Exhibit D - Initial Study-MND and Appendices — San Jose City Council, August 9, 2022 (part 7 of 10)

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Date Collected: 01/22/16 11:10 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 87.1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Toluene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1
1,2,3-Trichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2,4-Trichlorobenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,1,1-Trichloroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,1,2-Trichloroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Trichloroethene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Trichlorofluoromethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2,3-Trichloropropane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,2,4-Trimethylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 1,3,5-Trimethylbenzene ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Vinyl acetate ND 23 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Vinyl chloride ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Xylenes, Total ND 11 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 2,2-Dichloropropane ND 5.7 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 Gasoline Range Organics (GRO) 290 ug/Kg ☼ 01/27/16 19:40 01/29/16 03:40 1 -C5-C12
ND
4-Bromofluorobenzene 86 45 - 131 01/27/16 19:40 01/29/16 03:40 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 115 60 - 140 01/27/16 19:40 01/29/16 03:40 1 Toluene-d8 (Surr) 96 58 - 140 01/27/16 19:40 01/29/16 03:40 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 400 23 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:35 20 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 1100 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:35 20 [C24-C36]
2100
Capric Acid (Surr) 0 0 - 1 01/27/16 21:05 01/29/16 02:35 20 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 0 X D 38 - 148 01/27/16 21:05 01/29/16 02:35 20 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Endrin aldehyde ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Endrin ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2
Endrin ketone ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Heptachlor ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Heptachlor epoxide ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 4,4'-DDT ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 4,4'-DDE ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 4,4'-DDD ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Endosulfan I ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Endosulfan II ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 alpha-BHC ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 beta-BHC ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Date Collected: 01/22/16 11:10 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 87.1
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
gamma-BHC (Lindane) ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac delta-BHC ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Endosulfan sulfate ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Methoxychlor ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Toxaphene ND 90 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Chlordane (technical) ND 90 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 alpha-Chlordane ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 gamma-Chlordane ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Hexachlorobenzene ND 4.5 ug/Kg ☼ 01/27/16 15:48 01/28/16 19:00 2 Tetrachloro-m-xylene 67 57 - 122 01/27/16 15:48 01/28/16 19:00 2 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 119 21 - 136 01/27/16 15:48 01/28/16 19:00 2 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
PCB-1232 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
PCB-1242 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
PCB-1248 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
PCB-1254 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
PCB-1260 ND 56 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:38 1
Tetrachloro-m-xylene 78 45 - 132 01/27/16 15:59 01/28/16 18:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 68 42 - 146 01/27/16 15:59 01/28/16 18:38 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 0.50 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 1.0 1.0 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1 Barium 33 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4
Beryllium 0.20 0.10 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1 Cadmium ND 0.12 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1 Chromium 7.1 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4 Cobalt 1.6 0.80 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4 Copper 2.4 1.5 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1
Lead 3.5 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4
Molybdenum 0.89 0.50 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1 Nickel 4.8 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4
Selenium ND 1.0 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1 Silver ND 0.25 mg/Kg ☼ 01/26/16 14:13 01/28/16 16:27 1
Thallium ND 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4 Vanadium 9.4 2.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4 Zinc 10 6.0 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:26 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.024 0.010 mg/Kg ☼ 01/26/16 17:30 01/27/16 17:45 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-7.5-8' Lab Sample ID: 720-69933-44 Date Collected: 01/22/16 11:12 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.6
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 63 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1
Benzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1
Dichlorobromomethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Bromobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Chlorobromomethane ND 25 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Bromoform ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Bromomethane ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 2-Butanone (MEK) ND 63 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 n-Butylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 sec-Butylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 tert-Butylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Carbon disulfide ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Carbon tetrachloride ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Chlorobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Chloroethane ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Chloroform ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Chloromethane ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 2-Chlorotoluene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 4-Chlorotoluene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Chlorodibromomethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2-Dichlorobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,3-Dichlorobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,4-Dichlorobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,3-Dichloropropane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,1-Dichloropropene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2-Dibromo-3-Chloropropane ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Ethylene Dibromide ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Dibromomethane ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Dichlorodifluoromethane ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,1-Dichloroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2-Dichloroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,1-Dichloroethene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 cis-1,2-Dichloroethene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 trans-1,2-Dichloroethene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2-Dichloropropane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 cis-1,3-Dichloropropene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 trans-1,3-Dichloropropene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Ethylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Hexachlorobutadiene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 2-Hexanone ND 63 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Isopropylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 4-Isopropyltoluene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Methylene Chloride ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 4-Methyl-2-pentanone (MIBK) ND 63 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Naphthalene ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 N-Propylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Styrene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1
1,1,1,2-Tetrachloroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-7.5-8' Lab Sample ID: 720-69933-44 Date Collected: 01/22/16 11:12 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.6
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Toluene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1
1,2,3-Trichlorobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2,4-Trichlorobenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,1,1-Trichloroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,1,2-Trichloroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Trichloroethene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Trichlorofluoromethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2,3-Trichloropropane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,2,4-Trimethylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 1,3,5-Trimethylbenzene ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Vinyl acetate ND 25 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Vinyl chloride ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Xylenes, Total ND 13 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 2,2-Dichloropropane ND 6.3 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/29/16 19:09 01/30/16 00:38 1 -C5-C12
ND
4-Bromofluorobenzene 83 45 - 131 01/29/16 19:09 01/30/16 00:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 115 60 - 140 01/29/16 19:09 01/30/16 00:38 1 Toluene-d8 (Surr) 95 58 - 140 01/29/16 19:09 01/30/16 00:38 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 2.4 1.4 mg/Kg ☼ 01/27/16 21:05 01/28/16 23:10 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 68 mg/Kg ☼ 01/27/16 21:05 01/28/16 23:10 1 Capric Acid (Surr) 0.02 0 - 1 01/27/16 21:05 01/28/16 23:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 64 38 - 148 01/27/16 21:05 01/28/16 23:10 1 Method: 8081A - Organochlorine Pesticides (GC)
RL MDL
Aldrin ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Endrin aldehyde ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Endrin ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1
Endrin ketone ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Heptachlor ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Heptachlor epoxide ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 4,4'-DDT ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 4,4'-DDE ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 4,4'-DDD ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Endosulfan I ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Endosulfan II ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 alpha-BHC ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 beta-BHC ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 gamma-BHC (Lindane) ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-7.5-8' Lab Sample ID: 720-69933-44 Date Collected: 01/22/16 11:12 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.6
Method: 8081A - Organochlorine Pesticides (GC) (Continued) RL MDL
delta-BHC ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Endosulfan sulfate ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Methoxychlor ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Toxaphene ND 54 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Chlordane (technical) ND 54 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 alpha-Chlordane ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 gamma-Chlordane ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Hexachlorobenzene ND 2.7 ug/Kg ☼ 01/27/16 15:48 01/28/16 17:36 1 Tetrachloro-m-xylene 109 57 - 122 01/27/16 15:48 01/28/16 17:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 99 21 - 136 01/27/16 15:48 01/28/16 17:36 1 Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography RL MDL
PCB-1016 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
PCB-1232 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
PCB-1242 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
PCB-1248 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
PCB-1254 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
PCB-1260 ND 68 ug/Kg ☼ 01/27/16 15:59 01/28/16 18:55 1
Tetrachloro-m-xylene 77 45 - 132 01/27/16 15:59 01/28/16 18:55 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 69 42 - 146 01/27/16 15:59 01/28/16 18:55 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 5.6 3.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Barium 250 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Beryllium 0.74 0.36 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Cadmium ND 0.46 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Chromium 72 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Cobalt 15 0.73 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Copper 38 5.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Lead 11 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Molybdenum ND 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Nickel 90 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Selenium ND 3.6 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Silver ND 0.91 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Thallium ND 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Vanadium 57 1.8 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4 Zinc 73 5.5 mg/Kg ☼ 01/26/16 14:13 01/27/16 23:31 4
Method: 7471A - Mercury (CVAA)
RL MDL
Mercury 0.11 F1 0.012 mg/Kg ☼ 01/26/16 18:10 01/27/16 19:55 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-11-3.5-4' Lab Sample ID: 720-69933-47 Date Collected: 01/22/16 12:00 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 79.5
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1
Benzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1
Dichlorobromomethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Bromobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Chlorobromomethane ND 24 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Bromoform ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Bromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 2-Butanone (MEK) ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 n-Butylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 sec-Butylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 tert-Butylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Carbon disulfide ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Carbon tetrachloride ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Chlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Chloroethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Chloroform ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Chloromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 2-Chlorotoluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 4-Chlorotoluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Chlorodibromomethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,3-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,4-Dichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,3-Dichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,1-Dichloropropene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Ethylene Dibromide ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Dibromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,1-Dichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2-Dichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,1-Dichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 cis-1,2-Dichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 trans-1,2-Dichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2-Dichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 cis-1,3-Dichloropropene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 trans-1,3-Dichloropropene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Ethylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Hexachlorobutadiene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 2-Hexanone ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Isopropylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 4-Isopropyltoluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Methylene Chloride ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 4-Methyl-2-pentanone (MIBK) ND 60 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Naphthalene ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 N-Propylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Styrene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1
1,1,1,2-Tetrachloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-11-3.5-4' Lab Sample ID: 720-69933-47 Date Collected: 01/22/16 12:00 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 79.5
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Toluene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1
1,2,3-Trichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2,4-Trichlorobenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,1,1-Trichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,1,2-Trichloroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Trichloroethene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Trichlorofluoromethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2,3-Trichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,2,4-Trimethylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 1,3,5-Trimethylbenzene ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Vinyl acetate ND 24 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Vinyl chloride ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Xylenes, Total ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 2,2-Dichloropropane ND 6.0 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 Gasoline Range Organics (GRO) 300 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:08 1 -C5-C12
ND
4-Bromofluorobenzene 87 45 - 131 01/29/16 19:09 01/30/16 01:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 114 60 - 140 01/29/16 19:09 01/30/16 01:08 1 Toluene-d8 (Surr) 99 58 - 140 01/29/16 19:09 01/30/16 01:08 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 90 3.7 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:35 3 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics 190 mg/Kg ☼ 01/27/16 21:05 01/29/16 02:35 3 [C24-C36]
300
Capric Acid (Surr) 0.3 0 - 1 01/27/16 21:05 01/29/16 02:35 3 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 71 38 - 148 01/27/16 21:05 01/29/16 02:35 3 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND F1 F2 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 7.8 4.7 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Barium 140 F1 F2 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Beryllium ND 0.47 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Cadmium ND 0.59 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Chromium 480 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Cobalt 64 0.94 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4
Copper 35 7.1 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4
Lead 44 F1 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4
Molybdenum ND 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Nickel 1100 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Selenium ND 4.7 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 Silver ND 1.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4
Thallium ND 2.4 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:42 4 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-11-7.5-8' Lab Sample ID: 720-69933-48 Date Collected: 01/22/16 12:02 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 79.5
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Methyl tert-butyl ether ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 62 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1
Benzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1
Dichlorobromomethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Bromobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Chlorobromomethane ND 25 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Bromoform ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Bromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 2-Butanone (MEK) ND 62 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 n-Butylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 sec-Butylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 tert-Butylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Carbon disulfide ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Carbon tetrachloride ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Chlorobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Chloroethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Chloroform ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Chloromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 2-Chlorotoluene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 4-Chlorotoluene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Chlorodibromomethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2-Dichlorobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,3-Dichlorobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,4-Dichlorobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,3-Dichloropropane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,1-Dichloropropene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2-Dibromo-3-Chloropropane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Ethylene Dibromide ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Dibromomethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Dichlorodifluoromethane ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,1-Dichloroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2-Dichloroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,1-Dichloroethene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 cis-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 trans-1,2-Dichloroethene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 cis-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 trans-1,3-Dichloropropene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Ethylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Hexachlorobutadiene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 2-Hexanone ND 62 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Isopropylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 4-Isopropyltoluene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Methylene Chloride ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 4-Methyl-2-pentanone (MIBK) ND 62 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Naphthalene ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 N-Propylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Styrene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1
1,1,1,2-Tetrachloroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 TestAmerica Pleasanton

