 49.7 42.6 ug/Kg 86 55 - 140 3 30
p-Isopropyltoluene ND 49.7 53.1 ug/Kg 107 60 - 140 0 25 Toluene-d8 (Surr) 79 - 123
Surrogate
103

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 95 79 - 120
Dibromofluoromethane (Surr) 95 60 - 120
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Lab Sample ID: MB 440-343275/5 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 08:47 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/19/16 08:47 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/19/16 08:47 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/19/16 08:47 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/19/16 08:47 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/19/16 08:47 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/19/16 08:47 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 08:47 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Benzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Bromobenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Bromochloromethane ND 0.50 0.25 ug/L 07/19/16 08:47 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 Bromoform ND 1.0 0.40 ug/L 07/19/16 08:47 1
Bromomethane ND 0.50 0.25 ug/L 07/19/16 08:47 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/19/16 08:47 1 Chlorobenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Chloroethane ND 1.0 0.40 ug/L 07/19/16 08:47 1
Chloroform ND 0.50 0.25 ug/L 07/19/16 08:47 1
Chloromethane ND 0.50 0.25 ug/L 07/19/16 08:47 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 08:47 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 08:47 1 Dibromochloromethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 Dibromomethane ND 0.50 0.25 ug/L 07/19/16 08:47 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/19/16 08:47 1 Ethanol ND 150 75 ug/L 07/19/16 08:47 1
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/19/16 08:47 1 Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/19/16 08:47 1 Ethylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
m,p-Xylene ND 1.0 0.50 ug/L 07/19/16 08:47 1
Methylene Chloride ND 2.0 0.88 ug/L 07/19/16 08:47 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/19/16 08:47 1 Naphthalene ND 1.0 0.40 ug/L 07/19/16 08:47 1
n-Butylbenzene ND 1.0 0.40 ug/L 07/19/16 08:47 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-343275/5 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
RL MDL
N-Propylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac o-Xylene ND 0.50 0.25 ug/L 07/19/16 08:47 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/19/16 08:47 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Styrene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/19/16 08:47 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Toluene ND 0.50 0.25 ug/L 07/19/16 08:47 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/19/16 08:47 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/19/16 08:47 1 Trichloroethene ND 0.50 0.25 ug/L 07/19/16 08:47 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/19/16 08:47 1 Xylenes, Total ND 1.0 0.50 ug/L 07/19/16 08:47 1
Vinyl chloride ND 0.50 0.25 ug/L 07/19/16 08:47 1
tert-Butyl alcohol (TBA) ND 10 5.0 ug/L 07/19/16 08:47 1 4-Bromofluorobenzene (Surr) 102 80 - 120 07/19/16 08:47 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 113 76 - 132 07/19/16 08:47 1 Toluene-d8 (Surr) 111 80 - 128 07/19/16 08:47 1
Lab Sample ID: LCS 440-343275/6 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
1,1,1,2-Tetrachloroethane 25.0 27.9 ug/L 112 60 - 141
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 25.0 24.1 ug/L 96 70 - 130
1,1,2,2-Tetrachloroethane 25.0 23.8 ug/L 95 63 - 130
1,1,2-Trichloroethane 25.0 25.6 ug/L 103 70 - 130
1,1-Dichloroethane 25.0 25.1 ug/L 100 64 - 130
1,1-Dichloroethene 25.0 24.3 ug/L 97 70 - 130
1,1-Dichloropropene 25.0 23.6 ug/L 94 70 - 130
1,2,3-Trichlorobenzene 25.0 27.4 ug/L 110 60 - 140
1,2,3-Trichloropropane 25.0 22.6 ug/L 91 63 - 130
1,2,4-Trichlorobenzene 25.0 27.8 ug/L 111 60 - 140
1,2,4-Trimethylbenzene 25.0 24.0 ug/L 96 70 - 135
1,2-Dibromo-3-Chloropropane 25.0 20.1 ug/L 80 52 - 140
1,2-Dibromoethane (EDB) 25.0 28.5 ug/L 114 70 - 130
1,2-Dichlorobenzene 25.0 25.9 ug/L 104 70 - 130
1,2-Dichloroethane 25.0 26.0 ug/L 104 57 - 138
1,2-Dichloropropane 25.0 27.9 ug/L 112 67 - 130
1,3,5-Trimethylbenzene 25.0 23.6 ug/L 94 70 - 136
1,3-Dichlorobenzene 25.0 25.1 ug/L 100 70 - 130
1,3-Dichloropropane 25.0 24.0 ug/L 96 70 - 130
1,4-Dichlorobenzene 25.0 25.4 ug/L 102 70 - 130
2,2-Dichloropropane 25.0 23.7 ug/L 95 68 - 141
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343275/6 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
2-Chlorotoluene 25.0 23.5 ug/L 94 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Chlorotoluene 25.0 25.0 ug/L 100 70 - 130
Benzene 25.0 25.7 ug/L 103 68 - 130
Bromobenzene 25.0 26.0 ug/L 104 70 - 130
Bromochloromethane 25.0 26.5 ug/L 106 70 - 130
Bromodichloromethane 25.0 27.2 ug/L 109 70 - 132
Bromoform 25.0 28.9 ug/L 115 60 - 148
Bromomethane 25.0 21.3 ug/L 85 64 - 139
Carbon tetrachloride 25.0 24.2 ug/L 97 60 - 150
Chlorobenzene 25.0 26.3 ug/L 105 70 - 130
Chloroethane 25.0 20.8 ug/L 83 64 - 135
Chloroform 25.0 26.3 ug/L 105 70 - 130
Chloromethane 25.0 21.7 ug/L 87 47 - 140
cis-1,2-Dichloroethene 25.0 25.3 ug/L 101 70 - 133
cis-1,3-Dichloropropene 25.0 29.5 ug/L 118 70 - 133
Dibromochloromethane 25.0 28.2 ug/L 113 69 - 145
Dibromomethane 25.0 25.6 ug/L 102 70 - 130
Dichlorodifluoromethane 25.0 17.2 ug/L 69 29 - 150
Ethanol 1000 982 ug/L 98 50 - 149
Isopropyl Ether (DIPE) 25.0 28.9 ug/L 116 58 - 139
Ethyl-t-butyl ether (ETBE) 25.0 28.9 ug/L 116 60 - 136
Ethylbenzene 25.0 25.0 ug/L 100 70 - 130
Hexachlorobutadiene 25.0 24.0 ug/L 96 10 - 150
Isopropylbenzene 25.0 24.9 ug/L 99 70 - 136
m,p-Xylene 25.0 26.9 ug/L 107 70 - 130
Methylene Chloride 25.0 26.3 ug/L 105 52 - 130
Methyl-t-Butyl Ether (MTBE) 25.0 27.5 ug/L 110 63 - 131 Naphthalene 25.0 25.4 ug/L 102 60 - 140
n-Butylbenzene 25.0 22.8 ug/L 91 65 - 150
N-Propylbenzene 25.0 22.7 ug/L 91 67 - 139
o-Xylene 25.0 27.2 ug/L 109 70 - 130
p-Isopropyltoluene 25.0 23.1 ug/L 92 70 - 132
sec-Butylbenzene 25.0 22.5 ug/L 90 70 - 138
Styrene 25.0 28.5 ug/L 114 70 - 134
Tert-amyl-methyl ether (TAME) 25.0 29.1 ug/L 116 57 - 139 tert-Butylbenzene 25.0 22.9 ug/L 92 70 - 130
Tetrachloroethene 25.0 25.5 ug/L 102 70 - 130
Toluene 25.0 25.5 ug/L 102 70 - 130
trans-1,2-Dichloroethene 25.0 25.6 ug/L 102 70 - 130
trans-1,3-Dichloropropene 25.0 28.5 ug/L 114 70 - 132
Trichloroethene 25.0 22.5 ug/L 90 70 - 130
Trichlorofluoromethane 25.0 21.9 ug/L 88 60 - 150
Vinyl chloride 25.0 20.5 ug/L 82 59 - 133
tert-Butyl alcohol (TBA) 250 247 ug/L 99 70 - 130
4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
102

LCS LCS
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 112 76 - 132
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343275/6 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
Toluene-d8 (Surr) 80 - 128
Surrogate
110

LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 440-152586-7 MS Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
1,1,1,2-Tetrachloroethane ND 25.0 25.7 ug/L 103 60 - 149 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 25.0 23.4 ug/L 93 70 - 130
1,1,2,2-Tetrachloroethane ND 25.0 28.7 ug/L 115 63 - 130 1,1,2-Trichloroethane ND 25.0 26.2 ug/L 105 70 - 130
1,1-Dichloroethane ND 25.0 23.5 ug/L 94 65 - 130
1,1-Dichloroethene ND 25.0 22.8 ug/L 91 70 - 130
1,1-Dichloropropene ND 25.0 22.7 ug/L 91 64 - 130
1,2,3-Trichlorobenzene ND 25.0 28.0 ug/L 112 60 - 140
1,2,3-Trichloropropane ND 25.0 27.3 ug/L 109 60 - 130
1,2,4-Trichlorobenzene ND 25.0 27.4 ug/L 109 60 - 140
1,2,4-Trimethylbenzene ND 25.0 22.3 ug/L 89 70 - 130
1,2-Dibromo-3-Chloropropane ND 25.0 29.9 ug/L 119 48 - 140 1,2-Dibromoethane (EDB) ND 25.0 29.8 ug/L 119 70 - 131
1,2-Dichlorobenzene ND 25.0 25.0 ug/L 100 70 - 130
1,2-Dichloroethane ND 25.0 26.4 ug/L 106 56 - 146
1,2-Dichloropropane ND 25.0 26.6 ug/L 106 69 - 130
1,3,5-Trimethylbenzene ND 25.0 21.8 ug/L 87 70 - 130
1,3-Dichlorobenzene ND 25.0 23.7 ug/L 95 70 - 130
1,3-Dichloropropane ND 25.0 25.0 ug/L 100 70 - 130
1,4-Dichlorobenzene ND 25.0 24.2 ug/L 97 70 - 130
2,2-Dichloropropane ND 25.0 22.8 ug/L 91 69 - 138
2-Chlorotoluene ND 25.0 21.7 ug/L 87 70 - 130
4-Chlorotoluene ND 25.0 23.3 ug/L 93 70 - 130
Benzene ND 25.0 24.6 ug/L 98 66 - 130
Bromobenzene ND 25.0 24.7 ug/L 99 70 - 130
Bromochloromethane ND 25.0 26.0 ug/L 104 70 - 130
Bromodichloromethane ND 25.0 26.3 ug/L 105 70 - 138
Bromoform ND 25.0 31.1 ug/L 124 59 - 150
Bromomethane ND 25.0 19.9 ug/L 80 62 - 131
Carbon tetrachloride ND 25.0 23.2 ug/L 93 60 - 150
Chlorobenzene ND 25.0 24.6 ug/L 99 70 - 130
Chloroethane ND 25.0 20.1 ug/L 80 68 - 130
Chloroform ND 25.0 24.9 ug/L 100 70 - 130
Chloromethane ND 25.0 20.9 ug/L 83 39 - 144
cis-1,2-Dichloroethene ND 25.0 24.1 ug/L 97 70 - 130
cis-1,3-Dichloropropene ND 25.0 27.8 ug/L 111 70 - 133
Dibromochloromethane ND 25.0 27.2 ug/L 109 70 - 148
Dibromomethane ND 25.0 26.9 ug/L 108 70 - 130
Dichlorodifluoromethane ND 25.0 15.5 ug/L 62 25 - 142
Ethanol ND 1000 788 ug/L 79 54 - 150
Isopropyl Ether (DIPE) ND 25.0 27.9 ug/L 112 64 - 138
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152586-7 MS Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
Ethyl-t-butyl ether (ETBE) ND 25.0 28.5 ug/L 114 70 - 130 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Ethylbenzene ND 25.0 23.2 ug/L 93 70 - 130
Hexachlorobutadiene ND 25.0 22.7 ug/L 91 10 - 150
Isopropylbenzene ND 25.0 23.2 ug/L 93 70 - 132
m,p-Xylene ND 25.0 24.7 ug/L 99 70 - 133
Methylene Chloride ND 25.0 25.6 ug/L 102 52 - 130
Methyl-t-Butyl Ether (MTBE) ND 25.0 29.5 ug/L 118 70 - 130 Naphthalene ND 25.0 31.5 ug/L 126 60 - 140
n-Butylbenzene ND 25.0 21.3 ug/L 85 61 - 149
N-Propylbenzene ND 25.0 20.9 ug/L 84 66 - 135
o-Xylene ND 25.0 25.1 ug/L 100 70 - 133
p-Isopropyltoluene ND 25.0 20.9 ug/L 84 70 - 130
sec-Butylbenzene ND 25.0 20.6 ug/L 82 67 - 134
Styrene ND 25.0 26.9 ug/L 107 29 - 150
Tert-amyl-methyl ether (TAME) ND 25.0 29.6 ug/L 118 68 - 133 tert-Butylbenzene ND 25.0 21.3 ug/L 85 70 - 130
Tetrachloroethene ND 25.0 23.2 ug/L 93 70 - 137
Toluene ND 25.0 23.5 ug/L 94 70 - 130
trans-1,2-Dichloroethene ND 25.0 24.7 ug/L 99 70 - 130
trans-1,3-Dichloropropene ND 25.0 28.7 ug/L 115 70 - 138 Trichloroethene ND 25.0 20.8 ug/L 83 70 - 130
Trichlorofluoromethane ND 25.0 20.6 ug/L 82 60 - 150
Vinyl chloride ND 25.0 19.6 ug/L 78 50 - 137
tert-Butyl alcohol (TBA) 11 ID 250 259 ug/L 99 70 - 130 4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
102
MS MS
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 113 76 - 132
Toluene-d8 (Surr) 108 80 - 128
Lab Sample ID: 440-152586-7 MSD Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
1,1,1,2-Tetrachloroethane ND 25.0 26.0 ug/L 104 60 - 149 1 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 25.0 24.2 ug/L 97 70 - 130 4 20 1,1,2,2-Tetrachloroethane ND 25.0 30.2 ug/L 121 63 - 130 5 30 1,1,2-Trichloroethane ND 25.0 26.2 ug/L 105 70 - 130 0 25 1,1-Dichloroethane ND 25.0 24.7 ug/L 99 65 - 130 5 20
1,1-Dichloroethene ND 25.0 23.7 ug/L 95 70 - 130 4 20
1,1-Dichloropropene ND 25.0 24.1 ug/L 96 64 - 130 6 20
1,2,3-Trichlorobenzene ND 25.0 27.7 ug/L 111 60 - 140 1 20 1,2,3-Trichloropropane ND 25.0 28.9 ug/L 116 60 - 130 6 30 1,2,4-Trichlorobenzene ND 25.0 27.5 ug/L 110 60 - 140 0 20 1,2,4-Trimethylbenzene ND 25.0 23.0 ug/L 92 70 - 130 3 25 1,2-Dibromo-3-Chloropropane ND 25.0 31.9 ug/L 128 48 - 140 7 30 1,2-Dibromoethane (EDB) ND 25.0 30.4 ug/L 122 70 - 131 2 25 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152586-7 MSD Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
1,2-Dichlorobenzene ND 25.0 25.8 ug/L 103 70 - 130 3 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,2-Dichloroethane ND 25.0 27.6 ug/L 110 56 - 146 4 20
1,2-Dichloropropane ND 25.0 27.3 ug/L 109 69 - 130 3 20 1,3,5-Trimethylbenzene ND 25.0 22.5 ug/L 90 70 - 130 3 20 1,3-Dichlorobenzene ND 25.0 24.1 ug/L 97 70 - 130 2 20
1,3-Dichloropropane ND 25.0 25.3 ug/L 101 70 - 130 1 25 1,4-Dichlorobenzene ND 25.0 25.2 ug/L 101 70 - 130 4 20 2,2-Dichloropropane ND 25.0 23.2 ug/L 93 69 - 138 2 25
2-Chlorotoluene ND 25.0 22.7 ug/L 91 70 - 130 5 20
4-Chlorotoluene ND 25.0 24.2 ug/L 97 70 - 130 3 20
Benzene ND 25.0 25.7 ug/L 103 66 - 130 5 20
Bromobenzene ND 25.0 25.8 ug/L 103 70 - 130 5 20
Bromochloromethane ND 25.0 26.9 ug/L 108 70 - 130 4 25
Bromodichloromethane ND 25.0 27.3 ug/L 109 70 - 138 3 20 Bromoform ND 25.0 31.5 ug/L 126 59 - 150 1 25
Bromomethane ND 25.0 20.6 ug/L 82 62 - 131 3 25
Carbon tetrachloride ND 25.0 23.9 ug/L 95 60 - 150 3 25 Chlorobenzene ND 25.0 24.9 ug/L 100 70 - 130 1 20
Chloroethane ND 25.0 20.6 ug/L 82 68 - 130 2 25
Chloroform ND 25.0 26.1 ug/L 105 70 - 130 5 20
Chloromethane ND 25.0 21.4 ug/L 85 39 - 144 2 25
cis-1,2-Dichloroethene ND 25.0 24.6 ug/L 98 70 - 130 2 20 cis-1,3-Dichloropropene ND 25.0 28.0 ug/L 112 70 - 133 1 20 Dibromochloromethane ND 25.0 27.8 ug/L 111 70 - 148 2 25 Dibromomethane ND 25.0 27.7 ug/L 111 70 - 130 3 25
Dichlorodifluoromethane ND 25.0 15.9 ug/L 64 25 - 142 3 30 Ethanol ND 1000 806 * ug/L 81 54 - 150 2 30
Isopropyl Ether (DIPE) ND 25.0 28.9 ug/L 116 64 - 138 3 25 Ethyl-t-butyl ether (ETBE) ND 25.0 29.7 ug/L 119 70 - 130 4 25 Ethylbenzene ND 25.0 23.4 ug/L 94 70 - 130 1 20
Hexachlorobutadiene ND 25.0 20.6 ug/L 82 10 - 150 10 20 Isopropylbenzene ND 25.0 23.0 ug/L 92 70 - 132 1 20
m,p-Xylene ND 25.0 24.6 ug/L 98 70 - 133 0 25
Methylene Chloride ND 25.0 25.9 ug/L 104 52 - 130 1 20
Methyl-t-Butyl Ether (MTBE) ND 25.0 30.5 ug/L 122 70 - 130 4 25 Naphthalene ND 25.0 33.1 ug/L 133 60 - 140 5 30
n-Butylbenzene ND 25.0 21.2 ug/L 85 61 - 149 0 20
N-Propylbenzene ND 25.0 21.7 ug/L 87 66 - 135 4 20
o-Xylene ND 25.0 24.8 ug/L 99 70 - 133 1 20
p-Isopropyltoluene ND 25.0 21.5 ug/L 86 70 - 130 3 20
sec-Butylbenzene ND 25.0 20.9 ug/L 83 67 - 134 1 20
Styrene ND 25.0 26.9 ug/L 108 29 - 150 0 35
Tert-amyl-methyl ether (TAME) ND 25.0 30.9 ug/L 123 68 - 133 4 30 tert-Butylbenzene ND 25.0 21.6 ug/L 86 70 - 130 2 20
Tetrachloroethene ND 25.0 23.5 ug/L 94 70 - 137 1 20
Toluene ND 25.0 23.8 ug/L 95 70 - 130 1 20
trans-1,2-Dichloroethene ND 25.0 24.6 ug/L 98 70 - 130 0 20 trans-1,3-Dichloropropene ND 25.0 28.2 ug/L 113 70 - 138 2 25 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152586-7 MSD Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343275
Trichloroethene ND 25.0 22.0 ug/L 88 70 - 130 6 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Trichlorofluoromethane ND 25.0 21.5 ug/L 86 60 - 150 4 25 Vinyl chloride ND 25.0 20.0 ug/L 80 50 - 137 2 30
tert-Butyl alcohol (TBA) 11 ID 250 266 * ug/L 102 70 - 130 3 25 4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
103

