Exhibit D - Initial Study-MND and Appendices — San Jose City Council, August 9, 2022 (part 6 of 10)

FIGURES
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Address: 4701 North First Street Client Name: James C. Rees, Sainte Claire Corp.

City/State: Alviso Disbict, San Jose, Caflfomia

ENVIRONMENTAUENGINEERING CONSULTANTS
382 MARTIN AVENUE
SANTA CLARA, CALIFORNIA 95050-3112
TEL: 408.327.5700 FAX: 408.327-5707
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E2C Project Number: 2310SC01
Source:

Milpitas, Calif. Quadrangle
1961 (photorevised 1980)
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A= VACANT LOT
B = RV STORAGE
C = EXCEL LANDSCAPE
D =TURNER EQUIP & GRADING
E = PIN HIGH GOLF
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APPROXIMATE SCALE: 1 "=200' ENVIRONMENTAL I ENGINEERING CONSULTANTS 382 MARTIN AVENUE SANTA CLARA, CALIFORNIA 95050-3112
TEL: 408.327.5700 FAX: 408.327.5707
FIGURE 2 - SITE PLAN
4701 NORTH FIRST STREET

SAN JOSE, CALIFORNIA
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FILENAME: 2310SC01 JOB NUMBER:

DATE: SEPTEMBER 2004
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ENVIRONMENTAL I ENGINEERING CONSULTANTS
382 MARTIN AVENUE
SANTA CI.ARA, CALIFORNIA 95050-3112 lEL: 408.327.6700 FAX: 408.327.6707 /
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!=IGURE 3 ·SAMPLING LOCATIONS
4701 NORTH FIRST STREET

SAN JOSE, CALIFORNIA
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FILENAME: 2310SC01 JOB NUMBER:

DATE: SEPTEMBER zood REVISION:
2310SC01
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FIGURE 4- SAMPLING LOCATIONS

ENVIRONMENTAL/ENGINEERING CONSULTANTS
382 MARTIN AVENUE
SANTA CLARA, CALIFORNIA 950fi0.a112
TEL: 408.327.5700 FAX: 408.327.5707
4701 NORTH FIRST STREET

SAN JOSE, CALIFORNIA
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SCALE:1•=ao• -~--· FIGURE 5- SAMPLING LOCATIONS

ENVIRONMENTAL/ ENGINEERING CONSULTANTS
382 MARnN AVENUE
SANTA CLARA, CAUFORNIA 95050-3112
TEL: 408.327.5700 FAX: 408.327.5707
4701 NORTH FIRST STREET

SAN JOSE, CALIFORNIA
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2310SC01
Appendix B
Phase I Environmental Site Assessment geologica
4701 N. 1st Street, San Jose
Analytical Laboratory Testing Reports

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.

TestAmerica Pleasanton
1220 Quarry Lane
Pleasanton, CA 94566
Tel: (925)484-1919
TestAmerica Job ID: 720-70419-1
Client Project/Site: Pin High
For:

Geologica Inc
220 4th Street, suite 201
Oakland, California 94607
Attn: Brian Aubry
Authorized for release by:
3/1/2016 4:21:52 PM
Micah Smith, Project Manager II
(925)484-1919
[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2
3 4
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13 14
Table of Contents
Client: Geologica Inc
Project/Site: Pin High
TestAmerica Job ID: 720-70419-1

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TestAmerica Pleasanton
3/1/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 1 2
3 4
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9 10
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13 14
Definitions/Glossary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Qualifiers
GC Semi VOA
Qualifier Description
D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D.

Qualifier
X Surrogate is outside control limits
Glossary
These commonly used abbreviations may or may not be present in this report. ¤ Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Pleasanton

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Case Narrative
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Job ID: 720-70419-1
Laboratory: TestAmerica Pleasanton
Narrative
Job Narrative
720-70419-1
Comments
No additional comments.

Receipt
The samples were received on 2/23/2016 5:40 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 2.9º C.

GC Semi VOA
Method(s) 8015B: The following samples required a dilution due to the nature of the sample matrix: GP-2-N-7.5-8' (720-70419-13) and GP-2-S-7.5-8' (720-70419-16). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8015B: The following sample required a dilution due to the nature of the sample matrix: GP-2-E-7.5-8' (720-70419-10).

Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep
Method(s) 3510C SGC: EPA 8015B: A matrix spike/matrix spike duplicate was not included in batch 197615 because insufficient sample volume was available.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

TestAmerica Pleasanton Page 4 of 37 3/1/2016
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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-N Lab Sample ID: 720-70419-1
Diesel Range Organics [C10-C28]
RL
51 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
380 1 8015B
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
1100 1 8015B
Client Sample ID: GP-2-E Lab Sample ID: 720-70419-2
Motor Oil Range Organics [C24-C36]
RL
100 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
150 1 8015B
Client Sample ID: GP-2-E2 Lab Sample ID: 720-70419-3
Diesel Range Organics [C10-C28]
RL
52 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
130 1 8015B
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
310 1 8015B
Client Sample ID: GP-2-S Lab Sample ID: 720-70419-4
Diesel Range Organics [C10-C28]
RL
50 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
81 1 8015B
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
220 1 8015B
Client Sample ID: GP-2-W Lab Sample ID: 720-70419-5
No Detections.

Client Sample ID: GP-2-E2-3.5-4' Lab Sample ID: 720-70419-6 Diesel Range Organics [C10-C28] ☼
RL

1.2 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup

9.7 1 8015B
Client Sample ID: GP-2-E2-7.5-8' Lab Sample ID: 720-70419-7 Diesel Range Organics [C10-C28] ☼
RL

1.1 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
32 1 8015B
Motor Oil Range Organics [C24-C36] 55 mg/Kg ☼ Silica Gel Cleanup
92 1 8015B
Client Sample ID: GP-2-E-3.5-4' Lab Sample ID: 720-70419-9 Diesel Range Organics [C10-C28] ☼
RL

1.1 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup

4.8 1 8015B
Client Sample ID: GP-2-E-7.5-8' Lab Sample ID: 720-70419-10 TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E-7.5-8' (Continued) Lab Sample ID: 720-70419-10 Diesel Range Organics [C10-C28] ☼
RL
11 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
390 10 8015B
Motor Oil Range Organics [C24-C36] 570 mg/Kg ☼ Silica Gel Cleanup
1300 10 8015B
Client Sample ID: GP-2-N-3.5-4' Lab Sample ID: 720-70419-12 No Detections.

Client Sample ID: GP-2-N-7.5-8' Lab Sample ID: 720-70419-13 Diesel Range Organics [C10-C28] ☼
RL

6.0 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
610 5 8015B
Motor Oil Range Organics [C24-C36] 300 mg/Kg ☼ Silica Gel Cleanup
1000 5 8015B
Client Sample ID: GP-2-S-3.5-4' Lab Sample ID: 720-70419-15 Diesel Range Organics [C10-C28] ☼
RL

2.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
45 2 8015B
Motor Oil Range Organics [C24-C36] 120 mg/Kg ☼ Silica Gel Cleanup
230 2 8015B
Client Sample ID: GP-2-S-7.5-8' Lab Sample ID: 720-70419-16 Diesel Range Organics [C10-C28] ☼
RL
29 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
310 10 8015B
Motor Oil Range Organics [C24-C36] 1400 mg/Kg ☼ Silica Gel Cleanup
1900 10 8015B
Client Sample ID: GP-2-W-3.5-4' Lab Sample ID: 720-70419-18 Diesel Range Organics [C10-C28] ☼
RL

2.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
31 2 8015B
Motor Oil Range Organics [C24-C36] 120 mg/Kg ☼ Silica Gel Cleanup
140 2 8015B
Client Sample ID: GP-2-W-7.5-8' Lab Sample ID: 720-70419-19 Diesel Range Organics [C10-C28] ☼
RL

2.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
66 2 8015B
Motor Oil Range Organics [C24-C36] 110 mg/Kg ☼ Silica Gel Cleanup
250 2 8015B
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-N Lab Sample ID: 720-70419-1
Date Collected: 02/23/16 13:20 Matrix: Water
Date Received: 02/23/16 17:40
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 380 51 ug/L 02/25/16 09:29 02/25/16 19:51 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 02/25/16 09:29 02/25/16 19:51 1 [C24-C36]
1100
Capric Acid (Surr) 0.05 0 - 5 02/25/16 09:29 02/25/16 19:51 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 74 31 - 150 02/25/16 09:29 02/25/16 19:51 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E Lab Sample ID: 720-70419-2
Date Collected: 02/23/16 13:10 Matrix: Water
Date Received: 02/23/16 17:40
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] ND 51 ug/L 02/25/16 09:29 02/25/16 18:52 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 02/25/16 09:29 02/25/16 18:52 1 [C24-C36]
150
Capric Acid (Surr) 0.002 0 - 5 02/25/16 09:29 02/25/16 18:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 95 31 - 150 02/25/16 09:29 02/25/16 18:52 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E2 Lab Sample ID: 720-70419-3
Date Collected: 02/23/16 13:00 Matrix: Water
Date Received: 02/23/16 17:40
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 130 52 ug/L 02/25/16 09:29 02/25/16 17:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 02/25/16 09:29 02/25/16 17:53 1 [C24-C36]
310
Capric Acid (Surr) 0.01 0 - 5 02/25/16 09:29 02/25/16 17:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 95 31 - 150 02/25/16 09:29 02/25/16 17:53 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-S Lab Sample ID: 720-70419-4
Date Collected: 02/23/16 14:32 Matrix: Water
Date Received: 02/23/16 17:40
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 81 50 ug/L 02/25/16 09:29 02/25/16 19:21 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 02/25/16 09:29 02/25/16 19:21 1 [C24-C36]
220
Capric Acid (Surr) 0.04 0 - 5 02/25/16 09:29 02/25/16 19:21 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 96 31 - 150 02/25/16 09:29 02/25/16 19:21 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-W Lab Sample ID: 720-70419-5
Date Collected: 02/23/16 14:05 Matrix: Water
Date Received: 02/23/16 17:40
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] ND 51 ug/L 02/25/16 09:29 02/25/16 18:23 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 100 ug/L 02/25/16 09:29 02/25/16 18:23 1 Capric Acid (Surr) 0.003 0 - 5 02/25/16 09:29 02/25/16 18:23 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 103 31 - 150 02/25/16 09:29 02/25/16 18:23 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E2-3.5-4' Lab Sample ID: 720-70419-6 Date Collected: 02/23/16 09:44 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 84.4
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 9.7 1.2 mg/Kg ☼ 02/26/16 10:53 02/29/16 22:33 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 59 mg/Kg ☼ 02/26/16 10:53 02/29/16 22:33 1 p-Terphenyl 79 38 - 148 02/26/16 10:53 02/29/16 22:33 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 15.6 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E2-7.5-8' Lab Sample ID: 720-70419-7 Date Collected: 02/23/16 09:45 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 90.5
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 32 1.1 mg/Kg ☼ 02/26/16 10:53 02/29/16 23:02 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 55 mg/Kg ☼ 02/26/16 10:53 02/29/16 23:02 1 [C24-C36]
92 p-Terphenyl 62 38 - 148 02/26/16 10:53 02/29/16 23:02 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 9.5 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E-3.5-4' Lab Sample ID: 720-70419-9 Date Collected: 02/23/16 10:24 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 87.5
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 4.8 1.1 mg/Kg ☼ 02/26/16 10:53 02/29/16 22:04 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 57 mg/Kg ☼ 02/26/16 10:53 02/29/16 22:04 1 p-Terphenyl 83 38 - 148 02/26/16 10:53 02/29/16 22:04 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 12.5 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E-7.5-8' Lab Sample ID: 720-70419-10 Date Collected: 02/23/16 10:25 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 86.5
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 390 11 mg/Kg ☼ 02/26/16 10:53 03/01/16 12:57 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 570 mg/Kg ☼ 02/26/16 10:53 03/01/16 12:57 10 [C24-C36]
1300
p-Terphenyl 0 X D 38 - 148 02/26/16 10:53 03/01/16 12:57 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 13.5 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-N-3.5-4' Lab Sample ID: 720-70419-12 Date Collected: 02/23/16 10:52 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 90.7
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] ND 1.1 mg/Kg ☼ 02/26/16 10:53 02/29/16 21:34 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 55 mg/Kg ☼ 02/26/16 10:53 02/29/16 21:34 1 p-Terphenyl 87 38 - 148 02/26/16 10:53 02/29/16 21:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 9.3 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-N-7.5-8' Lab Sample ID: 720-70419-13 Date Collected: 02/23/16 10:53 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 82.5
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 610 6.0 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:30 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 300 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:30 5 [C24-C36]
1000
p-Terphenyl 0 D X 38 - 148 02/26/16 10:53 03/01/16 00:30 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 17.5 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-S-3.5-4' Lab Sample ID: 720-70419-15 Date Collected: 02/23/16 11:25 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 81.1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 45 2.4 mg/Kg ☼ 02/26/16 10:53 02/29/16 23:32 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 120 mg/Kg ☼ 02/26/16 10:53 02/29/16 23:32 2 [C24-C36]
230
p-Terphenyl 50 38 - 148 02/26/16 10:53 02/29/16 23:32 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 18.9 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-S-7.5-8' Lab Sample ID: 720-70419-16 Date Collected: 02/23/16 11:26 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 85.9
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 310 29 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:01 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 1400 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:01 10 [C24-C36]
1900
p-Terphenyl 0 D X 38 - 148 02/26/16 10:53 03/01/16 00:01 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 14.1 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-W-3.5-4' Lab Sample ID: 720-70419-18 Date Collected: 02/23/16 11:57 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 82.2
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 31 2.4 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:01 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 120 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:01 2 [C24-C36]
140
p-Terphenyl 52 38 - 148 02/26/16 10:53 03/01/16 00:01 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 17.8 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-W-7.5-8' Lab Sample ID: 720-70419-19 Date Collected: 02/23/16 11:58 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 87.9
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 66 2.3 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:30 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 110 mg/Kg ☼ 02/26/16 10:53 03/01/16 00:30 2 [C24-C36]
250
p-Terphenyl 51 38 - 148 02/26/16 10:53 03/01/16 00:30 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac General Chemistry
RL MDL
Percent Moisture 12.1 0.1 % 02/24/16 13:33 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Method: 8015B - Diesel Range Organics (DRO) (GC)
Lab Sample ID: MB 720-197615/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 197604 Prep Batch: 197615
RL MDL
Diesel Range Organics [C10-C28] ND 50 ug/L 02/25/16 09:29 02/25/16 20:20 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 99 ug/L 02/25/16 09:29 02/25/16 20:20 1 Capric Acid (Surr) 0 0 - 5 02/25/16 20:20 1
MB MB
Surrogate
02/25/16 09:29
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
p-Terphenyl 94 31 - 150 02/25/16 09:29 02/25/16 20:20 1 Lab Sample ID: LCS 720-197615/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 197604 Prep Batch: 197615
Diesel Range Organics
[C10-C28]
2500 1490 ug/L 60 32 - 119
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
p-Terphenyl 31 - 150
Surrogate
83 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: LCSD 720-197615/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 197604 Prep Batch: 197615
Diesel Range Organics
[C10-C28]
2500 1200 ug/L 48 32 - 119 22 35
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
p-Terphenyl 31 - 150
Surrogate
90 LCSD LCSD
%Recovery Qualifier Limits
Lab Sample ID: MB 720-197697/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 197773 Prep Batch: 197697
RL MDL
Diesel Range Organics [C10-C28] ND 1.0 mg/Kg 02/26/16 10:53 03/01/16 02:56 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 50 mg/Kg 02/26/16 10:53 03/01/16 02:56 1 Capric Acid (Surr) 0.006 0 - 1 03/01/16 02:56 1
MB MB
Surrogate
02/26/16 10:53
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
p-Terphenyl 96 38 - 148 02/26/16 10:53 03/01/16 02:56 1 Lab Sample ID: LCS 720-197697/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 197773 Prep Batch: 197697
Diesel Range Organics
[C10-C28]

83.3 49.6 mg/Kg 60 36 - 112
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
p-Terphenyl 38 - 148
Surrogate
97 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 720-70419-9 MS Client Sample ID: GP-2-E-3.5-4' Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 197773 Prep Batch: 197697
Diesel Range Organics
[C10-C28]

4.8 94.3 62.6 mg/Kg ☼ 61 50 - 150
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
p-Terphenyl 38 - 148
Surrogate
79 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 720-70419-9 MSD Client Sample ID: GP-2-E-3.5-4' Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 197773 Prep Batch: 197697
Diesel Range Organics
[C10-C28]

4.8 94.9 67.0 mg/Kg ☼ 66 50 - 150 7 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
p-Terphenyl 38 - 148
Surrogate
83 MSD MSD
%Recovery Qualifier Limits
Method: Moisture - Percent Moisture
Lab Sample ID: 720-70419-6 DU Client Sample ID: GP-2-E2-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 197550
Percent Moisture 15.6 14.9 % 5 20
Analyte
DU DU
Result Qualifier Unit D
Sample
Result
Sample
Qualifier RPD Limit
RPD
TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
GC Semi VOA
Analysis Batch: 197604
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCS 720-197615/2-A Lab Control Sample Silica Gel Cleanup Water 8015B 197615 LCSD 720-197615/3-A Lab Control Sample Dup Silica Gel Cleanup Water 8015B 197615 MB 720-197615/1-A Method Blank Silica Gel Cleanup Water 8015B 197615 Analysis Batch: 197605
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-1 GP-2-N Silica Gel Cleanup Water 8015B 197615 720-70419-2 GP-2-E Silica Gel Cleanup Water 8015B 197615 720-70419-3 GP-2-E2 Silica Gel Cleanup Water 8015B 197615 720-70419-4 GP-2-S Silica Gel Cleanup Water 8015B 197615 720-70419-5 GP-2-W Silica Gel Cleanup Water 8015B 197615 Prep Batch: 197615
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-1 GP-2-N Silica Gel Cleanup Water 3510C SGC
720-70419-2 GP-2-E Silica Gel Cleanup Water 3510C SGC
720-70419-3 GP-2-E2 Silica Gel Cleanup Water 3510C SGC
720-70419-4 GP-2-S Silica Gel Cleanup Water 3510C SGC
720-70419-5 GP-2-W Silica Gel Cleanup Water 3510C SGC
LCS 720-197615/2-A Lab Control Sample Silica Gel Cleanup Water 3510C SGC LCSD 720-197615/3-A Lab Control Sample Dup Silica Gel Cleanup Water 3510C SGC MB 720-197615/1-A Method Blank Silica Gel Cleanup Water 3510C SGC Prep Batch: 197697
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-6 GP-2-E2-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-7 GP-2-E2-7.5-8' Silica Gel Cleanup Solid 3546 720-70419-9 GP-2-E-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-9 MS GP-2-E-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-9 MSD GP-2-E-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-10 GP-2-E-7.5-8' Silica Gel Cleanup Solid 3546 720-70419-12 GP-2-N-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-13 GP-2-N-7.5-8' Silica Gel Cleanup Solid 3546 720-70419-15 GP-2-S-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-16 GP-2-S-7.5-8' Silica Gel Cleanup Solid 3546 720-70419-18 GP-2-W-3.5-4' Silica Gel Cleanup Solid 3546 720-70419-19 GP-2-W-7.5-8' Silica Gel Cleanup Solid 3546 LCS 720-197697/2-A Lab Control Sample Silica Gel Cleanup Solid 3546 MB 720-197697/1-A Method Blank Silica Gel Cleanup Solid 3546 Analysis Batch: 197773
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-6 GP-2-E2-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-7 GP-2-E2-7.5-8' Silica Gel Cleanup Solid 8015B 197697 720-70419-9 GP-2-E-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-9 MS GP-2-E-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-9 MSD GP-2-E-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-12 GP-2-N-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-13 GP-2-N-7.5-8' Silica Gel Cleanup Solid 8015B 197697 720-70419-15 GP-2-S-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-16 GP-2-S-7.5-8' Silica Gel Cleanup Solid 8015B 197697 TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
GC Semi VOA (Continued)
Analysis Batch: 197773 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCS 720-197697/2-A Lab Control Sample Silica Gel Cleanup Solid 8015B 197697 MB 720-197697/1-A Method Blank Silica Gel Cleanup Solid 8015B 197697 Analysis Batch: 197774
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-18 GP-2-W-3.5-4' Silica Gel Cleanup Solid 8015B 197697 720-70419-19 GP-2-W-7.5-8' Silica Gel Cleanup Solid 8015B 197697 Analysis Batch: 197859
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-10 GP-2-E-7.5-8' Silica Gel Cleanup Solid 8015B 197697 General Chemistry
Analysis Batch: 197550
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-70419-6 GP-2-E2-3.5-4' Total/NA Solid Moisture
720-70419-6 DU GP-2-E2-3.5-4' Total/NA Solid Moisture
720-70419-7 GP-2-E2-7.5-8' Total/NA Solid Moisture
720-70419-9 GP-2-E-3.5-4' Total/NA Solid Moisture
720-70419-10 GP-2-E-7.5-8' Total/NA Solid Moisture
720-70419-12 GP-2-N-3.5-4' Total/NA Solid Moisture
720-70419-13 GP-2-N-7.5-8' Total/NA Solid Moisture
720-70419-15 GP-2-S-3.5-4' Total/NA Solid Moisture
720-70419-16 GP-2-S-7.5-8' Total/NA Solid Moisture
720-70419-18 GP-2-W-3.5-4' Total/NA Solid Moisture
720-70419-19 GP-2-W-7.5-8' Total/NA Solid Moisture
TestAmerica Pleasanton