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Client Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-11-7.5-8' Lab Sample ID: 720-69933-48 Date Collected: 01/22/16 12:02 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 79.5
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL
1,1,2,2-Tetrachloroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Tetrachloroethene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Toluene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1
1,2,3-Trichlorobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2,4-Trichlorobenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,1,1-Trichloroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,1,2-Trichloroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Trichloroethene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Trichlorofluoromethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2,3-Trichloropropane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,2,4-Trimethylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 1,3,5-Trimethylbenzene ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Vinyl acetate ND 25 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Vinyl chloride ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Xylenes, Total ND 12 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 2,2-Dichloropropane ND 6.2 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 Gasoline Range Organics (GRO) 310 ug/Kg ☼ 01/29/16 19:09 01/30/16 01:39 1 -C5-C12
ND
4-Bromofluorobenzene 82 45 - 131 01/29/16 19:09 01/30/16 01:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 120 60 - 140 01/29/16 19:09 01/30/16 01:39 1 Toluene-d8 (Surr) 94 58 - 140 01/29/16 19:09 01/30/16 01:39 1 Method: 8015B - Diesel Range Organics (DRO) (GC) - Silica Gel Cleanup RL MDL
Diesel Range Organics [C10-C28] 17 1.2 mg/Kg ☼ 01/27/16 21:05 01/29/16 00:08 1 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 62 mg/Kg ☼ 01/27/16 21:05 01/29/16 00:08 1 Capric Acid (Surr) 0.01 0 - 1 01/27/16 21:05 01/29/16 00:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac p-Terphenyl 45 38 - 148 01/27/16 21:05 01/29/16 00:08 1 Method: 6010B - Metals (ICP)
RL MDL
Antimony ND 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic 9.4 4.3 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Barium 210 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4
Beryllium 0.60 0.43 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Cadmium ND 0.54 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Chromium 74 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Cobalt 17 0.86 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4
Copper 41 6.5 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4
Lead 11 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4
Molybdenum ND 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Nickel 100 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4
Selenium ND 4.3 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Silver ND 1.1 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4
Thallium ND 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 Vanadium 55 2.2 mg/Kg ☼ 01/26/16 14:58 01/28/16 18:46 4 TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 720-196192/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 196192
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/25/16 19:20 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/25/16 19:20 1
Benzene ND 0.50 ug/L 01/25/16 19:20 1
Dichlorobromomethane ND 0.50 ug/L 01/25/16 19:20 1
Bromobenzene ND 1.0 ug/L 01/25/16 19:20 1
Chlorobromomethane ND 1.0 ug/L 01/25/16 19:20 1
Bromoform ND 1.0 ug/L 01/25/16 19:20 1
Bromomethane ND 1.0 ug/L 01/25/16 19:20 1
2-Butanone (MEK) ND 50 ug/L 01/25/16 19:20 1
n-Butylbenzene ND 1.0 ug/L 01/25/16 19:20 1
sec-Butylbenzene ND 1.0 ug/L 01/25/16 19:20 1
tert-Butylbenzene ND 1.0 ug/L 01/25/16 19:20 1
Carbon disulfide ND 5.0 ug/L 01/25/16 19:20 1
Carbon tetrachloride ND 0.50 ug/L 01/25/16 19:20 1
Chlorobenzene ND 0.50 ug/L 01/25/16 19:20 1
Chloroethane ND 1.0 ug/L 01/25/16 19:20 1
Chloroform ND 1.0 ug/L 01/25/16 19:20 1
Chloromethane ND 1.0 ug/L 01/25/16 19:20 1
2-Chlorotoluene ND 0.50 ug/L 01/25/16 19:20 1
4-Chlorotoluene ND 0.50 ug/L 01/25/16 19:20 1
Chlorodibromomethane ND 0.50 ug/L 01/25/16 19:20 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/25/16 19:20 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/25/16 19:20 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/25/16 19:20 1
1,3-Dichloropropane ND 1.0 ug/L 01/25/16 19:20 1
1,1-Dichloropropene ND 0.50 ug/L 01/25/16 19:20 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/25/16 19:20 1 Ethylene Dibromide ND 0.50 ug/L 01/25/16 19:20 1
Dibromomethane ND 0.50 ug/L 01/25/16 19:20 1
Dichlorodifluoromethane ND 0.50 ug/L 01/25/16 19:20 1
1,1-Dichloroethane ND 0.50 ug/L 01/25/16 19:20 1
1,2-Dichloroethane ND 0.50 ug/L 01/25/16 19:20 1
1,1-Dichloroethene ND 0.50 ug/L 01/25/16 19:20 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/25/16 19:20 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/25/16 19:20 1
1,2-Dichloropropane ND 0.50 ug/L 01/25/16 19:20 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/25/16 19:20 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/25/16 19:20 1 Ethylbenzene ND 0.50 ug/L 01/25/16 19:20 1
Hexachlorobutadiene ND 1.0 ug/L 01/25/16 19:20 1
2-Hexanone ND 50 ug/L 01/25/16 19:20 1
Isopropylbenzene ND 0.50 ug/L 01/25/16 19:20 1
4-Isopropyltoluene ND 1.0 ug/L 01/25/16 19:20 1
Methylene Chloride ND 5.0 ug/L 01/25/16 19:20 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/25/16 19:20 1 Naphthalene ND 1.0 ug/L 01/25/16 19:20 1
N-Propylbenzene ND 1.0 ug/L 01/25/16 19:20 1
Styrene ND 0.50 ug/L 01/25/16 19:20 1
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 100 94.6 ug/L 95 26 - 180
Benzene 25.0 22.5 ug/L 90 79 - 130
Dichlorobromomethane 25.0 26.9 ug/L 108 70 - 130
Bromobenzene 25.0 24.1 ug/L 96 70 - 130
Chlorobromomethane 25.0 26.8 ug/L 107 70 - 130
Bromoform 25.0 29.8 ug/L 119 68 - 136
Bromomethane 25.0 31.2 ug/L 125 43 - 151
2-Butanone (MEK) 100 118 ug/L 118 54 - 130
n-Butylbenzene 25.0 21.0 ug/L 84 70 - 142
sec-Butylbenzene 25.0 22.1 ug/L 88 70 - 134
tert-Butylbenzene 25.0 23.1 ug/L 92 70 - 135
Carbon disulfide 25.0 22.8 ug/L 91 58 - 130
Carbon tetrachloride 25.0 30.0 ug/L 120 70 - 146
Chlorobenzene 25.0 24.6 ug/L 99 70 - 130
Chloroethane 25.0 24.3 ug/L 97 62 - 138
Chloroform 25.0 25.8 ug/L 103 70 - 130
Chloromethane 25.0 24.1 ug/L 96 52 - 175
2-Chlorotoluene 25.0 22.8 ug/L 91 70 - 130
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Chlorodibromomethane 25.0 28.1 ug/L 113 70 - 145
1,2-Dichlorobenzene 25.0 24.1 ug/L 96 70 - 130
1,3-Dichlorobenzene 25.0 23.8 ug/L 95 70 - 130
1,4-Dichlorobenzene 25.0 23.9 ug/L 95 70 - 130
1,3-Dichloropropane 25.0 23.8 ug/L 95 70 - 130
1,1-Dichloropropene 25.0 25.0 ug/L 100 70 - 130
1,2-Dibromo-3-Chloropropane 25.0 26.0 ug/L 104 70 - 136 Ethylene Dibromide 25.0 25.3 ug/L 101 70 - 130
Dibromomethane 25.0 26.3 ug/L 105 70 - 130
Dichlorodifluoromethane 25.0 37.0 * ug/L 148 34 - 132
1,1-Dichloroethane 25.0 22.9 ug/L 92 70 - 130
1,2-Dichloroethane 25.0 27.9 ug/L 112 61 - 132
1,1-Dichloroethene 25.0 22.6 ug/L 91 64 - 128
cis-1,2-Dichloroethene 25.0 23.8 ug/L 95 70 - 130
trans-1,2-Dichloroethene 25.0 23.8 ug/L 95 68 - 130
1,2-Dichloropropane 25.0 21.6 ug/L 86 70 - 130
cis-1,3-Dichloropropene 25.0 25.5 ug/L 102 70 - 130
trans-1,3-Dichloropropene 25.0 27.5 ug/L 110 70 - 140
Ethylbenzene 25.0 21.8 ug/L 87 80 - 120
Hexachlorobutadiene 25.0 25.8 ug/L 103 70 - 130
2-Hexanone 100 100 ug/L 100 60 - 164
Isopropylbenzene 25.0 23.6 ug/L 95 70 - 130
4-Isopropyltoluene 25.0 22.4 ug/L 90 70 - 130
Methylene Chloride 25.0 22.8 ug/L 91 70 - 147
4-Methyl-2-pentanone (MIBK) 100 102 ug/L 102 58 - 130
Naphthalene 25.0 23.0 ug/L 92 70 - 130
N-Propylbenzene 25.0 22.7 ug/L 91 70 - 130
Styrene 25.0 22.4 ug/L 90 70 - 130
1,1,1,2-Tetrachloroethane 25.0 25.9 ug/L 104 70 - 130
1,1,2,2-Tetrachloroethane 25.0 21.7 ug/L 87 70 - 130
Tetrachloroethene 25.0 25.7 ug/L 103 70 - 130
Toluene 25.0 22.1 ug/L 88 78 - 120
1,2,3-Trichlorobenzene 25.0 24.8 ug/L 99 70 - 130
1,2,4-Trichlorobenzene 25.0 25.0 ug/L 100 70 - 130
1,1,1-Trichloroethane 25.0 28.7 ug/L 115 70 - 130
1,1,2-Trichloroethane 25.0 23.2 ug/L 93 70 - 130
Trichloroethene 25.0 26.4 ug/L 106 70 - 130
Trichlorofluoromethane 25.0 34.0 * ug/L 136 66 - 132
1,2,3-Trichloropropane 25.0 24.7 ug/L 99 70 - 130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