MSD MSD
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 113 76 - 132
Toluene-d8 (Surr) 105 80 - 128
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS Lab Sample ID: MB 440-342992/6 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342992
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 10000 7000 ug/Kg 07/18/16 09:48 100 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4-C12) ND 10000 7000 ug/Kg 07/18/16 09:48 100 Dibromofluoromethane (Surr) 101 55 - 140 07/18/16 09:48 100 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 107 65 - 140 07/18/16 09:48 100 Toluene-d8 (Surr) 109 60 - 140 07/18/16 09:48 100
Lab Sample ID: LCS 440-342992/10 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342992
Volatile Fuel Hydrocarbons
(C4-C12)
50000 51100 ug/Kg 102 60 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 55 - 140
Surrogate
98 LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 104 65 - 140
Toluene-d8 (Surr) 111 60 - 140
Lab Sample ID: LCSD 440-342992/11 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342992
Volatile Fuel Hydrocarbons
(C4-C12)
50000 51800 ug/Kg 104 60 - 130 1 25
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCSD 440-342992/11 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342992
Dibromofluoromethane (Surr) 55 - 140
Surrogate
96 LCSD LCSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 106 65 - 140
Toluene-d8 (Surr) 112 60 - 140
Lab Sample ID: MB 440-343002/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343002
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 100 70 ug/Kg 07/18/16 08:35 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 96 60 - 120 07/18/16 08:35 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 98 79 - 120 07/18/16 08:35 1 Toluene-d8 (Surr) 103 79 - 123 07/18/16 08:35 1
Lab Sample ID: LCS 440-343002/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343002
Volatile Fuel Hydrocarbons
(C4-C12)
1000 1040 ug/Kg 104 60 - 135
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
97 LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 99 79 - 120
Toluene-d8 (Surr) 103 79 - 123
Lab Sample ID: 440-152882-A-2 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343002
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3440 3790 ug/Kg 110 55 - 140
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 60 - 120
Surrogate
94 MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 79 - 120
Toluene-d8 (Surr) 103 79 - 123
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 440-152882-A-2 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343002
Volatile Fuel Hydrocarbons
(C4-C12)
ND 3430 3910 ug/Kg 114 55 - 140 3 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 60 - 120
Surrogate
95 MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 95 79 - 120
Toluene-d8 (Surr) 103 79 - 123
Lab Sample ID: MB 440-343276/5 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343276
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 50 35 ug/L 07/19/16 08:47 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 113 76 - 132 07/19/16 08:47 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 80 - 120 07/19/16 08:47 1 Toluene-d8 (Surr) 111 80 - 128 07/19/16 08:47 1
Lab Sample ID: LCS 440-343276/7 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343276
Volatile Fuel Hydrocarbons
(C4-C12)
500 446 ug/L 89 55 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 76 - 132
Surrogate
110

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 106 80 - 120
Toluene-d8 (Surr) 109 80 - 128
Lab Sample ID: 440-152586-7 MS Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343276
Volatile Fuel Hydrocarbons
(C4-C12)
49 J 1730 1610 ug/L 90 50 - 145
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 76 - 132
Surrogate
113
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 80 - 120
Toluene-d8 (Surr) 108 80 - 128
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 440-152586-7 MSD Client Sample ID: AEC-3-W Matrix: Water Prep Type: Total/NA
Analysis Batch: 343276
Volatile Fuel Hydrocarbons
(C4-C12)
49 J 1730 1650 ug/L 93 50 - 145 2 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 76 - 132
Surrogate
113