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Lab Chronicle
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-N Lab Sample ID: 720-70419-1
Date Collected: 02/23/16 13:20 Matrix: Water
Date Received: 02/23/16 17:40
Prep 3510C SGC 197615 02/25/16 09:29 NDU TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197605 02/25/16 19:51 JXL TAL PLS Client Sample ID: GP-2-E Lab Sample ID: 720-70419-2
Date Collected: 02/23/16 13:10 Matrix: Water
Date Received: 02/23/16 17:40
Prep 3510C SGC 197615 02/25/16 09:29 NDU TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197605 02/25/16 18:52 JXL TAL PLS Client Sample ID: GP-2-E2 Lab Sample ID: 720-70419-3
Date Collected: 02/23/16 13:00 Matrix: Water
Date Received: 02/23/16 17:40
Prep 3510C SGC 197615 02/25/16 09:29 NDU TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197605 02/25/16 17:53 JXL TAL PLS Client Sample ID: GP-2-S Lab Sample ID: 720-70419-4
Date Collected: 02/23/16 14:32 Matrix: Water
Date Received: 02/23/16 17:40
Prep 3510C SGC 197615 02/25/16 09:29 NDU TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197605 02/25/16 19:21 JXL TAL PLS Client Sample ID: GP-2-W Lab Sample ID: 720-70419-5
Date Collected: 02/23/16 14:05 Matrix: Water
Date Received: 02/23/16 17:40
Prep 3510C SGC 197615 02/25/16 09:29 NDU TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197605 02/25/16 18:23 JXL TAL PLS Client Sample ID: GP-2-E2-3.5-4' Lab Sample ID: 720-70419-6 Date Collected: 02/23/16 09:44 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
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Lab Chronicle
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E2-3.5-4' Lab Sample ID: 720-70419-6 Date Collected: 02/23/16 09:44 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 84.4
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197773 02/29/16 22:33 JXL TAL PLS Client Sample ID: GP-2-E2-7.5-8' Lab Sample ID: 720-70419-7 Date Collected: 02/23/16 09:45 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-E2-7.5-8' Lab Sample ID: 720-70419-7 Date Collected: 02/23/16 09:45 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 90.5
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197773 02/29/16 23:02 JXL TAL PLS Client Sample ID: GP-2-E-3.5-4' Lab Sample ID: 720-70419-9 Date Collected: 02/23/16 10:24 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-E-3.5-4' Lab Sample ID: 720-70419-9 Date Collected: 02/23/16 10:24 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 87.5
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197773 02/29/16 22:04 JXL TAL PLS Client Sample ID: GP-2-E-7.5-8' Lab Sample ID: 720-70419-10 Date Collected: 02/23/16 10:25 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Lab Chronicle
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-E-7.5-8' Lab Sample ID: 720-70419-10 Date Collected: 02/23/16 10:25 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 86.5
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 10 197859 03/01/16 12:57 JXL TAL PLS Client Sample ID: GP-2-N-3.5-4' Lab Sample ID: 720-70419-12 Date Collected: 02/23/16 10:52 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-N-3.5-4' Lab Sample ID: 720-70419-12 Date Collected: 02/23/16 10:52 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 90.7
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 197773 02/29/16 21:34 JXL TAL PLS Client Sample ID: GP-2-N-7.5-8' Lab Sample ID: 720-70419-13 Date Collected: 02/23/16 10:53 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-N-7.5-8' Lab Sample ID: 720-70419-13 Date Collected: 02/23/16 10:53 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 82.5
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 5 197773 03/01/16 00:30 JXL TAL PLS Client Sample ID: GP-2-S-3.5-4' Lab Sample ID: 720-70419-15 Date Collected: 02/23/16 11:25 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Lab Chronicle
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-S-3.5-4' Lab Sample ID: 720-70419-15 Date Collected: 02/23/16 11:25 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 81.1
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 2 197773 02/29/16 23:32 JXL TAL PLS Client Sample ID: GP-2-S-7.5-8' Lab Sample ID: 720-70419-16 Date Collected: 02/23/16 11:26 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-S-7.5-8' Lab Sample ID: 720-70419-16 Date Collected: 02/23/16 11:26 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 85.9
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 10 197773 03/01/16 00:01 JXL TAL PLS Client Sample ID: GP-2-W-3.5-4' Lab Sample ID: 720-70419-18 Date Collected: 02/23/16 11:57 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-W-3.5-4' Lab Sample ID: 720-70419-18 Date Collected: 02/23/16 11:57 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 82.2
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 2 197774 03/01/16 00:01 JXL TAL PLS Client Sample ID: GP-2-W-7.5-8' Lab Sample ID: 720-70419-19 Date Collected: 02/23/16 11:58 Matrix: Solid
Date Received: 02/23/16 17:40
Analysis Moisture 1 197550 02/24/16 13:33 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Lab Chronicle
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Client Sample ID: GP-2-W-7.5-8' Lab Sample ID: 720-70419-19 Date Collected: 02/23/16 11:58 Matrix: Solid
Date Received: 02/23/16 17:40 Percent Solids: 87.9
Prep 3546 197697 02/26/16 10:53 BSY TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 2 197774 03/01/16 00:30 JXL TAL PLS Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 TestAmerica Pleasanton

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Certification Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Laboratory: TestAmerica Pleasanton
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.

Authority Program EPA Region Certification ID Expiration Date California State Program 9 2496 01-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:

Moisture Solid Percent Moisture
TestAmerica Pleasanton

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Method Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Method Method Description Protocol Laboratory
8015B Diesel Range Organics (DRO) (GC) SW846 TAL PLS
Moisture Percent Moisture EPA TAL PLS
Protocol References:

EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 TestAmerica Pleasanton

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Sample Summary
Client: Geologica Inc TestAmerica Job ID: 720-70419-1
Project/Site: Pin High
Lab Sample ID Client Sample ID Matrix Collected Received 720-70419-1 GP-2-N Water 02/23/16 13:20 02/23/16 17:40
720-70419-2 GP-2-E Water 02/23/16 13:10 02/23/16 17:40
720-70419-3 GP-2-E2 Water 02/23/16 13:00 02/23/16 17:40 720-70419-4 GP-2-S Water 02/23/16 14:32 02/23/16 17:40
720-70419-5 GP-2-W Water 02/23/16 14:05 02/23/16 17:40
720-70419-6 GP-2-E2-3.5-4' Solid 02/23/16 09:44 02/23/16 17:40 720-70419-7 GP-2-E2-7.5-8' Solid 02/23/16 09:45 02/23/16 17:40 720-70419-9 GP-2-E-3.5-4' Solid 02/23/16 10:24 02/23/16 17:40 720-70419-10 GP-2-E-7.5-8' Solid 02/23/16 10:25 02/23/16 17:40 720-70419-12 GP-2-N-3.5-4' Solid 02/23/16 10:52 02/23/16 17:40 720-70419-13 GP-2-N-7.5-8' Solid 02/23/16 10:53 02/23/16 17:40 720-70419-15 GP-2-S-3.5-4' Solid 02/23/16 11:25 02/23/16 17:40 720-70419-16 GP-2-S-7.5-8' Solid 02/23/16 11:26 02/23/16 17:40 720-70419-18 GP-2-W-3.5-4' Solid 02/23/16 11:57 02/23/16 17:40 720-70419-19 GP-2-W-7.5-8' Solid 02/23/16 11:58 02/23/16 17:40 TestAmerica Pleasanton

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14 Login Sample Receipt Checklist
Client: Geologica Inc Job Number: 720-70419-1
Login Number: 70419
Question Answer Comment
Creator: Arauz, Dennis
List Source: TestAmerica Pleasanton
List Number: 1
Radioactivity wasn't checked or is </= background as measured by a survey N/A meter.

The cooler's custody seal, if present, is intact. N/A
Sample custody seals, if present, are intact. N/A
The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4").

Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TestAmerica Pleasanton Page 37 of 37 3/1/2016
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.

TestAmerica Pleasanton
1220 Quarry Lane
Pleasanton, CA 94566
Tel: (925)484-1919
TestAmerica Job ID: 720-69933-1
Client Project/Site: Pin High
For:

Geologica Inc
220 4th Street, suite 201
Oakland, California 94607
Attn: Brian Aubry
Authorized for release by:
2/1/2016 5:24:48 PM
Micah Smith, Project Manager II
(925)484-1919
[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Page 2 of 210 ends

TestAmerica Pleasanton
2/1/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 108 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 177 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 188 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 201 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 202 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 203 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 204 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 210 1 2
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Definitions/Glossary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Qualifiers

GC/MS VOA
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier
* ISTD response or retention time outside acceptable limits F2 MS/MSD RPD exceeds control limits
* LCS or LCSD is outside acceptance limits.

GC Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D.

F1 MS and/or MSD Recovery is outside acceptance limits. p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported. 4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.

Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier
F2 MS/MSD RPD exceeds control limits
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.

Glossary
These commonly used abbreviations may or may not be present in this report. ¤ Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Pleasanton

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Case Narrative
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Job ID: 720-69933-1
Laboratory: TestAmerica Pleasanton
Narrative
Job Narrative
720-69933-1
Comments
No additional comments.

Receipt
The samples were received on 1/22/2016 5:10 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperatures of the 2 coolers at receipt time were 2.6º C and 2.8º C.

GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 720-196192 recovered outside control limits for the following analytes: Dichlorodifluoromethane and Trichlorofluoromethane. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.

Method(s) 8260B: The following samples were collected in properly preserved vials for analysis of volatile organic compounds (VOCs).

However, the pH was outside the required criteria when verified by the laboratory, and corrective action was not possible: GP-1 (720-69933-1), GP-2 (720-69933-2), GP-3 (720-69933-3) and GP-6 (720-69933-4). Samples were analyzed within 7 days of collection as recommended.

Method(s) 8260B: The following sample was collected in properly preserved vials for analysis of volatile organic compounds (VOCs).

However, the pH was outside the required criteria when verified by the laboratory, and corrective action was not possible: GP-10 (720-69933-6). Sample was analyzed within 7 days of collection as recommended.

Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 720-196293 recovered outside control limits for the following analytes: Dichlorodifluoromethane and Trichlorofluoromethane. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.

Method(s) 8260B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-196202 and analytical batch 720-196326 were outside control limits for Vinyl acetate. Sample matrix interference are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits.

Method(s) 8260B: Internal standard (ISTD) response for the following samples was outside control limits: GP-4-3.5-4' (720-69933-19) and GP-5-4.5-5' (720-69933-23). The sample(s) was re-extracted and/or re-analyzed with concurring results, and the original set of data has been reported.

Method(s) 8260B: Internal standard (ISTD) response for the following sample was outside control limits: GP-5-7.5-8' (720-69933-24). The sample was re-extracted and/or re-analyzed with concurring results, and the second set of data have been reported.

Method(s) 8260B: Internal standard (ISTD) response for the following samples were outside control limits: GP-2-7.5-8' (720-69933-13) and GP-3-3.5-4' (720-69933-15). The samples were re-analyzed with concurring results, and the data from re-analysis has been reported.

Method(s) 8260B: Internal standard responses were outside of acceptance limits for the following samples: GP-8-3.5-4' (720-69933-35) and (720-69933-A-35-E MS); non-homogeneity are suspected.

Method(s) 8260B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-196295 and analytical batch 720-196408 were outside control limits. Sample matrix non-homogeneity are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits.

The continuing calibration verification (CCV) associated with batch 720-196408 recovered above the upper control limit for Acetone. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following samples are impacted: GP-1-3.5-4' (720-69933-8), GP-2-7.5-8' (720-69933-13), GP-3-3.5-4' (720-69933-15), GP-7-3.5-4' (720-69933-31) and GP-8-3.5-4' (720-69933-35).

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Case Narrative
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Job ID: 720-69933-1 (Continued)
Laboratory: TestAmerica Pleasanton (Continued)
Method(s) 8260B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-196561 and analytical batch 720-196552 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits. 4-Methyl-2-pentanone (MIBK) and Vinyl acetate
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC Semi VOA
Method(s) 8015B: Capric acid Surrogate recovery for the following sample was outside control limits: GP-2-3.5-4' (720-69933-12).

Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8015B: The following samples required a dilution due to the nature of the sample matrix: GP-2 (720-69933-2), GP-2-7.5-8' (720-69933-13), GP-3-3.5-4' (720-69933-15), GP-10-3.5-4' (720-69933-43), (720-69933-A-43-F MS) and (720-69933-A-43-G MSD).

Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8015B: Due to the high concentration of C10-C28, the matrix spike / matrix spike duplicate (MS/MSD) for preparation batch 720-196404 and analytical batch 720-196414 could not be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.

Method(s) 8015B: The following sample required a dilution due to the nature of the sample matrix: GP-1-7.5-8' (720-69933-9). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method(s) 8081A: The matrix spike duplicate (MSD) recoveries for 196366 were outside control limits. Non-homogeneity is suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.

Method(s) 8081A: Surrogate recovery for the following sample was outside control limits: GP-6-7.5-8' (720-69933-28). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8081A: The %RPD between the primary and confirmation column exceeded 40% for 4,4'-DDT for the following samples:

GP-6-7.5-8' (720-69933-28). The lower value(s) has been reported and qualified in accordance with the laboratory's SOP.

Method(s) 8081A: The %RPD between the primary and confirmation column exceeded 40% for Dieldrin for the following samples:

GP-1-7.5-8' (720-69933-9). The lower value(s) has been reported and qualified in accordance with the laboratory's SOP.

Method(s) 8082: Surrogate recovery for the following sample was outside control limits: GP-6-7.5-8' (720-69933-28). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8082: The following samples required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by sulfur: GP-1-3.5-4' (720-69933-8), GP-1-7.5-8' (720-69933-9), GP-6-3.5-4' (720-69933-27), GP-6-7.5-8' (720-69933-28), GP-8-3.5-4' (720-69933-35), GP-8-7.5-8' (720-69933-36), GP-10-3.5-4' (720-69933-43), GP-10-7.5-8' (720-69933-44), (LCS 720-196367/2-A), (MB 720-196367/1-A), (720-69933-A-9-H MS) and (720-69933-A-9-I MSD).

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals
Method(s) 3005A: The following samples requested dissolved metals and were not filtered in the field: GP-1 (720-69933-1), GP-2 (720-69933-2), GP-3 (720-69933-3), GP-6 (720-69933-4), GP-7 (720-69933-5), GP-10 (720-69933-6), (720-69933-F-1-A MS) and (720-69933-F-1-A MSD). These samples were filtered and preserved upon receipt to the laboratory; ref #: 196284 Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-196275 and TestAmerica Pleasanton Page 5 of 210 2/1/2016
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Case Narrative
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Job ID: 720-69933-1 (Continued)
Laboratory: TestAmerica Pleasanton (Continued)
analytical batch 720-196432 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits.

Method(s) 6010B: The serial dilution performed for the following sample associated with batch 720-196432 was outside control limits:
(720-69933-A-8-D SD)
Method(s) 6010B: The following samples was diluted due to the abundance of non-target analytes: GP-1-3.5-4' (720-69933-8), GP-2-7.5-8' (720-69933-13), GP-3-3.5-4' (720-69933-15), GP-3-7.5-8' (720-69933-16), GP-5-4.5-5' (720-69933-23), GP-5-7.5-8' (720-69933-24), GP-6-7.5-8' (720-69933-28), GP-7-3.5-4' (720-69933-31), GP-7-7.5-8' (720-69933-32), GP-8-3.5-4' (720-69933-35), GP-8-7.5-8' (720-69933-36), GP-9-4.5-5' (720-69933-39), GP-9-7.5-8' (720-69933-40) and GP-10-7.5-8' (720-69933-44). Elevated reporting limits (RLs) are provided.

Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 720-196285 and analytical batch 720-196482 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits.

Method(s) 6010B: The serial dilution performed for the following sample associated with batch 720-196482 was outside control limits:
(720-69933-A-47-C SD)
Method(s) 6010B: The following samples was diluted due to the abundance of non-target analytes: GP-11-3.5-4' (720-69933-47) and GP-11-7.5-8' (720-69933-48). Elevated reporting limits (RLs) are provided.

Method(s) 7470A: The following samples requested dissolved metals and were not filtered in the field: GP-1 (720-69933-1), GP-2 (720-69933-2), GP-3 (720-69933-3), GP-6 (720-69933-4), GP-7 (720-69933-5) and GP-10 (720-69933-6). These samples were filtered and preserved upon receipt to the laboratory; ref #: 196284 Method(s) 7471A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 720-196312 and analytical batch 720-196405 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep
Method(s) 3510C SGC: Because more than ½” of sediment was present in the sample bottle, the liquid fraction was transferred to a separatory funnel before adding surrogate and/or spike solutions.