25.0 28.6 ug/L 114 42 - 162
1,2,4-Trimethylbenzene 25.0 23.5 ug/L 94 70 - 132
1,3,5-Trimethylbenzene 25.0 22.1 ug/L 88 70 - 130
Vinyl acetate 25.0 21.0 ug/L 84 43 - 163
Vinyl chloride 25.0 27.9 ug/L 112 54 - 135
m-Xylene & p-Xylene 25.0 24.7 ug/L 99 70 - 142
o-Xylene 25.0 24.9 ug/L 100 70 - 130
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 67 - 130
Surrogate
104

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 115 72 - 130
Toluene-d8 (Surr) 99 70 - 130
Lab Sample ID: LCSD 720-196192/6 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 196192
Methyl tert-butyl ether 25.0 26.6 ug/L 107 62 - 130 1 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 100 97.5 ug/L 97 26 - 180 3 30
Benzene 25.0 22.5 ug/L 90 79 - 130 0 20
Dichlorobromomethane 25.0 26.5 ug/L 106 70 - 130 2 20
Bromobenzene 25.0 24.7 ug/L 99 70 - 130 3 20
Chlorobromomethane 25.0 26.2 ug/L 105 70 - 130 2 20
Bromoform 25.0 29.6 ug/L 118 68 - 136 1 20
Bromomethane 25.0 29.1 ug/L 116 43 - 151 7 20
2-Butanone (MEK) 100 118 ug/L 118 54 - 130 0 20
n-Butylbenzene 25.0 20.7 ug/L 83 70 - 142 1 20
sec-Butylbenzene 25.0 22.5 ug/L 90 70 - 134 2 20
tert-Butylbenzene 25.0 23.5 ug/L 94 70 - 135 2 20
Carbon disulfide 25.0 22.5 ug/L 90 58 - 130 1 20
Carbon tetrachloride 25.0 29.7 ug/L 119 70 - 146 1 20
Chlorobenzene 25.0 24.4 ug/L 97 70 - 130 1 20
Chloroethane 25.0 24.3 ug/L 97 62 - 138 0 20
Chloroform 25.0 25.7 ug/L 103 70 - 130 0 20
Chloromethane 25.0 22.7 ug/L 91 52 - 175 6 20
2-Chlorotoluene 25.0 23.6 ug/L 94 70 - 130 3 20
4-Chlorotoluene 25.0 23.0 ug/L 92 70 - 130 3 20
Chlorodibromomethane 25.0 28.0 ug/L 112 70 - 145 0 20
1,2-Dichlorobenzene 25.0 23.9 ug/L 95 70 - 130 1 20
1,3-Dichlorobenzene 25.0 23.7 ug/L 95 70 - 130 1 20
1,4-Dichlorobenzene 25.0 23.9 ug/L 96 70 - 130 0 20
1,3-Dichloropropane 25.0 23.6 ug/L 94 70 - 130 1 20
1,1-Dichloropropene 25.0 24.6 ug/L 98 70 - 130 2 20
1,2-Dibromo-3-Chloropropane 25.0 26.0 ug/L 104 70 - 136 0 20 Ethylene Dibromide 25.0 25.3 ug/L 101 70 - 130 0 20
Dibromomethane 25.0 25.7 ug/L 103 70 - 130 2 20
Dichlorodifluoromethane 25.0 34.3 * ug/L 137 34 - 132 8 20 1,1-Dichloroethane 25.0 22.8 ug/L 91 70 - 130 0 20
1,2-Dichloroethane 25.0 27.4 ug/L 109 61 - 132 2 20
1,1-Dichloroethene 25.0 21.9 ug/L 87 64 - 128 3 20
cis-1,2-Dichloroethene 25.0 23.6 ug/L 94 70 - 130 1 20
trans-1,2-Dichloroethene 25.0 24.0 ug/L 96 68 - 130 1 20 1,2-Dichloropropane 25.0 21.3 ug/L 85 70 - 130 1 20
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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
trans-1,3-Dichloropropene 25.0 27.2 ug/L 109 70 - 140 1 20 Ethylbenzene 25.0 21.6 ug/L 86 80 - 120 1 20
Hexachlorobutadiene 25.0 24.9 ug/L 100 70 - 130 4 20
2-Hexanone 100 100 ug/L 100 60 - 164 0 20
Isopropylbenzene 25.0 23.1 ug/L 92 70 - 130 2 20
4-Isopropyltoluene 25.0 22.4 ug/L 90 70 - 130 0 20
Methylene Chloride 25.0 22.7 ug/L 91 70 - 147 1 20
4-Methyl-2-pentanone (MIBK) 100 102 ug/L 102 58 - 130 0 20 Naphthalene 25.0 22.7 ug/L 91 70 - 130 1 20
N-Propylbenzene 25.0 23.3 ug/L 93 70 - 130 3 20
Styrene 25.0 22.0 ug/L 88 70 - 130 2 20
1,1,1,2-Tetrachloroethane 25.0 25.6 ug/L 102 70 - 130 1 20 1,1,2,2-Tetrachloroethane 25.0 21.7 ug/L 87 70 - 130 0 20 Tetrachloroethene 25.0 25.5 ug/L 102 70 - 130 1 20
Toluene 25.0 22.1 ug/L 88 78 - 120 0 20
1,2,3-Trichlorobenzene 25.0 24.0 ug/L 96 70 - 130 3 20
1,2,4-Trichlorobenzene 25.0 23.7 ug/L 95 70 - 130 5 20
1,1,1-Trichloroethane 25.0 28.4 ug/L 113 70 - 130 1 20
1,1,2-Trichloroethane 25.0 22.9 ug/L 92 70 - 130 1 20
Trichloroethene 25.0 26.2 ug/L 105 70 - 130 1 20
Trichlorofluoromethane 25.0 32.0 ug/L 128 66 - 132 6 20 1,2,3-Trichloropropane 25.0 25.9 ug/L 104 70 - 130 5 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne

25.0 26.7 ug/L 107 42 - 162 7 20
1,2,4-Trimethylbenzene 25.0 23.7 ug/L 95 70 - 132 1 20
1,3,5-Trimethylbenzene 25.0 22.4 ug/L 90 70 - 130 2 20
Vinyl acetate 25.0 20.3 ug/L 81 43 - 163 3 20
Vinyl chloride 25.0 26.6 ug/L 107 54 - 135 5 20
m-Xylene & p-Xylene 25.0 24.2 ug/L 97 70 - 142 2 20
o-Xylene 25.0 24.5 ug/L 98 70 - 130 2 20
2,2-Dichloropropane 25.0 29.1 ug/L 116 70 - 140 8 20
4-Bromofluorobenzene 67 - 130
Surrogate
100

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 111 72 - 130
Toluene-d8 (Surr) 99 70 - 130
Lab Sample ID: 720-69933-12 MS Client Sample ID: GP-2-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326 Prep Batch: 196202
Methyl tert-butyl ether ND 66.3 72.2 ug/Kg ☼ 109 69 - 130 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Acetone ND 265 323 ug/Kg ☼ 122 37 - 150
Benzene ND 66.3 73.0 ug/Kg ☼ 110 70 - 130
Dichlorobromomethane ND 66.3 67.7 ug/Kg ☼ 102 64 - 135
Bromobenzene ND 66.3 82.6 ug/Kg ☼ 125 70 - 130
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Limits
Bromoform ND 66.3 71.5 ug/Kg ☼ 108 58 - 132
Bromomethane ND 66.3 65.7 ug/Kg ☼ 99 56 - 130
2-Butanone (MEK) ND 265 269 ug/Kg ☼ 102 41 - 150
n-Butylbenzene ND 66.3 70.3 ug/Kg ☼ 106 60 - 145
sec-Butylbenzene ND 66.3 75.5 ug/Kg ☼ 114 64 - 137
tert-Butylbenzene ND 66.3 78.4 ug/Kg ☼ 118 63 - 134
Carbon disulfide ND 66.3 63.1 ug/Kg ☼ 95 10 - 150
Carbon tetrachloride ND 66.3 65.6 ug/Kg ☼ 99 54 - 130
Chlorobenzene ND 66.3 70.3 ug/Kg ☼ 106 70 - 130
Chloroethane ND 66.3 65.7 ug/Kg ☼ 99 61 - 130
Chloroform ND 66.3 62.4 ug/Kg ☼ 94 67 - 130
Chloromethane ND 66.3 66.6 ug/Kg ☼ 101 50 - 131
2-Chlorotoluene ND 66.3 79.7 ug/Kg ☼ 120 70 - 130
4-Chlorotoluene ND 66.3 77.1 ug/Kg ☼ 116 70 - 130
Chlorodibromomethane ND 66.3 64.8 ug/Kg ☼ 98 60 - 141
1,2-Dichlorobenzene ND 66.3 71.0 ug/Kg ☼ 107 70 - 130
1,3-Dichlorobenzene ND 66.3 70.7 ug/Kg ☼ 107 70 - 130
1,4-Dichlorobenzene ND 66.3 70.7 ug/Kg ☼ 107 70 - 130
1,3-Dichloropropane ND 66.3 64.0 ug/Kg ☼ 96 70 - 130
1,1-Dichloropropene ND 66.3 69.0 ug/Kg ☼ 104 67 - 130
1,2-Dibromo-3-Chloropropane ND 66.3 67.8 ug/Kg ☼ 102 57 - 130 Ethylene Dibromide ND 66.3 66.3 ug/Kg ☼ 100 66 - 135
Dibromomethane ND 66.3 66.0 ug/Kg ☼ 100 65 - 131
Dichlorodifluoromethane ND 66.3 77.6 ug/Kg ☼ 117 38 - 130 1,1-Dichloroethane ND 66.3 68.0 ug/Kg ☼ 103 67 - 130
1,2-Dichloroethane ND 66.3 65.6 ug/Kg ☼ 99 70 - 130
1,1-Dichloroethene ND 66.3 61.9 ug/Kg ☼ 93 64 - 130
cis-1,2-Dichloroethene ND 66.3 66.4 ug/Kg ☼ 100 68 - 131 trans-1,2-Dichloroethene ND 66.3 69.8 ug/Kg ☼ 105 70 - 130 1,2-Dichloropropane ND 66.3 71.6 ug/Kg ☼ 108 65 - 133
cis-1,3-Dichloropropene ND 66.3 73.1 ug/Kg ☼ 110 46 - 139 trans-1,3-Dichloropropene ND 66.3 73.0 ug/Kg ☼ 110 55 - 131 Ethylbenzene ND 66.3 71.9 ug/Kg ☼ 108 65 - 130
Hexachlorobutadiene ND 66.3 53.0 ug/Kg ☼ 80 58 - 132
2-Hexanone ND 265 281 ug/Kg ☼ 106 44 - 150
Isopropylbenzene ND 66.3 66.8 ug/Kg ☼ 101 65 - 130
4-Isopropyltoluene ND 66.3 74.1 ug/Kg ☼ 112 69 - 134
Methylene Chloride ND 66.3 64.6 ug/Kg ☼ 98 63 - 130
4-Methyl-2-pentanone (MIBK) ND 265 318 ug/Kg ☼ 120 51 - 140 Naphthalene ND 66.3 53.9 ug/Kg ☼ 81 45 - 146
N-Propylbenzene ND 66.3 80.3 ug/Kg ☼ 121 70 - 130
Styrene ND 66.3 67.0 ug/Kg ☼ 101 58 - 135
1,1,1,2-Tetrachloroethane ND 66.3 78.7 ug/Kg ☼ 119 64 - 133 1,1,2,2-Tetrachloroethane ND 66.3 84.7 ug/Kg ☼ 128 70 - 131 Tetrachloroethene ND 66.3 67.0 ug/Kg ☼ 101 67 - 130
Toluene ND 66.3 75.2 ug/Kg ☼ 113 70 - 130
1,2,3-Trichlorobenzene ND 66.3 49.6 ug/Kg ☼ 75 58 - 138 TestAmerica Pleasanton