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 103 80 - 120
Toluene-d8 (Surr) 105 80 - 128
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) Lab Sample ID: MB 440-342341/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342341
RL MDL
Acenaphthene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Anthracene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Benzo[a]anthracene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Benzo[a]pyrene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Benzo[b]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Benzo[g,h,i]perylene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Benzo[k]fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Chrysene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Dibenz(a,h)anthracene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Fluoranthene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Fluorene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Indeno[1,2,3-cd]pyrene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Naphthalene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Phenanthrene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1 Pyrene ND 30 4.0 ug/Kg 07/14/16 09:34 07/15/16 10:49 1
2-Fluorobiphenyl (Surr) 69 39 - 111 07/15/16 10:49 1
MB MB
Surrogate
07/14/16 09:34
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Nitrobenzene-d5 66 41 - 119 07/14/16 09:34 07/15/16 10:49 1 Terphenyl-d14 81 43 - 150 07/14/16 09:34 07/15/16 10:49 1 Lab Sample ID: LCS 440-342341/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342341
Acenaphthene 66.7 48.8 ug/Kg 73 53 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acenaphthylene 66.7 48.9 ug/Kg 73 54 - 120
Anthracene 66.7 48.2 ug/Kg 72 53 - 120
Benzo[a]anthracene 66.7 53.1 ug/Kg 80 56 - 120
Benzo[a]pyrene 66.7 51.9 ug/Kg 78 53 - 120
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Lab Sample ID: LCS 440-342341/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342341
Benzo[b]fluoranthene 66.7 54.5 ug/Kg 82 53 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Benzo[g,h,i]perylene 66.7 74.5 ug/Kg 112 51 - 150
Benzo[k]fluoranthene 66.7 54.5 ug/Kg 82 53 - 124
Chrysene 66.7 53.7 ug/Kg 80 56 - 120
Dibenz(a,h)anthracene 66.7 53.8 ug/Kg 81 51 - 131
Fluoranthene 66.7 51.2 ug/Kg 77 57 - 120
Fluorene 66.7 49.9 ug/Kg 75 54 - 120
Indeno[1,2,3-cd]pyrene 66.7 56.3 ug/Kg 84 50 - 137
Naphthalene 66.7 46.7 ug/Kg 70 49 - 120
Phenanthrene 66.7 49.4 ug/Kg 74 55 - 120
Pyrene 66.7 51.7 ug/Kg 78 56 - 121
2-Fluorobiphenyl (Surr) 39 - 111
Surrogate
71 LCS LCS
%Recovery Qualifier Limits
Nitrobenzene-d5 67 41 - 119
Terphenyl-d14 85 43 - 150
Lab Sample ID: 440-152586-1 MS Client Sample ID: AEC-2-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342341
Acenaphthene ND 64.6 50.9 ug/Kg 79 45 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Acenaphthylene ND 64.6 51.4 ug/Kg 80 45 - 120
Anthracene ND 64.6 48.6 ug/Kg 75 55 - 120
Benzo[a]anthracene ND 64.6 52.9 ug/Kg 82 50 - 120
Benzo[a]pyrene ND 64.6 48.9 ug/Kg 76 45 - 125
Benzo[b]fluoranthene ND 64.6 53.2 ug/Kg 82 45 - 125
Benzo[g,h,i]perylene ND F2 64.6 43.6 ug/Kg 68 25 - 130
Benzo[k]fluoranthene ND 64.6 52.4 ug/Kg 81 45 - 125
Chrysene ND 64.6 53.4 ug/Kg 83 55 - 120
Dibenz(a,h)anthracene ND 64.6 34.5 ug/Kg 53 25 - 135
Fluoranthene ND 64.6 52.7 ug/Kg 82 45 - 120
Fluorene ND 64.6 50.7 ug/Kg 78 50 - 120
Indeno[1,2,3-cd]pyrene ND 64.6 34.5 ug/Kg 53 20 - 130
Naphthalene ND 64.6 47.9 ug/Kg 74 40 - 120
Phenanthrene ND 64.6 49.8 ug/Kg 77 50 - 120
Pyrene 5.5 J 64.6 53.7 ug/Kg 75 40 - 125
2-Fluorobiphenyl (Surr) 39 - 111
Surrogate
78 MS MS
%Recovery Qualifier Limits
Nitrobenzene-d5 71 41 - 119
Terphenyl-d14 113 43 - 150
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Lab Sample ID: 440-152586-1 MSD Client Sample ID: AEC-2-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342622 Prep Batch: 342341
Acenaphthene ND 66.4 50.8 ug/Kg 77 45 - 120 0 25
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Acenaphthylene ND 66.4 51.1 ug/Kg 77 45 - 120 0 20
Anthracene ND 66.4 49.5 ug/Kg 75 55 - 120 2 25
Benzo[a]anthracene ND 66.4 53.2 ug/Kg 80 50 - 120 1 25
Benzo[a]pyrene ND 66.4 50.2 ug/Kg 76 45 - 125 3 25
Benzo[b]fluoranthene ND 66.4 53.5 ug/Kg 81 45 - 125 1 30 Benzo[g,h,i]perylene ND F2 66.4 59.6 F2 ug/Kg 90 25 - 130 31 30 Benzo[k]fluoranthene ND 66.4 53.0 ug/Kg 80 45 - 125 1 30 Chrysene ND 66.4 54.0 ug/Kg 81 55 - 120 1 25
Dibenz(a,h)anthracene ND 66.4 41.4 ug/Kg 62 25 - 135 18 30 Fluoranthene ND 66.4 53.1 ug/Kg 80 45 - 120 1 25
Fluorene ND 66.4 52.3 ug/Kg 79 50 - 120 3 25
Indeno[1,2,3-cd]pyrene ND 66.4 43.3 ug/Kg 65 20 - 130 23 30 Naphthalene ND 66.4 47.4 ug/Kg 71 40 - 120 1 25
Phenanthrene ND 66.4 50.9 ug/Kg 77 50 - 120 2 25
Pyrene 5.5 J 66.4 54.8 ug/Kg 74 40 - 125 2 30
2-Fluorobiphenyl (Surr) 39 - 111
Surrogate
72 MSD MSD
%Recovery Qualifier Limits
Nitrobenzene-d5 67 41 - 119
Terphenyl-d14 101 43 - 150
Lab Sample ID: MB 440-342864/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343497 Prep Batch: 342864
RL MDL
Acenaphthene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Anthracene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Benzo[a]anthracene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Benzo[a]pyrene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Benzo[b]fluoranthene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Benzo[g,h,i]perylene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Benzo[k]fluoranthene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Chrysene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Dibenz(a,h)anthracene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Fluoranthene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Fluorene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Indeno[1,2,3-cd]pyrene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Naphthalene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Phenanthrene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 Pyrene ND 0.20 0.10 ug/L 07/16/16 09:00 07/19/16 18:11 1 2-Fluorobiphenyl (Surr) 67 50 - 104 07/19/16 18:11 1
MB MB
Surrogate
07/16/16 09:00
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Nitrobenzene-d5 51 46 - 109 07/16/16 09:00 07/19/16 18:11 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Lab Sample ID: MB 440-342864/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343497 Prep Batch: 342864
Terphenyl-d14 80 28 - 124 07/19/16 18:11 1
MB MB
Surrogate
07/16/16 09:00
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Lab Sample ID: LCS 440-342864/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343497 Prep Batch: 342864
Acenaphthene 1.00 0.689 ug/L 69 54 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acenaphthylene 1.00 0.676 ug/L 68 55 - 120
Anthracene 1.00 0.659 ug/L 66 56 - 120
Benzo[a]anthracene 1.00 0.721 ug/L 72 63 - 120
Benzo[a]pyrene 1.00 0.681 ug/L 68 54 - 120
Benzo[b]fluoranthene 1.00 0.799 ug/L 80 60 - 120
Benzo[g,h,i]perylene 1.00 0.895 ug/L 89 61 - 139
Benzo[k]fluoranthene 1.00 0.800 ug/L 80 62 - 120
Chrysene 1.00 0.746 ug/L 75 65 - 120
Dibenz(a,h)anthracene 1.00 0.663 ug/L 66 61 - 120
Fluoranthene 1.00 0.753 ug/L 75 61 - 120
Fluorene 1.00 0.820 ug/L 82 53 - 120
Indeno[1,2,3-cd]pyrene 1.00 0.677 ug/L 68 61 - 122
Naphthalene 1.00 0.708 ug/L 71 46 - 120
Phenanthrene 1.00 0.710 ug/L 71 60 - 120
Pyrene 1.00 0.754 ug/L 75 63 - 120
2-Fluorobiphenyl (Surr) 50 - 104
Surrogate
65 LCS LCS
%Recovery Qualifier Limits
Nitrobenzene-d5 64 46 - 109
Terphenyl-d14 83 28 - 124
Lab Sample ID: LCSD 440-342864/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 343497 Prep Batch: 342864
Acenaphthene 1.00 0.704 ug/L 70 54 - 120 2 35
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acenaphthylene 1.00 0.681 ug/L 68 55 - 120 1 35
Anthracene 1.00 0.651 ug/L 65 56 - 120 1 35
Benzo[a]anthracene 1.00 0.742 ug/L 74 63 - 120 3 35
Benzo[a]pyrene 1.00 0.683 ug/L 68 54 - 120 0 35
Benzo[b]fluoranthene 1.00 0.831 ug/L 83 60 - 120 4 35
Benzo[g,h,i]perylene 1.00 0.871 ug/L 87 61 - 139 3 35
Benzo[k]fluoranthene 1.00 0.837 ug/L 84 62 - 120 5 35
Chrysene 1.00 0.760 ug/L 76 65 - 120 2 35
Dibenz(a,h)anthracene 1.00 0.639 ug/L 64 61 - 120 4 35
Fluoranthene 1.00 0.774 ug/L 77 61 - 120 3 35
Fluorene 1.00 0.813 ug/L 81 53 - 120 1 35
Indeno[1,2,3-cd]pyrene 1.00 0.665 ug/L 67 61 - 122 2 35 Naphthalene 1.00 0.657 ug/L 66 46 - 120 8 35
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Lab Sample ID: LCSD 440-342864/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 343497 Prep Batch: 342864
Phenanthrene 1.00 0.723 ug/L 72 60 - 120 2 35
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Pyrene 1.00 0.766 ug/L 77 63 - 120 2 35
2-Fluorobiphenyl (Surr) 50 - 104
Surrogate
67 LCSD LCSD
%Recovery Qualifier Limits
Nitrobenzene-d5 66 46 - 109
Terphenyl-d14 85 28 - 124
Method: 8015B - Diesel Range Organics (DRO) (GC)
Lab Sample ID: MB 440-342333/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342652 Prep Batch: 342333
RL MDL
C13-C22 ND 5.0 2.5 mg/Kg 07/14/16 09:20 07/15/16 14:05 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 5.0 2.5 mg/Kg 07/14/16 09:20 07/15/16 14:05 1 n-Octacosane 93 40 - 140 07/15/16 14:05 1
MB MB
Surrogate
07/14/16 09:20
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Lab Sample ID: LCS 440-342333/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342652 Prep Batch: 342333
C10-C28 66.7 57.3 mg/Kg 86 45 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
n-Octacosane 40 - 140
Surrogate
91 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 440-152586-1 MS Client Sample ID: AEC-2-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342375 Prep Batch: 342333
C10-C28 8.8 66.5 35.8 mg/Kg 41 40 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
n-Octacosane 40 - 140
Surrogate
68 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 440-152586-1 MSD Client Sample ID: AEC-2-5' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342375 Prep Batch: 342333
C10-C28 8.8 66.5 41.1 mg/Kg 49 40 - 120 14 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
n-Octacosane 40 - 140
Surrogate
81 MSD MSD
%Recovery Qualifier Limits
Lab Sample ID: MB 440-343009/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343351 Prep Batch: 343009
RL MDL
C13-C22 ND 0.50 0.10 mg/L 07/18/16 06:55 07/19/16 14:37 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 0.50 0.10 mg/L 07/18/16 06:55 07/19/16 14:37 1 n-Octacosane 81 45 - 120 07/19/16 14:37 1
MB MB
Surrogate
07/18/16 06:55
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Lab Sample ID: LCS 440-343009/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343351 Prep Batch: 343009
C10-C28 1.00 0.669 mg/L 67 40 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
n-Octacosane 45 - 120
Surrogate
81 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: LCSD 440-343009/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 343351 Prep Batch: 343009
C10-C28 1.00 0.648 mg/L 65 40 - 115 3 25
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
n-Octacosane 45 - 120
Surrogate
74 LCSD LCSD
%Recovery Qualifier Limits
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Lab Sample ID: MB 440-342185/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
RL MDL
Aroclor 1016 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1232 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1242 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1248 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1254 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 Aroclor 1260 ND 50 17 ug/Kg 07/13/16 18:43 07/15/16 13:26 1 DCB Decachlorobiphenyl (Surr) 88 45 - 120 07/15/16 13:26 1 MB MB
Surrogate
07/13/16 18:43
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) Lab Sample ID: LCS 440-342185/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
Aroclor 1016 267 237 ug/Kg 89 65 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Aroclor 1260 267 240 ug/Kg 90 65 - 115
DCB Decachlorobiphenyl (Surr) 45 - 120
Surrogate
92 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 440-152462-A-1-D MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
Aroclor 1016 ND 539 448 ug/Kg 83 50 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Aroclor 1260 ND 539 453 ug/Kg 84 50 - 125
DCB Decachlorobiphenyl (Surr) 45 - 120
Surrogate
82 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 440-152462-A-1-E MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342640 Prep Batch: 342185
Aroclor 1016 ND 556 460 ug/Kg 83 50 - 120 3 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Aroclor 1260 ND 556 467 ug/Kg 84 50 - 125 3 30
DCB Decachlorobiphenyl (Surr) 45 - 120
Surrogate
82 MSD MSD
%Recovery Qualifier Limits
Lab Sample ID: MB 440-343105/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 344252 Prep Batch: 343105
RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 Aroclor 1242 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 Aroclor 1254 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 17:58 1 DCB Decachlorobiphenyl (Surr) 65 26 - 115 07/22/16 17:58 1 MB MB
Surrogate
07/18/16 12:42
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) Lab Sample ID: LCS 440-343105/4-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 344252 Prep Batch: 343105
Aroclor 1016 8.00 5.24 ug/L 65 59 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Aroclor 1260 8.00 5.67 ug/L 71 48 - 115
DCB Decachlorobiphenyl (Surr) 26 - 115
Surrogate
70 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: LCSD 440-343105/5-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 344252 Prep Batch: 343105
Aroclor 1016 8.00 5.45 ug/L 68 59 - 115 4 30
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Aroclor 1260 8.00 5.79 ug/L 72 48 - 115 2 30
DCB Decachlorobiphenyl (Surr) 26 - 115
Surrogate
70 LCSD LCSD
%Recovery Qualifier Limits
Method: 300.0 - Anions, Ion Chromatography
Lab Sample ID: MB 440-342634/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 342634
RL MDL
Chloride ND 0.50 0.25 mg/L 07/15/16 12:22 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate ND 0.50 0.25 mg/L 07/15/16 12:22 1
Lab Sample ID: LCS 440-342634/6 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 342634
Chloride 5.00 4.96 mg/L 99 90 - 110
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Sulfate 5.00 5.09 mg/L 102 90 - 110
Lab Sample ID: 440-152607-A-5 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 342634
Chloride 16 J F1 50.0 54.0 F1 mg/L 75 80 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 440-152607-A-5 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 342634
Chloride 16 J F1 50.0 54.0 F1 mg/L 75 80 - 120 0 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Lab Sample ID: MB 440-342822/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 342822
RL MDL
Chloride ND 0.50 0.25 mg/L 07/16/16 14:26 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-342822/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 342822
Chloride 5.00 4.67 mg/L 93 90 - 110
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: 440-152962-A-2 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 342822
Chloride 310 50.0 334 4 mg/L 52 80 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 440-152962-A-2 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 342822
Chloride 310 50.0 336 4 mg/L 56 80 - 120 1 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Method: 200.7 Rev 4.4 - Metals (ICP)
Lab Sample ID: MB 440-342888/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343234 Prep Batch: 342888
RL MDL
Antimony ND 0.010 0.0060 mg/L 07/16/16 11:58 07/18/16 18:03 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Barium ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Beryllium ND 0.0020 0.0010 mg/L 07/16/16 11:58 07/18/16 18:03 1 Cadmium ND 0.0050 0.0020 mg/L 07/16/16 11:58 07/18/16 18:03 1 Chromium ND 0.0050 0.0025 mg/L 07/16/16 11:58 07/18/16 18:03 1 Cobalt ND 0.010 0.0025 mg/L 07/16/16 11:58 07/18/16 18:03 1 Copper ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Molybdenum ND 0.020 0.010 mg/L 07/16/16 11:58 07/18/16 18:03 1 Nickel ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Silver ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Thallium 0.00638 J 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Vanadium ND 0.010 0.0050 mg/L 07/16/16 11:58 07/18/16 18:03 1 Zinc ND 0.020 0.010 mg/L 07/16/16 11:58 07/18/16 18:03 1 Lab Sample ID: MB 440-342888/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343507 Prep Batch: 342888
RL MDL
Lead ND 0.0050 0.0025 mg/L 07/16/16 11:58 07/19/16 17:32 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 200.7 Rev 4.4 - Metals (ICP) (Continued)
Lab Sample ID: MB 440-342888/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343507 Prep Batch: 342888
RL MDL
Selenium ND 0.010 0.0061 mg/L 07/16/16 11:58 07/19/16 17:32 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-342888/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343234 Prep Batch: 342888
Antimony 0.500 0.502 mg/L 100 85 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 0.500 0.477 mg/L 95 85 - 115
Barium 0.500 0.497 mg/L 99 85 - 115
Beryllium 0.500 0.474 mg/L 95 85 - 115
Cadmium 0.500 0.491 mg/L 98 85 - 115
Chromium 0.500 0.519 mg/L 104 85 - 115
Cobalt 0.500 0.503 mg/L 101 85 - 115
Copper 0.500 0.478 mg/L 96 85 - 115
Molybdenum 0.500 0.492 mg/L 98 85 - 115
Nickel 0.500 0.497 mg/L 99 85 - 115
Silver 0.250 0.230 mg/L 92 85 - 115
Thallium 0.500 0.487 mg/L 97 85 - 115
Vanadium 0.500 0.498 mg/L 100 85 - 115
Zinc 0.500 0.479 mg/L 96 85 - 115
Lab Sample ID: LCS 440-342888/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343507 Prep Batch: 342888
Lead 0.500 0.482 mg/L 96 85 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Selenium 0.500 0.478 mg/L 96 85 - 115
Lab Sample ID: 440-152574-C-7-B MS ^5 Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343234 Prep Batch: 342888
Antimony ND F1 0.500 0.598 mg/L 120 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic 0.13 F1 0.500 0.697 mg/L 114 70 - 130
Barium 0.035 J F1 0.500 0.624 mg/L 118 70 - 130
Beryllium ND 0.500 0.542 mg/L 108 70 - 130
Cadmium ND 0.500 0.533 mg/L 107 70 - 130
Chromium 8.4 0.500 9.13 4 mg/L 146 70 - 130
Cobalt ND 0.500 0.581 mg/L 116 70 - 130
Copper ND 0.500 0.550 mg/L 110 70 - 130
Molybdenum ND F1 0.500 0.584 mg/L 117 70 - 130
Nickel ND 0.500 0.570 mg/L 114 70 - 130
Silver ND 0.250 0.269 mg/L 108 70 - 130
Thallium ND 0.500 0.549 mg/L 110 70 - 130
Vanadium 0.051 F1 F2 0.500 0.628 mg/L 115 70 - 130
Zinc ND F1 0.500 0.577 mg/L 115 70 - 130
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Lab Sample ID: 440-152574-C-7-B MS ^5 Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343507 Prep Batch: 342888
Lead ND 0.500 0.393 mg/L 79 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Selenium ND 0.500 0.434 mg/L 87 70 - 130
Lab Sample ID: 440-152574-C-7-C MSD ^5 Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343234 Prep Batch: 342888
Antimony ND F1 0.500 0.668 F1 mg/L 134 70 - 130 11 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic 0.13 F1 0.500 0.790 F1 mg/L 133 70 - 130 12 20
Barium 0.035 J F1 0.500 0.697 F1 mg/L 132 70 - 130 11 20 Beryllium ND 0.500 0.650 mg/L 130 70 - 130 18 20
Cadmium ND 0.500 0.635 mg/L 127 70 - 130 17 20
Chromium 8.4 0.500 10.7 4 mg/L 464 70 - 130 16 20
Cobalt ND 0.500 0.651 mg/L 130 70 - 130 11 20
Copper ND 0.500 0.632 mg/L 126 70 - 130 14 20
Molybdenum ND F1 0.500 0.664 F1 mg/L 133 70 - 130 13 20 Nickel ND 0.500 0.639 mg/L 128 70 - 130 11 20
Silver ND 0.250 0.311 mg/L 124 70 - 130 14 20
Thallium ND 0.500 0.603 mg/L 121 70 - 130 9 20
Vanadium 0.051 F1 F2 0.500 0.777 F1 F2 mg/L 145 70 - 130 21 20 Zinc ND F1 0.500 0.701 F1 mg/L 140 70 - 130 19 20
Lab Sample ID: 440-152574-C-7-C MSD ^5 Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343507 Prep Batch: 342888
Lead ND 0.500 0.386 mg/L 77 70 - 130 2 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Selenium ND 0.500 0.397 mg/L 79 70 - 130 9 20
Lab Sample ID: MB 440-343049/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343712 Prep Batch: 343049
RL MDL
Antimony ND 0.010 0.0060 mg/L 07/18/16 09:51 07/20/16 12:50 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 Barium ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 Beryllium ND 0.0020 0.0010 mg/L 07/18/16 09:51 07/20/16 12:50 1 Cadmium ND 0.0050 0.0020 mg/L 07/18/16 09:51 07/20/16 12:50 1 Chromium ND 0.0050 0.0025 mg/L 07/18/16 09:51 07/20/16 12:50 1 Cobalt ND 0.010 0.0025 mg/L 07/18/16 09:51 07/20/16 12:50 1 Lead ND 0.0050 0.0025 mg/L 07/18/16 09:51 07/20/16 12:50 1 Copper ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 Molybdenum ND ^ 0.020 0.010 mg/L 07/18/16 09:51 07/20/16 12:50 1 Nickel ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 Selenium ND 0.010 0.0061 mg/L 07/18/16 09:51 07/20/16 12:50 1 Silver ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 Thallium ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 Vanadium ND 0.010 0.0050 mg/L 07/18/16 09:51 07/20/16 12:50 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 200.7 Rev 4.4 - Metals (ICP) (Continued)
Lab Sample ID: MB 440-343049/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343712 Prep Batch: 343049
RL MDL
Zinc ND 0.020 0.010 mg/L 07/18/16 09:51 07/20/16 12:50 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-343049/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343712 Prep Batch: 343049
Antimony 0.500 0.503 mg/L 101 85 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 0.500 0.472 mg/L 94 85 - 115
Barium 0.500 0.493 mg/L 99 85 - 115
Beryllium 0.500 0.483 mg/L 97 85 - 115
Cadmium 0.500 0.500 mg/L 100 85 - 115
Chromium 0.500 0.500 mg/L 100 85 - 115
Cobalt 0.500 0.518 mg/L 104 85 - 115
Lead 0.500 0.496 mg/L 99 85 - 115
Copper 0.500 0.475 mg/L 95 85 - 115
Molybdenum 0.500 0.524 ^ mg/L 105 85 - 115
Nickel 0.500 0.497 mg/L 99 85 - 115
Selenium 0.500 0.461 mg/L 92 85 - 115
Silver 0.250 0.242 mg/L 97 85 - 115
Thallium 0.500 0.492 mg/L 98 85 - 115
Vanadium 0.500 0.498 mg/L 100 85 - 115
Zinc 0.500 0.477 mg/L 95 85 - 115
Lab Sample ID: 440-152187-Q-8-C MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343712 Prep Batch: 343049
Antimony 0.0092 J F1 0.500 0.0994 F1 mg/L 18 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic 0.85 0.500 1.34 mg/L 99 70 - 130
Barium 0.078 F1 0.500 0.221 F1 mg/L 29 70 - 130
Beryllium ND 0.500 0.437 mg/L 87 70 - 130
Cadmium 0.0075 0.500 0.466 mg/L 92 70 - 130
Chromium 0.039 0.500 0.499 mg/L 92 70 - 130
Cobalt ND 0.500 0.470 mg/L 94 70 - 130
Lead ND L F1 0.500 0.336 F1 mg/L 67 70 - 130
Copper 0.037 0.500 0.564 mg/L 106 70 - 130
Molybdenum 0.70 ^ 0.500 1.10 ^ mg/L 79 70 - 130
Nickel 0.019 0.500 0.471 mg/L 90 70 - 130
Selenium 0.031 0.500 0.508 mg/L 95 70 - 130
Silver ND 0.250 0.273 mg/L 109 70 - 130
Thallium ND 0.500 0.438 mg/L 88 70 - 130
Vanadium 4.0 0.500 4.38 4 mg/L 72 70 - 130
Zinc 0.025 0.500 0.532 mg/L 101 70 - 130
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 200.7 Rev 4.4 - Metals (ICP) (Continued)
Lab Sample ID: 440-152187-Q-8-D MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 343712 Prep Batch: 343049
Antimony 0.0092 J F1 0.500 0.104 F1 mg/L 19 70 - 130 5 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic 0.85 0.500 1.40 mg/L 110 70 - 130 4 20
Barium 0.078 F1 0.500 0.252 F1 mg/L 35 70 - 130 13 20
Beryllium ND 0.500 0.448 mg/L 90 70 - 130 2 20
Cadmium 0.0075 0.500 0.471 mg/L 93 70 - 130 1 20
Chromium 0.039 0.500 0.503 mg/L 93 70 - 130 1 20
Cobalt ND 0.500 0.488 mg/L 98 70 - 130 4 20
Lead ND L F1 0.500 0.353 mg/L 71 70 - 130 5 20
Copper 0.037 0.500 0.573 mg/L 107 70 - 130 1 20
Molybdenum 0.70 ^ 0.500 1.10 ^ mg/L 81 70 - 130 1 20
Nickel 0.019 0.500 0.489 mg/L 94 70 - 130 4 20
Selenium 0.031 0.500 0.528 mg/L 99 70 - 130 4 20
Silver ND 0.250 0.279 mg/L 111 70 - 130 2 20
Thallium ND 0.500 0.449 mg/L 90 70 - 130 2 20
Vanadium 4.0 0.500 4.47 4 mg/L 90 70 - 130 2 20
Zinc 0.025 0.500 0.527 mg/L 100 70 - 130 1 20
Method: 245.1 - Mercury (CVAA)
Lab Sample ID: MB 440-343189/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343504 Prep Batch: 343189
RL MDL
Mercury ND 0.00020 0.00010 mg/L 07/18/16 17:00 07/19/16 16:10 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-343189/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343504 Prep Batch: 343189
Mercury 0.00800 0.00786 mg/L 98 85 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: 440-152394-E-2-H MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343504 Prep Batch: 343189
Mercury ND 0.00800 0.00793 mg/L 99 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 440-152394-E-2-I MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343504 Prep Batch: 343189
Mercury ND 0.00800 0.00812 mg/L 102 70 - 130 2 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 6020 - Metals (ICP/MS)
Lab Sample ID: MB 440-342296/1-A ^20 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342802 Prep Batch: 342296
RL MDL
Silver ND 0.50 0.099 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Barium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Beryllium ND 0.30 0.15 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Cadmium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Chromium ND 0.99 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Cobalt ND 0.50 0.21 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Copper ND 0.99 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Lead ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Nickel ND 0.99 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Selenium ND 0.99 0.20 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Thallium ND 0.50 0.25 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Vanadium ND 0.99 0.50 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Zinc ND 9.9 5.0 mg/Kg 07/14/16 08:13 07/15/16 12:25 20
Antimony ND 0.99 0.27 mg/Kg 07/14/16 08:13 07/15/16 12:25 20 Lab Sample ID: MB 440-342296/1-A ^20 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 343028 Prep Batch: 342296
RL MDL
Molybdenum ND 0.99 0.50 mg/Kg 07/14/16 08:13 07/15/16 22:50 20 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-342296/2-A ^20 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342802 Prep Batch: 342296
Silver 24.5 24.8 mg/Kg 101 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 49.0 48.3 mg/Kg 98 80 - 120
Barium 49.0 49.8 mg/Kg 102 80 - 120
Beryllium 49.0 49.2 mg/Kg 100 80 - 120
Cadmium 49.0 49.0 mg/Kg 100 80 - 120
Chromium 49.0 49.9 mg/Kg 102 80 - 120
Cobalt 49.0 50.8 mg/Kg 104 80 - 120
Copper 49.0 50.5 mg/Kg 103 80 - 120
Lead 49.0 49.6 mg/Kg 101 80 - 120
Molybdenum 49.0 49.6 mg/Kg 101 80 - 120
Nickel 49.0 50.5 mg/Kg 103 80 - 120
Selenium 49.0 49.1 mg/Kg 100 80 - 120
Thallium 49.0 49.4 mg/Kg 101 80 - 120
Vanadium 49.0 49.2 mg/Kg 100 80 - 120
Zinc 49.0 48.7 mg/Kg 99 80 - 120
Antimony 49.0 50.1 mg/Kg 102 80 - 120
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 6020 - Metals (ICP/MS) (Continued)
Lab Sample ID: 440-152165-H-1-C MS ^20 Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342802 Prep Batch: 342296
Silver ND 24.9 24.3 mg/Kg 98 80 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic 3.4 49.8 52.4 mg/Kg 98 80 - 120
Barium 75 F1 49.8 138 F1 mg/Kg 127 80 - 120
Beryllium 0.24 J 49.8 45.1 mg/Kg 90 80 - 120
Cadmium ND 49.8 48.8 mg/Kg 98 80 - 120
Chromium 15 49.8 60.8 mg/Kg 93 80 - 120
Cobalt 5.4 49.8 51.6 mg/Kg 93 80 - 120
Copper 9.0 49.8 56.3 mg/Kg 95 80 - 120
Lead 4.1 49.8 54.0 mg/Kg 100 80 - 120
Molybdenum 0.63 J B 49.8 50.3 mg/Kg 100 80 - 120
Nickel 9.7 49.8 55.1 mg/Kg 91 80 - 120
Selenium 0.34 J 49.8 47.6 mg/Kg 95 80 - 120
Thallium ND 49.8 49.0 mg/Kg 98 80 - 120
Vanadium 26 49.8 76.4 mg/Kg 102 80 - 120
Zinc 40 49.8 82.4 mg/Kg 85 80 - 120
Antimony ND F1 49.8 31.0 F1 mg/Kg 62 80 - 120
Lab Sample ID: 440-152165-H-1-D MSD ^20 Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342802 Prep Batch: 342296
Silver ND 24.6 24.0 mg/Kg 98 80 - 120 1 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic 3.4 49.3 50.3 mg/Kg 95 80 - 120 4 20
Barium 75 F1 49.3 141 F1 mg/Kg 134 80 - 120 2 20
Beryllium 0.24 J 49.3 44.3 mg/Kg 89 80 - 120 2 20
Cadmium ND 49.3 48.2 mg/Kg 98 80 - 120 1 20
Chromium 15 49.3 61.7 mg/Kg 95 80 - 120 1 20
Cobalt 5.4 49.3 51.5 mg/Kg 94 80 - 120 0 20
Copper 9.0 49.3 55.1 mg/Kg 94 80 - 120 2 20
Lead 4.1 49.3 53.1 mg/Kg 99 80 - 120 2 20
Molybdenum 0.63 J B 49.3 49.8 mg/Kg 100 80 - 120 1 20
Nickel 9.7 49.3 54.5 mg/Kg 91 80 - 120 1 20
Selenium 0.34 J 49.3 46.9 mg/Kg 95 80 - 120 1 20
Thallium ND 49.3 48.3 mg/Kg 98 80 - 120 1 20
Vanadium 26 49.3 77.6 mg/Kg 106 80 - 120 2 20
Zinc 40 49.3 84.7 mg/Kg 91 80 - 120 3 20
Antimony ND F1 49.3 28.4 F1 mg/Kg 58 80 - 120 9 20
Method: 7471A - Mercury (CVAA)
Lab Sample ID: MB 440-342507/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342536 Prep Batch: 342507
RL MDL
Mercury ND 0.020 0.012 mg/Kg 07/14/16 21:26 07/15/16 00:04 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Method: 7471A - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 440-342507/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342536 Prep Batch: 342507
Mercury 0.800 0.744 mg/Kg 93 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: 440-152793-A-1-C MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342536 Prep Batch: 342507
Mercury 0.072 0.784 0.716 mg/Kg 82 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 440-152793-A-1-D MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA
Analysis Batch: 342536 Prep Batch: 342507
Mercury 0.072 0.784 0.712 mg/Kg 82 70 - 130 1 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Method: SM 2540C - Solids, Total Dissolved (TDS)
Lab Sample ID: MB 440-343021/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343021
RL MDL
Total Dissolved Solids ND 10 5.0 mg/L 07/18/16 07:50 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 440-343021/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343021
Total Dissolved Solids 1000 984 mg/L 98 90 - 110
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: 440-152322-N-1 DU Client Sample ID: Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343021
Total Dissolved Solids 470 472 mg/L 1 5
Analyte
DU DU
Result Qualifier Unit D
Sample
Result
Sample
Qualifier RPD Limit
RPD
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch

GC/MS VOA
Prep Batch: 342437
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-3 AEC-2-15' Total/NA Solid 5035
440-152586-4 AEC-2-20' Total/NA Solid 5035
440-152586-5 AEC-1-5' Total/NA Solid 5035
Prep Batch: 342449
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 5035
440-152586-2 AEC-2-10' Total/NA Solid 5035
Analysis Batch: 342991
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-3 AEC-2-15' Total/NA Solid 8260B 342437
440-152586-4 AEC-2-20' Total/NA Solid 8260B 342437
440-152586-5 AEC-1-5' Total/NA Solid 8260B 342437
MB 440-342991/6 Method Blank Total/NA Solid 8260B
LCS 440-342991/7 Lab Control Sample Total/NA Solid 8260B LCSD 440-342991/9 Lab Control Sample Dup Total/NA Solid 8260B Analysis Batch: 342992
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152586-3 AEC-2-15' Total/NA 342437
Solid 8260B/CA_LUFT
MS
440-152586-4 AEC-2-20' Total/NA 342437
Solid 8260B/CA_LUFT
MS
440-152586-5 AEC-1-5' Total/NA 342437
Solid 8260B/CA_LUFT
MS
MB 440-342992/6 Method Blank Total/NA
Solid 8260B/CA_LUFT
MS
LCS 440-342992/10 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
LCSD 440-342992/11 Lab Control Sample Dup Total/NA
Analysis Batch: 343001
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 8260B 342449
440-152586-2 AEC-2-10' Total/NA Solid 8260B 342449
MB 440-343001/4 Method Blank Total/NA Solid 8260B
LCS 440-343001/5 Lab Control Sample Total/NA Solid 8260B 440-152882-A-2 MS Matrix Spike Total/NA Solid 8260B
440-152882-A-2 MSD Matrix Spike Duplicate Total/NA Solid 8260B Analysis Batch: 343002
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152586-1 AEC-2-5' Total/NA 342449
Solid 8260B/CA_LUFT
MS
440-152586-2 AEC-2-10' Total/NA 342449
Solid 8260B/CA_LUFT
MS
MB 440-343002/4 Method Blank Total/NA
Solid 8260B/CA_LUFT
MS
LCS 440-343002/6 Lab Control Sample Total/NA
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
GC/MS VOA (Continued)
Analysis Batch: 343002 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B/CA_LUFT
MS
440-152882-A-2 MS Matrix Spike Total/NA
Solid 8260B/CA_LUFT
MS
440-152882-A-2 MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 343275
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 8260B
440-152586-7 AEC-3-W Total/NA Water 8260B
440-152586-8 AEC-5-W Total/NA Water 8260B
MB 440-343275/5 Method Blank Total/NA Water 8260B
LCS 440-343275/6 Lab Control Sample Total/NA Water 8260B 440-152586-7 MS AEC-3-W Total/NA Water 8260B
440-152586-7 MSD AEC-3-W Total/NA Water 8260B
Analysis Batch: 343276
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260B/CA_LUFT
MS
440-152586-6 AEC-4-W Total/NA
Water 8260B/CA_LUFT
MS
440-152586-7 AEC-3-W Total/NA
Water 8260B/CA_LUFT
MS
440-152586-8 AEC-5-W Total/NA
Water 8260B/CA_LUFT
MS
MB 440-343276/5 Method Blank Total/NA
Water 8260B/CA_LUFT
MS
LCS 440-343276/7 Lab Control Sample Total/NA
Water 8260B/CA_LUFT
MS
440-152586-7 MS AEC-3-W Total/NA
Water 8260B/CA_LUFT
MS
440-152586-7 MSD AEC-3-W Total/NA
GC/MS Semi VOA
Prep Batch: 342341
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 3546
440-152586-2 AEC-2-10' Total/NA Solid 3546
440-152586-3 AEC-2-15' Total/NA Solid 3546
440-152586-4 AEC-2-20' Total/NA Solid 3546
440-152586-5 AEC-1-5' Total/NA Solid 3546
MB 440-342341/1-A Method Blank Total/NA Solid 3546
LCS 440-342341/2-A Lab Control Sample Total/NA Solid 3546 440-152586-1 MS AEC-2-5' Total/NA Solid 3546
440-152586-1 MSD AEC-2-5' Total/NA Solid 3546
Analysis Batch: 342622
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 8270C SIM 342341
440-152586-2 AEC-2-10' Total/NA Solid 8270C SIM 342341
MB 440-342341/1-A Method Blank Total/NA Solid 8270C SIM 342341 LCS 440-342341/2-A Lab Control Sample Total/NA Solid 8270C SIM 342341 440-152586-1 MS AEC-2-5' Total/NA Solid 8270C SIM 342341 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
GC/MS Semi VOA (Continued)
Analysis Batch: 342622 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 MSD AEC-2-5' Total/NA Solid 8270C SIM 342341 Prep Batch: 342864
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 3520C
440-152586-7 AEC-3-W Total/NA Water 3520C
440-152586-8 AEC-5-W Total/NA Water 3520C
MB 440-342864/1-A Method Blank Total/NA Water 3520C
LCS 440-342864/2-A Lab Control Sample Total/NA Water 3520C LCSD 440-342864/3-A Lab Control Sample Dup Total/NA Water 3520C Analysis Batch: 343497
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-3 AEC-2-15' Total/NA Solid 8270C SIM 342341
440-152586-4 AEC-2-20' Total/NA Solid 8270C SIM 342341
440-152586-5 AEC-1-5' Total/NA Solid 8270C SIM 342341
440-152586-6 AEC-4-W Total/NA Water 8270C SIM 342864
440-152586-7 AEC-3-W Total/NA Water 8270C SIM 342864
440-152586-8 AEC-5-W Total/NA Water 8270C SIM 342864
MB 440-342864/1-A Method Blank Total/NA Water 8270C SIM 342864 LCS 440-342864/2-A Lab Control Sample Total/NA Water 8270C SIM 342864 LCSD 440-342864/3-A Lab Control Sample Dup Total/NA Water 8270C SIM 342864 GC Semi VOA
Prep Batch: 342185
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 3546
440-152586-2 AEC-2-10' Total/NA Solid 3546
440-152586-3 AEC-2-15' Total/NA Solid 3546
440-152586-4 AEC-2-20' Total/NA Solid 3546
440-152586-5 AEC-1-5' Total/NA Solid 3546
MB 440-342185/1-A Method Blank Total/NA Solid 3546
LCS 440-342185/2-A Lab Control Sample Total/NA Solid 3546 440-152462-A-1-D MS Matrix Spike Total/NA Solid 3546
440-152462-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 3546 Prep Batch: 342333
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 3546
440-152586-2 AEC-2-10' Total/NA Solid 3546
440-152586-3 AEC-2-15' Total/NA Solid 3546
440-152586-4 AEC-2-20' Total/NA Solid 3546
440-152586-5 AEC-1-5' Total/NA Solid 3546
MB 440-342333/1-A Method Blank Total/NA Solid 3546
LCS 440-342333/2-A Lab Control Sample Total/NA Solid 3546 440-152586-1 MS AEC-2-5' Total/NA Solid 3546
440-152586-1 MSD AEC-2-5' Total/NA Solid 3546
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
GC Semi VOA (Continued)
Analysis Batch: 342375
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-5 AEC-1-5' Total/NA Solid 8015B 342333
440-152586-1 MS AEC-2-5' Total/NA Solid 8015B 342333
440-152586-1 MSD AEC-2-5' Total/NA Solid 8015B 342333
Analysis Batch: 342640
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 8082 342185
440-152586-2 AEC-2-10' Total/NA Solid 8082 342185
440-152586-3 AEC-2-15' Total/NA Solid 8082 342185
440-152586-4 AEC-2-20' Total/NA Solid 8082 342185
440-152586-5 AEC-1-5' Total/NA Solid 8082 342185
MB 440-342185/1-A Method Blank Total/NA Solid 8082 342185 LCS 440-342185/2-A Lab Control Sample Total/NA Solid 8082 342185 440-152462-A-1-D MS Matrix Spike Total/NA Solid 8082 342185 440-152462-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 8082 342185 Analysis Batch: 342644
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 8015B 342333
440-152586-2 AEC-2-10' Total/NA Solid 8015B 342333
440-152586-3 AEC-2-15' Total/NA Solid 8015B 342333
Analysis Batch: 342652
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch MB 440-342333/1-A Method Blank Total/NA Solid 8015B 342333 LCS 440-342333/2-A Lab Control Sample Total/NA Solid 8015B 342333 Prep Batch: 343009
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 3510C
440-152586-7 AEC-3-W Total/NA Water 3510C
440-152586-8 AEC-5-W Total/NA Water 3510C
MB 440-343009/1-A Method Blank Total/NA Water 3510C
LCS 440-343009/2-A Lab Control Sample Total/NA Water 3510C LCSD 440-343009/3-A Lab Control Sample Dup Total/NA Water 3510C Analysis Batch: 343048
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-4 AEC-2-20' Total/NA Solid 8082 342185
Analysis Batch: 343077
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-4 AEC-2-20' Total/NA Solid 8015B 342333
Prep Batch: 343105
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 3510C
440-152586-7 AEC-3-W Total/NA Water 3510C
440-152586-8 AEC-5-W Total/NA Water 3510C
MB 440-343105/1-A Method Blank Total/NA Water 3510C
LCS 440-343105/4-A Lab Control Sample Total/NA Water 3510C TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
GC Semi VOA (Continued)
Prep Batch: 343105 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCSD 440-343105/5-A Lab Control Sample Dup Total/NA Water 3510C Analysis Batch: 343351
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 8015B 343009
440-152586-7 AEC-3-W Total/NA Water 8015B 343009
440-152586-8 AEC-5-W Total/NA Water 8015B 343009
MB 440-343009/1-A Method Blank Total/NA Water 8015B 343009 LCS 440-343009/2-A Lab Control Sample Total/NA Water 8015B 343009 LCSD 440-343009/3-A Lab Control Sample Dup Total/NA Water 8015B 343009 Analysis Batch: 344252
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 8082 343105
440-152586-7 AEC-3-W Total/NA Water 8082 343105
440-152586-8 AEC-5-W Total/NA Water 8082 343105
MB 440-343105/1-A Method Blank Total/NA Water 8082 343105 LCS 440-343105/4-A Lab Control Sample Total/NA Water 8082 343105 LCSD 440-343105/5-A Lab Control Sample Dup Total/NA Water 8082 343105

HPLC/IC
Analysis Batch: 342634
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 300.0
440-152586-7 AEC-3-W Total/NA Water 300.0
440-152586-8 AEC-5-W Total/NA Water 300.0
MB 440-342634/4 Method Blank Total/NA Water 300.0
LCS 440-342634/6 Lab Control Sample Total/NA Water 300.0 440-152607-A-5 MS Matrix Spike Total/NA Water 300.0
440-152607-A-5 MSD Matrix Spike Duplicate Total/NA Water 300.0 Analysis Batch: 342822
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-7 AEC-3-W Total/NA Water 300.0
440-152586-8 AEC-5-W Total/NA Water 300.0
MB 440-342822/4 Method Blank Total/NA Water 300.0
LCS 440-342822/2 Lab Control Sample Total/NA Water 300.0 440-152962-A-2 MS Matrix Spike Total/NA Water 300.0
440-152962-A-2 MSD Matrix Spike Duplicate Total/NA Water 300.0 Metals
Prep Batch: 342296
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 3050B
440-152586-2 AEC-2-10' Total/NA Solid 3050B
440-152586-3 AEC-2-15' Total/NA Solid 3050B
440-152586-4 AEC-2-20' Total/NA Solid 3050B
440-152586-5 AEC-1-5' Total/NA Solid 3050B
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Metals (Continued)
Prep Batch: 342296 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch MB 440-342296/1-A ^20 Method Blank Total/NA Solid 3050B LCS 440-342296/2-A ^20 Lab Control Sample Total/NA Solid 3050B 440-152165-H-1-C MS ^20 Matrix Spike Total/NA Solid 3050B 440-152165-H-1-D MSD ^20 Matrix Spike Duplicate Total/NA Solid 3050B Prep Batch: 342507
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 7471A
440-152586-2 AEC-2-10' Total/NA Solid 7471A
440-152586-3 AEC-2-15' Total/NA Solid 7471A
440-152586-4 AEC-2-20' Total/NA Solid 7471A
440-152586-5 AEC-1-5' Total/NA Solid 7471A
MB 440-342507/1-A Method Blank Total/NA Solid 7471A
LCS 440-342507/2-A Lab Control Sample Total/NA Solid 7471A 440-152793-A-1-C MS Matrix Spike Total/NA Solid 7471A
440-152793-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 7471A Analysis Batch: 342536
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 7471A 342507
440-152586-2 AEC-2-10' Total/NA Solid 7471A 342507
440-152586-3 AEC-2-15' Total/NA Solid 7471A 342507
440-152586-4 AEC-2-20' Total/NA Solid 7471A 342507
440-152586-5 AEC-1-5' Total/NA Solid 7471A 342507
MB 440-342507/1-A Method Blank Total/NA Solid 7471A 342507 LCS 440-342507/2-A Lab Control Sample Total/NA Solid 7471A 342507 440-152793-A-1-C MS Matrix Spike Total/NA Solid 7471A 342507 440-152793-A-1-D MSD Matrix Spike Duplicate Total/NA Solid 7471A 342507 Analysis Batch: 342802
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 6020 342296
440-152586-2 AEC-2-10' Total/NA Solid 6020 342296
440-152586-3 AEC-2-15' Total/NA Solid 6020 342296
440-152586-4 AEC-2-20' Total/NA Solid 6020 342296
440-152586-5 AEC-1-5' Total/NA Solid 6020 342296
MB 440-342296/1-A ^20 Method Blank Total/NA Solid 6020 342296 LCS 440-342296/2-A ^20 Lab Control Sample Total/NA Solid 6020 342296 440-152165-H-1-C MS ^20 Matrix Spike Total/NA Solid 6020 342296 440-152165-H-1-D MSD ^20 Matrix Spike Duplicate Total/NA Solid 6020 342296 Prep Batch: 342888
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-7 AEC-3-W Total Recoverable Water 200.2
MB 440-342888/1-A Method Blank Total Recoverable Water 200.2 LCS 440-342888/2-A Lab Control Sample Total Recoverable Water 200.2 440-152574-C-7-B MS ^5 Matrix Spike Total Recoverable Water 200.2 440-152574-C-7-C MSD ^5 Matrix Spike Duplicate Total Recoverable Water 200.2 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Metals (Continued)
Analysis Batch: 343028
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-1 AEC-2-5' Total/NA Solid 6020 342296
440-152586-2 AEC-2-10' Total/NA Solid 6020 342296
440-152586-3 AEC-2-15' Total/NA Solid 6020 342296
440-152586-4 AEC-2-20' Total/NA Solid 6020 342296
440-152586-5 AEC-1-5' Total/NA Solid 6020 342296
MB 440-342296/1-A ^20 Method Blank Total/NA Solid 6020 342296 Prep Batch: 343049
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total Recoverable Water 200.2
440-152586-8 AEC-5-W Total Recoverable Water 200.2
MB 440-343049/1-A Method Blank Total Recoverable Water 200.2 LCS 440-343049/2-A Lab Control Sample Total Recoverable Water 200.2 440-152187-Q-8-C MS Matrix Spike Total Recoverable Water 200.2 440-152187-Q-8-D MSD Matrix Spike Duplicate Total Recoverable Water 200.2 Prep Batch: 343189
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 245.1
440-152586-7 AEC-3-W Total/NA Water 245.1
440-152586-8 AEC-5-W Total/NA Water 245.1
MB 440-343189/1-A Method Blank Total/NA Water 245.1
LCS 440-343189/2-A Lab Control Sample Total/NA Water 245.1 440-152394-E-2-H MS Matrix Spike Total/NA Water 245.1
440-152394-E-2-I MSD Matrix Spike Duplicate Total/NA Water 245.1 Analysis Batch: 343234
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-7 AEC-3-W Total Recoverable Water 200.7 Rev 4.4 342888 MB 440-342888/1-A Method Blank Total Recoverable Water 200.7 Rev 4.4 342888 LCS 440-342888/2-A Lab Control Sample Total Recoverable Water 200.7 Rev 4.4 342888 440-152574-C-7-B MS ^5 Matrix Spike Total Recoverable Water 200.7 Rev 4.4 342888 440-152574-C-7-C MSD ^5 Matrix Spike Duplicate Total Recoverable Water 200.7 Rev 4.4 342888 Analysis Batch: 343504
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water 245.1 343189
440-152586-7 AEC-3-W Total/NA Water 245.1 343189
440-152586-8 AEC-5-W Total/NA Water 245.1 343189
MB 440-343189/1-A Method Blank Total/NA Water 245.1 343189 LCS 440-343189/2-A Lab Control Sample Total/NA Water 245.1 343189 440-152394-E-2-H MS Matrix Spike Total/NA Water 245.1 343189 440-152394-E-2-I MSD Matrix Spike Duplicate Total/NA Water 245.1 343189 Analysis Batch: 343507
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-7 AEC-3-W Total Recoverable Water 200.7 Rev 4.4 342888 MB 440-342888/1-A Method Blank Total Recoverable Water 200.7 Rev 4.4 342888 LCS 440-342888/2-A Lab Control Sample Total Recoverable Water 200.7 Rev 4.4 342888 440-152574-C-7-B MS ^5 Matrix Spike Total Recoverable Water 200.7 Rev 4.4 342888 440-152574-C-7-C MSD ^5 Matrix Spike Duplicate Total Recoverable Water 200.7 Rev 4.4 342888 TestAmerica Irvine

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13 QC Association Summary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Analysis Batch: 343712
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total Recoverable Water 200.7 Rev 4.4 343049 440-152586-8 AEC-5-W Total Recoverable Water 200.7 Rev 4.4 343049 MB 440-343049/1-A Method Blank Total Recoverable Water 200.7 Rev 4.4 343049 LCS 440-343049/2-A Lab Control Sample Total Recoverable Water 200.7 Rev 4.4 343049 440-152187-Q-8-C MS Matrix Spike Total Recoverable Water 200.7 Rev 4.4 343049 440-152187-Q-8-D MSD Matrix Spike Duplicate Total Recoverable Water 200.7 Rev 4.4 343049 General Chemistry
Analysis Batch: 343021
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440-152586-6 AEC-4-W Total/NA Water SM 2540C
440-152586-7 AEC-3-W Total/NA Water SM 2540C
440-152586-8 AEC-5-W Total/NA Water SM 2540C
MB 440-343021/1 Method Blank Total/NA Water SM 2540C
LCS 440-343021/2 Lab Control Sample Total/NA Water SM 2540C 440-152322-N-1 DU Duplicate Total/NA Water SM 2540C
TestAmerica Irvine

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13 Definitions/Glossary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Qualifiers

GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier
ID Analyte identified by RT & presence of single mass ion * ISTD response or retention time outside acceptable limits GC/MS Semi VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

X Surrogate is outside control limits
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier
X Surrogate is outside control limits

HPLC/IC
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.

Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier
^ ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits. 4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.

F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary
These commonly used abbreviations may or may not be present in this report. ¤ Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TestAmerica Irvine

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13 Definitions/Glossary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Glossary (Continued)
These commonly used abbreviations may or may not be present in this report.

TEQ Toxicity Equivalent Quotient (Dioxin)
Abbreviation
TestAmerica Irvine

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13 Certification Summary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152586-1 Project/Site: Pumpkin Patch
Laboratory: TestAmerica Irvine
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date Alaska State Program 10 CA01531 06-30-17
Arizona State Program 9 AZ0671 10-13-16
California LA Cty Sanitation Districts 9 10256 01-31-17 * California State Program 9 CA ELAP 2706 06-30-18
Guam State Program 9 Cert. No. 12.002r 01-23-17
Hawaii State Program 9 N/A 01-29-17
Kansas NELAP Secondary AB 7 E-10420 07-31-16 *
Nevada State Program 9 CA015312016-2 07-31-16 *
New Mexico State Program 6 N/A 01-29-17
Northern Mariana Islands State Program 9 MP0002 01-29-17 Oregon NELAP 10 4028 01-29-17
USDA Federal P330-09-00080 07-08-18
Washington State Program 10 C900 09-03-16
TestAmerica Irvine
* Certification renewal pending - certification considered valid.

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13 Login Sample Receipt Checklist
Client: Advanced Environmental Concepts Inc Job Number: 440-152586-1 Login Number: 152586
Question Answer Comment
Creator: Soderblom, Tim
List Source: TestAmerica Irvine
List Number: 1
Radioactivity wasn't checked or is </= background as measured by a survey True meter.

The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True
The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? False Refer to Job Narrative for details.

There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4").

Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TestAmerica Irvine Page 85 of 85 7/25/2016
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13 ANALYTICAL REPORT
TestAmerica Laboratories, Inc.

TestAmerica Irvine
17461 Derian Ave
Suite 100
Irvine, CA 92614-5817
Tel: (949)261-1022
TestAmerica Job ID: 440-152822-1
Client Project/Site: Pumpkin Patch
For:

Advanced Environmental Concepts Inc
220 E. Truxtun Ave.

Bakersfield, California 93305
Attn: Jonathan Buck
Authorized for release by:
7/26/2016 9:31:53 AM
Danielle Roberts, Senior Project Manager
(949)261-1022
[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2
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13 Table of Contents
Client: Advanced Environmental Concepts Inc
Project/Site: Pumpkin Patch
TestAmerica Job ID: 440-152822-1

TestAmerica Irvine
7/26/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48 1 2
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13 Sample Summary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Lab Sample ID Client Sample ID Matrix Collected Received 440-152822-1 EW-1-W Water 07/13/16 16:05 07/14/16 10:34 440-152822-2 AEC-2-W Water 07/14/16 08:05 07/14/16 10:34 440-152822-3 AEC-1-W Water 07/14/16 09:30 07/14/16 10:34 TestAmerica Irvine

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13 Case Narrative
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Job ID: 440-152822-1
Laboratory: TestAmerica Irvine
Narrative
Job Narrative
440-152822-1
Comments
No additional comments.