GP-2 (720-69933-2) and GP-7 (720-69933-5)
Method(s) 3510C SGC: EPA 8015B: A matrix spike/matrix spike duplicate was not included in batch 196382 because insufficient sample volume was available. GP-1 (720-69933-1), GP-2 (720-69933-2), GP-3 (720-69933-3), GP-6 (720-69933-4), GP-7 (720-69933-5) and GP-10 (720-69933-6)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1 Lab Sample ID: 720-69933-1
Cobalt
RL

0.0020 mg/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

0.0038 1 6010B Dissolved
Molybdenum 0.049 0.010 mg/L 1 6010B Dissolved
Nickel 0.010 0.010 mg/L 1 6010B Dissolved
Mercury 0.00021 0.00020 mg/L 1 7470A Dissolved
Client Sample ID: GP-2 Lab Sample ID: 720-69933-2
1,1-Dichloroethane
RL

0.50 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

2.5 1 8260B/CA_LUFT Total/NA
MS
1,1-Dichloroethene 18 0.50 ug/L 1 8260B/CA_LUFT Total/NA MS
cis-1,2-Dichloroethene 0.62 0.50 ug/L 1 8260B/CA_LUFT Total/NA MS
trans-1,2-Dichloroethene 1.1 0.50 ug/L 1 8260B/CA_LUFT Total/NA MS
1,1,1-Trichloroethane 1.8 0.50 ug/L 1 8260B/CA_LUFT Total/NA MS
1,1,2-Trichloro-1,2,2-trifluoroethane 1.6 0.50 ug/L 1 8260B/CA_LUFT Total/NA MS
Vinyl chloride 0.99 0.50 ug/L 1 8260B/CA_LUFT Total/NA
MS
Diesel Range Organics [C10-C28] 270 ug/L Silica Gel
Cleanup
1900 5 8015B
Motor Oil Range Organics [C24-C36] 540 ug/L Silica Gel
Cleanup
10000 5 8015B
Barium 0.081 0.050 mg/L 1 6010B Dissolved
Cobalt 0.0081 0.0020 mg/L 1 6010B Dissolved
Molybdenum 0.035 0.010 mg/L 1 6010B Dissolved
Nickel 0.025 0.010 mg/L 1 6010B Dissolved
Zinc 0.024 0.020 mg/L 1 6010B Dissolved
Client Sample ID: GP-3 Lab Sample ID: 720-69933-3
Benzene
RL

0.50 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

6.5 1 8260B/CA_LUFT Total/NA
MS
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
170 1 8015B
Barium 0.052 0.050 mg/L 1 6010B Dissolved
Cobalt 0.010 0.0020 mg/L 1 6010B Dissolved
Molybdenum 0.020 0.010 mg/L 1 6010B Dissolved
Nickel 0.024 0.010 mg/L 1 6010B Dissolved
Client Sample ID: GP-6 Lab Sample ID: 720-69933-4
Benzene
RL

0.50 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

0.73 1 8260B/CA_LUFT Total/NA
MS
Diesel Range Organics [C10-C28] 50 ug/L Silica Gel
Cleanup
84 1 8015B
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
120 1 8015B
Arsenic 0.023 0.010 mg/L 1 6010B Dissolved
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6 (Continued) Lab Sample ID: 720-69933-4 Barium
RL

0.050 mg/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

1.3 1 6010B Dissolved
Cobalt 0.0033 0.0020 mg/L 1 6010B Dissolved
Molybdenum 0.019 0.010 mg/L 1 6010B Dissolved
Nickel 0.013 0.010 mg/L 1 6010B Dissolved
Client Sample ID: GP-7 Lab Sample ID: 720-69933-5
Methyl tert-butyl ether
RL

0.50 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

1.6 1 8260B/CA_LUFT Total/NA
MS
cis-1,2-Dichloroethene 0.94 0.50 ug/L 1 8260B/CA_LUFT Total/NA MS
Trichloroethene 2.0 0.50 ug/L 1 8260B/CA_LUFT Total/NA
MS
Diesel Range Organics [C10-C28] 52 ug/L Silica Gel
Cleanup
65 1 8015B
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
350 1 8015B
Barium 0.069 0.050 mg/L 1 6010B Dissolved
Cobalt 0.0020 0.0020 mg/L 1 6010B Dissolved
Molybdenum 0.072 0.010 mg/L 1 6010B Dissolved
Mercury 0.00025 0.00020 mg/L 1 7470A Dissolved
Client Sample ID: GP-10 Lab Sample ID: 720-69933-6
Diesel Range Organics [C10-C28]
RL
51 ug/L
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
150 1 8015B
Motor Oil Range Organics [C24-C36] 100 ug/L Silica Gel
Cleanup
390 1 8015B
Barium 0.097 0.050 mg/L 1 6010B Dissolved
Cobalt 0.0093 0.0020 mg/L 1 6010B Dissolved
Molybdenum 0.018 0.010 mg/L 1 6010B Dissolved
Nickel 0.013 0.010 mg/L 1 6010B Dissolved
Mercury 0.00023 0.00020 mg/L 1 7470A Dissolved
Client Sample ID: TRIP BLANK Lab Sample ID: 720-69933-7 No Detections.

Client Sample ID: GP-1-3.5-4' Lab Sample ID: 720-69933-8 Diesel Range Organics [C10-C28] ☼
RL

1.1 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
46 1 8015B
Motor Oil Range Organics [C24-C36] 57 mg/Kg ☼ Silica Gel Cleanup
160 1 8015B
4,4'-DDE 28 2.3 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDD 4.6 2.3 ug/Kg 1 ☼ 8081A Total/NA
Antimony 2.5 F1 1.9 mg/Kg 4 ☼ 6010B Total/NA
Arsenic 8.7 3.8 mg/Kg 4 ☼ 6010B Total/NA
Barium 160 F1 F2 1.9 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.54 0.38 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-3.5-4' (Continued) Lab Sample ID: 720-69933-8 Chromium ☼
RL

1.9 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type F173 4 6010B Total/NA
Cobalt 17 0.75 mg/Kg 4 ☼ 6010B Total/NA
Copper 36 5.7 mg/Kg 4 ☼ 6010B Total/NA
Lead 14 1.9 mg/Kg 4 ☼ 6010B Total/NA
Molybdenum 2.7 1.9 mg/Kg 4 ☼ 6010B Total/NA
Nickel 94 F1 1.9 mg/Kg 4 ☼ 6010B Total/NA
Thallium 2.1 1.9 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 41 1.9 mg/Kg 4 ☼ 6010B Total/NA
Zinc 58 5.7 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.63 0.010 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-1-7.5-8' Lab Sample ID: 720-69933-9 Acetone ☼
RL
55 ug/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type 110 1 8260B Total/NA
Diesel Range Organics [C10-C28] 12 mg/Kg ☼ Silica Gel
Cleanup
390 10 8015B
Motor Oil Range Organics [C24-C36] 580 mg/Kg ☼ Silica Gel Cleanup
1500 10 8015B
Dieldrin 6.4 p 4.6 ug/Kg 2 ☼ 8081A Total/NA
4,4'-DDE 57 4.6 ug/Kg 2 ☼ 8081A Total/NA
4,4'-DDD 31 4.6 ug/Kg 2 ☼ 8081A Total/NA
alpha-Chlordane 11 p 4.6 ug/Kg 2 ☼ 8081A Total/NA
gamma-Chlordane 14 4.6 ug/Kg 2 ☼ 8081A Total/NA
Arsenic 7.8 4.5 mg/Kg 4 ☼ 6010B Total/NA
Barium 180 2.3 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.18 0.11 mg/Kg 1 ☼ 6010B Total/NA
Cadmium 0.15 0.14 mg/Kg 1 ☼ 6010B Total/NA
Chromium 86 2.3 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 18 0.91 mg/Kg 4 ☼ 6010B Total/NA
Copper 41 6.8 mg/Kg 4 ☼ 6010B Total/NA
Lead 42 2.3 mg/Kg 4 ☼ 6010B Total/NA
Nickel 120 2.3 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 61 2.3 mg/Kg 4 ☼ 6010B Total/NA
Zinc 79 6.8 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.30 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-2-3.5-4' Lab Sample ID: 720-69933-12 Diesel Range Organics [C10-C28] ☼
RL

1.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
17 1 8015B
Motor Oil Range Organics [C24-C36] 68 mg/Kg ☼ Silica Gel Cleanup
120 1 8015B
Arsenic 5.7 4.9 mg/Kg 4 ☼ 6010B Total/NA
Barium 220 2.4 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.36 0.12 mg/Kg 1 ☼ 6010B Total/NA
Cadmium 0.18 0.15 mg/Kg 1 ☼ 6010B Total/NA
Chromium 60 2.4 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 12 0.98 mg/Kg 4 ☼ 6010B Total/NA
Copper 29 7.3 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2-3.5-4' (Continued) Lab Sample ID: 720-69933-12 Lead ☼
RL

2.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type 31 4 6010B Total/NA
Nickel 82 2.4 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 36 2.4 mg/Kg 4 ☼ 6010B Total/NA
Zinc 99 7.3 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.21 0.012 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-2-7.5-8' Lab Sample ID: 720-69933-13 Diesel Range Organics [C10-C28] ☼
RL
26 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
1400 20 8015B
Motor Oil Range Organics [C24-C36] 1300 mg/Kg ☼ Silica Gel Cleanup
4800 20 8015B
Arsenic 5.0 4.5 mg/Kg 4 ☼ 6010B Total/NA
Barium 150 2.2 mg/Kg 4 ☼ 6010B Total/NA
Chromium 280 2.2 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 48 0.90 mg/Kg 4 ☼ 6010B Total/NA
Copper 27 6.7 mg/Kg 4 ☼ 6010B Total/NA
Lead 15 2.2 mg/Kg 4 ☼ 6010B Total/NA
Nickel 600 2.2 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 43 2.2 mg/Kg 4 ☼ 6010B Total/NA
Zinc 46 6.7 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.21 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-3-3.5-4' Lab Sample ID: 720-69933-15 Diesel Range Organics [C10-C28] ☼
RL
11 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
290 10 8015B
Motor Oil Range Organics [C24-C36] 550 mg/Kg ☼ Silica Gel Cleanup
1200 10 8015B
Barium 140 1.9 mg/Kg 4 ☼ 6010B Total/NA
Chromium 32 1.9 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 11 0.78 mg/Kg 4 ☼ 6010B Total/NA
Copper 25 5.8 mg/Kg 4 ☼ 6010B Total/NA
Lead 3.6 1.9 mg/Kg 4 ☼ 6010B Total/NA
Nickel 32 1.9 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 50 1.9 mg/Kg 4 ☼ 6010B Total/NA
Zinc 37 5.8 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.055 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-3-7.5-8' Lab Sample ID: 720-69933-16 Diesel Range Organics [C10-C28] ☼
RL

1.2 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
11 1 8015B
Barium 100 1.6 mg/Kg 4 ☼ 6010B Total/NA
Chromium 83 1.6 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 16 0.65 mg/Kg 4 ☼ 6010B Total/NA
Copper 63 4.9 mg/Kg 4 ☼ 6010B Total/NA
Lead 5.9 1.6 mg/Kg 4 ☼ 6010B Total/NA
Nickel 86 1.6 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3-7.5-8' (Continued) Lab Sample ID: 720-69933-16 Vanadium ☼
RL

1.6 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type 69 4 6010B Total/NA
Zinc 56 4.9 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.27 0.010 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-4-3.5-4' Lab Sample ID: 720-69933-19 Diesel Range Organics [C10-C28] ☼
RL

1.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup

5.1 1 8015B
Arsenic 5.7 5.3 mg/Kg 4 ☼ 6010B Total/NA
Barium 180 2.6 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.79 0.53 mg/Kg 4 ☼ 6010B Total/NA
Cadmium 0.37 0.16 mg/Kg 1 ☼ 6010B Total/NA
Chromium 63 2.6 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 13 1.1 mg/Kg 4 ☼ 6010B Total/NA
Copper 45 7.9 mg/Kg 4 ☼ 6010B Total/NA
Lead 39 2.6 mg/Kg 4 ☼ 6010B Total/NA
Molybdenum 0.76 0.66 mg/Kg 1 ☼ 6010B Total/NA
Nickel 77 2.6 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 51 2.6 mg/Kg 4 ☼ 6010B Total/NA
Zinc 120 7.9 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.18 0.013 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-5-4.5-5' Lab Sample ID: 720-69933-23 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
43 1 8015B
Motor Oil Range Organics [C24-C36] 63 mg/Kg ☼ Silica Gel Cleanup
110 1 8015B
Arsenic 5.1 3.8 mg/Kg 4 ☼ 6010B Total/NA
Barium 34 1.9 mg/Kg 4 ☼ 6010B Total/NA
Cadmium 0.85 0.48 mg/Kg 4 ☼ 6010B Total/NA
Chromium 32 1.9 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 5.7 0.77 mg/Kg 4 ☼ 6010B Total/NA
Copper 62 5.8 mg/Kg 4 ☼ 6010B Total/NA
Lead 210 1.9 mg/Kg 4 ☼ 6010B Total/NA
Molybdenum 8.0 1.9 mg/Kg 4 ☼ 6010B Total/NA
Nickel 130 1.9 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 11 1.9 mg/Kg 4 ☼ 6010B Total/NA
Zinc 2000 5.8 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.093 0.012 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-5-7.5-8' Lab Sample ID: 720-69933-24 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
46 1 8015B
Motor Oil Range Organics [C24-C36] 63 mg/Kg ☼ Silica Gel Cleanup
98 1 8015B
Arsenic 7.5 4.1 mg/Kg 4 ☼ 6010B Total/NA
Barium 510 2.0 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-5-7.5-8' (Continued) Lab Sample ID: 720-69933-24 Cadmium ☼
RL

0.51 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

2.8 4 6010B Total/NA
Chromium 39 2.0 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 13 0.81 mg/Kg 4 ☼ 6010B Total/NA
Copper 140 6.1 mg/Kg 4 ☼ 6010B Total/NA
Lead 290 2.0 mg/Kg 4 ☼ 6010B Total/NA
Nickel 50 2.0 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 38 2.0 mg/Kg 4 ☼ 6010B Total/NA
Zinc 1100 6.1 mg/Kg 4 ☼ 6010B Total/NA
Mercury 1.1 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-6-3.5-4' Lab Sample ID: 720-69933-27 Diesel Range Organics [C10-C28] ☼
RL

1.1 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
25 1 8015B
Motor Oil Range Organics [C24-C36] 57 mg/Kg ☼ Silica Gel Cleanup
99 1 8015B
Dieldrin 11 2.3 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDT 11 2.3 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDE 18 2.3 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDD 4.4 2.3 ug/Kg 1 ☼ 8081A Total/NA
Arsenic 2.7 0.85 mg/Kg 1 ☼ 6010B Total/NA
Barium 38 1.7 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.095 0.085 mg/Kg 1 ☼ 6010B Total/NA
Chromium 24 1.7 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 3.9 0.68 mg/Kg 4 ☼ 6010B Total/NA
Copper 20 5.1 mg/Kg 4 ☼ 6010B Total/NA
Lead 23 1.7 mg/Kg 4 ☼ 6010B Total/NA
Molybdenum 4.5 1.7 mg/Kg 4 ☼ 6010B Total/NA
Nickel 40 1.7 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 14 1.7 mg/Kg 4 ☼ 6010B Total/NA
Zinc 28 5.1 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.081 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-6-7.5-8' Lab Sample ID: 720-69933-28 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup

9.0 1 8015B
Dieldrin 4.1 2.5 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDT 3.4 p 2.5 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDE 35 2.5 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDD 62 2.5 ug/Kg 1 ☼ 8081A Total/NA
PCB-1260 130 62 ug/Kg 1 ☼ 8082 Total/NA
Antimony 6.7 2.4 mg/Kg 4 ☼ 6010B Total/NA
Arsenic 11 4.8 mg/Kg 4 ☼ 6010B Total/NA
Barium 650 2.4 mg/Kg 4 ☼ 6010B Total/NA
Cadmium 4.9 0.60 mg/Kg 4 ☼ 6010B Total/NA
Chromium 65 2.4 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 15 0.95 mg/Kg 4 ☼ 6010B Total/NA
Copper 99 7.2 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-7.5-8' (Continued) Lab Sample ID: 720-69933-28 Lead ☼
RL

2.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type 710 4 6010B Total/NA
Nickel 79 2.4 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 47 2.4 mg/Kg 4 ☼ 6010B Total/NA
Zinc 460 7.2 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.16 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-7-3.5-4' Lab Sample ID: 720-69933-31 Diesel Range Organics [C10-C28] ☼
RL

1.2 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
21 1 8015B
Motor Oil Range Organics [C24-C36] 61 mg/Kg ☼ Silica Gel Cleanup
72 1 8015B
Arsenic 7.1 4.6 mg/Kg 4 ☼ 6010B Total/NA
Barium 150 2.3 mg/Kg 4 ☼ 6010B Total/NA
Chromium 60 2.3 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 14 0.91 mg/Kg 4 ☼ 6010B Total/NA
Copper 34 6.8 mg/Kg 4 ☼ 6010B Total/NA
Lead 38 2.3 mg/Kg 4 ☼ 6010B Total/NA
Nickel 94 2.3 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 39 2.3 mg/Kg 4 ☼ 6010B Total/NA
Zinc 81 6.8 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.66 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-7-7.5-8' Lab Sample ID: 720-69933-32 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup

1.5 1 8015B
Arsenic 8.3 3.2 mg/Kg 4 ☼ 6010B Total/NA
Barium 250 1.6 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.67 0.32 mg/Kg 4 ☼ 6010B Total/NA
Chromium 69 1.6 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 17 0.63 mg/Kg 4 ☼ 6010B Total/NA
Copper 39 4.7 mg/Kg 4 ☼ 6010B Total/NA
Lead 12 1.6 mg/Kg 4 ☼ 6010B Total/NA
Nickel 94 1.6 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 55 1.6 mg/Kg 4 ☼ 6010B Total/NA
Zinc 79 4.7 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.19 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
21 1 8015B
Motor Oil Range Organics [C24-C36] 65 mg/Kg ☼ Silica Gel Cleanup
90 1 8015B
4,4'-DDT 18 2.6 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDE 60 2.6 ug/Kg 1 ☼ 8081A Total/NA
4,4'-DDD 16 2.6 ug/Kg 1 ☼ 8081A Total/NA
Arsenic 44 4.1 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-3.5-4' (Continued) Lab Sample ID: 720-69933-35 Barium ☼
RL

2.1 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type 250 4 6010B Total/NA
Beryllium 0.61 0.41 mg/Kg 4 ☼ 6010B Total/NA
Chromium 89 2.1 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 21 0.83 mg/Kg 4 ☼ 6010B Total/NA
Copper 53 6.2 mg/Kg 4 ☼ 6010B Total/NA
Lead 130 2.1 mg/Kg 4 ☼ 6010B Total/NA
Nickel 150 2.1 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 55 2.1 mg/Kg 4 ☼ 6010B Total/NA
Zinc 130 6.2 mg/Kg 4 ☼ 6010B Total/NA
Mercury 5.4 0.11 mg/Kg 10 ☼ 7471A Total/NA
Client Sample ID: GP-8-7.5-8' Lab Sample ID: 720-69933-36 Arsenic ☼
RL