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Limits
1,1,1-Trichloroethane ND 66.3 64.8 ug/Kg ☼ 98 57 - 133
1,1,2-Trichloroethane ND 66.3 70.4 ug/Kg ☼ 106 68 - 132 Trichloroethene ND 66.3 71.3 ug/Kg ☼ 108 66 - 130
Trichlorofluoromethane ND 66.3 65.0 ug/Kg ☼ 98 61 - 130 1,2,3-Trichloropropane ND 66.3 82.2 ug/Kg ☼ 124 62 - 150 1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 66.3 63.5 ug/Kg ☼ 96 52 - 130
1,2,4-Trimethylbenzene ND 66.3 79.3 ug/Kg ☼ 120 64 - 140 1,3,5-Trimethylbenzene ND 66.3 81.6 ug/Kg ☼ 123 67 - 134 Vinyl acetate ND F1 66.3 ND F1 ug/Kg ☼ 0 52 - 150
Vinyl chloride ND 66.3 68.8 ug/Kg ☼ 104 62 - 130
m-Xylene & p-Xylene ND 66.3 71.7 ug/Kg ☼ 108 70 - 130
o-Xylene ND 66.3 67.6 ug/Kg ☼ 102 68 - 130
2,2-Dichloropropane ND 66.3 66.4 ug/Kg ☼ 100 63 - 130
4-Bromofluorobenzene 45 - 131
Surrogate
98 MS MS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 92 60 - 140
Toluene-d8 (Surr) 106 58 - 140
Lab Sample ID: 720-69933-12 MSD Client Sample ID: GP-2-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326 Prep Batch: 196202
Methyl tert-butyl ether ND 63.0 71.0 ug/Kg ☼
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Acetone ND 252 360 ug/Kg ☼
Benzene ND 63.0 68.2 ug/Kg ☼
Dichlorobromomethane ND 63.0 64.3 ug/Kg ☼
Bromobenzene ND 63.0 80.6 ug/Kg ☼
Chlorobromomethane ND 63.0 67.7 ug/Kg ☼
Bromoform ND 63.0 71.6 ug/Kg ☼
Bromomethane ND 63.0 62.1 ug/Kg ☼
2-Butanone (MEK) ND 252 264 ug/Kg ☼
n-Butylbenzene ND 63.0 66.6 ug/Kg ☼
sec-Butylbenzene ND 63.0 74.3 ug/Kg ☼
tert-Butylbenzene ND 63.0 78.0 ug/Kg ☼
Carbon disulfide ND 63.0 58.5 ug/Kg ☼
Carbon tetrachloride ND 63.0 61.6 ug/Kg ☼
Chlorobenzene ND 63.0 65.6 ug/Kg ☼
Chloroethane ND 63.0 61.8 ug/Kg ☼
Chloroform ND 63.0 58.5 ug/Kg ☼
Chloromethane ND 63.0 62.8 ug/Kg ☼
2-Chlorotoluene ND 63.0 77.7 ug/Kg ☼
4-Chlorotoluene ND 63.0 74.1 ug/Kg ☼
Chlorodibromomethane ND 63.0 62.3 ug/Kg ☼
1,2-Dichlorobenzene ND 63.0 66.8 ug/Kg ☼
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MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
1,4-Dichlorobenzene ND 63.0 66.0 ug/Kg ☼
1,3-Dichloropropane ND 63.0 61.8 ug/Kg ☼
1,1-Dichloropropene ND 63.0 64.1 ug/Kg ☼
1,2-Dibromo-3-Chloropropane ND 63.0 76.1 ug/Kg ☼
Ethylene Dibromide ND 63.0 64.5 ug/Kg ☼
Dibromomethane ND 63.0 65.0 ug/Kg ☼
Dichlorodifluoromethane ND 63.0 74.9 ug/Kg ☼
1,1-Dichloroethane ND 63.0 64.3 ug/Kg ☼
1,2-Dichloroethane ND 63.0 63.5 ug/Kg ☼
1,1-Dichloroethene ND 63.0 57.8 ug/Kg ☼
cis-1,2-Dichloroethene ND 63.0 62.4 ug/Kg ☼
trans-1,2-Dichloroethene ND 63.0 65.4 ug/Kg ☼
1,2-Dichloropropane ND 63.0 67.8 ug/Kg ☼
cis-1,3-Dichloropropene ND 63.0 69.4 ug/Kg ☼
trans-1,3-Dichloropropene ND 63.0 69.0 ug/Kg ☼
Ethylbenzene ND 63.0 67.6 ug/Kg ☼
Hexachlorobutadiene ND 63.0 51.2 ug/Kg ☼
2-Hexanone ND 252 292 ug/Kg ☼
Isopropylbenzene ND 63.0 62.1 ug/Kg ☼
4-Isopropyltoluene ND 63.0 72.2 ug/Kg ☼
Methylene Chloride ND 63.0 61.4 ug/Kg ☼
4-Methyl-2-pentanone (MIBK) ND 252 336 ug/Kg ☼
Naphthalene ND 63.0 49.9 ug/Kg ☼
N-Propylbenzene ND 63.0 79.2 ug/Kg ☼
Styrene ND 63.0 61.3 ug/Kg ☼
1,1,1,2-Tetrachloroethane ND 63.0 75.8 ug/Kg ☼
1,1,2,2-Tetrachloroethane ND 63.0 93.8 ug/Kg ☼
Tetrachloroethene ND 63.0 61.7 ug/Kg ☼
Toluene ND 63.0 71.6 ug/Kg ☼
1,2,3-Trichlorobenzene ND 63.0 43.5 ug/Kg ☼
1,2,4-Trichlorobenzene ND 63.0 45.9 ug/Kg ☼
1,1,1-Trichloroethane ND 63.0 61.2 ug/Kg ☼
1,1,2-Trichloroethane ND 63.0 69.2 ug/Kg ☼
Trichloroethene ND 63.0 66.8 ug/Kg ☼
Trichlorofluoromethane ND 63.0 63.6 ug/Kg ☼
1,2,3-Trichloropropane ND 63.0 90.5 ug/Kg ☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 63.0 60.1 ug/Kg ☼
1,2,4-Trimethylbenzene ND 63.0 76.7 ug/Kg ☼
1,3,5-Trimethylbenzene ND 63.0 80.4 ug/Kg ☼
Vinyl acetate ND F1 63.0 ND ug/Kg ☼
Vinyl chloride ND 63.0 66.1 ug/Kg ☼
m-Xylene & p-Xylene ND 63.0 67.0 ug/Kg ☼
o-Xylene ND 63.0 63.8 ug/Kg ☼
2,2-Dichloropropane ND 63.0 62.1 ug/Kg ☼
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MSD MSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
Lab Sample ID: MB 720-196288/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196288
RL MDL
Methyl tert-butyl ether ND 5.0 ug/Kg 01/26/16 20:00 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/Kg 01/26/16 20:00 1
Benzene ND 5.0 ug/Kg 01/26/16 20:00 1
Dichlorobromomethane ND 5.0 ug/Kg 01/26/16 20:00 1
Bromobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
Chlorobromomethane ND 20 ug/Kg 01/26/16 20:00 1
Bromoform ND 5.0 ug/Kg 01/26/16 20:00 1
Bromomethane ND 10 ug/Kg 01/26/16 20:00 1
2-Butanone (MEK) ND 50 ug/Kg 01/26/16 20:00 1
n-Butylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
sec-Butylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
tert-Butylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
Carbon disulfide ND 5.0 ug/Kg 01/26/16 20:00 1
Carbon tetrachloride ND 5.0 ug/Kg 01/26/16 20:00 1
Chlorobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
Chloroethane ND 10 ug/Kg 01/26/16 20:00 1
Chloroform ND 5.0 ug/Kg 01/26/16 20:00 1
Chloromethane ND 10 ug/Kg 01/26/16 20:00 1
2-Chlorotoluene ND 5.0 ug/Kg 01/26/16 20:00 1
4-Chlorotoluene ND 5.0 ug/Kg 01/26/16 20:00 1
Chlorodibromomethane ND 5.0 ug/Kg 01/26/16 20:00 1
1,2-Dichlorobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
1,3-Dichlorobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
1,4-Dichlorobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
1,3-Dichloropropane ND 5.0 ug/Kg 01/26/16 20:00 1
1,1-Dichloropropene ND 5.0 ug/Kg 01/26/16 20:00 1
1,2-Dibromo-3-Chloropropane ND 10 ug/Kg 01/26/16 20:00 1 Ethylene Dibromide ND 5.0 ug/Kg 01/26/16 20:00 1
Dibromomethane ND 10 ug/Kg 01/26/16 20:00 1
Dichlorodifluoromethane ND 10 ug/Kg 01/26/16 20:00 1
1,1-Dichloroethane ND 5.0 ug/Kg 01/26/16 20:00 1