Receipt
The samples were received on 7/14/2016 10:34 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 3.1º C and 3.2º C.

Receipt Exceptions
A trip blank was submitted for analysis with these samples; however, it was not listed on the Chain of Custody (COC).

The Field Sampler was not listed on the Chain of Custody.

GC/MS VOA
Method(s) 8260B/CA_LUFTMS: The following sample was diluted due to the nature of the sample matrix (dark brown color): AEC-2-W (440-152822-2). Elevated reporting limits (RLs) are provided.

Method(s) 8260B/CA_LUFTMS: The following samples were collected in properly preserved vials for analysis of volatile organic compounds (VOCs). However, the pH of 7 was outside the required criteria when verified by the laboratory, and corrective action was not possible: EW-1-W (440-152822-1) and AEC-2-W (440-152822-2).

The sample was analyzed within 7 days per EPA recommendation Method(s) 8260B: The following sample was diluted due to the nature of the sample matrix (dark brown color): AEC-2-W (440-152822-2).

Elevated reporting limits (RLs) are provided.

Method(s) 8260B: The following sample was collected in properly preserved vial for analysis of volatile organic compounds (VOCs).

However, the pH of 7 was outside the required criteria when verified by the laboratory, and corrective action was not possible: EW-1-W (440-152822-1) and AEC-2-W (440-152822-2).

The sample was analyzed within 7 days per EPA recommendation.

Method(s) 8260B: The following sample(s) was received unpreserved and presented a pH 7. Analysis was performed within 7 days per EPA recommendation: AEC-1-W (440-152822-3)
Method(s) 8260B: The following sample was diluted due to the nature of the sample matrix: Dark brown color. AEC-1-W (440-152822-3).

Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA
Method(s) 8270C SIM: Surrogate recovery for the following samples was outside control limits: AEC-2-W (440-152822-2) and AEC-1-W (440-152822-3). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8270C SIM: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-343113 and analytical batch 440-343497. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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13 Case Narrative
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Job ID: 440-152822-1 (Continued)
Laboratory: TestAmerica Irvine (Continued)

HPLC/IC
Method(s) 300.0: The following samples was diluted for Sulfate due to the nature of the sample matrix: AEC-2-W (440-152822-2) and AEC-1-W (440-152822-3). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC Semi VOA
Method(s) 8015B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-343009 and analytical batch 440-343351. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.

Method(s) 8015B: Surrogate recovery for the following sample was outside control limits: AEC-2-W (440-152822-2). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8082: Surrogate recovery for the following sample was outside control limits: AEC-1-W (440-152822-3). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8082: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-343105 and analytical batch 440-344252.The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.(LCS 440-343105/4-A) No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals
Method(s) 200.7 Rev 4.4: The following samples was diluted due to the nature of the sample matrix: AEC-2-W (440-152822-2) and AEC-1-W (440-152822-3). Elevated reporting limits (RLs) are provided. Sample appears to be yellow.

Method(s) 200.7 Rev 4.4: The following samples was diluted due to the nature of the sample matrix: AEC-2-W (440-152822-2) and AEC-1-W (440-152822-3). Elevated reporting limits (RLs) are provided. Sample appears to be yellow.

Method(s) 245.1: The following samples was diluted due to the nature of the sample matrix: AEC-2-W (440-152822-2) and AEC-1-W (440-152822-3). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: EW-1-W Lab Sample ID: 440-152822-1
Date Collected: 07/13/16 16:05 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 50 35 ug/L 07/20/16 17:14 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 91 76 - 132 07/20/16 17:14 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 97 80 - 120 07/20/16 17:14 1 Toluene-d8 (Surr) 106 80 - 128 07/20/16 17:14 1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/20/16 17:14 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/20/16 17:14 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/20/16 17:14 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/20/16 17:14 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/20/16 17:14 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/20/16 17:14 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/20/16 17:14 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/20/16 17:14 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Benzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Bromobenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Bromochloromethane ND 0.50 0.25 ug/L 07/20/16 17:14 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 Bromoform ND 1.0 0.40 ug/L 07/20/16 17:14 1
Bromomethane ND 0.50 0.25 ug/L 07/20/16 17:14 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/20/16 17:14 1 Chlorobenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Chloroethane ND 1.0 0.40 ug/L 07/20/16 17:14 1
Chloroform ND 0.50 0.25 ug/L 07/20/16 17:14 1
Chloromethane ND 0.50 0.25 ug/L 07/20/16 17:14 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/20/16 17:14 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/20/16 17:14 1 Dibromochloromethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 Dibromomethane ND 0.50 0.25 ug/L 07/20/16 17:14 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/20/16 17:14 1 Ethanol ND 150 75 ug/L 07/20/16 17:14 1
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/20/16 17:14 1 TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: EW-1-W Lab Sample ID: 440-152822-1
Date Collected: 07/13/16 16:05 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/20/16 17:14 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
m,p-Xylene ND 1.0 0.50 ug/L 07/20/16 17:14 1
Methylene Chloride ND 2.0 0.88 ug/L 07/20/16 17:14 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/20/16 17:14 1 Naphthalene ND 1.0 0.40 ug/L 07/20/16 17:14 1
n-Butylbenzene ND 1.0 0.40 ug/L 07/20/16 17:14 1
N-Propylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
o-Xylene ND 0.50 0.25 ug/L 07/20/16 17:14 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/20/16 17:14 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Styrene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/20/16 17:14 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Toluene ND 0.50 0.25 ug/L 07/20/16 17:14 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/20/16 17:14 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/20/16 17:14 1 Trichloroethene ND 0.50 0.25 ug/L 07/20/16 17:14 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/20/16 17:14 1 Xylenes, Total ND 1.0 0.50 ug/L 07/20/16 17:14 1
Vinyl chloride ND 0.50 0.25 ug/L 07/20/16 17:14 1
tert-Butyl alcohol (TBA) ND 10 5.0 ug/L 07/20/16 17:14 1 4-Bromofluorobenzene (Surr) 97 80 - 120 07/20/16 17:14 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 91 76 - 132 07/20/16 17:14 1 Toluene-d8 (Surr) 106 80 - 128 07/20/16 17:14 1
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Anthracene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Benzo[a]anthracene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Benzo[a]pyrene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Benzo[b]fluoranthene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Benzo[g,h,i]perylene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Benzo[k]fluoranthene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Chrysene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Dibenz(a,h)anthracene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Fluoranthene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Fluorene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Indeno[1,2,3-cd]pyrene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Naphthalene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Phenanthrene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 Pyrene ND 0.19 0.097 ug/L 07/18/16 13:01 07/19/16 22:18 1 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: EW-1-W Lab Sample ID: 440-152822-1
Date Collected: 07/13/16 16:05 Matrix: Water
Date Received: 07/14/16 10:34
2-Fluorobiphenyl (Surr) 61 50 - 104 07/18/16 13:01 07/19/16 22:18 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 63 46 - 109 07/18/16 13:01 07/19/16 22:18 1 Terphenyl-d14 84 28 - 124 07/18/16 13:01 07/19/16 22:18 1 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 ND 0.47 0.093 mg/L 07/18/16 06:55 07/20/16 00:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 ND 0.47 0.093 mg/L 07/18/16 06:55 07/20/16 00:38 1 n-Octacosane 60 45 - 120 07/18/16 06:55 07/20/16 00:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 Aroclor 1242 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 Aroclor 1254 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:42 1 DCB Decachlorobiphenyl (Surr) 69 26 - 115 07/18/16 12:42 07/22/16 19:42 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 300.0 - Anions, Ion Chromatography
RL MDL
Chloride 4000 500 250 mg/L 07/18/16 15:37 1000
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate 470 50 25 mg/L 07/18/16 17:36 100
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable RL MDL
Antimony ND 0.010 0.0060 mg/L 07/19/16 14:16 07/20/16 12:05 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Barium 0.12 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Beryllium ND 0.0020 0.0010 mg/L 07/19/16 14:16 07/20/16 12:05 1 Cadmium ND 0.0050 0.0020 mg/L 07/19/16 14:16 07/20/16 12:05 1 Chromium 0.0030 J 0.0050 0.0025 mg/L 07/19/16 14:16 07/20/16 12:05 1 Cobalt 0.0068 J 0.010 0.0025 mg/L 07/19/16 14:16 07/20/16 12:05 1 Lead ND 0.0050 0.0025 mg/L 07/19/16 14:16 07/20/16 12:05 1 Copper 0.010 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Molybdenum 0.057 0.020 0.010 mg/L 07/19/16 14:16 07/20/16 10:08 1 Nickel 0.0075 J 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Selenium ND 0.010 0.0061 mg/L 07/19/16 14:16 07/20/16 12:05 1 Silver ND 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Thallium ND 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Vanadium 0.0084 J 0.010 0.0050 mg/L 07/19/16 14:16 07/20/16 12:05 1 Zinc ND 0.020 0.010 mg/L 07/19/16 14:16 07/20/16 12:05 1 Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury ND 0.00020 0.00010 mg/L 07/20/16 13:00 07/20/16 22:10 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
General Chemistry
RL MDL
Total Dissolved Solids 9700 100 50 mg/L 07/19/16 07:51 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Client Sample ID: AEC-2-W Lab Sample ID: 440-152822-2
Date Collected: 07/14/16 08:05 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
1600 100 70 ug/L 07/20/16 18:14 2
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 89 76 - 132 07/20/16 18:14 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 80 - 120 07/20/16 18:14 2 Toluene-d8 (Surr) 106 80 - 128 07/20/16 18:14 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.0 0.50 ug/L 07/20/16 18:14 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 1.0 0.50 ug/L 07/20/16 18:14 2 1,1,2,2-Tetrachloroethane ND 1.0 0.50 ug/L 07/20/16 18:14 2 1,1,2-Trichloroethane ND 1.0 0.50 ug/L 07/20/16 18:14 2 1,1-Dichloroethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,1-Dichloroethene ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,1-Dichloropropene ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,2,3-Trichlorobenzene ND 2.0 0.80 ug/L 07/20/16 18:14 2 1,2,3-Trichloropropane ND 2.0 0.50 ug/L 07/20/16 18:14 2 1,2,4-Trichlorobenzene ND 2.0 0.80 ug/L 07/20/16 18:14 2 1,2,4-Trimethylbenzene 61 1.0 0.50 ug/L 07/20/16 18:14 2 1,2-Dibromo-3-Chloropropane ND 2.0 1.0 ug/L 07/20/16 18:14 2 1,2-Dibromoethane (EDB) ND 1.0 0.50 ug/L 07/20/16 18:14 2 1,2-Dichlorobenzene ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,2-Dichloroethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,2-Dichloropropane ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,3,5-Trimethylbenzene 14 1.0 0.50 ug/L 07/20/16 18:14 2 1,3-Dichlorobenzene ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,3-Dichloropropane ND 1.0 0.50 ug/L 07/20/16 18:14 2
1,4-Dichlorobenzene 46 1.0 0.50 ug/L 07/20/16 18:14 2
2,2-Dichloropropane ND 2.0 0.80 ug/L 07/20/16 18:14 2
2-Chlorotoluene ND 1.0 0.50 ug/L 07/20/16 18:14 2
4-Chlorotoluene ND 1.0 0.50 ug/L 07/20/16 18:14 2
Benzene 3.8 1.0 0.50 ug/L 07/20/16 18:14 2
Bromobenzene ND 1.0 0.50 ug/L 07/20/16 18:14 2
Bromochloromethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
Bromodichloromethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
Bromoform ND 2.0 0.80 ug/L 07/20/16 18:14 2
Bromomethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
Carbon tetrachloride ND 1.0 0.50 ug/L 07/20/16 18:14 2
Chlorobenzene 2.6 1.0 0.50 ug/L 07/20/16 18:14 2
Chloroethane ND 2.0 0.80 ug/L 07/20/16 18:14 2
Chloroform ND 1.0 0.50 ug/L 07/20/16 18:14 2
Chloromethane 0.82 J 1.0 0.50 ug/L 07/20/16 18:14 2
cis-1,2-Dichloroethene ND 1.0 0.50 ug/L 07/20/16 18:14 2 cis-1,3-Dichloropropene ND 1.0 0.50 ug/L 07/20/16 18:14 2 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-W Lab Sample ID: 440-152822-2
Date Collected: 07/14/16 08:05 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Dibromochloromethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromomethane ND 1.0 0.50 ug/L 07/20/16 18:14 2
Dichlorodifluoromethane ND 2.0 0.50 ug/L 07/20/16 18:14 2 Ethanol 200 J 300 150 ug/L 07/20/16 18:14 2
Isopropyl Ether (DIPE) ND 1.0 0.50 ug/L 07/20/16 18:14 2 Ethyl-t-butyl ether (ETBE) ND 1.0 0.50 ug/L 07/20/16 18:14 2 Ethylbenzene 14 1.0 0.50 ug/L 07/20/16 18:14 2
Hexachlorobutadiene ND 1.0 0.50 ug/L 07/20/16 18:14 2
Isopropylbenzene 2.7 1.0 0.50 ug/L 07/20/16 18:14 2
m,p-Xylene 16 2.0 1.0 ug/L 07/20/16 18:14 2
Methylene Chloride ND 4.0 1.8 ug/L 07/20/16 18:14 2
Methyl-t-Butyl Ether (MTBE) ND 1.0 0.50 ug/L 07/20/16 18:14 2 Naphthalene 51 2.0 0.80 ug/L 07/20/16 18:14 2
n-Butylbenzene 5.8 2.0 0.80 ug/L 07/20/16 18:14 2
N-Propylbenzene 6.0 1.0 0.50 ug/L 07/20/16 18:14 2
o-Xylene 10 1.0 0.50 ug/L 07/20/16 18:14 2
p-Isopropyltoluene 12 1.0 0.50 ug/L 07/20/16 18:14 2
sec-Butylbenzene 3.2 1.0 0.50 ug/L 07/20/16 18:14 2
Styrene 1.2 1.0 0.50 ug/L 07/20/16 18:14 2
Tert-amyl-methyl ether (TAME) ND 1.0 0.50 ug/L 07/20/16 18:14 2 tert-Butylbenzene 0.79 J 1.0 0.50 ug/L 07/20/16 18:14 2 Tetrachloroethene ND 1.0 0.50 ug/L 07/20/16 18:14 2
Toluene 28 1.0 0.50 ug/L 07/20/16 18:14 2
trans-1,2-Dichloroethene ND 1.0 0.50 ug/L 07/20/16 18:14 2 trans-1,3-Dichloropropene ND 1.0 0.50 ug/L 07/20/16 18:14 2 Trichloroethene ND 1.0 0.50 ug/L 07/20/16 18:14 2
Trichlorofluoromethane ND 1.0 0.50 ug/L 07/20/16 18:14 2 Xylenes, Total 26 2.0 1.0 ug/L 07/20/16 18:14 2
Vinyl chloride ND 1.0 0.50 ug/L 07/20/16 18:14 2
tert-Butyl alcohol (TBA) 25 ID 20 10 ug/L 07/20/16 18:14 2 4-Bromofluorobenzene (Surr) 103 80 - 120 07/20/16 18:14 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 89 76 - 132 07/20/16 18:14 2 Toluene-d8 (Surr) 106 80 - 128 07/20/16 18:14 2
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene 1.6 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Anthracene 0.30 J 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Benzo[a]anthracene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Benzo[a]pyrene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Benzo[b]fluoranthene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Benzo[g,h,i]perylene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Benzo[k]fluoranthene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Chrysene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Dibenz(a,h)anthracene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Fluoranthene 0.31 J 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Fluorene 2.0 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-W Lab Sample ID: 440-152822-2
Date Collected: 07/14/16 08:05 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) RL MDL
Indeno[1,2,3-cd]pyrene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Naphthalene 29 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Phenanthrene 2.9 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 Pyrene 0.35 J 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:39 2 2-Fluorobiphenyl (Surr) 46 X 50 - 104 07/18/16 13:01 07/19/16 22:39 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 107 46 - 109 07/18/16 13:01 07/19/16 22:39 2 Terphenyl-d14 66 28 - 124 07/18/16 13:01 07/19/16 22:39 2 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 0.91 0.47 0.093 mg/L 07/18/16 06:55 07/20/16 01:00 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 0.36 J 0.47 0.093 mg/L 07/18/16 06:55 07/20/16 01:00 1 n-Octacosane 40 X 45 - 120 07/18/16 06:55 07/20/16 01:00 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 Aroclor 1242 5.5 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 Aroclor 1254 1.4 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 19:55 1 DCB Decachlorobiphenyl (Surr) 31 26 - 115 07/18/16 12:42 07/22/16 19:55 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 300.0 - Anions, Ion Chromatography
RL MDL
Chloride 14000 1000 500 mg/L 07/18/16 15:51 2000
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate 40 J 50 25 mg/L 07/18/16 17:50 100
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable RL MDL
Antimony ND 0.10 0.060 mg/L 07/19/16 14:16 07/20/16 12:11 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 Barium 2.4 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 Beryllium ND 0.020 0.010 mg/L 07/19/16 14:16 07/20/16 12:11 10 Cadmium ND 0.050 0.020 mg/L 07/19/16 14:16 07/20/16 12:11 10 Chromium 0.14 0.050 0.025 mg/L 07/19/16 14:16 07/20/16 12:11 10 Cobalt 0.031 J 0.10 0.025 mg/L 07/19/16 14:16 07/20/16 12:11 10 Lead 0.27 0.050 0.025 mg/L 07/19/16 14:16 07/20/16 12:11 10 Copper 0.13 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 Molybdenum ND 0.20 0.10 mg/L 07/19/16 14:16 07/20/16 10:13 10 Nickel 0.075 J 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 Selenium ND 0.10 0.061 mg/L 07/19/16 14:16 07/20/16 12:11 10 Silver ND 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-2-W Lab Sample ID: 440-152822-2
Date Collected: 07/14/16 08:05 Matrix: Water
Date Received: 07/14/16 10:34
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable (Continued) RL MDL
Thallium 0.055 J 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Vanadium ND 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:11 10 Zinc 0.47 0.20 0.10 mg/L 07/19/16 14:16 07/20/16 12:11 10 Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury ND 0.00080 0.00040 mg/L 07/20/16 13:00 07/20/16 22:13 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac General Chemistry
RL MDL
Total Dissolved Solids 26000 1000 500 mg/L 07/19/16 09:21 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Client Sample ID: AEC-1-W Lab Sample ID: 440-152822-3
Date Collected: 07/14/16 09:30 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS RL MDL
Volatile Fuel Hydrocarbons
(C4-C12)
2300 250 180 ug/L 07/21/16 12:15 5
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 97 76 - 132 07/21/16 12:15 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 106 80 - 120 07/21/16 12:15 5 Toluene-d8 (Surr) 107 80 - 128 07/21/16 12:15 5
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane ND 2.5 1.3 ug/L 07/21/16 12:15 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,1,2,2-Tetrachloroethane ND 2.5 1.3 ug/L 07/21/16 12:15 5 1,1,2-Trichloroethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,1-Dichloroethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,1-Dichloroethene ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,1-Dichloropropene ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,2,3-Trichlorobenzene ND 5.0 2.0 ug/L 07/21/16 12:15 5 1,2,3-Trichloropropane ND 5.0 1.3 ug/L 07/21/16 12:15 5 1,2,4-Trichlorobenzene ND 5.0 2.0 ug/L 07/21/16 12:15 5 1,2,4-Trimethylbenzene 35 2.5 1.3 ug/L 07/21/16 12:15 5 1,2-Dibromo-3-Chloropropane ND 5.0 2.5 ug/L 07/21/16 12:15 5 1,2-Dibromoethane (EDB) ND 2.5 1.3 ug/L 07/21/16 12:15 5 1,2-Dichlorobenzene ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,2-Dichloroethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,2-Dichloropropane ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,3,5-Trimethylbenzene 8.0 2.5 1.3 ug/L 07/21/16 12:15 5 1,3-Dichlorobenzene ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,3-Dichloropropane ND 2.5 1.3 ug/L 07/21/16 12:15 5
1,4-Dichlorobenzene 17 2.5 1.3 ug/L 07/21/16 12:15 5
2,2-Dichloropropane ND 5.0 2.0 ug/L 07/21/16 12:15 5
2-Chlorotoluene ND 2.5 1.3 ug/L 07/21/16 12:15 5
4-Chlorotoluene ND 2.5 1.3 ug/L 07/21/16 12:15 5
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-W Lab Sample ID: 440-152822-3
Date Collected: 07/14/16 09:30 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
Benzene 4.6 2.5 1.3 ug/L 07/21/16 12:15 5
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Bromobenzene ND 2.5 1.3 ug/L 07/21/16 12:15 5
Bromochloromethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
Bromodichloromethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
Bromoform ND 5.0 2.0 ug/L 07/21/16 12:15 5
Bromomethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
Carbon tetrachloride ND 2.5 1.3 ug/L 07/21/16 12:15 5
Chlorobenzene 1.6 J 2.5 1.3 ug/L 07/21/16 12:15 5
Chloroethane ND 5.0 2.0 ug/L 07/21/16 12:15 5
Chloroform ND 2.5 1.3 ug/L 07/21/16 12:15 5
Chloromethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
cis-1,2-Dichloroethene ND 2.5 1.3 ug/L 07/21/16 12:15 5 cis-1,3-Dichloropropene ND 2.5 1.3 ug/L 07/21/16 12:15 5 Dibromochloromethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
Dibromomethane ND 2.5 1.3 ug/L 07/21/16 12:15 5
Dichlorodifluoromethane ND 5.0 1.3 ug/L 07/21/16 12:15 5 Ethanol ND 750 380 ug/L 07/21/16 12:15 5
Isopropyl Ether (DIPE) ND 2.5 1.3 ug/L 07/21/16 12:15 5 Ethyl-t-butyl ether (ETBE) ND 2.5 1.3 ug/L 07/21/16 12:15 5 Ethylbenzene 19 2.5 1.3 ug/L 07/21/16 12:15 5
Hexachlorobutadiene ND 2.5 1.3 ug/L 07/21/16 12:15 5
Isopropylbenzene 1.5 J 2.5 1.3 ug/L 07/21/16 12:15 5
m,p-Xylene 37 5.0 2.5 ug/L 07/21/16 12:15 5
Methylene Chloride ND 10 4.4 ug/L 07/21/16 12:15 5
Methyl-t-Butyl Ether (MTBE) ND 2.5 1.3 ug/L 07/21/16 12:15 5 Naphthalene 87 5.0 2.0 ug/L 07/21/16 12:15 5
n-Butylbenzene 3.5 J 5.0 2.0 ug/L 07/21/16 12:15 5
N-Propylbenzene 3.2 2.5 1.3 ug/L 07/21/16 12:15 5
o-Xylene 21 2.5 1.3 ug/L 07/21/16 12:15 5
p-Isopropyltoluene 13 2.5 1.3 ug/L 07/21/16 12:15 5
sec-Butylbenzene 2.5 2.5 1.3 ug/L 07/21/16 12:15 5
Styrene ND 2.5 1.3 ug/L 07/21/16 12:15 5
Tert-amyl-methyl ether (TAME) ND 2.5 1.3 ug/L 07/21/16 12:15 5 tert-Butylbenzene ND 2.5 1.3 ug/L 07/21/16 12:15 5
Tetrachloroethene ND 2.5 1.3 ug/L 07/21/16 12:15 5
Toluene 53 2.5 1.3 ug/L 07/21/16 12:15 5
trans-1,2-Dichloroethene ND 2.5 1.3 ug/L 07/21/16 12:15 5 trans-1,3-Dichloropropene ND 2.5 1.3 ug/L 07/21/16 12:15 5 Trichloroethene ND 2.5 1.3 ug/L 07/21/16 12:15 5
Trichlorofluoromethane ND 2.5 1.3 ug/L 07/21/16 12:15 5 Xylenes, Total 58 5.0 2.5 ug/L 07/21/16 12:15 5
Vinyl chloride ND 2.5 1.3 ug/L 07/21/16 12:15 5
tert-Butyl alcohol (TBA) 53 50 25 ug/L 07/21/16 12:15 5 4-Bromofluorobenzene (Surr) 106 80 - 120 07/21/16 12:15 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 97 76 - 132 07/21/16 12:15 5 Toluene-d8 (Surr) 107 80 - 128 07/21/16 12:15 5
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-W Lab Sample ID: 440-152822-3
Date Collected: 07/14/16 09:30 Matrix: Water
Date Received: 07/14/16 10:34
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL
Acenaphthene 0.68 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Anthracene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Benzo[a]anthracene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Benzo[a]pyrene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Benzo[b]fluoranthene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Benzo[g,h,i]perylene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Benzo[k]fluoranthene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Chrysene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Dibenz(a,h)anthracene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Fluoranthene 0.51 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Fluorene 0.68 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Indeno[1,2,3-cd]pyrene ND 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Naphthalene 21 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Phenanthrene 2.1 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 Pyrene 0.41 0.38 0.19 ug/L 07/18/16 13:01 07/19/16 22:59 2 2-Fluorobiphenyl (Surr) 34 X 50 - 104 07/18/16 13:01 07/19/16 22:59 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Nitrobenzene-d5 127 X 46 - 109 07/18/16 13:01 07/19/16 22:59 2 Terphenyl-d14 57 28 - 124 07/18/16 13:01 07/19/16 22:59 2 Method: 8015B - Diesel Range Organics (DRO) (GC)
RL MDL
C13-C22 2.5 0.47 0.094 mg/L 07/18/16 06:55 07/22/16 14:09 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac C23-C40 1.2 0.47 0.094 mg/L 07/18/16 06:55 07/22/16 14:09 1 n-Octacosane 53 45 - 120 07/18/16 06:55 07/22/16 14:09 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
Aroclor 1016 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Aroclor 1221 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 Aroclor 1232 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 Aroclor 1242 1.7 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 Aroclor 1248 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 Aroclor 1254 1.1 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 Aroclor 1260 ND 1.0 0.50 ug/L 07/18/16 12:42 07/22/16 20:08 1 DCB Decachlorobiphenyl (Surr) 23 X 26 - 115 07/18/16 12:42 07/22/16 20:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Method: 300.0 - Anions, Ion Chromatography
RL MDL
Chloride 15000 1000 500 mg/L 07/18/16 16:04 2000
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Sulfate 42 J 50 25 mg/L 07/18/16 18:04 100
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable RL MDL
Antimony ND 0.10 0.060 mg/L 07/19/16 14:16 07/20/16 12:13 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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13 Client Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-W Lab Sample ID: 440-152822-3
Date Collected: 07/14/16 09:30 Matrix: Water
Date Received: 07/14/16 10:34
Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable (Continued) RL MDL
Arsenic 0.063 J 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Barium 3.4 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Beryllium ND 0.020 0.010 mg/L 07/19/16 14:16 07/20/16 12:13 10 Cadmium ND 0.050 0.020 mg/L 07/19/16 14:16 07/20/16 12:13 10 Chromium 0.68 0.050 0.025 mg/L 07/19/16 14:16 07/20/16 12:13 10 Cobalt 0.075 J 0.10 0.025 mg/L 07/19/16 14:16 07/20/16 12:13 10 Lead 1.1 0.050 0.025 mg/L 07/19/16 14:16 07/20/16 12:13 10 Copper 0.60 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Molybdenum ND 0.20 0.10 mg/L 07/19/16 14:16 07/20/16 10:15 10 Nickel 0.31 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Selenium 0.078 J 0.10 0.061 mg/L 07/19/16 14:16 07/20/16 12:13 10 Silver ND 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Thallium ND 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Vanadium 0.19 0.10 0.050 mg/L 07/19/16 14:16 07/20/16 12:13 10 Zinc 2.0 0.20 0.10 mg/L 07/19/16 14:16 07/20/16 12:13 10 Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 0.0030 0.00080 0.00040 mg/L 07/20/16 13:00 07/20/16 23:24 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac General Chemistry
RL MDL
Total Dissolved Solids 30000 1000 500 mg/L 07/19/16 09:22 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Irvine