4.6 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type

7.1 4 6010B Total/NA
Barium 160 2.3 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.81 0.46 mg/Kg 4 ☼ 6010B Total/NA
Chromium 68 2.3 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 14 0.91 mg/Kg 4 ☼ 6010B Total/NA
Copper 37 6.8 mg/Kg 4 ☼ 6010B Total/NA
Lead 11 2.3 mg/Kg 4 ☼ 6010B Total/NA
Nickel 82 2.3 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 54 2.3 mg/Kg 4 ☼ 6010B Total/NA
Zinc 77 6.8 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.12 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-9-4.5-5' Lab Sample ID: 720-69933-39 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
12 1 8015B
Arsenic 17 5.0 mg/Kg 4 ☼ 6010B Total/NA
Barium 250 2.5 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.65 0.50 mg/Kg 4 ☼ 6010B Total/NA
Chromium 84 2.5 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 22 1.0 mg/Kg 4 ☼ 6010B Total/NA
Copper 45 7.5 mg/Kg 4 ☼ 6010B Total/NA
Lead 37 2.5 mg/Kg 4 ☼ 6010B Total/NA
Nickel 140 2.5 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 58 2.5 mg/Kg 4 ☼ 6010B Total/NA
Zinc 94 7.5 mg/Kg 4 ☼ 6010B Total/NA
Mercury 3.8 0.11 mg/Kg 10 ☼ 7471A Total/NA
Client Sample ID: GP-9-7.5-8' Lab Sample ID: 720-69933-40 Diesel Range Organics [C10-C28] ☼
RL

1.3 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
56 1 8015B
Motor Oil Range Organics [C24-C36] 64 mg/Kg ☼ Silica Gel Cleanup
240 1 8015B
Arsenic 7.5 4.9 mg/Kg 4 ☼ 6010B Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-9-7.5-8' (Continued) Lab Sample ID: 720-69933-40 Barium ☼
RL

2.5 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type 210 4 6010B Total/NA
Beryllium 0.78 0.49 mg/Kg 4 ☼ 6010B Total/NA
Chromium 64 2.5 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 16 0.98 mg/Kg 4 ☼ 6010B Total/NA
Copper 43 7.4 mg/Kg 4 ☼ 6010B Total/NA
Lead 11 2.5 mg/Kg 4 ☼ 6010B Total/NA
Nickel 88 2.5 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 51 2.5 mg/Kg 4 ☼ 6010B Total/NA
Zinc 73 7.4 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.087 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Diesel Range Organics [C10-C28] ☼
RL
23 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
400 20 8015B
Motor Oil Range Organics [C24-C36] 1100 mg/Kg ☼ Silica Gel Cleanup
2100 20 8015B
Arsenic 1.0 1.0 mg/Kg 1 ☼ 6010B Total/NA
Barium 33 2.0 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.20 0.10 mg/Kg 1 ☼ 6010B Total/NA
Chromium 7.1 2.0 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 1.6 0.80 mg/Kg 4 ☼ 6010B Total/NA
Copper 2.4 1.5 mg/Kg 1 ☼ 6010B Total/NA
Lead 3.5 2.0 mg/Kg 4 ☼ 6010B Total/NA
Molybdenum 0.89 0.50 mg/Kg 1 ☼ 6010B Total/NA
Nickel 4.8 2.0 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 9.4 2.0 mg/Kg 4 ☼ 6010B Total/NA
Zinc 10 6.0 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.024 0.010 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-10-7.5-8' Lab Sample ID: 720-69933-44 Diesel Range Organics [C10-C28] ☼
RL

1.4 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup

2.4 1 8015B
Arsenic 5.6 3.6 mg/Kg 4 ☼ 6010B Total/NA
Barium 250 1.8 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.74 0.36 mg/Kg 4 ☼ 6010B Total/NA
Chromium 72 1.8 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 15 0.73 mg/Kg 4 ☼ 6010B Total/NA
Copper 38 5.5 mg/Kg 4 ☼ 6010B Total/NA
Lead 11 1.8 mg/Kg 4 ☼ 6010B Total/NA
Nickel 90 1.8 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 57 1.8 mg/Kg 4 ☼ 6010B Total/NA
Zinc 73 5.5 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.11 F1 0.012 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-11-3.5-4' Lab Sample ID: 720-69933-47 TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Detection Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-11-3.5-4' (Continued) Lab Sample ID: 720-69933-47 Diesel Range Organics [C10-C28] ☼
RL

3.7 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
90 3 8015B
Motor Oil Range Organics [C24-C36] 190 mg/Kg ☼ Silica Gel Cleanup
300 3 8015B
Arsenic 7.8 4.7 mg/Kg 4 ☼ 6010B Total/NA
Barium 140 F1 F2 2.4 mg/Kg 4 ☼ 6010B Total/NA
Chromium 480 2.4 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 64 0.94 mg/Kg 4 ☼ 6010B Total/NA
Copper 35 7.1 mg/Kg 4 ☼ 6010B Total/NA
Lead 44 F1 2.4 mg/Kg 4 ☼ 6010B Total/NA
Nickel 1100 2.4 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 39 2.4 mg/Kg 4 ☼ 6010B Total/NA
Zinc 68 F1 7.1 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.10 0.011 mg/Kg 1 ☼ 7471A Total/NA
Client Sample ID: GP-11-7.5-8' Lab Sample ID: 720-69933-48 Diesel Range Organics [C10-C28] ☼
RL

1.2 mg/Kg
Analyte Result Qualifier MDL Unit Dil Fac D Method Prep Type Silica Gel
Cleanup
17 1 8015B
Arsenic 9.4 4.3 mg/Kg 4 ☼ 6010B Total/NA
Barium 210 2.2 mg/Kg 4 ☼ 6010B Total/NA
Beryllium 0.60 0.43 mg/Kg 4 ☼ 6010B Total/NA
Chromium 74 2.2 mg/Kg 4 ☼ 6010B Total/NA
Cobalt 17 0.86 mg/Kg 4 ☼ 6010B Total/NA
Copper 41 6.5 mg/Kg 4 ☼ 6010B Total/NA
Lead 11 2.2 mg/Kg 4 ☼ 6010B Total/NA
Nickel 100 2.2 mg/Kg 4 ☼ 6010B Total/NA
Vanadium 55 2.2 mg/Kg 4 ☼ 6010B Total/NA
Zinc 82 6.5 mg/Kg 4 ☼ 6010B Total/NA
Mercury 0.12 0.011 mg/Kg 1 ☼ 7471A Total/NA
TestAmerica Pleasanton
This Detection Summary does not include radiochemical test results.

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1 Lab Sample ID: 720-69933-1
Date Collected: 01/21/16 15:00 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 15:19 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 15:19 1
Benzene ND 0.50 ug/L 01/26/16 15:19 1
Dichlorobromomethane ND 0.50 ug/L 01/26/16 15:19 1
Bromobenzene ND 1.0 ug/L 01/26/16 15:19 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 15:19 1
Bromoform ND 1.0 ug/L 01/26/16 15:19 1
Bromomethane ND 1.0 ug/L 01/26/16 15:19 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 15:19 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 15:19 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 15:19 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 15:19 1
Carbon disulfide ND 5.0 ug/L 01/26/16 15:19 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 15:19 1
Chlorobenzene ND 0.50 ug/L 01/26/16 15:19 1
Chloroethane ND 1.0 ug/L 01/26/16 15:19 1
Chloroform ND 1.0 ug/L 01/26/16 15:19 1
Chloromethane ND 1.0 ug/L 01/26/16 15:19 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 15:19 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 15:19 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 15:19 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 15:19 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 15:19 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 15:19 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 15:19 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 15:19 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 15:19 1 Ethylene Dibromide ND 0.50 ug/L 01/26/16 15:19 1
Dibromomethane ND 0.50 ug/L 01/26/16 15:19 1
Dichlorodifluoromethane ND 0.50 ug/L 01/26/16 15:19 1
1,1-Dichloroethane ND 0.50 ug/L 01/26/16 15:19 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 15:19 1
1,1-Dichloroethene ND 0.50 ug/L 01/26/16 15:19 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 15:19 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 15:19 1
1,2-Dichloropropane ND 0.50 ug/L 01/26/16 15:19 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 15:19 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 15:19 1 Ethylbenzene ND 0.50 ug/L 01/26/16 15:19 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 15:19 1
2-Hexanone ND 50 ug/L 01/26/16 15:19 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 15:19 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 15:19 1
Methylene Chloride ND 5.0 ug/L 01/26/16 15:19 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 15:19 1 Naphthalene ND 1.0 ug/L 01/26/16 15:19 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 15:19 1
Styrene ND 0.50 ug/L 01/26/16 15:19 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 15:19 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1 Lab Sample ID: 720-69933-1
Date Collected: 01/21/16 15:00 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 15:19 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 0.50 ug/L 01/26/16 15:19 1
Toluene ND 0.50 ug/L 01/26/16 15:19 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 01/26/16 15:19 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 01/26/16 15:19 1
1,1,1-Trichloroethane ND 0.50 ug/L 01/26/16 15:19 1
1,1,2-Trichloroethane ND 0.50 ug/L 01/26/16 15:19 1
Trichloroethene ND 0.50 ug/L 01/26/16 15:19 1
Trichlorofluoromethane ND 1.0 ug/L 01/26/16 15:19 1
1,2,3-Trichloropropane ND 0.50 ug/L 01/26/16 15:19 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 01/26/16 15:19 1 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/26/16 15:19 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 01/26/16 15:19 1
Vinyl acetate ND 10 ug/L 01/26/16 15:19 1
Vinyl chloride ND 0.50 ug/L 01/26/16 15:19 1
Xylenes, Total ND 1.0 ug/L 01/26/16 15:19 1
2,2-Dichloropropane ND 0.50 ug/L 01/26/16 15:19 1
Gasoline Range Organics (GRO) 50 ug/L 01/26/16 15:19 1
-C5-C12
ND
4-Bromofluorobenzene 111 67 - 130 01/26/16 15:19 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 105 72 - 130 01/26/16 15:19 1 Toluene-d8 (Surr) 104 70 - 130 01/26/16 15:19 1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] ND 50 ug/L 01/27/16 16:40 01/28/16 14:53 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 100 ug/L 01/27/16 16:40 01/28/16 14:53 1 Capric Acid (Surr) 0.01 0 - 5 01/27/16 16:40 01/28/16 14:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 105 31 - 150 01/27/16 16:40 01/28/16 14:53 1 Method: 6010B - Metals (ICP) - Dissolved
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1
Barium ND 0.050 mg/L 01/27/16 14:17 01/28/16 17:44 1
Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:44 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:44 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1
Cobalt 0.0038 0.0020 mg/L 01/27/16 14:17 01/28/16 17:44 1 Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:44 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:44 1
Molybdenum 0.049 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1 Nickel 0.010 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1 Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:44 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:44 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1
Vanadium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:44 1
TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2 Lab Sample ID: 720-69933-2
Date Collected: 01/21/16 12:00 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 15:47 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 15:47 1
Benzene ND 0.50 ug/L 01/26/16 15:47 1
Dichlorobromomethane ND 0.50 ug/L 01/26/16 15:47 1
Bromobenzene ND 1.0 ug/L 01/26/16 15:47 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 15:47 1
Bromoform ND 1.0 ug/L 01/26/16 15:47 1
Bromomethane ND 1.0 ug/L 01/26/16 15:47 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 15:47 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 15:47 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 15:47 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 15:47 1
Carbon disulfide ND 5.0 ug/L 01/26/16 15:47 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 15:47 1
Chlorobenzene ND 0.50 ug/L 01/26/16 15:47 1
Chloroethane ND 1.0 ug/L 01/26/16 15:47 1
Chloroform ND 1.0 ug/L 01/26/16 15:47 1
Chloromethane ND 1.0 ug/L 01/26/16 15:47 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 15:47 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 15:47 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 15:47 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 15:47 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 15:47 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 15:47 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 15:47 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 15:47 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 15:47 1 Ethylene Dibromide ND 0.50 ug/L 01/26/16 15:47 1
Dibromomethane ND 0.50 ug/L 01/26/16 15:47 1
Dichlorodifluoromethane ND 0.50 ug/L 01/26/16 15:47 1
1,1-Dichloroethane 2.5 0.50 ug/L 01/26/16 15:47 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 15:47 1
1,1-Dichloroethene 18 0.50 ug/L 01/26/16 15:47 1
cis-1,2-Dichloroethene 0.62 0.50 ug/L 01/26/16 15:47 1
trans-1,2-Dichloroethene 1.1 0.50 ug/L 01/26/16 15:47 1 1,2-Dichloropropane ND 0.50 ug/L 01/26/16 15:47 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 15:47 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 15:47 1 Ethylbenzene ND 0.50 ug/L 01/26/16 15:47 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 15:47 1
2-Hexanone ND 50 ug/L 01/26/16 15:47 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 15:47 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 15:47 1
Methylene Chloride ND 5.0 ug/L 01/26/16 15:47 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 15:47 1 Naphthalene ND 1.0 ug/L 01/26/16 15:47 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 15:47 1
Styrene ND 0.50 ug/L 01/26/16 15:47 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 15:47 1 TestAmerica Pleasanton