1,2-Dichloroethane ND 5.0 ug/Kg 01/26/16 20:00 1
1,1-Dichloroethene ND 5.0 ug/Kg 01/26/16 20:00 1
cis-1,2-Dichloroethene ND 5.0 ug/Kg 01/26/16 20:00 1
trans-1,2-Dichloroethene ND 5.0 ug/Kg 01/26/16 20:00 1
1,2-Dichloropropane ND 5.0 ug/Kg 01/26/16 20:00 1
cis-1,3-Dichloropropene ND 5.0 ug/Kg 01/26/16 20:00 1
trans-1,3-Dichloropropene ND 5.0 ug/Kg 01/26/16 20:00 1 Ethylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
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1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 720-196288/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196288
RL MDL
Hexachlorobutadiene ND 5.0 ug/Kg 01/26/16 20:00 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 2-Hexanone ND 50 ug/Kg 01/26/16 20:00 1
Isopropylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
4-Isopropyltoluene ND 5.0 ug/Kg 01/26/16 20:00 1
Methylene Chloride ND 10 ug/Kg 01/26/16 20:00 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/Kg 01/26/16 20:00 1 Naphthalene ND 10 ug/Kg 01/26/16 20:00 1
N-Propylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
Styrene ND 5.0 ug/Kg 01/26/16 20:00 1
1,1,1,2-Tetrachloroethane ND 5.0 ug/Kg 01/26/16 20:00 1 1,1,2,2-Tetrachloroethane ND 5.0 ug/Kg 01/26/16 20:00 1 Tetrachloroethene ND 5.0 ug/Kg 01/26/16 20:00 1
Toluene ND 5.0 ug/Kg 01/26/16 20:00 1
1,2,3-Trichlorobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
1,2,4-Trichlorobenzene ND 5.0 ug/Kg 01/26/16 20:00 1
1,1,1-Trichloroethane ND 5.0 ug/Kg 01/26/16 20:00 1
1,1,2-Trichloroethane ND 5.0 ug/Kg 01/26/16 20:00 1
Trichloroethene ND 5.0 ug/Kg 01/26/16 20:00 1
Trichlorofluoromethane ND 5.0 ug/Kg 01/26/16 20:00 1
1,2,3-Trichloropropane ND 5.0 ug/Kg 01/26/16 20:00 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.0 ug/Kg 01/26/16 20:00 1 1,2,4-Trimethylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
1,3,5-Trimethylbenzene ND 5.0 ug/Kg 01/26/16 20:00 1
Vinyl acetate ND 20 ug/Kg 01/26/16 20:00 1
Vinyl chloride ND 5.0 ug/Kg 01/26/16 20:00 1
Xylenes, Total ND 10 ug/Kg 01/26/16 20:00 1
2,2-Dichloropropane ND 5.0 ug/Kg 01/26/16 20:00 1
Gasoline Range Organics (GRO) ND 250 ug/Kg 01/26/16 20:00 1 -C5-C12
4-Bromofluorobenzene 98 45 - 131 01/26/16 20:00 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 107 60 - 140 01/26/16 20:00 1 Toluene-d8 (Surr) 103 58 - 140 01/26/16 20:00 1
Lab Sample ID: LCS 720-196288/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196288
Methyl tert-butyl ether 50.0 55.8 ug/Kg 112 70 - 144
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 200 197 ug/Kg 98 30 - 162
Benzene 50.0 52.4 ug/Kg 105 70 - 130
Dichlorobromomethane 50.0 52.6 ug/Kg 105 70 - 140
Bromobenzene 50.0 54.2 ug/Kg 108 70 - 130
Chlorobromomethane 50.0 53.1 ug/Kg 106 70 - 130
Bromoform 50.0 57.4 ug/Kg 115 59 - 158
Bromomethane 50.0 46.7 ug/Kg 93 59 - 132
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
n-Butylbenzene 50.0 47.9 ug/Kg 96 70 - 142
sec-Butylbenzene 50.0 47.1 ug/Kg 94 70 - 136
tert-Butylbenzene 50.0 48.0 ug/Kg 96 70 - 130
Carbon disulfide 50.0 43.1 ug/Kg 86 60 - 140
Carbon tetrachloride 50.0 47.9 ug/Kg 96 70 - 142
Chlorobenzene 50.0 51.2 ug/Kg 102 70 - 130
Chloroethane 50.0 44.0 ug/Kg 88 65 - 130
Chloroform 50.0 46.6 ug/Kg 93 77 - 127
Chloromethane 50.0 41.9 ug/Kg 84 55 - 140
2-Chlorotoluene 50.0 50.2 ug/Kg 100 70 - 138
4-Chlorotoluene 50.0 50.4 ug/Kg 101 70 - 136
Chlorodibromomethane 50.0 53.6 ug/Kg 107 70 - 146
1,2-Dichlorobenzene 50.0 52.3 ug/Kg 105 70 - 130
1,3-Dichlorobenzene 50.0 50.7 ug/Kg 101 70 - 131
1,4-Dichlorobenzene 50.0 51.0 ug/Kg 102 70 - 130
1,3-Dichloropropane 50.0 50.3 ug/Kg 101 70 - 140
1,1-Dichloropropene 50.0 48.7 ug/Kg 97 70 - 130
1,2-Dibromo-3-Chloropropane 50.0 50.5 ug/Kg 101 60 - 145 Ethylene Dibromide 50.0 54.1 ug/Kg 108 70 - 140
Dibromomethane 50.0 52.2 ug/Kg 104 70 - 139
Dichlorodifluoromethane 50.0 51.2 ug/Kg 102 37 - 158
1,1-Dichloroethane 50.0 48.3 ug/Kg 97 70 - 130
1,2-Dichloroethane 50.0 52.6 ug/Kg 105 70 - 130
1,1-Dichloroethene 50.0 42.0 ug/Kg 84 74 - 122
cis-1,2-Dichloroethene 50.0 49.0 ug/Kg 98 70 - 138
trans-1,2-Dichloroethene 50.0 48.8 ug/Kg 98 67 - 130
1,2-Dichloropropane 50.0 52.4 ug/Kg 105 73 - 127
cis-1,3-Dichloropropene 50.0 56.4 ug/Kg 113 68 - 147
trans-1,3-Dichloropropene 50.0 58.7 ug/Kg 117 70 - 155
Ethylbenzene 50.0 49.7 ug/Kg 99 80 - 137
Hexachlorobutadiene 50.0 49.2 ug/Kg 98 70 - 132
2-Hexanone 200 236 ug/Kg 118 44 - 133
Isopropylbenzene 50.0 47.1 ug/Kg 94 70 - 130
4-Isopropyltoluene 50.0 47.1 ug/Kg 94 70 - 133
Methylene Chloride 50.0 49.5 ug/Kg 99 70 - 134
4-Methyl-2-pentanone (MIBK) 200 265 ug/Kg 132 60 - 160
Naphthalene 50.0 52.7 ug/Kg 105 60 - 147
N-Propylbenzene 50.0 47.6 ug/Kg 95 70 - 130
Styrene 50.0 51.1 ug/Kg 102 70 - 130
1,1,1,2-Tetrachloroethane 50.0 56.8 ug/Kg 114 70 - 130
1,1,2,2-Tetrachloroethane 50.0 54.4 ug/Kg 109 70 - 146
Tetrachloroethene 50.0 49.5 ug/Kg 99 70 - 132
Toluene 50.0 50.6 ug/Kg 101 75 - 120
1,2,3-Trichlorobenzene 50.0 53.7 ug/Kg 107 60 - 140
1,2,4-Trichlorobenzene 50.0 55.1 ug/Kg 110 60 - 140
1,1,1-Trichloroethane 50.0 47.4 ug/Kg 95 70 - 130
1,1,2-Trichloroethane 50.0 55.8 ug/Kg 112 70 - 130
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Trichlorofluoromethane 50.0 45.4 ug/Kg 91 60 - 140
1,2,3-Trichloropropane 50.0 53.8 ug/Kg 108 70 - 146
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 43.3 ug/Kg 87 60 - 140
1,2,4-Trimethylbenzene 50.0 50.3 ug/Kg 101 70 - 130
1,3,5-Trimethylbenzene 50.0 50.1 ug/Kg 100 70 - 131
Vinyl acetate 50.0 46.9 ug/Kg 94 38 - 176
Vinyl chloride 50.0 44.2 ug/Kg 88 58 - 125
m-Xylene & p-Xylene 50.0 51.0 ug/Kg 102 70 - 146
o-Xylene 50.0 48.7 ug/Kg 97 70 - 140
2,2-Dichloropropane 50.0 46.0 ug/Kg 92 70 - 162
4-Bromofluorobenzene 45 - 131
Surrogate
109