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13 Method Summary
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL IRV
8260B/CA_LUFTM SW846
S
Volatile Organic Compounds by GC/MS TAL IRV
8270C SIM Semivolatile Organic Compounds (GC/MS SIM) SW846 TAL IRV 8015B Diesel Range Organics (DRO) (GC) SW846 TAL IRV
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL IRV 300.0 Anions, Ion Chromatography MCAWW TAL IRV
200.7 Rev 4.4 Metals (ICP) EPA TAL IRV
245.1 Mercury (CVAA) EPA TAL IRV
SM 2540C Solids, Total Dissolved (TDS) SM TAL IRV
Protocol References:

EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater", SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: EW-1-W Lab Sample ID: 440-152822-1
Date Collected: 07/13/16 16:05 Matrix: Water
Date Received: 07/14/16 10:34
Analysis 8260B 1 343557 07/20/16 17:14 AYL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 10 mL 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 1 10 mL 10 mL 343558 07/20/16 17:14 HR TAL IRV Total/NA Prep 3520C 1035 mL 1 mL 343113 07/18/16 13:01 FTD TAL IRV Total/NA Analysis 8270C SIM 1 343497 07/19/16 22:18 AI TAL IRV Total/NA Prep 3510C 1070 mL 1 mL 343009 07/18/16 06:55 L2A TAL IRV Total/NA Analysis 8015B 1 343451 07/20/16 00:38 JM TAL IRV Total/NA Prep 3510C 125 mL 2 mL 343105 07/18/16 12:42 L2A TAL IRV Total/NA Analysis 8082 1 344252 07/22/16 19:42 JM TAL IRV Total/NA Analysis 300.0 1000 343062 07/18/16 15:37 NTN TAL IRV Total/NA Analysis 300.0 100 343062 07/18/16 17:36 NTN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343425 07/19/16 14:16 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 1 343665 07/20/16 10:08 EN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343425 07/19/16 14:16 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 1 343681 07/20/16 12:05 EN TAL IRV Total/NA Prep 245.1 20 mL 20 mL 343699 07/20/16 13:00 DB TAL IRV Total/NA Analysis 245.1 1 343952 07/20/16 22:10 DB TAL IRV Total/NA Analysis SM 2540C 1 10 mL 100 mL 343022 07/19/16 07:51 XL TAL IRV Client Sample ID: AEC-2-W Lab Sample ID: 440-152822-2
Date Collected: 07/14/16 08:05 Matrix: Water
Date Received: 07/14/16 10:34
Analysis 8260B 2 343557 07/20/16 18:14 AYL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 10 mL 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 2 10 mL 10 mL 343558 07/20/16 18:14 HR TAL IRV Total/NA Prep 3520C 1045 mL 1 mL 343113 07/18/16 13:01 FTD TAL IRV Total/NA Analysis 8270C SIM 2 343497 07/19/16 22:39 AI TAL IRV Total/NA Prep 3510C 1070 mL 1 mL 343009 07/18/16 06:55 L2A TAL IRV Total/NA Analysis 8015B 1 343451 07/20/16 01:00 JM TAL IRV Total/NA Prep 3510C 125 mL 2 mL 343105 07/18/16 12:42 L2A TAL IRV Total/NA Analysis 8082 1 344252 07/22/16 19:55 JM TAL IRV Total/NA Analysis 300.0 2000 343062 07/18/16 15:51 NTN TAL IRV Total/NA Analysis 300.0 100 343062 07/18/16 17:50 NTN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343425 07/19/16 14:16 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 10 343665 07/20/16 10:13 EN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343425 07/19/16 14:16 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 10 343681 07/20/16 12:11 EN TAL IRV Total/NA Prep 245.1 5 mL 20 mL 343699 07/20/16 13:00 DB TAL IRV Total/NA Analysis 245.1 1 343952 07/20/16 22:13 DB TAL IRV Total/NA Analysis SM 2540C 1 1 mL 100 mL 343022 07/19/16 09:21 XL TAL IRV TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Client Sample ID: AEC-1-W Lab Sample ID: 440-152822-3
Date Collected: 07/14/16 09:30 Matrix: Water
Date Received: 07/14/16 10:34
Analysis 8260B 5 343879 07/21/16 12:15 AYL TAL IRV
Type
Batch
Method
Batch
Prep Type Run Analyst Lab
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
Factor Number
Dil
Total/NA 10 mL 10 mL
Analysis 8260B/CA_LUFTM
S
Total/NA 5 10 mL 10 mL 343880 07/21/16 12:15 AYL TAL IRV Total/NA Prep 3520C 1055 mL 1 mL 343113 07/18/16 13:01 FTD TAL IRV Total/NA Analysis 8270C SIM 2 343497 07/19/16 22:59 AI TAL IRV Total/NA Prep 3510C 1065 mL 1 mL 343009 07/18/16 06:55 L2A TAL IRV Total/NA Analysis 8015B 1 344271 07/22/16 14:09 CN TAL IRV Total/NA Prep 3510C 125 mL 2 mL 343105 07/18/16 12:42 L2A TAL IRV Total/NA Analysis 8082 1 344252 07/22/16 20:08 JM TAL IRV Total/NA Analysis 300.0 2000 343062 07/18/16 16:04 NTN TAL IRV Total/NA Analysis 300.0 100 343062 07/18/16 18:04 NTN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343425 07/19/16 14:16 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 10 343665 07/20/16 10:15 EN TAL IRV Total Recoverable Prep 200.2 25 mL 25 mL 343425 07/19/16 14:16 Q1N TAL IRV Total Recoverable Analysis 200.7 Rev 4.4 10 343681 07/20/16 12:13 EN TAL IRV Total/NA Prep 245.1 5 mL 20 mL 343699 07/20/16 13:00 DB TAL IRV Total/NA Analysis 245.1 1 343953 07/20/16 23:24 DB TAL IRV Total/NA Analysis SM 2540C 1 1 mL 100 mL 343022 07/19/16 09:22 XL TAL IRV Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 440-343557/8 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/20/16 10:53 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/20/16 10:53 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/20/16 10:53 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/20/16 10:53 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/20/16 10:53 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/20/16 10:53 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/20/16 10:53 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/20/16 10:53 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Benzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Bromobenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Bromochloromethane ND 0.50 0.25 ug/L 07/20/16 10:53 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 Bromoform ND 1.0 0.40 ug/L 07/20/16 10:53 1
Bromomethane ND 0.50 0.25 ug/L 07/20/16 10:53 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/20/16 10:53 1 Chlorobenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Chloroethane ND 1.0 0.40 ug/L 07/20/16 10:53 1
Chloroform ND 0.50 0.25 ug/L 07/20/16 10:53 1
Chloromethane ND 0.50 0.25 ug/L 07/20/16 10:53 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/20/16 10:53 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/20/16 10:53 1 Dibromochloromethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 Dibromomethane ND 0.50 0.25 ug/L 07/20/16 10:53 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/20/16 10:53 1 Ethanol ND 150 75 ug/L 07/20/16 10:53 1
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/20/16 10:53 1 Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/20/16 10:53 1 Ethylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
m,p-Xylene ND 1.0 0.50 ug/L 07/20/16 10:53 1
Methylene Chloride ND 2.0 0.88 ug/L 07/20/16 10:53 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/20/16 10:53 1 TestAmerica Irvine