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1.6 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/26/16 15:47 1 1,3,5-Trimethylbenzene ND 0.50 ug/L 01/26/16 15:47 1
Vinyl acetate ND 10 ug/L 01/26/16 15:47 1
Vinyl chloride 0.99 0.50 ug/L 01/26/16 15:47 1
Xylenes, Total ND 1.0 ug/L 01/26/16 15:47 1
2,2-Dichloropropane ND 0.50 ug/L 01/26/16 15:47 1
Gasoline Range Organics (GRO) 50 ug/L 01/26/16 15:47 1
-C5-C12
ND
4-Bromofluorobenzene 101 67 - 130 01/26/16 15:47 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 95 72 - 130 01/26/16 15:47 1 Toluene-d8 (Surr) 102 70 - 130 01/26/16 15:47 1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 1900 270 ug/L 01/27/16 16:40 01/28/16 16:55 5 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 540 ug/L 01/27/16 16:40 01/28/16 16:55 5 [C24-C36]
10000
Capric Acid (Surr) 0 0 - 5 01/27/16 16:40 01/28/16 16:55 5 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 0 X D 31 - 150 01/27/16 16:40 01/28/16 16:55 5 Method: 6010B - Metals (ICP) - Dissolved
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:49 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:49 1
Barium 0.081 0.050 mg/L 01/27/16 14:17 01/28/16 17:49 1 Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:49 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:49 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:49 1
Cobalt 0.0081 0.0020 mg/L 01/27/16 14:17 01/28/16 17:49 1 Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:49 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:49 1
Molybdenum 0.035 0.010 mg/L 01/27/16 14:17 01/28/16 17:49 1 Nickel 0.025 0.010 mg/L 01/27/16 14:17 01/28/16 17:49 1 Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:49 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:49 1
TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3 Lab Sample ID: 720-69933-3
Date Collected: 01/21/16 14:10 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 16:14 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 16:14 1
Benzene 6.5 0.50 ug/L 01/26/16 16:14 1
Dichlorobromomethane ND 0.50 ug/L 01/26/16 16:14 1
Bromobenzene ND 1.0 ug/L 01/26/16 16:14 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 16:14 1
Bromoform ND 1.0 ug/L 01/26/16 16:14 1
Bromomethane ND 1.0 ug/L 01/26/16 16:14 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 16:14 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 16:14 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 16:14 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 16:14 1
Carbon disulfide ND 5.0 ug/L 01/26/16 16:14 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 16:14 1
Chlorobenzene ND 0.50 ug/L 01/26/16 16:14 1
Chloroethane ND 1.0 ug/L 01/26/16 16:14 1
Chloroform ND 1.0 ug/L 01/26/16 16:14 1
Chloromethane ND 1.0 ug/L 01/26/16 16:14 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 16:14 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 16:14 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 16:14 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 16:14 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 16:14 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 16:14 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 16:14 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 16:14 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 16:14 1 Ethylene Dibromide ND 0.50 ug/L 01/26/16 16:14 1
Dibromomethane ND 0.50 ug/L 01/26/16 16:14 1
Dichlorodifluoromethane ND 0.50 ug/L 01/26/16 16:14 1
1,1-Dichloroethane ND 0.50 ug/L 01/26/16 16:14 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 16:14 1
1,1-Dichloroethene ND 0.50 ug/L 01/26/16 16:14 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 16:14 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 16:14 1
1,2-Dichloropropane ND 0.50 ug/L 01/26/16 16:14 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 16:14 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 16:14 1 Ethylbenzene ND 0.50 ug/L 01/26/16 16:14 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 16:14 1
2-Hexanone ND 50 ug/L 01/26/16 16:14 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 16:14 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 16:14 1
Methylene Chloride ND 5.0 ug/L 01/26/16 16:14 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 16:14 1 Naphthalene ND 1.0 ug/L 01/26/16 16:14 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 16:14 1
Styrene ND 0.50 ug/L 01/26/16 16:14 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 16:14 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3 Lab Sample ID: 720-69933-3
Date Collected: 01/21/16 14:10 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 16:14 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 0.50 ug/L 01/26/16 16:14 1
Toluene ND 0.50 ug/L 01/26/16 16:14 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 01/26/16 16:14 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 01/26/16 16:14 1
1,1,1-Trichloroethane ND 0.50 ug/L 01/26/16 16:14 1
1,1,2-Trichloroethane ND 0.50 ug/L 01/26/16 16:14 1
Trichloroethene ND 0.50 ug/L 01/26/16 16:14 1
Trichlorofluoromethane ND 1.0 ug/L 01/26/16 16:14 1
1,2,3-Trichloropropane ND 0.50 ug/L 01/26/16 16:14 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 01/26/16 16:14 1 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/26/16 16:14 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 01/26/16 16:14 1
Vinyl acetate ND 10 ug/L 01/26/16 16:14 1
Vinyl chloride ND 0.50 ug/L 01/26/16 16:14 1
Xylenes, Total ND 1.0 ug/L 01/26/16 16:14 1
2,2-Dichloropropane ND 0.50 ug/L 01/26/16 16:14 1
Gasoline Range Organics (GRO) 50 ug/L 01/26/16 16:14 1
-C5-C12
ND
4-Bromofluorobenzene 103 67 - 130 01/26/16 16:14 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 102 72 - 130 01/26/16 16:14 1 Toluene-d8 (Surr) 104 70 - 130 01/26/16 16:14 1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] ND 52 ug/L 01/27/16 16:40 01/28/16 15:42 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 01/27/16 16:40 01/28/16 15:42 1 [C24-C36]
170
Capric Acid (Surr) 0.006 0 - 5 01/27/16 16:40 01/28/16 15:42 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 104 31 - 150 01/27/16 16:40 01/28/16 15:42 1 Method: 6010B - Metals (ICP) - Dissolved
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:54 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:54 1
Barium 0.052 0.050 mg/L 01/27/16 14:17 01/28/16 17:54 1 Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:54 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:54 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:54 1
Cobalt 0.010 0.0020 mg/L 01/27/16 14:17 01/28/16 17:54 1 Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:54 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:54 1
Molybdenum 0.020 0.010 mg/L 01/27/16 14:17 01/28/16 17:54 1 Nickel 0.024 0.010 mg/L 01/27/16 14:17 01/28/16 17:54 1 Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:54 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:54 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:54 1
TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6 Lab Sample ID: 720-69933-4
Date Collected: 01/21/16 16:55 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 16:42 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 16:42 1
Benzene 0.73 0.50 ug/L 01/26/16 16:42 1
Dichlorobromomethane ND 0.50 ug/L 01/26/16 16:42 1
Bromobenzene ND 1.0 ug/L 01/26/16 16:42 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 16:42 1
Bromoform ND 1.0 ug/L 01/26/16 16:42 1
Bromomethane ND 1.0 ug/L 01/26/16 16:42 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 16:42 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 16:42 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 16:42 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 16:42 1
Carbon disulfide ND 5.0 ug/L 01/26/16 16:42 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 16:42 1
Chlorobenzene ND 0.50 ug/L 01/26/16 16:42 1
Chloroethane ND 1.0 ug/L 01/26/16 16:42 1
Chloroform ND 1.0 ug/L 01/26/16 16:42 1
Chloromethane ND 1.0 ug/L 01/26/16 16:42 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 16:42 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 16:42 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 16:42 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 16:42 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 16:42 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 16:42 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 16:42 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 16:42 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 16:42 1 Ethylene Dibromide ND 0.50 ug/L 01/26/16 16:42 1
Dibromomethane ND 0.50 ug/L 01/26/16 16:42 1
Dichlorodifluoromethane ND 0.50 ug/L 01/26/16 16:42 1
1,1-Dichloroethane ND 0.50 ug/L 01/26/16 16:42 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 16:42 1
1,1-Dichloroethene ND 0.50 ug/L 01/26/16 16:42 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 16:42 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 16:42 1
1,2-Dichloropropane ND 0.50 ug/L 01/26/16 16:42 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 16:42 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 16:42 1 Ethylbenzene ND 0.50 ug/L 01/26/16 16:42 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 16:42 1
2-Hexanone ND 50 ug/L 01/26/16 16:42 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 16:42 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 16:42 1
Methylene Chloride ND 5.0 ug/L 01/26/16 16:42 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 16:42 1 Naphthalene ND 1.0 ug/L 01/26/16 16:42 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 16:42 1
Styrene ND 0.50 ug/L 01/26/16 16:42 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 16:42 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6 Lab Sample ID: 720-69933-4
Date Collected: 01/21/16 16:55 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 16:42 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 0.50 ug/L 01/26/16 16:42 1
Toluene ND 0.50 ug/L 01/26/16 16:42 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 01/26/16 16:42 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 01/26/16 16:42 1
1,1,1-Trichloroethane ND 0.50 ug/L 01/26/16 16:42 1
1,1,2-Trichloroethane ND 0.50 ug/L 01/26/16 16:42 1
Trichloroethene ND 0.50 ug/L 01/26/16 16:42 1
Trichlorofluoromethane ND 1.0 ug/L 01/26/16 16:42 1
1,2,3-Trichloropropane ND 0.50 ug/L 01/26/16 16:42 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 01/26/16 16:42 1 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/26/16 16:42 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 01/26/16 16:42 1
Vinyl acetate ND 10 ug/L 01/26/16 16:42 1
Vinyl chloride ND 0.50 ug/L 01/26/16 16:42 1
Xylenes, Total ND 1.0 ug/L 01/26/16 16:42 1
2,2-Dichloropropane ND 0.50 ug/L 01/26/16 16:42 1
Gasoline Range Organics (GRO) 50 ug/L 01/26/16 16:42 1
-C5-C12
ND
4-Bromofluorobenzene 101 67 - 130 01/26/16 16:42 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 102 72 - 130 01/26/16 16:42 1 Toluene-d8 (Surr) 104 70 - 130 01/26/16 16:42 1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 84 50 ug/L 01/27/16 16:40 01/28/16 16:06 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 01/27/16 16:40 01/28/16 16:06 1 [C24-C36]
120
Capric Acid (Surr) 0.006 0 - 5 01/27/16 16:40 01/28/16 16:06 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 115 31 - 150 01/27/16 16:40 01/28/16 16:06 1 Method: 6010B - Metals (ICP) - Dissolved
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:10 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 0.023 0.010 mg/L 01/27/16 14:17 01/28/16 18:10 1 Barium 1.3 0.050 mg/L 01/27/16 14:17 01/28/16 18:10 1
Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 18:10 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 18:10 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:10 1
Cobalt 0.0033 0.0020 mg/L 01/27/16 14:17 01/28/16 18:10 1 Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 18:10 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 18:10 1
Molybdenum 0.019 0.010 mg/L 01/27/16 14:17 01/28/16 18:10 1 Nickel 0.013 0.010 mg/L 01/27/16 14:17 01/28/16 18:10 1 Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 18:10 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 18:10 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:10 1
TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7 Lab Sample ID: 720-69933-5
Date Collected: 01/22/16 09:10 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
RL MDL
Methyl tert-butyl ether 1.6 0.50 ug/L 01/27/16 04:14 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/27/16 04:14 1
Benzene ND 0.50 ug/L 01/27/16 04:14 1
Dichlorobromomethane ND 0.50 ug/L 01/27/16 04:14 1
Bromobenzene ND 1.0 ug/L 01/27/16 04:14 1
Chlorobromomethane ND 1.0 ug/L 01/27/16 04:14 1
Bromoform ND 1.0 ug/L 01/27/16 04:14 1
Bromomethane ND 1.0 ug/L 01/27/16 04:14 1
2-Butanone (MEK) ND 50 ug/L 01/27/16 04:14 1
n-Butylbenzene ND 1.0 ug/L 01/27/16 04:14 1
sec-Butylbenzene ND 1.0 ug/L 01/27/16 04:14 1
tert-Butylbenzene ND 1.0 ug/L 01/27/16 04:14 1
Carbon disulfide ND 5.0 ug/L 01/27/16 04:14 1
Carbon tetrachloride ND 0.50 ug/L 01/27/16 04:14 1
Chlorobenzene ND 0.50 ug/L 01/27/16 04:14 1
Chloroethane ND 1.0 ug/L 01/27/16 04:14 1
Chloroform ND 1.0 ug/L 01/27/16 04:14 1
Chloromethane ND 1.0 ug/L 01/27/16 04:14 1
2-Chlorotoluene ND 0.50 ug/L 01/27/16 04:14 1
4-Chlorotoluene ND 0.50 ug/L 01/27/16 04:14 1
Chlorodibromomethane ND 0.50 ug/L 01/27/16 04:14 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/27/16 04:14 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/27/16 04:14 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/27/16 04:14 1
1,3-Dichloropropane ND 1.0 ug/L 01/27/16 04:14 1
1,1-Dichloropropene ND 0.50 ug/L 01/27/16 04:14 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/27/16 04:14 1 Ethylene Dibromide ND 0.50 ug/L 01/27/16 04:14 1
Dibromomethane ND 0.50 ug/L 01/27/16 04:14 1
Dichlorodifluoromethane ND * 0.50 ug/L 01/27/16 04:14 1 1,1-Dichloroethane ND 0.50 ug/L 01/27/16 04:14 1
1,2-Dichloroethane ND 0.50 ug/L 01/27/16 04:14 1
1,1-Dichloroethene ND 0.50 ug/L 01/27/16 04:14 1
cis-1,2-Dichloroethene 0.94 0.50 ug/L 01/27/16 04:14 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/27/16 04:14 1
1,2-Dichloropropane ND 0.50 ug/L 01/27/16 04:14 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/27/16 04:14 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/27/16 04:14 1 Ethylbenzene ND 0.50 ug/L 01/27/16 04:14 1
Hexachlorobutadiene ND 1.0 ug/L 01/27/16 04:14 1
2-Hexanone ND 50 ug/L 01/27/16 04:14 1
Isopropylbenzene ND 0.50 ug/L 01/27/16 04:14 1
4-Isopropyltoluene ND 1.0 ug/L 01/27/16 04:14 1
Methylene Chloride ND 5.0 ug/L 01/27/16 04:14 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/27/16 04:14 1 Naphthalene ND 1.0 ug/L 01/27/16 04:14 1
N-Propylbenzene ND 1.0 ug/L 01/27/16 04:14 1
Styrene ND 0.50 ug/L 01/27/16 04:14 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/27/16 04:14 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7 Lab Sample ID: 720-69933-5
Date Collected: 01/22/16 09:10 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/27/16 04:14 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 0.50 ug/L 01/27/16 04:14 1
Toluene ND 0.50 ug/L 01/27/16 04:14 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 01/27/16 04:14 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 01/27/16 04:14 1
1,1,1-Trichloroethane ND 0.50 ug/L 01/27/16 04:14 1
1,1,2-Trichloroethane ND 0.50 ug/L 01/27/16 04:14 1
Trichloroethene 2.0 0.50 ug/L 01/27/16 04:14 1
Trichlorofluoromethane ND * 1.0 ug/L 01/27/16 04:14 1
1,2,3-Trichloropropane ND 0.50 ug/L 01/27/16 04:14 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 01/27/16 04:14 1 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/27/16 04:14 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 01/27/16 04:14 1
Vinyl acetate ND 10 ug/L 01/27/16 04:14 1
Vinyl chloride ND 0.50 ug/L 01/27/16 04:14 1
Xylenes, Total ND 1.0 ug/L 01/27/16 04:14 1
2,2-Dichloropropane ND 0.50 ug/L 01/27/16 04:14 1
Gasoline Range Organics (GRO) 50 ug/L 01/27/16 04:14 1
-C5-C12
ND
4-Bromofluorobenzene 98 67 - 130 01/27/16 04:14 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 119 72 - 130 01/27/16 04:14 1 Toluene-d8 (Surr) 97 70 - 130 01/27/16 04:14 1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 65 52 ug/L 01/27/16 16:40 01/28/16 16:30 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 01/27/16 16:40 01/28/16 16:30 1 [C24-C36]
350
Capric Acid (Surr) 0.006 0 - 5 01/27/16 16:40 01/28/16 16:30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 117 31 - 150 01/27/16 16:40 01/28/16 16:30 1 Method: 6010B - Metals (ICP) - Dissolved
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:15 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:15 1
Barium 0.069 0.050 mg/L 01/27/16 14:17 01/28/16 18:15 1 Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 18:15 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 18:15 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:15 1
Cobalt 0.0020 0.0020 mg/L 01/27/16 14:17 01/28/16 18:15 1 Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 18:15 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 18:15 1
Molybdenum 0.072 0.010 mg/L 01/27/16 14:17 01/28/16 18:15 1 Nickel ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:15 1
Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 18:15 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 18:15 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:15 1
TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10 Lab Sample ID: 720-69933-6
Date Collected: 01/22/16 11:50 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/27/16 04:42 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/27/16 04:42 1
Benzene ND 0.50 ug/L 01/27/16 04:42 1
Dichlorobromomethane ND 0.50 ug/L 01/27/16 04:42 1
Bromobenzene ND 1.0 ug/L 01/27/16 04:42 1
Chlorobromomethane ND 1.0 ug/L 01/27/16 04:42 1
Bromoform ND 1.0 ug/L 01/27/16 04:42 1
Bromomethane ND 1.0 ug/L 01/27/16 04:42 1
2-Butanone (MEK) ND 50 ug/L 01/27/16 04:42 1
n-Butylbenzene ND 1.0 ug/L 01/27/16 04:42 1
sec-Butylbenzene ND 1.0 ug/L 01/27/16 04:42 1
tert-Butylbenzene ND 1.0 ug/L 01/27/16 04:42 1
Carbon disulfide ND 5.0 ug/L 01/27/16 04:42 1
Carbon tetrachloride ND 0.50 ug/L 01/27/16 04:42 1
Chlorobenzene ND 0.50 ug/L 01/27/16 04:42 1
Chloroethane ND 1.0 ug/L 01/27/16 04:42 1
Chloroform ND 1.0 ug/L 01/27/16 04:42 1
Chloromethane ND 1.0 ug/L 01/27/16 04:42 1
2-Chlorotoluene ND 0.50 ug/L 01/27/16 04:42 1
4-Chlorotoluene ND 0.50 ug/L 01/27/16 04:42 1
Chlorodibromomethane ND 0.50 ug/L 01/27/16 04:42 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/27/16 04:42 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/27/16 04:42 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/27/16 04:42 1
1,3-Dichloropropane ND 1.0 ug/L 01/27/16 04:42 1
1,1-Dichloropropene ND 0.50 ug/L 01/27/16 04:42 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/27/16 04:42 1 Ethylene Dibromide ND 0.50 ug/L 01/27/16 04:42 1
Dibromomethane ND 0.50 ug/L 01/27/16 04:42 1
Dichlorodifluoromethane ND * 0.50 ug/L 01/27/16 04:42 1 1,1-Dichloroethane ND 0.50 ug/L 01/27/16 04:42 1
1,2-Dichloroethane ND 0.50 ug/L 01/27/16 04:42 1
1,1-Dichloroethene ND 0.50 ug/L 01/27/16 04:42 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/27/16 04:42 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/27/16 04:42 1
1,2-Dichloropropane ND 0.50 ug/L 01/27/16 04:42 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/27/16 04:42 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/27/16 04:42 1 Ethylbenzene ND 0.50 ug/L 01/27/16 04:42 1
Hexachlorobutadiene ND 1.0 ug/L 01/27/16 04:42 1
2-Hexanone ND 50 ug/L 01/27/16 04:42 1
Isopropylbenzene ND 0.50 ug/L 01/27/16 04:42 1
4-Isopropyltoluene ND 1.0 ug/L 01/27/16 04:42 1
Methylene Chloride ND 5.0 ug/L 01/27/16 04:42 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/27/16 04:42 1 Naphthalene ND 1.0 ug/L 01/27/16 04:42 1
N-Propylbenzene ND 1.0 ug/L 01/27/16 04:42 1
Styrene ND 0.50 ug/L 01/27/16 04:42 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/27/16 04:42 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10 Lab Sample ID: 720-69933-6
Date Collected: 01/22/16 11:50 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/27/16 04:42 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 0.50 ug/L 01/27/16 04:42 1
Toluene ND 0.50 ug/L 01/27/16 04:42 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 01/27/16 04:42 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 01/27/16 04:42 1
1,1,1-Trichloroethane ND 0.50 ug/L 01/27/16 04:42 1
1,1,2-Trichloroethane ND 0.50 ug/L 01/27/16 04:42 1
Trichloroethene ND 0.50 ug/L 01/27/16 04:42 1
Trichlorofluoromethane ND * 1.0 ug/L 01/27/16 04:42 1
1,2,3-Trichloropropane ND 0.50 ug/L 01/27/16 04:42 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 01/27/16 04:42 1 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/27/16 04:42 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 01/27/16 04:42 1
Vinyl acetate ND 10 ug/L 01/27/16 04:42 1
Vinyl chloride ND 0.50 ug/L 01/27/16 04:42 1
Xylenes, Total ND 1.0 ug/L 01/27/16 04:42 1
2,2-Dichloropropane ND 0.50 ug/L 01/27/16 04:42 1
Gasoline Range Organics (GRO) 50 ug/L 01/27/16 04:42 1
-C5-C12
ND
4-Bromofluorobenzene 98 67 - 130 01/27/16 04:42 1
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 127 72 - 130 01/27/16 04:42 1 Toluene-d8 (Surr) 99 70 - 130 01/27/16 04:42 1
Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 150 51 ug/L 01/27/16 16:40 01/28/16 15:18 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 100 ug/L 01/27/16 16:40 01/28/16 15:18 1 [C24-C36]
390
Capric Acid (Surr) 0.008 0 - 5 01/27/16 16:40 01/28/16 15:18 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 102 31 - 150 01/27/16 16:40 01/28/16 15:18 1 Method: 6010B - Metals (ICP) - Dissolved
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:20 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:20 1
Barium 0.097 0.050 mg/L 01/27/16 14:17 01/28/16 18:20 1 Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 18:20 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 18:20 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:20 1
Cobalt 0.0093 0.0020 mg/L 01/27/16 14:17 01/28/16 18:20 1 Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 18:20 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 18:20 1
Molybdenum 0.018 0.010 mg/L 01/27/16 14:17 01/28/16 18:20 1 Nickel 0.013 0.010 mg/L 01/27/16 14:17 01/28/16 18:20 1 Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 18:20 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 18:20 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 18:20 1
TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: TRIP BLANK Lab Sample ID: 720-69933-7 Date Collected: 01/22/16 12:30 Matrix: Water
Date Received: 01/22/16 17:10
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 01:36 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 01:36 1
Benzene ND 0.50 ug/L 01/26/16 01:36 1
Dichlorobromomethane ND 0.50 ug/L 01/26/16 01:36 1
Bromobenzene ND 1.0 ug/L 01/26/16 01:36 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 01:36 1
Bromoform ND 1.0 ug/L 01/26/16 01:36 1
Bromomethane ND 1.0 ug/L 01/26/16 01:36 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 01:36 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 01:36 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 01:36 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 01:36 1
Carbon disulfide ND 5.0 ug/L 01/26/16 01:36 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 01:36 1
Chlorobenzene ND 0.50 ug/L 01/26/16 01:36 1
Chloroethane ND 1.0 ug/L 01/26/16 01:36 1
Chloroform ND 1.0 ug/L 01/26/16 01:36 1
Chloromethane ND 1.0 ug/L 01/26/16 01:36 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 01:36 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 01:36 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 01:36 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 01:36 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 01:36 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 01:36 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 01:36 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 01:36 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 01:36 1 Ethylene Dibromide ND 0.50 ug/L 01/26/16 01:36 1
Dibromomethane ND 0.50 ug/L 01/26/16 01:36 1
Dichlorodifluoromethane ND * 0.50 ug/L 01/26/16 01:36 1 1,1-Dichloroethane ND 0.50 ug/L 01/26/16 01:36 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 01:36 1
1,1-Dichloroethene ND 0.50 ug/L 01/26/16 01:36 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 01:36 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 01:36 1
1,2-Dichloropropane ND 0.50 ug/L 01/26/16 01:36 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 01:36 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 01:36 1 Ethylbenzene ND 0.50 ug/L 01/26/16 01:36 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 01:36 1
2-Hexanone ND 50 ug/L 01/26/16 01:36 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 01:36 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 01:36 1
Methylene Chloride ND 5.0 ug/L 01/26/16 01:36 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 01:36 1 Naphthalene ND 1.0 ug/L 01/26/16 01:36 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 01:36 1
Styrene ND 0.50 ug/L 01/26/16 01:36 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 01:36 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-3.5-4' Lab Sample ID: 720-69933-8 Date Collected: 01/21/16 10:25 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.9
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 57 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1
Benzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1
Dichlorobromomethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Bromobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Chlorobromomethane ND 23 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Bromoform ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Bromomethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 2-Butanone (MEK) ND 57 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 n-Butylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 sec-Butylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 tert-Butylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Carbon disulfide ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Carbon tetrachloride ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Chlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Chloroethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Chloroform ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Chloromethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 2-Chlorotoluene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 4-Chlorotoluene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Chlorodibromomethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2-Dichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,3-Dichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,4-Dichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,3-Dichloropropane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,1-Dichloropropene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2-Dibromo-3-Chloropropane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Ethylene Dibromide ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Dibromomethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Dichlorodifluoromethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,1-Dichloroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2-Dichloroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,1-Dichloroethene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 cis-1,2-Dichloroethene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 trans-1,2-Dichloroethene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2-Dichloropropane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 cis-1,3-Dichloropropene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 trans-1,3-Dichloropropene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Ethylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Hexachlorobutadiene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 2-Hexanone ND 57 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Isopropylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 4-Isopropyltoluene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Methylene Chloride ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 4-Methyl-2-pentanone (MIBK) ND 57 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Naphthalene ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 N-Propylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Styrene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1
1,1,1,2-Tetrachloroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-3.5-4' Lab Sample ID: 720-69933-8 Date Collected: 01/21/16 10:25 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.9
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Toluene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1
1,2,3-Trichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2,4-Trichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,1,1-Trichloroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,1,2-Trichloroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Trichloroethene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Trichlorofluoromethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2,3-Trichloropropane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,2,4-Trimethylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 1,3,5-Trimethylbenzene ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Vinyl acetate ND 23 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Vinyl chloride ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Xylenes, Total ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 2,2-Dichloropropane ND 5.7 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 Gasoline Range Organics (GRO) 290 ug/Kg ☼ 01/27/16 18:59 01/28/16 14:59 1 -C5-C12
ND
4-Bromofluorobenzene 87 45 - 131 01/27/16 18:59 01/28/16 14:59 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 102 60 - 140 01/27/16 18:59 01/28/16 14:59 1 Toluene-d8 (Surr) 98 58 - 140 01/27/16 18:59 01/28/16 14:59 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 46 1.1 mg/Kg ☼ 01/27/16 20:37 01/29/16 02:34 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 57 mg/Kg ☼ 01/27/16 20:37 01/29/16 02:34 1 [C24-C36]
160
Capric Acid (Surr) 0.4 0 - 1 01/27/16 20:37 01/29/16 02:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 85 38 - 148 01/27/16 20:37 01/29/16 02:34 1 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Endrin aldehyde ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Endrin ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1
Endrin ketone ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Heptachlor ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Heptachlor epoxide ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 4,4'-DDT ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 4,4'-DDE 28 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 4,4'-DDD 4.6 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Endosulfan I ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Endosulfan II ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 alpha-BHC ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 beta-BHC ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-3.5-4' Lab Sample ID: 720-69933-8 Date Collected: 01/21/16 10:25 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.9
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
gamma-BHC (Lindane) ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac delta-BHC ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Endosulfan sulfate ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Methoxychlor ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Toxaphene ND 46 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Chlordane (technical) ND 46 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 alpha-Chlordane ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 gamma-Chlordane ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Hexachlorobenzene ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:29 1 Tetrachloro-m-xylene 99 57 - 122 01/27/16 15:48 01/28/16 16:29 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 101 21 - 136 01/27/16 15:48 01/28/16 16:29 1 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
PCB-1232 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
PCB-1242 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
PCB-1248 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
PCB-1254 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
PCB-1260 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:15 1
Tetrachloro-m-xylene 81 45 - 132 01/27/16 15:59 01/28/16 17:15 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 68 42 - 146 01/27/16 15:59 01/28/16 17:15 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony 2.5 F1 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 8.7 3.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Barium 160 F1 F2 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Beryllium 0.54 0.38 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Cadmium ND 0.47 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Chromium 73 F1 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Cobalt 17 0.75 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4
Copper 36 5.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4
Lead 14 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4
Molybdenum 2.7 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Nickel 94 F1 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Selenium ND 3.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Silver ND 0.94 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4
Thallium 2.1 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Vanadium 41 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4 Zinc 58 5.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:42 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.63 0.010 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:00 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-7.5-8' Lab Sample ID: 720-69933-9 Date Collected: 01/21/16 10:26 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.3
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone 110 55 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1
Benzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1
Dichlorobromomethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Bromobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Chlorobromomethane ND 22 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Bromoform ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Bromomethane ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 2-Butanone (MEK) ND 55 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 n-Butylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 sec-Butylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 tert-Butylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Carbon disulfide ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Carbon tetrachloride ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Chlorobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Chloroethane ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Chloroform ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Chloromethane ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 2-Chlorotoluene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 4-Chlorotoluene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Chlorodibromomethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2-Dichlorobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,3-Dichlorobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,4-Dichlorobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,3-Dichloropropane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,1-Dichloropropene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2-Dibromo-3-Chloropropane ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Ethylene Dibromide ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Dibromomethane ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Dichlorodifluoromethane ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,1-Dichloroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2-Dichloroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,1-Dichloroethene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 cis-1,2-Dichloroethene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 trans-1,2-Dichloroethene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2-Dichloropropane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 cis-1,3-Dichloropropene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 trans-1,3-Dichloropropene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Ethylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Hexachlorobutadiene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 2-Hexanone ND 55 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Isopropylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 4-Isopropyltoluene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Methylene Chloride ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 4-Methyl-2-pentanone (MIBK) ND 55 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Naphthalene ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 N-Propylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Styrene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1