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCS 720-196288/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196288
Gasoline Range Organics (GRO)
-C5-C12
1000 1210 ug/Kg 121 61 - 128
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 45 - 131
Surrogate
107

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 100 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCSD 720-196288/6 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196288
Methyl tert-butyl ether 50.0 57.8 ug/Kg 116 70 - 144 4 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 200 198 ug/Kg 99 30 - 162 1 30
Benzene 50.0 52.9 ug/Kg 106 70 - 130 1 20
Dichlorobromomethane 50.0 52.7 ug/Kg 105 70 - 140 0 20
Bromobenzene 50.0 53.5 ug/Kg 107 70 - 130 1 20
Chlorobromomethane 50.0 54.1 ug/Kg 108 70 - 130 2 20
Bromoform 50.0 58.3 ug/Kg 117 59 - 158 2 20
Bromomethane 50.0 46.7 ug/Kg 93 59 - 132 0 20
2-Butanone (MEK) 200 233 ug/Kg 116 53 - 133 3 20
n-Butylbenzene 50.0 48.3 ug/Kg 97 70 - 142 1 20
sec-Butylbenzene 50.0 47.4 ug/Kg 95 70 - 136 1 20
tert-Butylbenzene 50.0 48.1 ug/Kg 96 70 - 130 0 20
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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Carbon tetrachloride 50.0 47.1 ug/Kg 94 70 - 142 2 20
Chlorobenzene 50.0 51.8 ug/Kg 104 70 - 130 1 20
Chloroethane 50.0 43.8 ug/Kg 88 65 - 130 0 20
Chloroform 50.0 46.8 ug/Kg 94 77 - 127 0 20
Chloromethane 50.0 43.4 ug/Kg 87 55 - 140 3 20
2-Chlorotoluene 50.0 51.4 ug/Kg 103 70 - 138 2 20
4-Chlorotoluene 50.0 51.1 ug/Kg 102 70 - 136 1 20
Chlorodibromomethane 50.0 53.6 ug/Kg 107 70 - 146 0 20
1,2-Dichlorobenzene 50.0 53.2 ug/Kg 106 70 - 130 2 20
1,3-Dichlorobenzene 50.0 51.2 ug/Kg 102 70 - 131 1 20
1,4-Dichlorobenzene 50.0 51.8 ug/Kg 104 70 - 130 2 20
1,3-Dichloropropane 50.0 50.9 ug/Kg 102 70 - 140 1 20
1,1-Dichloropropene 50.0 48.7 ug/Kg 97 70 - 130 0 20
1,2-Dibromo-3-Chloropropane 50.0 51.9 ug/Kg 104 60 - 145 3 20 Ethylene Dibromide 50.0 54.2 ug/Kg 108 70 - 140 0 20
Dibromomethane 50.0 52.8 ug/Kg 106 70 - 139 1 20
Dichlorodifluoromethane 50.0 50.9 ug/Kg 102 37 - 158 1 20 1,1-Dichloroethane 50.0 49.1 ug/Kg 98 70 - 130 1 20
1,2-Dichloroethane 50.0 52.6 ug/Kg 105 70 - 130 0 20
1,1-Dichloroethene 50.0 42.4 ug/Kg 85 74 - 122 1 20
cis-1,2-Dichloroethene 50.0 49.1 ug/Kg 98 70 - 138 0 20 trans-1,2-Dichloroethene 50.0 49.3 ug/Kg 99 67 - 130 1 20 1,2-Dichloropropane 50.0 52.8 ug/Kg 106 73 - 127 1 20
cis-1,3-Dichloropropene 50.0 57.1 ug/Kg 114 68 - 147 1 20 trans-1,3-Dichloropropene 50.0 59.5 ug/Kg 119 70 - 155 1 20 Ethylbenzene 50.0 49.9 ug/Kg 100 80 - 137 0 20
Hexachlorobutadiene 50.0 49.0 ug/Kg 98 70 - 132 0 20
2-Hexanone 200 243 ug/Kg 121 44 - 133 3 20
Isopropylbenzene 50.0 46.9 ug/Kg 94 70 - 130 0 20
4-Isopropyltoluene 50.0 47.6 ug/Kg 95 70 - 133 1 20
Methylene Chloride 50.0 50.5 ug/Kg 101 70 - 134 2 20
4-Methyl-2-pentanone (MIBK) 200 274 ug/Kg 137 60 - 160 3 20 Naphthalene 50.0 54.2 ug/Kg 108 60 - 147 3 20
N-Propylbenzene 50.0 48.3 ug/Kg 97 70 - 130 1 20
Styrene 50.0 51.3 ug/Kg 103 70 - 130 0 20
1,1,1,2-Tetrachloroethane 50.0 57.2 ug/Kg 114 70 - 130 1 20 1,1,2,2-Tetrachloroethane 50.0 55.7 ug/Kg 111 70 - 146 2 20 Tetrachloroethene 50.0 49.6 ug/Kg 99 70 - 132 0 20
Toluene 50.0 50.9 ug/Kg 102 75 - 120 1 20
1,2,3-Trichlorobenzene 50.0 55.4 ug/Kg 111 60 - 140 3 20 1,2,4-Trichlorobenzene 50.0 56.4 ug/Kg 113 60 - 140 2 20 1,1,1-Trichloroethane 50.0 47.0 ug/Kg 94 70 - 130 1 20
1,1,2-Trichloroethane 50.0 56.5 ug/Kg 113 70 - 130 1 20 Trichloroethene 50.0 51.3 ug/Kg 103 70 - 133 0 20
Trichlorofluoromethane 50.0 44.7 ug/Kg 89 60 - 140 2 20 1,2,3-Trichloropropane 50.0 53.9 ug/Kg 108 70 - 146 0 20 TestAmerica Pleasanton

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50.0 43.1 ug/Kg 86 60 - 140 0 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,2,4-Trimethylbenzene 50.0 51.0 ug/Kg 102 70 - 130 1 20 1,3,5-Trimethylbenzene 50.0 50.7 ug/Kg 101 70 - 131 1 20 Vinyl acetate 50.0 48.6 ug/Kg 97 38 - 176 4 20
Vinyl chloride 50.0 44.7 ug/Kg 89 58 - 125 1 20
m-Xylene & p-Xylene 50.0 50.8 ug/Kg 102 70 - 146 0 20
o-Xylene 50.0 48.9 ug/Kg 98 70 - 140 0 20
2,2-Dichloropropane 50.0 46.6 ug/Kg 93 70 - 162 1 20
4-Bromofluorobenzene 45 - 131
Surrogate
107

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 100 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCSD 720-196288/8 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196288
Gasoline Range Organics (GRO)
-C5-C12
1000 1130 ug/Kg 113 61 - 128 6 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 45 - 131
Surrogate
107

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: 720-69933-35 MS Client Sample ID: GP-8-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408 Prep Batch: 196295
Methyl tert-butyl ether ND 64.8 75.3 ug/Kg ☼ 116 69 - 130 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Acetone ND F1 259 499 F1 ug/Kg ☼ 192 37 - 150
Benzene ND 64.8 72.5 ug/Kg ☼ 112 70 - 130
Dichlorobromomethane ND 64.8 62.9 ug/Kg ☼ 97 64 - 135
Bromobenzene ND * F1 F2 64.8 91.0 * F1 ug/Kg ☼ 140 70 - 130 Chlorobromomethane ND 64.8 68.1 ug/Kg ☼ 105 65 - 130
Bromoform ND 64.8 67.5 ug/Kg ☼ 104 58 - 132
Bromomethane ND 64.8 61.3 ug/Kg ☼ 95 56 - 130
2-Butanone (MEK) ND 259 305 ug/Kg ☼ 118 41 - 150
n-Butylbenzene ND * 64.8 69.9 * ug/Kg ☼ 108 60 - 145
sec-Butylbenzene ND * F1 F2 64.8 90.9 * F1 ug/Kg ☼ 140 64 - 137 tert-Butylbenzene ND * F1 F2 64.8 104 * F1 ug/Kg ☼ 160 63 - 134 Carbon disulfide ND 64.8 65.5 ug/Kg ☼ 101 10 - 150
Carbon tetrachloride ND 64.8 66.5 ug/Kg ☼ 103 54 - 130
Chlorobenzene ND 64.8 70.9 ug/Kg ☼ 109 70 - 130
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Limits
Chloroform ND 64.8 65.9 ug/Kg ☼ 102 67 - 130
Chloromethane ND 64.8 69.7 ug/Kg ☼ 108 50 - 131
2-Chlorotoluene ND * F1 F2 64.8 91.3 * F1 ug/Kg ☼ 141 70 - 130 4-Chlorotoluene ND * F2 64.8 83.9 * ug/Kg ☼ 129 70 - 130 Chlorodibromomethane ND 64.8 57.0 ug/Kg ☼ 88 60 - 141
1,2-Dichlorobenzene ND * 64.8 63.1 * ug/Kg ☼ 97 70 - 130 1,3-Dichlorobenzene ND * 64.8 68.0 * ug/Kg ☼ 105 70 - 130 1,4-Dichlorobenzene ND * 64.8 66.8 * ug/Kg ☼ 103 70 - 130 1,3-Dichloropropane ND 64.8 62.6 ug/Kg ☼ 96 70 - 130
1,1-Dichloropropene ND 64.8 65.1 ug/Kg ☼ 100 67 - 130
1,2-Dibromo-3-Chloropropane ND * F1 64.8 87.6 * F1 ug/Kg ☼ 135 57 - 130 Ethylene Dibromide ND 64.8 59.3 ug/Kg ☼ 91 66 - 135
Dibromomethane ND 64.8 59.2 ug/Kg ☼ 91 65 - 131
Dichlorodifluoromethane ND 64.8 60.4 ug/Kg ☼ 93 38 - 130 1,1-Dichloroethane ND 64.8 71.9 ug/Kg ☼ 111 67 - 130
1,2-Dichloroethane ND 64.8 68.4 ug/Kg ☼ 105 70 - 130
1,1-Dichloroethene ND 64.8 67.0 ug/Kg ☼ 103 64 - 130
cis-1,2-Dichloroethene ND 64.8 64.3 ug/Kg ☼ 99 68 - 131 trans-1,2-Dichloroethene ND 64.8 70.3 ug/Kg ☼ 108 70 - 130 1,2-Dichloropropane ND 64.8 68.9 ug/Kg ☼ 106 65 - 133
cis-1,3-Dichloropropene ND 64.8 61.5 ug/Kg ☼ 95 46 - 139 trans-1,3-Dichloropropene ND 64.8 60.2 ug/Kg ☼ 93 55 - 131 Ethylbenzene ND 64.8 66.6 ug/Kg ☼ 103 65 - 130
Hexachlorobutadiene ND * 64.8 48.8 * ug/Kg ☼ 75 58 - 132 2-Hexanone ND 259 252 ug/Kg ☼ 97 44 - 150
Isopropylbenzene ND 64.8 64.4 ug/Kg ☼ 99 65 - 130
4-Isopropyltoluene ND * F2 64.8 81.0 * ug/Kg ☼ 125 69 - 134 Methylene Chloride ND 64.8 77.3 ug/Kg ☼ 119 63 - 130
4-Methyl-2-pentanone (MIBK) ND 259 302 ug/Kg ☼ 117 51 - 140 Naphthalene ND * F2 64.8 39.1 * ug/Kg ☼ 60 45 - 146
N-Propylbenzene ND * F1 F2 64.8 97.6 * F1 ug/Kg ☼ 151 70 - 130 Styrene ND 64.8 59.7 ug/Kg ☼ 92 58 - 135
1,1,1,2-Tetrachloroethane ND 64.8 73.8 ug/Kg ☼ 114 64 - 133 1,1,2,2-Tetrachloroethane ND * F1 64.8 97.5 * F1 ug/Kg ☼ 150 70 - 131 Tetrachloroethene ND 64.8 60.0 ug/Kg ☼ 93 67 - 130
Toluene ND 64.8 79.2 ug/Kg ☼ 122 70 - 130
1,2,3-Trichlorobenzene ND * F1 F2 64.8 26.0 * F1 ug/Kg ☼ 40 58 - 138 1,2,4-Trichlorobenzene ND * F1 F2 64.8 30.3 * F1 ug/Kg ☼ 47 49 - 144 1,1,1-Trichloroethane ND 64.8 66.0 ug/Kg ☼ 102 57 - 133 1,1,2-Trichloroethane ND 64.8 63.8 ug/Kg ☼ 98 68 - 132
Trichloroethene ND 64.8 68.4 ug/Kg ☼ 105 66 - 130
Trichlorofluoromethane ND 64.8 68.9 ug/Kg ☼ 106 61 - 130 1,2,3-Trichloropropane ND * F1 F2 64.8 118 * F1 ug/Kg ☼ 181 62 - 150 1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 64.8 66.4 ug/Kg ☼ 102 52 - 130
1,2,4-Trimethylbenzene ND * F2 64.8 84.1 * ug/Kg ☼ 130 64 - 140 1,3,5-Trimethylbenzene ND * F1 F2 64.8 91.2 * F1 ug/Kg ☼ 141 67 - 134 TestAmerica Pleasanton