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13 QC Sample Results
Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-343557/8 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
RL MDL
Naphthalene ND 1.0 0.40 ug/L 07/20/16 10:53 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac n-Butylbenzene ND 1.0 0.40 ug/L 07/20/16 10:53 1
N-Propylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
o-Xylene ND 0.50 0.25 ug/L 07/20/16 10:53 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/20/16 10:53 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Styrene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/20/16 10:53 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Toluene ND 0.50 0.25 ug/L 07/20/16 10:53 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/20/16 10:53 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/20/16 10:53 1 Trichloroethene ND 0.50 0.25 ug/L 07/20/16 10:53 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/20/16 10:53 1 Xylenes, Total ND 1.0 0.50 ug/L 07/20/16 10:53 1
Vinyl chloride ND 0.50 0.25 ug/L 07/20/16 10:53 1
tert-Butyl alcohol (TBA) ND 10 5.0 ug/L 07/20/16 10:53 1 4-Bromofluorobenzene (Surr) 101 80 - 120 07/20/16 10:53 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 101 76 - 132 07/20/16 10:53 1 Toluene-d8 (Surr) 106 80 - 128 07/20/16 10:53 1
Lab Sample ID: LCS 440-343557/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
1,1,1,2-Tetrachloroethane 25.0 23.3 ug/L 93 60 - 141
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 25.0 22.6 ug/L 90 70 - 130
1,1,2,2-Tetrachloroethane 25.0 23.1 ug/L 93 63 - 130
1,1,2-Trichloroethane 25.0 22.7 ug/L 91 70 - 130
1,1-Dichloroethane 25.0 23.0 ug/L 92 64 - 130
1,1-Dichloroethene 25.0 23.8 ug/L 95 70 - 130
1,1-Dichloropropene 25.0 26.0 ug/L 104 70 - 130
1,2,3-Trichlorobenzene 25.0 23.1 ug/L 92 60 - 140
1,2,3-Trichloropropane 25.0 21.6 ug/L 86 63 - 130
1,2,4-Trichlorobenzene 25.0 23.6 ug/L 94 60 - 140
1,2,4-Trimethylbenzene 25.0 22.9 ug/L 92 70 - 135
1,2-Dibromo-3-Chloropropane 25.0 22.0 ug/L 88 52 - 140
1,2-Dibromoethane (EDB) 25.0 25.2 ug/L 101 70 - 130
1,2-Dichlorobenzene 25.0 22.4 ug/L 90 70 - 130
1,2-Dichloroethane 25.0 22.8 ug/L 91 57 - 138
1,2-Dichloropropane 25.0 24.9 ug/L 100 67 - 130
1,3,5-Trimethylbenzene 25.0 22.7 ug/L 91 70 - 136
1,3-Dichlorobenzene 25.0 21.9 ug/L 88 70 - 130
1,3-Dichloropropane 25.0 23.5 ug/L 94 70 - 130
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343557/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
1,4-Dichlorobenzene 25.0 20.6 ug/L 82 70 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
2,2-Dichloropropane 25.0 23.4 ug/L 93 68 - 141
2-Chlorotoluene 25.0 21.8 ug/L 87 70 - 130
4-Chlorotoluene 25.0 21.9 ug/L 88 70 - 130
Benzene 25.0 24.5 ug/L 98 68 - 130
Bromobenzene 25.0 23.7 ug/L 95 70 - 130
Bromochloromethane 25.0 24.5 ug/L 98 70 - 130
Bromodichloromethane 25.0 24.0 ug/L 96 70 - 132
Bromoform 25.0 23.8 ug/L 95 60 - 148
Bromomethane 25.0 23.6 ug/L 94 64 - 139
Carbon tetrachloride 25.0 24.5 ug/L 98 60 - 150
Chlorobenzene 25.0 22.2 ug/L 89 70 - 130
Chloroethane 25.0 22.7 ug/L 91 64 - 135
Chloroform 25.0 23.4 ug/L 93 70 - 130
Chloromethane 25.0 20.2 ug/L 81 47 - 140
cis-1,2-Dichloroethene 25.0 25.4 ug/L 102 70 - 133
cis-1,3-Dichloropropene 25.0 23.5 ug/L 94 70 - 133
Dibromochloromethane 25.0 24.0 ug/L 96 69 - 145
Dibromomethane 25.0 24.1 ug/L 96 70 - 130
Dichlorodifluoromethane 25.0 18.5 ug/L 74 29 - 150
Ethanol 1000 858 ug/L 86 50 - 149
Isopropyl Ether (DIPE) 25.0 26.3 ug/L 105 58 - 139
Ethyl-t-butyl ether (ETBE) 25.0 24.6 ug/L 98 60 - 136
Ethylbenzene 25.0 25.4 ug/L 102 70 - 130
Hexachlorobutadiene 25.0 21.2 ug/L 85 10 - 150
Isopropylbenzene 25.0 24.6 ug/L 98 70 - 136
m,p-Xylene 25.0 24.7 ug/L 99 70 - 130
Methylene Chloride 25.0 23.4 ug/L 93 52 - 130
Methyl-t-Butyl Ether (MTBE) 25.0 25.3 ug/L 101 63 - 131 Naphthalene 25.0 23.0 ug/L 92 60 - 140
n-Butylbenzene 25.0 22.6 ug/L 90 65 - 150
N-Propylbenzene 25.0 22.6 ug/L 90 67 - 139
o-Xylene 25.0 22.8 ug/L 91 70 - 130
p-Isopropyltoluene 25.0 23.6 ug/L 95 70 - 132
sec-Butylbenzene 25.0 22.2 ug/L 89 70 - 138
Styrene 25.0 22.5 ug/L 90 70 - 134
Tert-amyl-methyl ether (TAME) 25.0 24.7 ug/L 99 57 - 139 tert-Butylbenzene 25.0 22.6 ug/L 90 70 - 130
Tetrachloroethene 25.0 23.1 ug/L 93 70 - 130
Toluene 25.0 24.7 ug/L 99 70 - 130
trans-1,2-Dichloroethene 25.0 25.9 ug/L 104 70 - 130
trans-1,3-Dichloropropene 25.0 22.3 ug/L 89 70 - 132
Trichloroethene 25.0 24.9 ug/L 100 70 - 130
Trichlorofluoromethane 25.0 20.8 ug/L 83 60 - 150
Vinyl chloride 25.0 21.4 ug/L 86 59 - 133
tert-Butyl alcohol (TBA) 250 225 ug/L 90 70 - 130
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343557/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
96 LCS LCS
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 100 76 - 132
Toluene-d8 (Surr) 101 80 - 128
Lab Sample ID: 440-152803-E-3 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
1,1,1,2-Tetrachloroethane ND 5000 4790 ug/L 96 60 - 149 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 5000 4220 ug/L 84 70 - 130
1,1,2,2-Tetrachloroethane ND F1 5000 6440 ug/L 129 63 - 130 1,1,2-Trichloroethane ND 5000 5900 ug/L 118 70 - 130
1,1-Dichloroethane ND 5000 4800 ug/L 96 65 - 130
1,1-Dichloroethene ND 5000 4940 ug/L 99 70 - 130
1,1-Dichloropropene ND 5000 5600 ug/L 112 64 - 130
1,2,3-Trichlorobenzene ND 5000 5840 ug/L 117 60 - 140
1,2,3-Trichloropropane ND 5000 5560 ug/L 111 60 - 130
1,2,4-Trichlorobenzene ND 5000 6100 ug/L 122 60 - 140
1,2,4-Trimethylbenzene 3400 5000 9270 ug/L 117 70 - 130 1,2-Dibromo-3-Chloropropane ND 5000 5810 ug/L 116 48 - 140 1,2-Dibromoethane (EDB) ND 5000 6000 ug/L 120 70 - 131
1,2-Dichlorobenzene ND 5000 5470 ug/L 109 70 - 130
1,2-Dichloroethane ND 5000 4340 ug/L 87 56 - 146
1,2-Dichloropropane ND 5000 5740 ug/L 115 69 - 130
1,3,5-Trimethylbenzene 1100 5000 6720 ug/L 112 70 - 130 1,3-Dichlorobenzene ND 5000 5290 ug/L 106 70 - 130
1,3-Dichloropropane ND 5000 5610 ug/L 112 70 - 130
1,4-Dichlorobenzene ND 5000 4960 ug/L 99 70 - 130
2,2-Dichloropropane ND 5000 4410 ug/L 88 69 - 138
2-Chlorotoluene ND 5000 5580 ug/L 112 70 - 130
4-Chlorotoluene ND 5000 5340 ug/L 107 70 - 130
Benzene 18000 5000 22800 ug/L 104 66 - 130
Bromobenzene ND 5000 5820 ug/L 116 70 - 130
Bromochloromethane ND 5000 5510 ug/L 110 70 - 130
Bromodichloromethane ND 5000 5220 ug/L 104 70 - 138
Bromoform ND 5000 5310 ug/L 106 59 - 150
Bromomethane ND 5000 4260 ug/L 85 62 - 131
Carbon tetrachloride ND 5000 4340 ug/L 87 60 - 150
Chlorobenzene ND 5000 5060 ug/L 101 70 - 130
Chloroethane ND 5000 4380 ug/L 88 68 - 130
Chloroform ND 5000 4770 ug/L 95 70 - 130
Chloromethane ND 5000 3910 ug/L 78 39 - 144
cis-1,2-Dichloroethene ND 5000 5620 ug/L 112 70 - 130
cis-1,3-Dichloropropene ND 5000 5690 ug/L 114 70 - 133
Dibromochloromethane ND 5000 4950 ug/L 99 70 - 148
Dibromomethane ND 5000 5440 ug/L 109 70 - 130
Dichlorodifluoromethane ND 5000 3350 ug/L 67 25 - 142
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152803-E-3 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
Ethanol ND 200000 164000 ug/L 82 54 - 150
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Isopropyl Ether (DIPE) 860 5000 6470 ug/L 112 64 - 138
Ethyl-t-butyl ether (ETBE) ND 5000 5620 ug/L 112 70 - 130 Ethylbenzene 3300 5000 9060 ug/L 114 70 - 130
Hexachlorobutadiene ND 5000 4800 ug/L 96 10 - 150
Isopropylbenzene 470 5000 5820 ug/L 107 70 - 132
m,p-Xylene 11000 5000 16700 ug/L 120 70 - 133
Methylene Chloride ND 5000 5170 ug/L 103 52 - 130
Methyl-t-Butyl Ether (MTBE) ND 5000 6060 ug/L 121 70 - 130 Naphthalene 770 5000 7390 ug/L 132 60 - 140
n-Butylbenzene 380 5000 6080 ug/L 114 61 - 149
N-Propylbenzene 710 5000 6390 ug/L 114 66 - 135
o-Xylene 1900 5000 6890 ug/L 101 70 - 133
p-Isopropyltoluene 270 5000 6060 ug/L 116 70 - 130
sec-Butylbenzene 190 5000 5530 ug/L 107 67 - 134
Styrene ND 5000 5360 ug/L 107 29 - 150
Tert-amyl-methyl ether (TAME) ND 5000 6160 ug/L 123 68 - 133 tert-Butylbenzene 64 J 5000 5430 ug/L 107 70 - 130
Tetrachloroethene ND 5000 5060 ug/L 101 70 - 137
Toluene 19000 5000 23500 E ug/L 96 70 - 130
trans-1,2-Dichloroethene ND 5000 5760 ug/L 115 70 - 130 trans-1,3-Dichloropropene ND 5000 5310 ug/L 106 70 - 138 Trichloroethene ND 5000 5120 ug/L 102 70 - 130
Trichlorofluoromethane ND 5000 3700 ug/L 74 60 - 150
Vinyl chloride ND 5000 4010 ug/L 80 50 - 137
tert-Butyl alcohol (TBA) ND 50000 47300 ug/L 95 70 - 130 4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
103
MS MS
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 94 76 - 132
Toluene-d8 (Surr) 102 80 - 128
Lab Sample ID: 440-152803-E-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
1,1,1,2-Tetrachloroethane ND 5000 4840 ug/L 97 60 - 149 1 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 5000 4400 ug/L 88 70 - 130 4 20 1,1,2,2-Tetrachloroethane ND F1 5000 6650 F1 ug/L 133 63 - 130 3 30 1,1,2-Trichloroethane ND 5000 5890 ug/L 118 70 - 130 0 25 1,1-Dichloroethane ND 5000 5090 ug/L 102 65 - 130 6 20
1,1-Dichloroethene ND 5000 5150 ug/L 103 70 - 130 4 20
1,1-Dichloropropene ND 5000 5780 ug/L 116 64 - 130 3 20 1,2,3-Trichlorobenzene ND 5000 5900 ug/L 118 60 - 140 1 20 1,2,3-Trichloropropane ND 5000 5520 ug/L 110 60 - 130 1 30 1,2,4-Trichlorobenzene ND 5000 6100 ug/L 122 60 - 140 0 20 1,2,4-Trimethylbenzene 3400 5000 8630 ug/L 104 70 - 130 7 25 TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152803-E-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
1,2-Dibromo-3-Chloropropane ND 5000 5740 ug/L 115 48 - 140 1 30 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,2-Dibromoethane (EDB) ND 5000 5870 ug/L 117 70 - 131 2 25 1,2-Dichlorobenzene ND 5000 5480 ug/L 110 70 - 130 0 20 1,2-Dichloroethane ND 5000 4390 ug/L 88 56 - 146 1 20
1,2-Dichloropropane ND 5000 6030 ug/L 121 69 - 130 5 20 1,3,5-Trimethylbenzene 1100 5000 6050 ug/L 99 70 - 130 11 20 1,3-Dichlorobenzene ND 5000 5330 ug/L 107 70 - 130 1 20 1,3-Dichloropropane ND 5000 5550 ug/L 111 70 - 130 1 25 1,4-Dichlorobenzene ND 5000 5000 ug/L 100 70 - 130 1 20 2,2-Dichloropropane ND 5000 4650 ug/L 93 69 - 138 5 25
2-Chlorotoluene ND 5000 5570 ug/L 111 70 - 130 0 20
4-Chlorotoluene ND 5000 5320 ug/L 106 70 - 130 1 20
Benzene 18000 5000 23100 ug/L 110 66 - 130 1 20
Bromobenzene ND 5000 5830 ug/L 117 70 - 130 0 20
Bromochloromethane ND 5000 5530 ug/L 111 70 - 130 0 25
Bromodichloromethane ND 5000 5190 ug/L 104 70 - 138 1 20 Bromoform ND 5000 5440 ug/L 109 59 - 150 2 25
Bromomethane ND 5000 4320 ug/L 86 62 - 131 1 25
Carbon tetrachloride ND 5000 4450 ug/L 89 60 - 150 2 25 Chlorobenzene ND 5000 4990 ug/L 100 70 - 130 1 20
Chloroethane ND 5000 4450 ug/L 89 68 - 130 2 25
Chloroform ND 5000 4880 ug/L 98 70 - 130 2 20
Chloromethane ND 5000 4100 ug/L 82 39 - 144 5 25
cis-1,2-Dichloroethene ND 5000 5720 ug/L 114 70 - 130 2 20 cis-1,3-Dichloropropene ND 5000 5740 ug/L 115 70 - 133 1 20 Dibromochloromethane ND 5000 4990 ug/L 100 70 - 148 1 25 Dibromomethane ND 5000 5590 ug/L 112 70 - 130 3 25
Dichlorodifluoromethane ND 5000 3490 ug/L 70 25 - 142 4 30 Ethanol ND 200000 166000 ug/L 83 54 - 150 1 30
Isopropyl Ether (DIPE) 860 5000 6690 ug/L 117 64 - 138 3 25 Ethyl-t-butyl ether (ETBE) ND 5000 5810 ug/L 116 70 - 130 3 25 Ethylbenzene 3300 5000 8590 ug/L 105 70 - 130 5 20
Hexachlorobutadiene ND 5000 4770 ug/L 95 10 - 150 1 20
Isopropylbenzene 470 5000 5800 ug/L 107 70 - 132 0 20
m,p-Xylene 11000 5000 15000 ug/L 86 70 - 133 11 25
Methylene Chloride ND 5000 5260 ug/L 105 52 - 130 2 20
Methyl-t-Butyl Ether (MTBE) ND 5000 6130 ug/L 123 70 - 130 1 25 Naphthalene 770 5000 7230 ug/L 129 60 - 140 2 30
n-Butylbenzene 380 5000 5950 ug/L 111 61 - 149 2 20
N-Propylbenzene 710 5000 6390 ug/L 114 66 - 135 0 20
o-Xylene 1900 5000 6760 ug/L 98 70 - 133 2 20
p-Isopropyltoluene 270 5000 6030 ug/L 115 70 - 130 0 20 sec-Butylbenzene 190 5000 5670 ug/L 110 67 - 134 2 20
Styrene ND 5000 5470 ug/L 109 29 - 150 2 35
Tert-amyl-methyl ether (TAME) ND 5000 6430 ug/L 129 68 - 133 4 30 tert-Butylbenzene 64 J 5000 5470 ug/L 108 70 - 130 1 20 Tetrachloroethene ND 5000 5130 ug/L 103 70 - 137 1 20
Toluene 19000 5000 22400 E ug/L 74 70 - 130 5 20
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152803-E-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343557
trans-1,2-Dichloroethene ND 5000 5990 ug/L 120 70 - 130 4 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
trans-1,3-Dichloropropene ND 5000 5300 ug/L 106 70 - 138 0 25 Trichloroethene ND 5000 5300 ug/L 106 70 - 130 4 20
Trichlorofluoromethane ND 5000 3800 ug/L 76 60 - 150 2 25 Vinyl chloride ND 5000 4180 ug/L 84 50 - 137 4 30
tert-Butyl alcohol (TBA) ND 50000 47300 ug/L 95 70 - 130 0 25 4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
101

MSD MSD
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 92 76 - 132
Toluene-d8 (Surr) 101 80 - 128
Lab Sample ID: MB 440-343879/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
RL MDL
1,1,1,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 1,1,1-Trichloroethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 1,1,2,2-Tetrachloroethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 1,1,2-Trichloroethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 1,1-Dichloroethane ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,1-Dichloroethene ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,1-Dichloropropene ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,2,3-Trichlorobenzene ND 1.0 0.40 ug/L 07/21/16 09:29 1 1,2,3-Trichloropropane ND 1.0 0.25 ug/L 07/21/16 09:29 1 1,2,4-Trichlorobenzene ND 1.0 0.40 ug/L 07/21/16 09:29 1 1,2,4-Trimethylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1 1,2-Dibromo-3-Chloropropane ND 1.0 0.50 ug/L 07/21/16 09:29 1 1,2-Dibromoethane (EDB) ND 0.50 0.25 ug/L 07/21/16 09:29 1 1,2-Dichlorobenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,2-Dichloroethane ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,2-Dichloropropane ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,3,5-Trimethylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1 1,3-Dichlorobenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,3-Dichloropropane ND 0.50 0.25 ug/L 07/21/16 09:29 1
1,4-Dichlorobenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
2,2-Dichloropropane ND 1.0 0.40 ug/L 07/21/16 09:29 1
2-Chlorotoluene ND 0.50 0.25 ug/L 07/21/16 09:29 1
4-Chlorotoluene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Benzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Bromobenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Bromochloromethane ND 0.50 0.25 ug/L 07/21/16 09:29 1
Bromodichloromethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 Bromoform ND 1.0 0.40 ug/L 07/21/16 09:29 1
Bromomethane ND 0.50 0.25 ug/L 07/21/16 09:29 1
Carbon tetrachloride ND 0.50 0.25 ug/L 07/21/16 09:29 1 Chlorobenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-343879/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
RL MDL
Chloroethane ND 1.0 0.40 ug/L 07/21/16 09:29 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Chloroform ND 0.50 0.25 ug/L 07/21/16 09:29 1
Chloromethane ND 0.50 0.25 ug/L 07/21/16 09:29 1
cis-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/21/16 09:29 1 cis-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/21/16 09:29 1 Dibromochloromethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 Dibromomethane ND 0.50 0.25 ug/L 07/21/16 09:29 1
Dichlorodifluoromethane ND 1.0 0.25 ug/L 07/21/16 09:29 1 Ethanol ND 150 75 ug/L 07/21/16 09:29 1
Isopropyl Ether (DIPE) ND 0.50 0.25 ug/L 07/21/16 09:29 1 Ethyl-t-butyl ether (ETBE) ND 0.50 0.25 ug/L 07/21/16 09:29 1 Ethylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Hexachlorobutadiene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Isopropylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
m,p-Xylene ND 1.0 0.50 ug/L 07/21/16 09:29 1
Methylene Chloride ND 2.0 0.88 ug/L 07/21/16 09:29 1
Methyl-t-Butyl Ether (MTBE) ND 0.50 0.25 ug/L 07/21/16 09:29 1 Naphthalene ND 1.0 0.40 ug/L 07/21/16 09:29 1
n-Butylbenzene ND 1.0 0.40 ug/L 07/21/16 09:29 1
N-Propylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
o-Xylene ND 0.50 0.25 ug/L 07/21/16 09:29 1
p-Isopropyltoluene ND 0.50 0.25 ug/L 07/21/16 09:29 1
sec-Butylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Styrene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Tert-amyl-methyl ether (TAME) ND 0.50 0.25 ug/L 07/21/16 09:29 1 tert-Butylbenzene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Tetrachloroethene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Toluene ND 0.50 0.25 ug/L 07/21/16 09:29 1
trans-1,2-Dichloroethene ND 0.50 0.25 ug/L 07/21/16 09:29 1 trans-1,3-Dichloropropene ND 0.50 0.25 ug/L 07/21/16 09:29 1 Trichloroethene ND 0.50 0.25 ug/L 07/21/16 09:29 1
Trichlorofluoromethane ND 0.50 0.25 ug/L 07/21/16 09:29 1 Xylenes, Total ND 1.0 0.50 ug/L 07/21/16 09:29 1
Vinyl chloride ND 0.50 0.25 ug/L 07/21/16 09:29 1
tert-Butyl alcohol (TBA) ND 10 5.0 ug/L 07/21/16 09:29 1 4-Bromofluorobenzene (Surr) 102 80 - 120 07/21/16 09:29 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 102 76 - 132 07/21/16 09:29 1 Toluene-d8 (Surr) 107 80 - 128 07/21/16 09:29 1
Lab Sample ID: LCS 440-343879/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
1,1,1,2-Tetrachloroethane 25.0 26.8 ug/L 107 60 - 141
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,1-Trichloroethane 25.0 26.6 ug/L 106 70 - 130
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343879/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
1,1,2,2-Tetrachloroethane 25.0 25.5 ug/L 102 63 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,2-Trichloroethane 25.0 25.7 ug/L 103 70 - 130
1,1-Dichloroethane 25.0 26.0 ug/L 104 64 - 130
1,1-Dichloroethene 25.0 26.0 ug/L 104 70 - 130
1,1-Dichloropropene 25.0 26.5 ug/L 106 70 - 130
1,2,3-Trichlorobenzene 25.0 26.3 ug/L 105 60 - 140
1,2,3-Trichloropropane 25.0 27.7 ug/L 111 63 - 130
1,2,4-Trichlorobenzene 25.0 27.1 ug/L 109 60 - 140
1,2,4-Trimethylbenzene 25.0 25.8 ug/L 103 70 - 135
1,2-Dibromo-3-Chloropropane 25.0 27.4 ug/L 109 52 - 140 1,2-Dibromoethane (EDB) 25.0 27.0 ug/L 108 70 - 130
1,2-Dichlorobenzene 25.0 25.3 ug/L 101 70 - 130
1,2-Dichloroethane 25.0 27.0 ug/L 108 57 - 138
1,2-Dichloropropane 25.0 27.7 ug/L 111 67 - 130
1,3,5-Trimethylbenzene 25.0 26.0 ug/L 104 70 - 136
1,3-Dichlorobenzene 25.0 25.1 ug/L 100 70 - 130
1,3-Dichloropropane 25.0 23.9 ug/L 96 70 - 130
1,4-Dichlorobenzene 25.0 25.4 ug/L 102 70 - 130
2,2-Dichloropropane 25.0 27.0 ug/L 108 68 - 141
2-Chlorotoluene 25.0 25.4 ug/L 102 70 - 130
4-Chlorotoluene 25.0 25.7 ug/L 103 70 - 130
Benzene 25.0 25.9 ug/L 104 68 - 130
Bromobenzene 25.0 27.7 ug/L 111 70 - 130
Bromochloromethane 25.0 28.3 ug/L 113 70 - 130
Bromodichloromethane 25.0 28.2 ug/L 113 70 - 132
Bromoform 25.0 27.6 ug/L 110 60 - 148
Bromomethane 25.0 25.7 ug/L 103 64 - 139
Carbon tetrachloride 25.0 27.4 ug/L 110 60 - 150
Chlorobenzene 25.0 24.1 ug/L 96 70 - 130
Chloroethane 25.0 25.9 ug/L 104 64 - 135
Chloroform 25.0 26.7 ug/L 107 70 - 130
Chloromethane 25.0 25.1 ug/L 100 47 - 140
cis-1,2-Dichloroethene 25.0 27.4 ug/L 109 70 - 133
cis-1,3-Dichloropropene 25.0 28.6 ug/L 114 70 - 133
Dibromochloromethane 25.0 27.8 ug/L 111 69 - 145
Dibromomethane 25.0 26.2 ug/L 105 70 - 130
Dichlorodifluoromethane 25.0 21.3 ug/L 85 29 - 150
Ethanol 1000 983 ug/L 98 50 - 149
Isopropyl Ether (DIPE) 25.0 28.2 ug/L 113 58 - 139
Ethyl-t-butyl ether (ETBE) 25.0 27.9 ug/L 112 60 - 136
Ethylbenzene 25.0 24.0 ug/L 96 70 - 130
Hexachlorobutadiene 25.0 24.6 ug/L 98 10 - 150
Isopropylbenzene 25.0 24.4 ug/L 98 70 - 136
m,p-Xylene 25.0 25.6 ug/L 102 70 - 130
Methylene Chloride 25.0 27.5 ug/L 110 52 - 130
Methyl-t-Butyl Ether (MTBE) 25.0 27.5 ug/L 110 63 - 131 Naphthalene 25.0 26.3 ug/L 105 60 - 140
n-Butylbenzene 25.0 24.8 ug/L 99 65 - 150
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 440-343879/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
N-Propylbenzene 25.0 24.7 ug/L 99 67 - 139
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
o-Xylene 25.0 24.3 ug/L 97 70 - 130
p-Isopropyltoluene 25.0 25.0 ug/L 100 70 - 132
sec-Butylbenzene 25.0 24.1 ug/L 96 70 - 138
Styrene 25.0 25.7 ug/L 103 70 - 134
Tert-amyl-methyl ether (TAME) 25.0 27.9 ug/L 111 57 - 139 tert-Butylbenzene 25.0 25.6 ug/L 102 70 - 130
Tetrachloroethene 25.0 25.1 ug/L 100 70 - 130
Toluene 25.0 25.0 ug/L 100 70 - 130
trans-1,2-Dichloroethene 25.0 28.2 ug/L 113 70 - 130
trans-1,3-Dichloropropene 25.0 28.7 ug/L 115 70 - 132
Trichloroethene 25.0 27.9 ug/L 112 70 - 130
Trichlorofluoromethane 25.0 23.9 ug/L 95 60 - 150
Vinyl chloride 25.0 24.1 ug/L 96 59 - 133
tert-Butyl alcohol (TBA) 250 254 ug/L 102 70 - 130
4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
103