1,1,1,2-Tetrachloroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-7.5-8' Lab Sample ID: 720-69933-9 Date Collected: 01/21/16 10:26 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.3
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Toluene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1
1,2,3-Trichlorobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2,4-Trichlorobenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,1,1-Trichloroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,1,2-Trichloroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Trichloroethene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Trichlorofluoromethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2,3-Trichloropropane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,2,4-Trimethylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 1,3,5-Trimethylbenzene ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Vinyl acetate ND 22 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Vinyl chloride ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Xylenes, Total ND 11 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 2,2-Dichloropropane ND 5.5 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 Gasoline Range Organics (GRO) 280 ug/Kg ☼ 01/25/16 19:58 01/27/16 04:39 1 -C5-C12
ND
4-Bromofluorobenzene 83 45 - 131 01/25/16 19:58 01/27/16 04:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 112 60 - 140 01/25/16 19:58 01/27/16 04:39 1 Toluene-d8 (Surr) 95 58 - 140 01/25/16 19:58 01/27/16 04:39 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 390 12 mg/Kg ☼ 01/27/16 20:37 01/28/16 22:58 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 580 mg/Kg ☼ 01/27/16 20:37 01/28/16 22:58 10 [C24-C36]
1500
Capric Acid (Surr) 0 0 - 1 01/27/16 20:37 01/28/16 22:58 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 0 X D 38 - 148 01/27/16 20:37 01/28/16 22:58 10 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin 6.4 p 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Endrin aldehyde ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Endrin ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2
Endrin ketone ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Heptachlor ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Heptachlor epoxide ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 4,4'-DDT ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 4,4'-DDE 57 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 4,4'-DDD 31 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Endosulfan I ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Endosulfan II ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 alpha-BHC ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 beta-BHC ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1-7.5-8' Lab Sample ID: 720-69933-9 Date Collected: 01/21/16 10:26 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.3
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
gamma-BHC (Lindane) ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac delta-BHC ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Endosulfan sulfate ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Methoxychlor ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Toxaphene ND 91 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Chlordane (technical) ND 91 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 alpha-Chlordane 11 p 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 gamma-Chlordane 14 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Hexachlorobenzene ND 4.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 18:44 2 Tetrachloro-m-xylene 86 57 - 122 01/27/16 15:48 01/28/16 18:44 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 92 21 - 136 01/27/16 15:48 01/28/16 18:44 2 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
PCB-1232 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
PCB-1242 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
PCB-1248 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
PCB-1254 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
PCB-1260 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 16:58 1
Tetrachloro-m-xylene 88 45 - 132 01/27/16 15:59 01/28/16 16:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 76 42 - 146 01/27/16 15:59 01/28/16 16:58 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 0.57 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 7.8 4.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4 Barium 180 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4
Beryllium 0.18 0.11 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1 Cadmium 0.15 0.14 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1 Chromium 86 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4 Cobalt 18 0.91 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4
Copper 41 6.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4
Lead 42 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4
Molybdenum ND 0.57 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1 Nickel 120 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4
Selenium ND 1.1 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1 Silver ND 0.28 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1
Thallium ND 0.57 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:02 1 Vanadium 61 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4 Zinc 79 6.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:47 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.30 0.011 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:02 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2-3.5-4' Lab Sample ID: 720-69933-12 Date Collected: 01/21/16 11:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.7
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 64 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1
Benzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1
Dichlorobromomethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Bromobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Chlorobromomethane ND 26 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Bromoform ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Bromomethane ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 2-Butanone (MEK) ND 64 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 n-Butylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 sec-Butylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 tert-Butylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Carbon disulfide ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Carbon tetrachloride ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Chlorobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Chloroethane ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Chloroform ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Chloromethane ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 2-Chlorotoluene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 4-Chlorotoluene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Chlorodibromomethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2-Dichlorobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,3-Dichlorobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,4-Dichlorobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,3-Dichloropropane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,1-Dichloropropene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2-Dibromo-3-Chloropropane ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Ethylene Dibromide ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Dibromomethane ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Dichlorodifluoromethane ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,1-Dichloroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2-Dichloroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,1-Dichloroethene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 cis-1,2-Dichloroethene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 trans-1,2-Dichloroethene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2-Dichloropropane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 cis-1,3-Dichloropropene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 trans-1,3-Dichloropropene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Ethylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Hexachlorobutadiene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 2-Hexanone ND 64 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Isopropylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 4-Isopropyltoluene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Methylene Chloride ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 4-Methyl-2-pentanone (MIBK) ND 64 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Naphthalene ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 N-Propylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Styrene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1
1,1,1,2-Tetrachloroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2-3.5-4' Lab Sample ID: 720-69933-12 Date Collected: 01/21/16 11:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.7
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Toluene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1
1,2,3-Trichlorobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2,4-Trichlorobenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,1,1-Trichloroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,1,2-Trichloroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Trichloroethene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Trichlorofluoromethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2,3-Trichloropropane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,2,4-Trimethylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 1,3,5-Trimethylbenzene ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Vinyl acetate ND F1 26 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Vinyl chloride ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Xylenes, Total ND 13 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 2,2-Dichloropropane ND 6.4 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 Gasoline Range Organics (GRO) 320 ug/Kg ☼ 01/25/16 19:58 01/27/16 12:37 1 -C5-C12
ND
4-Bromofluorobenzene 83 45 - 131 01/25/16 19:58 01/27/16 12:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 99 60 - 140 01/25/16 19:58 01/27/16 12:37 1 Toluene-d8 (Surr) 98 58 - 140 01/25/16 19:58 01/27/16 12:37 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 17 1.4 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:10 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 68 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:10 1 [C24-C36]
120
Capric Acid (Surr) 2 X 0 - 1 01/27/16 21:05 01/29/16 02:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 69 38 - 148 01/27/16 21:05 01/29/16 02:10 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 0.61 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.7 4.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4 Barium 220 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4
Beryllium 0.36 0.12 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1 Cadmium 0.18 0.15 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1 Chromium 60 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4 Cobalt 12 0.98 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4
Copper 29 7.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4
Lead 31 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4
Molybdenum ND 0.61 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1 Nickel 82 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 21:52 4
Selenium ND 1.2 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1 Silver ND 0.31 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1
Thallium ND 0.61 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:07 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2-7.5-8' Lab Sample ID: 720-69933-13 Date Collected: 01/21/16 11:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 76.9
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 62 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1
Benzene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1
Dichlorobromomethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Bromobenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Chlorobromomethane ND 25 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Bromoform ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Bromomethane ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 2-Butanone (MEK) ND 62 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 n-Butylbenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 sec-Butylbenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 tert-Butylbenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Carbon disulfide ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Carbon tetrachloride ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Chlorobenzene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Chloroethane ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Chloroform ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Chloromethane ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 2-Chlorotoluene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 4-Chlorotoluene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Chlorodibromomethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,3-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,4-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,3-Dichloropropane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,1-Dichloropropene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2-Dibromo-3-Chloropropane ND * 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Ethylene Dibromide ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Dibromomethane ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,1-Dichloroethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2-Dichloroethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,1-Dichloroethene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 cis-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 trans-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 cis-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 trans-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Ethylbenzene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Hexachlorobutadiene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 2-Hexanone ND 62 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Isopropylbenzene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 4-Isopropyltoluene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Methylene Chloride ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 4-Methyl-2-pentanone (MIBK) ND 62 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Naphthalene ND * 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 N-Propylbenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Styrene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1
1,1,1,2-Tetrachloroethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2-7.5-8' Lab Sample ID: 720-69933-13 Date Collected: 01/21/16 11:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 76.9
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Toluene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1
1,2,3-Trichlorobenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2,4-Trichlorobenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,1,1-Trichloroethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,1,2-Trichloroethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Trichloroethene ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Trichlorofluoromethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2,3-Trichloropropane ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,2,4-Trimethylbenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 1,3,5-Trimethylbenzene ND * 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Vinyl acetate ND 25 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Vinyl chloride ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Xylenes, Total ND 12 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 2,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:28 1 -C5-C12
ND
4-Bromofluorobenzene 79 45 - 131 01/27/16 18:59 01/28/16 15:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 102 60 - 140 01/27/16 18:59 01/28/16 15:28 1 Toluene-d8 (Surr) 90 58 - 140 01/27/16 18:59 01/28/16 15:28 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 1400 26 mg/Kg ☼ 01/27/16 20:37 01/28/16 23:22 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 1300 mg/Kg ☼ 01/27/16 20:37 01/28/16 23:22 20 [C24-C36]
4800
Capric Acid (Surr) 0 0 - 1 01/27/16 20:37 01/28/16 23:22 20 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 0 X D 38 - 148 01/27/16 20:37 01/28/16 23:22 20 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.0 4.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Barium 150 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4
Beryllium ND 0.45 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Cadmium ND 0.56 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Chromium 280 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Cobalt 48 0.90 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4
Copper 27 6.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4
Lead 15 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4
Molybdenum ND 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Nickel 600 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4
Selenium ND 4.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 Silver ND 1.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4
Thallium ND 2.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:07 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3-3.5-4' Lab Sample ID: 720-69933-15 Date Collected: 01/21/16 13:45 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 89.7
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 54 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1
Benzene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1
Dichlorobromomethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Bromobenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Chlorobromomethane ND 21 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Bromoform ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Bromomethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 2-Butanone (MEK) ND 54 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 n-Butylbenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 sec-Butylbenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 tert-Butylbenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Carbon disulfide ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Carbon tetrachloride ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Chlorobenzene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Chloroethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Chloroform ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Chloromethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 2-Chlorotoluene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 4-Chlorotoluene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Chlorodibromomethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2-Dichlorobenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,3-Dichlorobenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,4-Dichlorobenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,3-Dichloropropane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,1-Dichloropropene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2-Dibromo-3-Chloropropane ND * 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Ethylene Dibromide ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Dibromomethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Dichlorodifluoromethane ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,1-Dichloroethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2-Dichloroethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,1-Dichloroethene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 cis-1,2-Dichloroethene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 trans-1,2-Dichloroethene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2-Dichloropropane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 cis-1,3-Dichloropropene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 trans-1,3-Dichloropropene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Ethylbenzene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Hexachlorobutadiene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 2-Hexanone ND 54 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Isopropylbenzene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 4-Isopropyltoluene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Methylene Chloride ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 4-Methyl-2-pentanone (MIBK) ND 54 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Naphthalene ND * 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 N-Propylbenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Styrene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1
1,1,1,2-Tetrachloroethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3-3.5-4' Lab Sample ID: 720-69933-15 Date Collected: 01/21/16 13:45 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 89.7
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Toluene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1
1,2,3-Trichlorobenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2,4-Trichlorobenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,1,1-Trichloroethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,1,2-Trichloroethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Trichloroethene ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Trichlorofluoromethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2,3-Trichloropropane ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,2,4-Trimethylbenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 1,3,5-Trimethylbenzene ND * 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Vinyl acetate ND 21 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Vinyl chloride ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Xylenes, Total ND 11 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 2,2-Dichloropropane ND 5.4 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 Gasoline Range Organics (GRO) 270 ug/Kg ☼ 01/27/16 18:59 01/28/16 15:57 1 -C5-C12
ND
4-Bromofluorobenzene 83 45 - 131 01/27/16 18:59 01/28/16 15:57 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 102 60 - 140 01/27/16 18:59 01/28/16 15:57 1 Toluene-d8 (Surr) 93 58 - 140 01/27/16 18:59 01/28/16 15:57 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 290 11 mg/Kg ☼ 01/27/16 20:37 01/28/16 23:46 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 550 mg/Kg ☼ 01/27/16 20:37 01/28/16 23:46 10 [C24-C36]
1200
Capric Acid (Surr) 0 0 - 1 01/27/16 20:37 01/28/16 23:46 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 0 X D 38 - 148 01/27/16 20:37 01/28/16 23:46 10 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 3.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Barium 140 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Beryllium ND 0.39 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 Cadmium ND 0.48 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 Chromium 32 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 Cobalt 11 0.78 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Copper 25 5.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Lead 3.6 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Molybdenum ND 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 Nickel 32 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Selenium ND 3.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 Silver ND 0.97 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4
Thallium ND 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:12 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3-7.5-8' Lab Sample ID: 720-69933-16 Date Collected: 01/21/16 13:46 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 83.0
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 59 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1
Benzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1
Dichlorobromomethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Bromobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Chlorobromomethane ND 24 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Bromoform ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Bromomethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 2-Butanone (MEK) ND 59 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 n-Butylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 sec-Butylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 tert-Butylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Carbon disulfide ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Carbon tetrachloride ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Chlorobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Chloroethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Chloroform ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Chloromethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 2-Chlorotoluene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 4-Chlorotoluene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Chlorodibromomethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2-Dichlorobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,3-Dichlorobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,4-Dichlorobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,3-Dichloropropane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,1-Dichloropropene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Ethylene Dibromide ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Dibromomethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,1-Dichloroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2-Dichloroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,1-Dichloroethene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 cis-1,2-Dichloroethene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 trans-1,2-Dichloroethene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2-Dichloropropane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 cis-1,3-Dichloropropene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 trans-1,3-Dichloropropene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Ethylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Hexachlorobutadiene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 2-Hexanone ND 59 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Isopropylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 4-Isopropyltoluene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Methylene Chloride ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 4-Methyl-2-pentanone (MIBK) ND 59 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Naphthalene ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 N-Propylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Styrene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1
1,1,1,2-Tetrachloroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-3-7.5-8' Lab Sample ID: 720-69933-16 Date Collected: 01/21/16 13:46 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 83.0
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Toluene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1
1,2,3-Trichlorobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2,4-Trichlorobenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,1,1-Trichloroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,1,2-Trichloroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Trichloroethene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Trichlorofluoromethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2,3-Trichloropropane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,2,4-Trimethylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 1,3,5-Trimethylbenzene ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Vinyl acetate ND 24 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Vinyl chloride ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Xylenes, Total ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 2,2-Dichloropropane ND 5.9 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 Gasoline Range Organics (GRO) 300 ug/Kg ☼ 01/25/16 19:58 01/27/16 06:11 1 -C5-C12
ND
4-Bromofluorobenzene 84 45 - 131 01/25/16 19:58 01/27/16 06:11 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 112 60 - 140 01/25/16 19:58 01/27/16 06:11 1 Toluene-d8 (Surr) 97 58 - 140 01/25/16 19:58 01/27/16 06:11 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 11 1.2 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:10 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 60 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:10 1 Capric Acid (Surr) 0.004 0 - 1 01/27/16 21:05 01/29/16 02:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 84 38 - 148 01/27/16 21:05 01/29/16 02:10 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 3.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Barium 100 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Beryllium ND 0.32 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Cadmium ND 0.40 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Chromium 83 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Cobalt 16 0.65 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Copper 63 4.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Lead 5.9 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Molybdenum ND 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Nickel 86 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Selenium ND 3.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Silver ND 0.81 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4
Thallium ND 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 Vanadium 69 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:17 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-4-3.5-4' Lab Sample ID: 720-69933-19 Date Collected: 01/21/16 15:35 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 69.1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 70 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1
Benzene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1
Dichlorobromomethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Bromobenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Chlorobromomethane ND 28 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Bromoform ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Bromomethane ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 2-Butanone (MEK) ND 70 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 n-Butylbenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 sec-Butylbenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 tert-Butylbenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Carbon disulfide ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Carbon tetrachloride ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Chlorobenzene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Chloroethane ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Chloroform ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Chloromethane ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 2-Chlorotoluene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 4-Chlorotoluene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Chlorodibromomethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2-Dichlorobenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,3-Dichlorobenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,4-Dichlorobenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,3-Dichloropropane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,1-Dichloropropene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2-Dibromo-3-Chloropropane ND * 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Ethylene Dibromide ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Dibromomethane ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Dichlorodifluoromethane ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,1-Dichloroethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2-Dichloroethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,1-Dichloroethene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 cis-1,2-Dichloroethene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 trans-1,2-Dichloroethene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2-Dichloropropane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 cis-1,3-Dichloropropene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 trans-1,3-Dichloropropene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Ethylbenzene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Hexachlorobutadiene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 2-Hexanone ND 70 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Isopropylbenzene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 4-Isopropyltoluene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Methylene Chloride ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 4-Methyl-2-pentanone (MIBK) ND 70 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Naphthalene ND * 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 N-Propylbenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Styrene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1
1,1,1,2-Tetrachloroethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-4-3.5-4' Lab Sample ID: 720-69933-19 Date Collected: 01/21/16 15:35 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 69.1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Toluene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1
1,2,3-Trichlorobenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2,4-Trichlorobenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,1,1-Trichloroethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,1,2-Trichloroethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Trichloroethene ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Trichlorofluoromethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2,3-Trichloropropane ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,2,4-Trimethylbenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 1,3,5-Trimethylbenzene ND * 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Vinyl acetate ND 28 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Vinyl chloride ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Xylenes, Total ND 14 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 2,2-Dichloropropane ND 7.0 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 Gasoline Range Organics (GRO) 350 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:07 1 -C5-C12
ND
4-Bromofluorobenzene 81 45 - 131 01/25/16 19:58 01/27/16 13:07 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 105 60 - 140 01/25/16 19:58 01/27/16 13:07 1 Toluene-d8 (Surr) 97 58 - 140 01/25/16 19:58 01/27/16 13:07 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 5.1 1.4 mg/Kg ☼ 01/27/16 21:05 01/29/16 00:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 71 mg/Kg ☼ 01/27/16 21:05 01/29/16 00:37 1 Capric Acid (Surr) 0.03 0 - 1 01/27/16 21:05 01/29/16 00:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 51 38 - 148 01/27/16 21:05 01/29/16 00:37 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 0.66 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:12 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.7 5.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4 Barium 180 2.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4
Beryllium 0.79 0.53 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4 Cadmium 0.37 0.16 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:12 1 Chromium 63 2.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4 Cobalt 13 1.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4
Copper 45 7.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4
Lead 39 2.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4
Molybdenum 0.76 0.66 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:12 1 Nickel 77 2.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4
Selenium ND 1.3 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:12 1 Silver ND 0.33 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:12 1