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Limits
Vinyl chloride ND 64.8 60.1 ug/Kg ☼ 93 62 - 130
m-Xylene & p-Xylene ND 64.8 67.6 ug/Kg ☼ 104 70 - 130
o-Xylene ND 64.8 64.3 ug/Kg ☼ 99 68 - 130
2,2-Dichloropropane ND 64.8 67.4 ug/Kg ☼ 104 63 - 130
4-Bromofluorobenzene 45 - 131
Surrogate
85 MS MS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 97 60 - 140
Toluene-d8 (Surr) 96 58 - 140
Lab Sample ID: 720-69933-35 MSD Client Sample ID: GP-8-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408 Prep Batch: 196295
Methyl tert-butyl ether ND 63.8 77.1 ug/Kg ☼ 121 69 - 130 2 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Acetone ND F1 255 523 F1 ug/Kg ☼ 205 37 - 150 5 20
Benzene ND 63.8 69.7 ug/Kg ☼ 109 70 - 130 4 20
Dichlorobromomethane ND 63.8 62.8 ug/Kg ☼ 98 64 - 135 0 20 Bromobenzene ND * F1 F2 63.8 74.0 F2 ug/Kg ☼ 116 70 - 130 21 20 Chlorobromomethane ND 63.8 66.0 ug/Kg ☼ 103 65 - 130 3 20 Bromoform ND 63.8 71.8 ug/Kg ☼ 113 58 - 132 6 20
Bromomethane ND 63.8 62.4 ug/Kg ☼ 98 56 - 130 2 20
2-Butanone (MEK) ND 255 321 ug/Kg ☼ 126 41 - 150 5 20
n-Butylbenzene ND * 63.8 57.8 ug/Kg ☼ 91 60 - 145 19 20 sec-Butylbenzene ND * F1 F2 63.8 69.2 F2 ug/Kg ☼ 108 64 - 137 27 20 tert-Butylbenzene ND * F1 F2 63.8 78.5 F2 ug/Kg ☼ 123 63 - 134 28 20 Carbon disulfide ND 63.8 61.9 ug/Kg ☼ 97 10 - 150 6 20
Carbon tetrachloride ND 63.8 63.7 ug/Kg ☼ 100 54 - 130 4 20 Chlorobenzene ND 63.8 68.0 ug/Kg ☼ 107 70 - 130 4 20
Chloroethane ND 63.8 66.3 ug/Kg ☼ 104 61 - 130 1 20
Chloroform ND 63.8 63.4 ug/Kg ☼ 99 67 - 130 4 20
Chloromethane ND 63.8 68.6 ug/Kg ☼ 107 50 - 131 2 20
2-Chlorotoluene ND * F1 F2 63.8 72.2 F2 ug/Kg ☼ 113 70 - 130 23 20 4-Chlorotoluene ND * F2 63.8 68.3 F2 ug/Kg ☼ 107 70 - 130 21 20 Chlorodibromomethane ND 63.8 60.7 ug/Kg ☼ 95 60 - 141 6 20 1,2-Dichlorobenzene ND * 63.8 62.8 ug/Kg ☼ 98 70 - 130 1 20 1,3-Dichlorobenzene ND * 63.8 63.1 ug/Kg ☼ 99 70 - 130 7 20 1,4-Dichlorobenzene ND * 63.8 63.2 ug/Kg ☼ 99 70 - 130 5 20 1,3-Dichloropropane ND 63.8 64.6 ug/Kg ☼ 101 70 - 130 3 20 1,1-Dichloropropene ND 63.8 62.0 ug/Kg ☼ 97 67 - 130 5 20 1,2-Dibromo-3-Chloropropane ND * F1 63.8 76.8 ug/Kg ☼ 120 57 - 130 13 20 Ethylene Dibromide ND 63.8 64.4 ug/Kg ☼ 101 66 - 135 8 20 Dibromomethane ND 63.8 60.1 ug/Kg ☼ 94 65 - 131 2 20
Dichlorodifluoromethane ND 63.8 59.7 ug/Kg ☼ 93 38 - 130 1 20 1,1-Dichloroethane ND 63.8 70.4 ug/Kg ☼ 110 67 - 130 2 20 1,2-Dichloroethane ND 63.8 68.0 ug/Kg ☼ 107 70 - 130 1 20 TestAmerica Pleasanton