LCS LCS
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 104 76 - 132
Toluene-d8 (Surr) 101 80 - 128
Lab Sample ID: 440-152934-B-20 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
1,1,1,2-Tetrachloroethane ND 25.0 27.2 ug/L 109 60 - 149 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
1,1,1-Trichloroethane ND 25.0 27.0 ug/L 108 70 - 130
1,1,2,2-Tetrachloroethane ND 25.0 27.2 ug/L 109 63 - 130 1,1,2-Trichloroethane ND 25.0 26.7 ug/L 107 70 - 130
1,1-Dichloroethane ND 25.0 26.2 ug/L 105 65 - 130
1,1-Dichloroethene ND 25.0 26.7 ug/L 107 70 - 130
1,1-Dichloropropene ND 25.0 26.9 ug/L 108 64 - 130
1,2,3-Trichlorobenzene ND 25.0 28.1 ug/L 112 60 - 140
1,2,3-Trichloropropane ND 25.0 29.1 ug/L 116 60 - 130
1,2,4-Trichlorobenzene ND 25.0 28.2 ug/L 113 60 - 140
1,2,4-Trimethylbenzene ND 25.0 25.9 ug/L 104 70 - 130
1,2-Dibromo-3-Chloropropane ND 25.0 30.6 ug/L 122 48 - 140 1,2-Dibromoethane (EDB) ND 25.0 28.1 ug/L 112 70 - 131
1,2-Dichlorobenzene ND 25.0 26.7 ug/L 107 70 - 130
1,2-Dichloroethane ND 25.0 28.3 ug/L 113 56 - 146
1,2-Dichloropropane ND 25.0 28.4 ug/L 114 69 - 130
1,3,5-Trimethylbenzene ND 25.0 26.0 ug/L 104 70 - 130
1,3-Dichlorobenzene ND 25.0 25.6 ug/L 102 70 - 130
1,3-Dichloropropane ND 25.0 25.2 ug/L 101 70 - 130
1,4-Dichlorobenzene ND 25.0 26.2 ug/L 105 70 - 130
2,2-Dichloropropane ND 25.0 26.7 ug/L 107 69 - 138
2-Chlorotoluene ND 25.0 25.2 ug/L 101 70 - 130
TestAmerica Irvine

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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152934-B-20 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
4-Chlorotoluene ND 25.0 25.2 ug/L 101 70 - 130
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Benzene ND 25.0 26.4 ug/L 106 66 - 130
Bromobenzene ND 25.0 27.7 ug/L 111 70 - 130
Bromochloromethane ND 25.0 29.0 ug/L 116 70 - 130
Bromodichloromethane ND 25.0 29.0 ug/L 116 70 - 138
Bromoform ND 25.0 29.5 ug/L 118 59 - 150
Bromomethane ND 25.0 26.5 ug/L 106 62 - 131
Carbon tetrachloride ND 25.0 28.0 ug/L 112 60 - 150
Chlorobenzene ND 25.0 24.7 ug/L 99 70 - 130
Chloroethane ND 25.0 27.1 ug/L 108 68 - 130
Chloroform 6.2 25.0 33.3 ug/L 109 70 - 130
Chloromethane ND 25.0 26.3 ug/L 105 39 - 144
cis-1,2-Dichloroethene ND 25.0 27.4 ug/L 110 70 - 130
cis-1,3-Dichloropropene ND 25.0 29.7 ug/L 119 70 - 133
Dibromochloromethane ND 25.0 29.5 ug/L 118 70 - 148
Dibromomethane ND 25.0 28.4 ug/L 114 70 - 130
Dichlorodifluoromethane ND 25.0 22.5 ug/L 90 25 - 142
Ethanol ND 1000 924 ug/L 92 54 - 150
Isopropyl Ether (DIPE) ND 25.0 29.0 ug/L 116 64 - 138
Ethyl-t-butyl ether (ETBE) ND 25.0 29.3 ug/L 117 70 - 130 Ethylbenzene ND 25.0 24.6 ug/L 98 70 - 130
Hexachlorobutadiene ND 25.0 25.5 ug/L 102 10 - 150
Isopropylbenzene ND 25.0 25.0 ug/L 100 70 - 132
m,p-Xylene ND 25.0 25.7 ug/L 103 70 - 133
Methylene Chloride 0.88 J 25.0 27.8 ug/L 108 52 - 130
Methyl-t-Butyl Ether (MTBE) ND 25.0 29.5 ug/L 118 70 - 130 Naphthalene ND 25.0 28.6 ug/L 114 60 - 140
n-Butylbenzene ND 25.0 25.5 ug/L 102 61 - 149
N-Propylbenzene ND 25.0 24.4 ug/L 98 66 - 135
o-Xylene ND 25.0 25.3 ug/L 101 70 - 133
p-Isopropyltoluene ND 25.0 25.5 ug/L 102 70 - 130
sec-Butylbenzene ND 25.0 24.2 ug/L 97 67 - 134
Styrene ND 25.0 25.9 ug/L 104 29 - 150
Tert-amyl-methyl ether (TAME) ND 25.0 29.3 ug/L 117 68 - 133 tert-Butylbenzene ND 25.0 25.3 ug/L 101 70 - 130
Tetrachloroethene ND 25.0 25.5 ug/L 102 70 - 137
Toluene 9.3 25.0 32.6 ug/L 93 70 - 130
trans-1,2-Dichloroethene ND 25.0 28.0 ug/L 112 70 - 130 trans-1,3-Dichloropropene ND 25.0 29.9 ug/L 120 70 - 138 Trichloroethene ND 25.0 27.8 ug/L 111 70 - 130
Trichlorofluoromethane ND 25.0 25.3 ug/L 101 60 - 150
Vinyl chloride ND 25.0 25.7 ug/L 103 50 - 137
tert-Butyl alcohol (TBA) ND 250 258 ug/L 103 70 - 130
4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
101
MS MS
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 105 76 - 132
Toluene-d8 (Surr) 100 80 - 128
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Lab Sample ID: 440-152934-B-20 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
1,1,1,2-Tetrachloroethane ND 25.0 28.0 ug/L 112 60 - 149 3 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,1,1-Trichloroethane ND 25.0 27.5 ug/L 110 70 - 130 2 20 1,1,2,2-Tetrachloroethane ND 25.0 25.7 ug/L 103 63 - 130 5 30 1,1,2-Trichloroethane ND 25.0 26.4 ug/L 106 70 - 130 1 25 1,1-Dichloroethane ND 25.0 26.2 ug/L 105 65 - 130 0 20
1,1-Dichloroethene ND 25.0 27.5 ug/L 110 70 - 130 3 20
1,1-Dichloropropene ND 25.0 28.4 ug/L 113 64 - 130 5 20 1,2,3-Trichlorobenzene ND 25.0 27.9 ug/L 112 60 - 140 1 20 1,2,3-Trichloropropane ND 25.0 27.3 ug/L 109 60 - 130 6 30 1,2,4-Trichlorobenzene ND 25.0 28.3 ug/L 113 60 - 140 0 20 1,2,4-Trimethylbenzene ND 25.0 26.4 ug/L 106 70 - 130 2 25 1,2-Dibromo-3-Chloropropane ND 25.0 27.8 ug/L 111 48 - 140 10 30 1,2-Dibromoethane (EDB) ND 25.0 27.7 ug/L 111 70 - 131 1 25 1,2-Dichlorobenzene ND 25.0 26.5 ug/L 106 70 - 130 0 20 1,2-Dichloroethane ND 25.0 27.4 ug/L 110 56 - 146 3 20
1,2-Dichloropropane ND 25.0 28.6 ug/L 114 69 - 130 1 20 1,3,5-Trimethylbenzene ND 25.0 26.5 ug/L 106 70 - 130 2 20 1,3-Dichlorobenzene ND 25.0 26.0 ug/L 104 70 - 130 2 20 1,3-Dichloropropane ND 25.0 25.1 ug/L 101 70 - 130 0 25 1,4-Dichlorobenzene ND 25.0 26.2 ug/L 105 70 - 130 0 20 2,2-Dichloropropane ND 25.0 27.3 ug/L 109 69 - 138 2 25 2-Chlorotoluene ND 25.0 25.9 ug/L 103 70 - 130 2 20
4-Chlorotoluene ND 25.0 25.9 ug/L 104 70 - 130 3 20
Benzene ND 25.0 26.7 ug/L 107 66 - 130 1 20
Bromobenzene ND 25.0 27.9 ug/L 112 70 - 130 1 20
Bromochloromethane ND 25.0 29.0 ug/L 116 70 - 130 0 25
Bromodichloromethane ND 25.0 29.9 ug/L 119 70 - 138 3 20 Bromoform ND 25.0 28.1 ug/L 112 59 - 150 5 25
Bromomethane ND 25.0 26.8 ug/L 107 62 - 131 1 25
Carbon tetrachloride ND 25.0 28.1 ug/L 112 60 - 150 1 25 Chlorobenzene ND 25.0 24.9 ug/L 100 70 - 130 1 20
Chloroethane ND 25.0 26.7 ug/L 107 68 - 130 1 25
Chloroform 6.2 25.0 33.0 ug/L 107 70 - 130 1 20
Chloromethane ND 25.0 27.2 ug/L 109 39 - 144 3 25
cis-1,2-Dichloroethene ND 25.0 28.3 ug/L 113 70 - 130 3 20 cis-1,3-Dichloropropene ND 25.0 29.5 ug/L 118 70 - 133 1 20 Dibromochloromethane ND 25.0 29.3 ug/L 117 70 - 148 1 25 Dibromomethane ND 25.0 27.4 ug/L 109 70 - 130 4 25
Dichlorodifluoromethane ND 25.0 22.7 ug/L 91 25 - 142 1 30 Ethanol ND 1000 991 ug/L 99 54 - 150 7 30
Isopropyl Ether (DIPE) ND 25.0 28.8 ug/L 115 64 - 138 1 25 Ethyl-t-butyl ether (ETBE) ND 25.0 29.0 ug/L 116 70 - 130 1 25 Ethylbenzene ND 25.0 25.0 ug/L 100 70 - 130 2 20
Hexachlorobutadiene ND 25.0 25.7 ug/L 103 10 - 150 1 20 Isopropylbenzene ND 25.0 25.6 ug/L 102 70 - 132 2 20
m,p-Xylene ND 25.0 26.6 ug/L 106 70 - 133 3 25
Methylene Chloride 0.88 J 25.0 30.8 ug/L 120 52 - 130 10 20 Methyl-t-Butyl Ether (MTBE) ND 25.0 29.0 ug/L 116 70 - 130 2 25 Naphthalene ND 25.0 27.7 ug/L 111 60 - 140 3 30
n-Butylbenzene ND 25.0 26.2 ug/L 105 61 - 149 3 20
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 440-152934-B-20 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343879
N-Propylbenzene ND 25.0 25.2 ug/L 101 66 - 135 3 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
o-Xylene ND 25.0 25.2 ug/L 101 70 - 133 1 20
p-Isopropyltoluene ND 25.0 26.2 ug/L 105 70 - 130 3 20
sec-Butylbenzene ND 25.0 25.2 ug/L 101 67 - 134 4 20
Styrene ND 25.0 25.7 ug/L 103 29 - 150 1 35
Tert-amyl-methyl ether (TAME) ND 25.0 29.0 ug/L 116 68 - 133 1 30 tert-Butylbenzene ND 25.0 26.1 ug/L 104 70 - 130 3 20
Tetrachloroethene ND 25.0 26.2 ug/L 105 70 - 137 3 20
Toluene 9.3 25.0 33.9 ug/L 98 70 - 130 4 20
trans-1,2-Dichloroethene ND 25.0 28.4 ug/L 114 70 - 130 1 20 trans-1,3-Dichloropropene ND 25.0 29.4 ug/L 118 70 - 138 2 25 Trichloroethene ND 25.0 28.6 ug/L 114 70 - 130 3 20
Trichlorofluoromethane ND 25.0 25.2 ug/L 101 60 - 150 0 25 Vinyl chloride ND 25.0 26.9 ug/L 108 50 - 137 5 30
tert-Butyl alcohol (TBA) ND 250 261 ug/L 104 70 - 130 1 25 4-Bromofluorobenzene (Surr) 80 - 120
Surrogate
101

MSD MSD
%Recovery Qualifier Limits
Dibromofluoromethane (Surr) 107 76 - 132
Toluene-d8 (Surr) 101 80 - 128
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS Lab Sample ID: MB 440-343558/8 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343558
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 50 35 ug/L 07/20/16 10:53 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 101 76 - 132 07/20/16 10:53 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 80 - 120 07/20/16 10:53 1 Toluene-d8 (Surr) 106 80 - 128 07/20/16 10:53 1
Lab Sample ID: LCS 440-343558/6 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343558
Volatile Fuel Hydrocarbons
(C4-C12)
500 447 ug/L 89 55 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 76 - 132
Surrogate
96 LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 98 80 - 120
Toluene-d8 (Surr) 101 80 - 128
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 440-152803-E-3 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343558
Volatile Fuel Hydrocarbons
(C4-C12)
460000 F1 345000 983000 E F1 ug/L 153 50 - 145
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 76 - 132
Surrogate
94 MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 103 80 - 120
Toluene-d8 (Surr) 102 80 - 128
Lab Sample ID: 440-152803-E-3 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343558
Volatile Fuel Hydrocarbons
(C4-C12)
460000 F1 345000 855000 E ug/L 116 50 - 145 14 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 76 - 132
Surrogate
92 MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 101 80 - 120
Toluene-d8 (Surr) 101 80 - 128
Lab Sample ID: MB 440-343880/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343880
RL MDL
Volatile Fuel Hydrocarbons (C4-C12) ND 50 35 ug/L 07/21/16 09:29 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 102 76 - 132 07/21/16 09:29 1 MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 80 - 120 07/21/16 09:29 1 Toluene-d8 (Surr) 107 80 - 128 07/21/16 09:29 1
Lab Sample ID: LCS 440-343880/6 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 343880
Volatile Fuel Hydrocarbons
(C4-C12)
500 440 ug/L 88 55 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dibromofluoromethane (Surr) 76 - 132
Surrogate
101

LCS LCS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 105 80 - 120
Toluene-d8 (Surr) 105 80 - 128
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Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-152822-1 Project/Site: Pumpkin Patch
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 440-152934-B-20 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA
Analysis Batch: 343880
Volatile Fuel Hydrocarbons
(C4-C12)
48 J 1730 2040 ug/L 116 50 - 145
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dibromofluoromethane (Surr) 76 - 132
Surrogate
105
MS MS
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 101 80 - 120
Toluene-d8 (Surr) 100 80 - 128
Lab Sample ID: 440-152934-B-20 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA
Analysis Batch: 343880
Volatile Fuel Hydrocarbons
(C4-C12)
48 J 1730 1960 ug/L 111 50 - 145 4 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dibromofluoromethane (Surr) 76 - 132
Surrogate
107

MSD MSD
%Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 101 80 - 120
Toluene-d8 (Surr) 101 80 - 128
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) Lab Sample ID: MB 440-343113/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 343497 Prep Batch: 343113
RL MDL
Acenaphthene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acenaphthylene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Anthracene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Benzo[a]anthracene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Benzo[a]pyrene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Benzo[b]fluoranthene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Benzo[g,h,i]perylene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Benzo[k]fluoranthene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Chrysene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Dibenz(a,h)anthracene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Fluoranthene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Fluorene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Indeno[1,2,3-cd]pyrene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Naphthalene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Phenanthrene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 Pyrene ND 0.20 0.10 ug/L 07/18/16 13:01 07/19/16 19:12 1 2-Fluorobiphenyl (Surr) 73 50 - 104 07/19/16 19:12 1
MB MB
Surrogate
07/18/16 13:01
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
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