Thallium ND 0.66 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:12 1 Vanadium 51 2.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:22 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-5-4.5-5' Lab Sample ID: 720-69933-23 Date Collected: 01/21/16 16:06 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.9
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 62 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1
Benzene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1
Dichlorobromomethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Bromobenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Chlorobromomethane ND 25 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Bromoform ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Bromomethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 2-Butanone (MEK) ND 62 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 n-Butylbenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 sec-Butylbenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 tert-Butylbenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Carbon disulfide ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Carbon tetrachloride ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Chlorobenzene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Chloroethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Chloroform ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Chloromethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 2-Chlorotoluene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 4-Chlorotoluene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Chlorodibromomethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,3-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,4-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,3-Dichloropropane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,1-Dichloropropene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2-Dibromo-3-Chloropropane ND * 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Ethylene Dibromide ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Dibromomethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,1-Dichloroethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2-Dichloroethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,1-Dichloroethene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 cis-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 trans-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 cis-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 trans-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Ethylbenzene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Hexachlorobutadiene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 2-Hexanone ND 62 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Isopropylbenzene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 4-Isopropyltoluene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Methylene Chloride ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 4-Methyl-2-pentanone (MIBK) ND 62 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Naphthalene ND * 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 N-Propylbenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Styrene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1
1,1,1,2-Tetrachloroethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-5-4.5-5' Lab Sample ID: 720-69933-23 Date Collected: 01/21/16 16:06 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.9
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Toluene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1
1,2,3-Trichlorobenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2,4-Trichlorobenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,1,1-Trichloroethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,1,2-Trichloroethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Trichloroethene ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Trichlorofluoromethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2,3-Trichloropropane ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,2,4-Trimethylbenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 1,3,5-Trimethylbenzene ND * 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Vinyl acetate ND 25 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Vinyl chloride ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Xylenes, Total ND 12 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 2,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/25/16 19:58 01/27/16 13:38 1 -C5-C12
ND
4-Bromofluorobenzene 71 45 - 131 01/25/16 19:58 01/27/16 13:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 116 60 - 140 01/25/16 19:58 01/27/16 13:38 1 Toluene-d8 (Surr) 81 58 - 140 01/25/16 19:58 01/27/16 13:38 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 43 1.3 mg/Kg ☼ 01/27/16 21:05 01/29/16 03:32 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 63 mg/Kg ☼ 01/27/16 21:05 01/29/16 03:32 1 [C24-C36]
110
Capric Acid (Surr) 0.7 0 - 1 01/27/16 21:05 01/29/16 03:32 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 45 38 - 148 01/27/16 21:05 01/29/16 03:32 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 1.9 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:17 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.1 3.8 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:17 4 Barium 34 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4
Beryllium ND 0.38 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4 Cadmium 0.85 0.48 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:17 4 Chromium 32 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4 Cobalt 5.7 0.77 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4 Copper 62 5.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4
Lead 210 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4
Molybdenum 8.0 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4 Nickel 130 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4
Selenium ND 3.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4 Silver ND 0.96 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4
Thallium ND 1.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:27 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-5-7.5-8' Lab Sample ID: 720-69933-24 Date Collected: 01/21/16 16:05 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.0
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 62 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1
Benzene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1
Dichlorobromomethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Bromobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Chlorobromomethane ND 25 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Bromoform ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Bromomethane ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 2-Butanone (MEK) ND 62 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 n-Butylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 sec-Butylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 tert-Butylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Carbon disulfide ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Carbon tetrachloride ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Chlorobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Chloroethane ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Chloroform ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Chloromethane ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 2-Chlorotoluene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 4-Chlorotoluene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Chlorodibromomethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,3-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,4-Dichlorobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,3-Dichloropropane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1-Dichloropropene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2-Dibromo-3-Chloropropane ND * 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Ethylene Dibromide ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Dibromomethane ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1-Dichloroethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2-Dichloroethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1-Dichloroethene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 cis-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 trans-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 cis-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 trans-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Ethylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Hexachlorobutadiene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 2-Hexanone ND 62 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Isopropylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 4-Isopropyltoluene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Methylene Chloride ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 4-Methyl-2-pentanone (MIBK) ND 62 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Naphthalene ND * 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 N-Propylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Styrene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1,1,2-Tetrachloroethane ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-5-7.5-8' Lab Sample ID: 720-69933-24 Date Collected: 01/21/16 16:05 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.0
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Toluene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2,3-Trichlorobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2,4-Trichlorobenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1,1-Trichloroethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1,2-Trichloroethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Trichloroethene ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Trichlorofluoromethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2,3-Trichloropropane ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,2,4-Trimethylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 1,3,5-Trimethylbenzene ND * 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Vinyl acetate ND 25 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Vinyl chloride ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Xylenes, Total ND 12 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 2,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/28/16 18:30 01/29/16 00:36 1 -C5-C12
ND
4-Bromofluorobenzene 61 * 45 - 131 01/28/16 18:30 01/29/16 00:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 115 60 - 140 01/28/16 18:30 01/29/16 00:36 1 Toluene-d8 (Surr) 93 58 - 140 01/28/16 18:30 01/29/16 00:36 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 46 1.3 mg/Kg ☼ 01/27/16 21:05 01/29/16 04:02 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 63 mg/Kg ☼ 01/27/16 21:05 01/29/16 04:02 1 [C24-C36]
98 Capric Acid (Surr) 0.4 0 - 1 01/27/16 21:05 01/29/16 04:02 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 47 38 - 148 01/27/16 21:05 01/29/16 04:02 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 7.5 4.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Barium 510 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4
Beryllium ND 0.41 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Cadmium 2.8 0.51 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Chromium 39 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Cobalt 13 0.81 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4
Copper 140 6.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4
Lead 290 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4
Molybdenum ND 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Nickel 50 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4
Selenium ND 4.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 Silver ND 1.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4
Thallium ND 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:31 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-3.5-4' Lab Sample ID: 720-69933-27 Date Collected: 01/21/16 16:30 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.8
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 55 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1
Benzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1
Dichlorobromomethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Bromobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Chlorobromomethane ND 22 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Bromoform ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Bromomethane ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 2-Butanone (MEK) ND 55 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 n-Butylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 sec-Butylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 tert-Butylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Carbon disulfide ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Carbon tetrachloride ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Chlorobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Chloroethane ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Chloroform ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Chloromethane ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 2-Chlorotoluene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 4-Chlorotoluene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Chlorodibromomethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2-Dichlorobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,3-Dichlorobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,4-Dichlorobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,3-Dichloropropane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,1-Dichloropropene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2-Dibromo-3-Chloropropane ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Ethylene Dibromide ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Dibromomethane ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Dichlorodifluoromethane ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,1-Dichloroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2-Dichloroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,1-Dichloroethene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 cis-1,2-Dichloroethene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 trans-1,2-Dichloroethene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2-Dichloropropane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 cis-1,3-Dichloropropene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 trans-1,3-Dichloropropene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Ethylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Hexachlorobutadiene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 2-Hexanone ND 55 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Isopropylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 4-Isopropyltoluene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Methylene Chloride ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 4-Methyl-2-pentanone (MIBK) ND 55 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Naphthalene ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 N-Propylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Styrene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1
1,1,1,2-Tetrachloroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-3.5-4' Lab Sample ID: 720-69933-27 Date Collected: 01/21/16 16:30 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.8
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Toluene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1
1,2,3-Trichlorobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2,4-Trichlorobenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,1,1-Trichloroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,1,2-Trichloroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Trichloroethene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Trichlorofluoromethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2,3-Trichloropropane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,2,4-Trimethylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 1,3,5-Trimethylbenzene ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Vinyl acetate ND 22 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Vinyl chloride ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Xylenes, Total ND 11 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 2,2-Dichloropropane ND 5.5 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 Gasoline Range Organics (GRO) 270 ug/Kg ☼ 01/28/16 18:30 01/29/16 01:07 1 -C5-C12
ND
4-Bromofluorobenzene 79 45 - 131 01/28/16 18:30 01/29/16 01:07 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 113 60 - 140 01/28/16 18:30 01/29/16 01:07 1 Toluene-d8 (Surr) 95 58 - 140 01/28/16 18:30 01/29/16 01:07 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 25 1.1 mg/Kg ☼ 01/27/16 20:37 01/29/16 02:34 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 57 mg/Kg ☼ 01/27/16 20:37 01/29/16 02:34 1 [C24-C36]
99 Capric Acid (Surr) 0.4 0 - 1 01/27/16 20:37 01/29/16 02:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 70 38 - 148 01/27/16 20:37 01/29/16 02:34 1 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin 11 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Endrin aldehyde ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Endrin ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1
Endrin ketone ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Heptachlor ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Heptachlor epoxide ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 4,4'-DDT 11 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 4,4'-DDE 18 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 4,4'-DDD 4.4 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Endosulfan I ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Endosulfan II ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 alpha-BHC ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 beta-BHC ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-3.5-4' Lab Sample ID: 720-69933-27 Date Collected: 01/21/16 16:30 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.8
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
gamma-BHC (Lindane) ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac delta-BHC ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Endosulfan sulfate ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Methoxychlor ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Toxaphene ND 46 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Chlordane (technical) ND 46 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 alpha-Chlordane ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 gamma-Chlordane ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Hexachlorobenzene ND 2.3 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:12 1 Tetrachloro-m-xylene 100 57 - 122 01/27/16 15:48 01/28/16 16:12 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 83 21 - 136 01/27/16 15:48 01/28/16 16:12 1 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
PCB-1232 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
PCB-1242 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
PCB-1248 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
PCB-1254 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
PCB-1260 ND 57 ug/Kg ☼ 01/27/16 15:59 01/28/16 17:32 1
Tetrachloro-m-xylene 77 45 - 132 01/27/16 15:59 01/28/16 17:32 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 69 42 - 146 01/27/16 15:59 01/28/16 17:32 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 0.43 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 2.7 0.85 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1 Barium 38 1.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4
Beryllium 0.095 0.085 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1 Cadmium ND 0.11 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1 Chromium 24 1.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4 Cobalt 3.9 0.68 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4 Copper 20 5.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4
Lead 23 1.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4
Molybdenum 4.5 1.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4 Nickel 40 1.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4
Selenium ND 0.85 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1 Silver ND 0.21 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1
Thallium ND 0.43 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:22 1 Vanadium 14 1.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4 Zinc 28 5.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:36 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.081 0.011 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:21 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-7.5-8' Lab Sample ID: 720-69933-28 Date Collected: 01/21/16 16:32 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.4
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 59 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1
Benzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1
Dichlorobromomethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Bromobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Chlorobromomethane ND 24 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Bromoform ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Bromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 2-Butanone (MEK) ND 59 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 n-Butylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 sec-Butylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 tert-Butylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Carbon disulfide ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Carbon tetrachloride ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Chlorobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Chloroethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Chloroform ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Chloromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 2-Chlorotoluene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 4-Chlorotoluene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Chlorodibromomethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2-Dichlorobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,3-Dichlorobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,4-Dichlorobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,3-Dichloropropane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,1-Dichloropropene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Ethylene Dibromide ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Dibromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,1-Dichloroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2-Dichloroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,1-Dichloroethene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 cis-1,2-Dichloroethene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 trans-1,2-Dichloroethene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2-Dichloropropane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 cis-1,3-Dichloropropene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 trans-1,3-Dichloropropene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Ethylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Hexachlorobutadiene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 2-Hexanone ND 59 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Isopropylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 4-Isopropyltoluene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Methylene Chloride ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 4-Methyl-2-pentanone (MIBK) ND 59 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Naphthalene ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 N-Propylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Styrene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1
1,1,1,2-Tetrachloroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-7.5-8' Lab Sample ID: 720-69933-28 Date Collected: 01/21/16 16:32 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Toluene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1
1,2,3-Trichlorobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2,4-Trichlorobenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,1,1-Trichloroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,1,2-Trichloroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Trichloroethene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Trichlorofluoromethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2,3-Trichloropropane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,2,4-Trimethylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 1,3,5-Trimethylbenzene ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Vinyl acetate ND 24 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Vinyl chloride ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Xylenes, Total ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 2,2-Dichloropropane ND 5.9 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 Gasoline Range Organics (GRO) 290 ug/Kg ☼ 01/29/16 19:09 01/29/16 21:35 1 -C5-C12
ND
4-Bromofluorobenzene 89 45 - 131 01/29/16 19:09 01/29/16 21:35 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 105 60 - 140 01/29/16 19:09 01/29/16 21:35 1 Toluene-d8 (Surr) 101 58 - 140 01/29/16 19:09 01/29/16 21:35 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 9.0 1.3 mg/Kg ☼ 01/27/16 20:37 01/28/16 23:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 63 mg/Kg ☼ 01/27/16 20:37 01/28/16 23:39 1 Capric Acid (Surr) 0.04 0 - 1 01/27/16 20:37 01/28/16 23:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 73 38 - 148 01/27/16 20:37 01/28/16 23:39 1 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin 4.1 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Endrin aldehyde ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Endrin ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1
Endrin ketone ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Heptachlor ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Heptachlor epoxide ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 4,4'-DDT 3.4 p 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 4,4'-DDE 35 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 4,4'-DDD 62 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Endosulfan I ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Endosulfan II ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 alpha-BHC ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 beta-BHC ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 gamma-BHC (Lindane) ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6-7.5-8' Lab Sample ID: 720-69933-28 Date Collected: 01/21/16 16:32 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.4
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
delta-BHC ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Endosulfan sulfate ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Methoxychlor ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Toxaphene ND 50 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Chlordane (technical) ND 50 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 alpha-Chlordane ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 gamma-Chlordane ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Hexachlorobenzene ND 2.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 16:46 1 Tetrachloro-m-xylene 92 57 - 122 01/27/16 15:48 01/28/16 16:46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 273 X 21 - 136 01/27/16 15:48 01/28/16 16:46 1 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1
PCB-1232 ND 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1
PCB-1242 ND 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1
PCB-1248 ND 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1
PCB-1254 ND 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1
PCB-1260 130 62 ug/Kg ☼ 01/27/16 15:59 01/28/16 20:51 1 Tetrachloro-m-xylene 72 45 - 132 01/27/16 15:59 01/28/16 20:51 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 201 X 42 - 146 01/27/16 15:59 01/28/16 20:51 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony 6.7 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 11 4.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Barium 650 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Beryllium ND 0.48 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Cadmium 4.9 0.60 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Chromium 65 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Cobalt 15 0.95 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Copper 99 7.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Lead 710 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Molybdenum ND 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Nickel 79 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Selenium ND 4.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Silver ND 1.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Thallium ND 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Vanadium 47 2.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4 Zinc 460 7.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:41 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.16 0.011 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:28 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7-3.5-4' Lab Sample ID: 720-69933-31 Date Collected: 01/22/16 08:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 82.1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 60 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1
Benzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1
Dichlorobromomethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Bromobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Chlorobromomethane ND 24 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Bromoform ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Bromomethane ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 2-Butanone (MEK) ND 60 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 n-Butylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 sec-Butylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 tert-Butylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Carbon disulfide ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Carbon tetrachloride ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Chlorobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Chloroethane ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Chloroform ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Chloromethane ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 2-Chlorotoluene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 4-Chlorotoluene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Chlorodibromomethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,3-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,4-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,3-Dichloropropane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,1-Dichloropropene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Ethylene Dibromide ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Dibromomethane ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,1-Dichloroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2-Dichloroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,1-Dichloroethene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 cis-1,2-Dichloroethene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 trans-1,2-Dichloroethene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2-Dichloropropane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 cis-1,3-Dichloropropene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 trans-1,3-Dichloropropene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Ethylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Hexachlorobutadiene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 2-Hexanone ND 60 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Isopropylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 4-Isopropyltoluene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Methylene Chloride ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 4-Methyl-2-pentanone (MIBK) ND 60 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Naphthalene ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 N-Propylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Styrene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1
1,1,1,2-Tetrachloroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7-3.5-4' Lab Sample ID: 720-69933-31 Date Collected: 01/22/16 08:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 82.1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Toluene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1
1,2,3-Trichlorobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2,4-Trichlorobenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,1,1-Trichloroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,1,2-Trichloroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Trichloroethene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Trichlorofluoromethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2,3-Trichloropropane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,2,4-Trimethylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 1,3,5-Trimethylbenzene ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Vinyl acetate ND 24 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Vinyl chloride ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Xylenes, Total ND 12 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 2,2-Dichloropropane ND 6.0 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 Gasoline Range Organics (GRO) 300 ug/Kg ☼ 01/27/16 19:40 01/28/16 16:56 1 -C5-C12
ND
4-Bromofluorobenzene 88 45 - 131 01/27/16 19:40 01/28/16 16:56 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 98 60 - 140 01/27/16 19:40 01/28/16 16:56 1 Toluene-d8 (Surr) 94 58 - 140 01/27/16 19:40 01/28/16 16:56 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 21 1.2 mg/Kg ☼ 01/27/16 20:37 01/29/16 01:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 61 mg/Kg ☼ 01/27/16 20:37 01/29/16 01:36 1 [C24-C36]
72 Capric Acid (Surr) 0.02 0 - 1 01/27/16 20:37 01/29/16 01:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 71 38 - 148 01/27/16 20:37 01/29/16 01:36 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 7.1 4.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Barium 150 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4
Beryllium ND 0.46 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Cadmium ND 0.57 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Chromium 60 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Cobalt 14 0.91 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4
Copper 34 6.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4
Lead 38 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4
Molybdenum ND 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Nickel 94 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4
Selenium ND 4.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 Silver ND 1.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4
Thallium ND 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:46 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7-7.5-8' Lab Sample ID: 720-69933-32 Date Collected: 01/22/16 08:45 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.2
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 56 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1
Benzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1
Dichlorobromomethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Bromobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Chlorobromomethane ND 22 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Bromoform ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Bromomethane ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 2-Butanone (MEK) ND 56 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 n-Butylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 sec-Butylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 tert-Butylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Carbon disulfide ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Carbon tetrachloride ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Chlorobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Chloroethane ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Chloroform ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Chloromethane ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 2-Chlorotoluene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 4-Chlorotoluene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Chlorodibromomethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2-Dichlorobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,3-Dichlorobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,4-Dichlorobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,3-Dichloropropane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,1-Dichloropropene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2-Dibromo-3-Chloropropane ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Ethylene Dibromide ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Dibromomethane ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Dichlorodifluoromethane ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,1-Dichloroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2-Dichloroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,1-Dichloroethene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 cis-1,2-Dichloroethene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 trans-1,2-Dichloroethene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2-Dichloropropane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 cis-1,3-Dichloropropene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 trans-1,3-Dichloropropene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Ethylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Hexachlorobutadiene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 2-Hexanone ND 56 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Isopropylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 4-Isopropyltoluene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Methylene Chloride ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 4-Methyl-2-pentanone (MIBK) ND 56 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Naphthalene ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 N-Propylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Styrene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1
1,1,1,2-Tetrachloroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7-7.5-8' Lab Sample ID: 720-69933-32 Date Collected: 01/22/16 08:45 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Toluene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1
1,2,3-Trichlorobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2,4-Trichlorobenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,1,1-Trichloroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,1,2-Trichloroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Trichloroethene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Trichlorofluoromethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2,3-Trichloropropane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,2,4-Trimethylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 1,3,5-Trimethylbenzene ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Vinyl acetate ND 22 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Vinyl chloride ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Xylenes, Total ND 11 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 2,2-Dichloropropane ND 5.6 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 Gasoline Range Organics (GRO) 280 ug/Kg ☼ 01/27/16 09:20 01/27/16 15:09 1 -C5-C12
ND
4-Bromofluorobenzene 84 45 - 131 01/27/16 09:20 01/27/16 15:09 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 110 60 - 140 01/27/16 09:20 01/27/16 15:09 1 Toluene-d8 (Surr) 97 58 - 140 01/27/16 09:20 01/27/16 15:09 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 1.5 1.3 mg/Kg ☼ 01/27/16 21:05 01/28/16 22:40 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 64 mg/Kg ☼ 01/27/16 21:05 01/28/16 22:40 1 Capric Acid (Surr) 0.02 0 - 1 01/27/16 21:05 01/28/16 22:40 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 76 38 - 148 01/27/16 21:05 01/28/16 22:40 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 8.3 3.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Barium 250 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4
Beryllium 0.67 0.32 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Cadmium ND 0.39 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Chromium 69 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Cobalt 17 0.63 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4
Copper 39 4.7 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4
Lead 12 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4
Molybdenum ND 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Nickel 94 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4
Selenium ND 3.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Silver ND 0.79 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4
Thallium ND 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 Vanadium 55 1.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 22:51 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Date Collected: 01/22/16 09:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.0
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND F1 65 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Benzene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1
Dichlorobromomethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Bromobenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Chlorobromomethane ND 26 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Bromoform ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Bromomethane ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 2-Butanone (MEK) ND 65 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 n-Butylbenzene ND * 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 sec-Butylbenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 tert-Butylbenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Carbon disulfide ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Carbon tetrachloride ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Chlorobenzene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Chloroethane ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Chloroform ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Chloromethane ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 2-Chlorotoluene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 4-Chlorotoluene ND * F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Chlorodibromomethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2-Dichlorobenzene ND * 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,3-Dichlorobenzene ND * 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,4-Dichlorobenzene ND * 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,3-Dichloropropane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,1-Dichloropropene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2-Dibromo-3-Chloropropane ND * F1 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Ethylene Dibromide ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Dibromomethane ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Dichlorodifluoromethane ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,1-Dichloroethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2-Dichloroethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,1-Dichloroethene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 cis-1,2-Dichloroethene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 trans-1,2-Dichloroethene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2-Dichloropropane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 cis-1,3-Dichloropropene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 trans-1,3-Dichloropropene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Ethylbenzene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Hexachlorobutadiene ND * 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 2-Hexanone ND 65 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Isopropylbenzene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 4-Isopropyltoluene ND * F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Methylene Chloride ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 4-Methyl-2-pentanone (MIBK) ND 65 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Naphthalene ND * F2 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 N-Propylbenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Styrene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1
1,1,1,2-Tetrachloroethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Date Collected: 01/22/16 09:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.0
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND * F1 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Toluene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1
1,2,3-Trichlorobenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2,4-Trichlorobenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,1,1-Trichloroethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,1,2-Trichloroethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Trichloroethene ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Trichlorofluoromethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2,3-Trichloropropane ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,2,4-Trimethylbenzene ND * F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 1,3,5-Trimethylbenzene ND * F1 F2 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Vinyl acetate ND F1 F2 26 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Vinyl chloride ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Xylenes, Total ND 13 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 2,2-Dichloropropane ND 6.5 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 Gasoline Range Organics (GRO) 320 ug/Kg ☼ 01/27/16 19:40 01/28/16 14:29 1 -C5-C12
ND
4-Bromofluorobenzene 80 45 - 131 01/27/16 19:40 01/28/16 14:29 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 105 60 - 140 01/27/16 19:40 01/28/16 14:29 1 Toluene-d8 (Surr) 93 58 - 140 01/27/16 19:40 01/28/16 14:29 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 21 1.3 mg/Kg ☼ 01/27/16 20:37 01/29/16 02:05 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 65 mg/Kg ☼ 01/27/16 20:37 01/29/16 02:05 1 [C24-C36]
90 Capric Acid (Surr) 0.04 0 - 1 01/27/16 20:37 01/29/16 02:05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 65 38 - 148 01/27/16 20:37 01/29/16 02:05 1 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Endrin aldehyde ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Endrin ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1
Endrin ketone ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Heptachlor ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Heptachlor epoxide ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 4,4'-DDT 18 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 4,4'-DDE 60 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 4,4'-DDD 16 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Endosulfan I ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Endosulfan II ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 alpha-BHC ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 beta-BHC ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Date Collected: 01/22/16 09:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.0
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
gamma-BHC (Lindane) ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac delta-BHC ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Endosulfan sulfate ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Methoxychlor ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Toxaphene ND 52 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Chlordane (technical) ND 52 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 alpha-Chlordane ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 gamma-Chlordane ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Hexachlorobenzene ND 2.6 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:03 1 Tetrachloro-m-xylene 83 57 - 122 01/27/16 15:48 01/28/16 17:03 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 83 21 - 136 01/27/16 15:48 01/28/16 17:03 1 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
PCB-1232 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
PCB-1242 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
PCB-1248 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
PCB-1254 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
PCB-1260 ND 65 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:05 1
Tetrachloro-m-xylene 69 45 - 132 01/27/16 15:59 01/28/16 18:05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 66 42 - 146 01/27/16 15:59 01/28/16 18:05 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 44 4.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Barium 250 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Beryllium 0.61 0.41 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Cadmium ND 0.52 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Chromium 89 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Cobalt 21 0.83 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Copper 53 6.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Lead 130 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Molybdenum ND 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Nickel 150 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Selenium ND 4.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Silver ND 1.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Thallium ND 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Vanadium 55 2.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4 Zinc 130 6.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:06 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 5.4 0.11 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:59 10 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-7.5-8' Lab Sample ID: 720-69933-36 Date Collected: 01/22/16 09:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 81.3
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1
Benzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1
Dichlorobromomethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Bromobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Chlorobromomethane ND 24 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Bromoform ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Bromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 2-Butanone (MEK) ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 n-Butylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 sec-Butylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 tert-Butylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Carbon disulfide ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Carbon tetrachloride ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Chlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Chloroethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Chloroform ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Chloromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 2-Chlorotoluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 4-Chlorotoluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Chlorodibromomethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2-Dichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,3-Dichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,4-Dichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,3-Dichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,1-Dichloropropene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Ethylene Dibromide ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Dibromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,1-Dichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2-Dichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,1-Dichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 cis-1,2-Dichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 trans-1,2-Dichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2-Dichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 cis-1,3-Dichloropropene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 trans-1,3-Dichloropropene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Ethylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Hexachlorobutadiene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 2-Hexanone ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Isopropylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 4-Isopropyltoluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Methylene Chloride ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 4-Methyl-2-pentanone (MIBK) ND F1 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Naphthalene ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 N-Propylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Styrene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1
1,1,1,2-Tetrachloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-7.5-8' Lab Sample ID: 720-69933-36 Date Collected: 01/22/16 09:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 81.3
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Toluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1
1,2,3-Trichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2,4-Trichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,1,1-Trichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,1,2-Trichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Trichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Trichlorofluoromethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2,3-Trichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,2,4-Trimethylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 1,3,5-Trimethylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Vinyl acetate ND F1 F2 24 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Vinyl chloride ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Xylenes, Total ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 2,2-Dichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:07 1 -C5-C12
ND
4-Bromofluorobenzene 89 45 - 131 01/29/16 19:09 01/29/16 23:07 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 107 60 - 140 01/29/16 19:09 01/29/16 23:07 1 Toluene-d8 (Surr) 101 58 - 140 01/29/16 19:09 01/29/16 23:07 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] ND 1.2 mg/Kg ☼ 01/27/16 20:37 01/28/16 22:11 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 61 mg/Kg ☼ 01/27/16 20:37 01/28/16 22:11 1 Capric Acid (Surr) 0.01 0 - 1 01/27/16 20:37 01/28/16 22:11 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 87 38 - 148 01/27/16 20:37 01/28/16 22:11 1 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Endrin aldehyde ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Endrin ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1
Endrin ketone ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Heptachlor ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Heptachlor epoxide ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 4,4'-DDT ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 4,4'-DDE ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 4,4'-DDD ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Endosulfan I ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Endosulfan II ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 alpha-BHC ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 beta-BHC ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 gamma-BHC (Lindane) ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-7.5-8' Lab Sample ID: 720-69933-36 Date Collected: 01/22/16 09:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 81.3
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
delta-BHC ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Endosulfan sulfate ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Methoxychlor ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Toxaphene ND 49 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Chlordane (technical) ND 49 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 alpha-Chlordane ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 gamma-Chlordane ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Hexachlorobenzene ND 2.4 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:19 1 Tetrachloro-m-xylene 96 57 - 122 01/27/16 15:48 01/28/16 17:19 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 116 21 - 136 01/27/16 15:48 01/28/16 17:19 1 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
PCB-1232 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
PCB-1242 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
PCB-1248 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
PCB-1254 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
PCB-1260 ND 61 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:22 1
Tetrachloro-m-xylene 68 45 - 132 01/27/16 15:59 01/28/16 18:22 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 73 42 - 146 01/27/16 15:59 01/28/16 18:22 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 7.1 4.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Barium 160 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Beryllium 0.81 0.46 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Cadmium ND 0.57 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Chromium 68 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Cobalt 14 0.91 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Copper 37 6.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Lead 11 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Molybdenum ND 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Nickel 82 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Selenium ND 4.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Silver ND 1.1 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Thallium ND 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Vanadium 54 2.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4 Zinc 77 6.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:11 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.12 0.011 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-9-4.5-5' Lab Sample ID: 720-69933-39 Date Collected: 01/22/16 10:22 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.2
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1
Benzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1
Dichlorobromomethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Bromobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Chlorobromomethane ND 25 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Bromoform ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Bromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 2-Butanone (MEK) ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 n-Butylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 sec-Butylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 tert-Butylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Carbon disulfide ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Carbon tetrachloride ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Chlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Chloroethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Chloroform ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Chloromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 2-Chlorotoluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 4-Chlorotoluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Chlorodibromomethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2-Dichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,3-Dichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,4-Dichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,3-Dichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,1-Dichloropropene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Ethylene Dibromide ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Dibromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,1-Dichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2-Dichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,1-Dichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 cis-1,2-Dichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 trans-1,2-Dichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2-Dichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 cis-1,3-Dichloropropene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 trans-1,3-Dichloropropene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Ethylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Hexachlorobutadiene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 2-Hexanone ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Isopropylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 4-Isopropyltoluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Methylene Chloride ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 4-Methyl-2-pentanone (MIBK) ND 61 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Naphthalene ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 N-Propylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Styrene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1
1,1,1,2-Tetrachloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-9-4.5-5' Lab Sample ID: 720-69933-39 Date Collected: 01/22/16 10:22 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Toluene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1
1,2,3-Trichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2,4-Trichlorobenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,1,1-Trichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,1,2-Trichloroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Trichloroethene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Trichlorofluoromethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2,3-Trichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,2,4-Trimethylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 1,3,5-Trimethylbenzene ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Vinyl acetate ND 25 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Vinyl chloride ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Xylenes, Total ND 12 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 2,2-Dichloropropane ND 6.1 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/29/16 19:09 01/29/16 23:37 1 -C5-C12
ND
4-Bromofluorobenzene 85 45 - 131 01/29/16 19:09 01/29/16 23:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 111 60 - 140 01/29/16 19:09 01/29/16 23:37 1 Toluene-d8 (Surr) 93 58 - 140 01/29/16 19:09 01/29/16 23:37 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 12 1.3 mg/Kg ☼ 01/27/16 21:05 01/29/16 01:06 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 64 mg/Kg ☼ 01/27/16 21:05 01/29/16 01:06 1 Capric Acid (Surr) 0.08 0 - 1 01/27/16 21:05 01/29/16 01:06 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 49 38 - 148 01/27/16 21:05 01/29/16 01:06 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 17 5.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Barium 250 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Beryllium 0.65 0.50 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Cadmium ND 0.63 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Chromium 84 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Cobalt 22 1.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Copper 45 7.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Lead 37 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Molybdenum ND 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Nickel 140 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Selenium ND 5.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Silver ND 1.3 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4
Thallium ND 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 Vanadium 58 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:16 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-9-7.5-8' Lab Sample ID: 720-69933-40 Date Collected: 01/22/16 10:24 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.4
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1
Benzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1
Dichlorobromomethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Bromobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Chlorobromomethane ND 24 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Bromoform ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Bromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 2-Butanone (MEK) ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 n-Butylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 sec-Butylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 tert-Butylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Carbon disulfide ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Carbon tetrachloride ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Chlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Chloroethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Chloroform ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Chloromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 2-Chlorotoluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 4-Chlorotoluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Chlorodibromomethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,3-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,4-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,3-Dichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,1-Dichloropropene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Ethylene Dibromide ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Dibromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,1-Dichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2-Dichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,1-Dichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 cis-1,2-Dichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 trans-1,2-Dichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2-Dichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 cis-1,3-Dichloropropene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 trans-1,3-Dichloropropene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Ethylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Hexachlorobutadiene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 2-Hexanone ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Isopropylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 4-Isopropyltoluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Methylene Chloride ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 4-Methyl-2-pentanone (MIBK) ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Naphthalene ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 N-Propylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Styrene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1
1,1,1,2-Tetrachloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-9-7.5-8' Lab Sample ID: 720-69933-40 Date Collected: 01/22/16 10:24 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Toluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1
1,2,3-Trichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2,4-Trichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,1,1-Trichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,1,2-Trichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Trichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Trichlorofluoromethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2,3-Trichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,2,4-Trimethylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 1,3,5-Trimethylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Vinyl acetate ND 24 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Vinyl chloride ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Xylenes, Total ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 2,2-Dichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 Gasoline Range Organics (GRO) 300 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:08 1 -C5-C12
ND
4-Bromofluorobenzene 87 45 - 131 01/29/16 19:09 01/30/16 00:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 113 60 - 140 01/29/16 19:09 01/30/16 00:08 1 Toluene-d8 (Surr) 98 58 - 140 01/29/16 19:09 01/30/16 00:08 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 56 1.3 mg/Kg ☼ 01/27/16 21:05 01/29/16 03:03 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 64 mg/Kg ☼ 01/27/16 21:05 01/29/16 03:03 1 [C24-C36]
240
Capric Acid (Surr) 0.02 0 - 1 01/27/16 21:05 01/29/16 03:03 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 42 38 - 148 01/27/16 21:05 01/29/16 03:03 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 7.5 4.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Barium 210 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4
Beryllium 0.78 0.49 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Cadmium ND 0.61 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Chromium 64 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Cobalt 16 0.98 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4
Copper 43 7.4 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4
Lead 11 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4
Molybdenum ND 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Nickel 88 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4
Selenium ND 4.9 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 Silver ND 1.2 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4
Thallium ND 2.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:21 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Date Collected: 01/22/16 11:10 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 87.1
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 57 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1
Benzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1
Dichlorobromomethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Bromobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Chlorobromomethane ND 23 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Bromoform ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Bromomethane ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 2-Butanone (MEK) ND 57 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 n-Butylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 sec-Butylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 tert-Butylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Carbon disulfide ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Carbon tetrachloride ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Chlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Chloroethane ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Chloroform ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Chloromethane ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 2-Chlorotoluene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 4-Chlorotoluene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Chlorodibromomethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2-Dichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,3-Dichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,4-Dichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,3-Dichloropropane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,1-Dichloropropene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2-Dibromo-3-Chloropropane ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Ethylene Dibromide ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Dibromomethane ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Dichlorodifluoromethane ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,1-Dichloroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2-Dichloroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,1-Dichloroethene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 cis-1,2-Dichloroethene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 trans-1,2-Dichloroethene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2-Dichloropropane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 cis-1,3-Dichloropropene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 trans-1,3-Dichloropropene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Ethylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Hexachlorobutadiene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 2-Hexanone ND 57 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Isopropylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 4-Isopropyltoluene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Methylene Chloride ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 4-Methyl-2-pentanone (MIBK) ND 57 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Naphthalene ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 N-Propylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Styrene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1
1,1,1,2-Tetrachloroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 TestAmerica Pleasanton

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San Jose City CouncilAugust 9, 2022

San Jose City Council
August 9, 2022