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MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
cis-1,2-Dichloroethene ND 63.8 61.7 ug/Kg ☼ 97 68 - 131 4 20 trans-1,2-Dichloroethene ND 63.8 68.3 ug/Kg ☼ 107 70 - 130 3 20 1,2-Dichloropropane ND 63.8 68.1 ug/Kg ☼ 107 65 - 133 1 20 cis-1,3-Dichloropropene ND 63.8 61.5 ug/Kg ☼ 96 46 - 139 0 20 trans-1,3-Dichloropropene ND 63.8 63.0 ug/Kg ☼ 99 55 - 131 5 20 Ethylbenzene ND 63.8 62.0 ug/Kg ☼ 97 65 - 130 7 20
Hexachlorobutadiene ND * 63.8 43.6 ug/Kg ☼ 68 58 - 132 11 20 2-Hexanone ND 255 290 ug/Kg ☼ 113 44 - 150 14 20
Isopropylbenzene ND 63.8 61.6 ug/Kg ☼ 97 65 - 130 4 20
4-Isopropyltoluene ND * F2 63.8 65.0 F2 ug/Kg ☼ 102 69 - 134 22 20 Methylene Chloride ND 63.8 76.0 ug/Kg ☼ 119 63 - 130 2 20 4-Methyl-2-pentanone (MIBK) ND 255 332 ug/Kg ☼ 130 51 - 140 9 20 Naphthalene ND * F2 63.8 58.1 F2 ug/Kg ☼ 91 45 - 146 39 20 N-Propylbenzene ND * F1 F2 63.8 73.6 F2 ug/Kg ☼ 115 70 - 130 28 20 Styrene ND 63.8 59.9 ug/Kg ☼ 94 58 - 135 0 20
1,1,1,2-Tetrachloroethane ND 63.8 69.8 ug/Kg ☼ 109 64 - 133 6 20 1,1,2,2-Tetrachloroethane ND * F1 63.8 79.6 ug/Kg ☼ 125 70 - 131 20 20 Tetrachloroethene ND 63.8 58.5 ug/Kg ☼ 92 67 - 130 3 20 Toluene ND 63.8 71.6 ug/Kg ☼ 112 70 - 130 10 20
1,2,3-Trichlorobenzene ND * F1 F2 63.8 44.7 F2 ug/Kg ☼ 70 58 - 138 53 20 1,2,4-Trichlorobenzene ND * F1 F2 63.8 46.4 F2 ug/Kg ☼ 73 49 - 144 42 20 1,1,1-Trichloroethane ND 63.8 63.7 ug/Kg ☼ 100 57 - 133 4 20 1,1,2-Trichloroethane ND 63.8 67.1 ug/Kg ☼ 105 68 - 132 5 20 Trichloroethene ND 63.8 65.0 ug/Kg ☼ 102 66 - 130 5 20
Trichlorofluoromethane ND 63.8 67.2 ug/Kg ☼ 105 61 - 130 3 20 1,2,3-Trichloropropane ND * F1 F2 63.8 91.7 F2 ug/Kg ☼ 144 62 - 150 25 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 63.8 65.5 ug/Kg ☼ 103 52 - 130 1 20
1,2,4-Trimethylbenzene ND * F2 63.8 68.2 F2 ug/Kg ☼ 107 64 - 140 21 20 1,3,5-Trimethylbenzene ND * F1 F2 63.8 70.4 F2 ug/Kg ☼ 110 67 - 134 26 20 Vinyl acetate ND F1 F2 63.8 ND F1 F2 ug/Kg ☼ 23 52 - 150 95 20 Vinyl chloride ND 63.8 58.8 ug/Kg ☼ 92 62 - 130 2 20
m-Xylene & p-Xylene ND 63.8 63.8 ug/Kg ☼ 100 70 - 130 6 20 o-Xylene ND 63.8 62.0 ug/Kg ☼ 97 68 - 130 4 20
2,2-Dichloropropane ND 63.8 62.8 ug/Kg ☼ 98 63 - 130 7 20 4-Bromofluorobenzene 45 - 131
Surrogate
92 MSD MSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 60 - 140
Toluene-d8 (Surr) 98 58 - 140
Lab Sample ID: MB 720-196326/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326
RL MDL
Methyl tert-butyl ether ND 5.0 ug/Kg 01/27/16 09:03 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 720-196326/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326
RL MDL
Acetone ND 50 ug/Kg 01/27/16 09:03 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Benzene ND 5.0 ug/Kg 01/27/16 09:03 1
Dichlorobromomethane ND 5.0 ug/Kg 01/27/16 09:03 1
Bromobenzene ND 5.0 ug/Kg 01/27/16 09:03 1
Chlorobromomethane ND 20 ug/Kg 01/27/16 09:03 1
Bromoform ND 5.0 ug/Kg 01/27/16 09:03 1
Bromomethane ND 10 ug/Kg 01/27/16 09:03 1
2-Butanone (MEK) ND 50 ug/Kg 01/27/16 09:03 1
n-Butylbenzene ND 5.0 ug/Kg 01/27/16 09:03 1
sec-Butylbenzene ND 5.0 ug/Kg 01/27/16 09:03 1
tert-Butylbenzene ND 5.0 ug/Kg 01/27/16 09:03 1
Carbon disulfide ND 5.0 ug/Kg 01/27/16 09:03 1
Carbon tetrachloride ND 5.0 ug/Kg 01/27/16 09:03 1
Chlorobenzene ND 5.0 ug/Kg 01/27/16 09:03 1
Chloroethane ND 10 ug/Kg 01/27/16 09:03 1
Chloroform ND 5.0 ug/Kg 01/27/16 09:03 1
Chloromethane ND 10 ug/Kg 01/27/16 09:03 1
2-Chlorotoluene ND 5.0 ug/Kg 01/27/16 09:03 1
4-Chlorotoluene ND 5.0 ug/Kg 01/27/16 09:03 1
Chlorodibromomethane ND 5.0 ug/Kg 01/27/16 09:03 1
1,2-Dichlorobenzene ND 5.0 ug/Kg 01/27/16 09:03 1
1,3-Dichlorobenzene ND 5.0 ug/Kg 01/27/16 09:03 1
1,4-Dichlorobenzene ND 5.0 ug/Kg 01/27/16 09:03 1
1,3-Dichloropropane ND 5.0 ug/Kg 01/27/16 09:03 1
1,1-Dichloropropene ND 5.0 ug/Kg 01/27/16 09:03 1
1,2-Dibromo-3-Chloropropane ND 10 ug/Kg 01/27/16 09:03 1 Ethylene Dibromide ND 5.0 ug/Kg 01/27/16 09:03 1
Dibromomethane ND 10 ug/Kg 01/27/16 09:03 1
Dichlorodifluoromethane ND 10 ug/Kg 01/27/16 09:03 1
1,1-Dichloroethane ND 5.0 ug/Kg 01/27/16 09:03 1
1,2-Dichloroethane ND 5.0 ug/Kg 01/27/16 09:03 1
1,1-Dichloroethene ND 5.0 ug/Kg 01/27/16 09:03 1
cis-1,2-Dichloroethene ND 5.0 ug/Kg 01/27/16 09:03 1
trans-1,2-Dichloroethene ND 5.0 ug/Kg 01/27/16 09:03 1
1,2-Dichloropropane ND 5.0 ug/Kg 01/27/16 09:03 1
cis-1,3-Dichloropropene ND 5.0 ug/Kg 01/27/16 09:03 1
trans-1,3-Dichloropropene ND 5.0 ug/Kg 01/27/16 09:03 1 Ethylbenzene ND 5.0 ug/Kg 01/27/16 09:03 1
Hexachlorobutadiene ND 5.0 ug/Kg 01/27/16 09:03 1
2-Hexanone ND 50 ug/Kg 01/27/16 09:03 1
Isopropylbenzene ND 5.0 ug/Kg 01/27/16 09:03 1
4-Isopropyltoluene ND 5.0 ug/Kg 01/27/16 09:03 1
Methylene Chloride ND 10 ug/Kg 01/27/16 09:03 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/Kg 01/27/16 09:03 1 Naphthalene ND 10 ug/Kg 01/27/16 09:03 1
N-Propylbenzene ND 5.0 ug/Kg 01/27/16 09:03 1
Styrene ND 5.0 ug/Kg 01/27/16 09:03 1
1,1,1,2-Tetrachloroethane ND 5.0 ug/Kg 01/27/16 09:03 1 TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 200 217 ug/Kg 109 30 - 162
Benzene 50.0 51.7 ug/Kg 103 70 - 130
Dichlorobromomethane 50.0 52.3 ug/Kg 105 70 - 140
Bromobenzene 50.0 51.9 ug/Kg 104 70 - 130
Chlorobromomethane 50.0 51.6 ug/Kg 103 70 - 130
Bromoform 50.0 54.3 ug/Kg 109 59 - 158
Bromomethane 50.0 47.3 ug/Kg 95 59 - 132
2-Butanone (MEK) 200 207 ug/Kg 104 53 - 133
n-Butylbenzene 50.0 50.0 ug/Kg 100 70 - 142
sec-Butylbenzene 50.0 47.4 ug/Kg 95 70 - 136
tert-Butylbenzene 50.0 47.4 ug/Kg 95 70 - 130
Carbon disulfide 50.0 42.8 ug/Kg 86 60 - 140
Carbon tetrachloride 50.0 49.0 ug/Kg 98 70 - 142
Chlorobenzene 50.0 50.7 ug/Kg 101 70 - 130
Chloroethane 50.0 45.0 ug/Kg 90 65 - 130
Chloroform 50.0 46.5 ug/Kg 93 77 - 127
Chloromethane 50.0 43.2 ug/Kg 86 55 - 140
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Chlorotoluene 50.0 50.8 ug/Kg 102 70 - 136
Chlorodibromomethane 50.0 51.9 ug/Kg 104 70 - 146
1,2-Dichlorobenzene 50.0 51.1 ug/Kg 102 70 - 130
1,3-Dichlorobenzene 50.0 50.4 ug/Kg 101 70 - 131
1,4-Dichlorobenzene 50.0 50.7 ug/Kg 101 70 - 130
1,3-Dichloropropane 50.0 48.7 ug/Kg 97 70 - 140
1,1-Dichloropropene 50.0 48.9 ug/Kg 98 70 - 130
1,2-Dibromo-3-Chloropropane 50.0 45.6 ug/Kg 91 60 - 145 Ethylene Dibromide 50.0 50.9 ug/Kg 102 70 - 140
Dibromomethane 50.0 50.4 ug/Kg 101 70 - 139
Dichlorodifluoromethane 50.0 52.2 ug/Kg 104 37 - 158
1,1-Dichloroethane 50.0 48.2 ug/Kg 96 70 - 130
1,2-Dichloroethane 50.0 51.6 ug/Kg 103 70 - 130
1,1-Dichloroethene 50.0 41.5 ug/Kg 83 74 - 122
cis-1,2-Dichloroethene 50.0 48.5 ug/Kg 97 70 - 138
trans-1,2-Dichloroethene 50.0 47.7 ug/Kg 95 67 - 130
1,2-Dichloropropane 50.0 51.1 ug/Kg 102 73 - 127
cis-1,3-Dichloropropene 50.0 55.9 ug/Kg 112 68 - 147
trans-1,3-Dichloropropene 50.0 57.6 ug/Kg 115 70 - 155
Ethylbenzene 50.0 50.1 ug/Kg 100 80 - 137
Hexachlorobutadiene 50.0 51.0 ug/Kg 102 70 - 132
2-Hexanone 200 218 ug/Kg 109 44 - 133
Isopropylbenzene 50.0 47.4 ug/Kg 95 70 - 130
4-Isopropyltoluene 50.0 47.9 ug/Kg 96 70 - 133
Methylene Chloride 50.0 45.7 ug/Kg 91 70 - 134
4-Methyl-2-pentanone (MIBK) 200 243 ug/Kg 122 60 - 160
Naphthalene 50.0 49.5 ug/Kg 99 60 - 147
N-Propylbenzene 50.0 48.1 ug/Kg 96 70 - 130
Styrene 50.0 50.5 ug/Kg 101 70 - 130
1,1,1,2-Tetrachloroethane 50.0 56.0 ug/Kg 112 70 - 130
1,1,2,2-Tetrachloroethane 50.0 49.8 ug/Kg 100 70 - 146
Tetrachloroethene 50.0 49.7 ug/Kg 99 70 - 132
Toluene 50.0 49.9 ug/Kg 100 75 - 120
1,2,3-Trichlorobenzene 50.0 53.6 ug/Kg 107 60 - 140
1,2,4-Trichlorobenzene 50.0 56.5 ug/Kg 113 60 - 140
1,1,1-Trichloroethane 50.0 48.1 ug/Kg 96 70 - 130
1,1,2-Trichloroethane 50.0 52.8 ug/Kg 106 70 - 130
Trichloroethene 50.0 51.1 ug/Kg 102 70 - 133
Trichlorofluoromethane 50.0 48.2 ug/Kg 96 60 - 140
1,2,3-Trichloropropane 50.0 48.7 ug/Kg 97 70 - 146
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 43.5 ug/Kg 87 60 - 140
1,2,4-Trimethylbenzene 50.0 50.6 ug/Kg 101 70 - 130
1,3,5-Trimethylbenzene 50.0 50.2 ug/Kg 100 70 - 131
Vinyl acetate 50.0 45.1 ug/Kg 90 38 - 176
Vinyl chloride 50.0 46.0 ug/Kg 92 58 - 125
m-Xylene & p-Xylene 50.0 51.5 ug/Kg 103 70 - 146
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
2,2-Dichloropropane 50.0 49.9 ug/Kg 100 70 - 162
4-Bromofluorobenzene 45 - 131
Surrogate
108

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCS 720-196326/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326
Gasoline Range Organics (GRO)
-C5-C12
1000 1180 ug/Kg 118 61 - 128
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 45 - 131
Surrogate
107

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 60 - 140
Toluene-d8 (Surr) 111 58 - 140
Lab Sample ID: LCSD 720-196326/6 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326
Methyl tert-butyl ether 50.0 52.1 ug/Kg 104 70 - 144 1 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 200 180 ug/Kg 90 30 - 162 19 30
Benzene 50.0 52.4 ug/Kg 105 70 - 130 1 20
Dichlorobromomethane 50.0 51.1 ug/Kg 102 70 - 140 2 20
Bromobenzene 50.0 52.2 ug/Kg 104 70 - 130 1 20
Chlorobromomethane 50.0 51.8 ug/Kg 104 70 - 130 0 20
Bromoform 50.0 52.9 ug/Kg 106 59 - 158 3 20
Bromomethane 50.0 46.7 ug/Kg 93 59 - 132 1 20
2-Butanone (MEK) 200 206 ug/Kg 103 53 - 133 1 20
n-Butylbenzene 50.0 50.5 ug/Kg 101 70 - 142 1 20
sec-Butylbenzene 50.0 47.8 ug/Kg 96 70 - 136 1 20
tert-Butylbenzene 50.0 48.1 ug/Kg 96 70 - 130 1 20
Carbon disulfide 50.0 43.4 ug/Kg 87 60 - 140 1 20
Carbon tetrachloride 50.0 47.2 ug/Kg 94 70 - 142 4 20
Chlorobenzene 50.0 50.8 ug/Kg 102 70 - 130 0 20
Chloroethane 50.0 44.3 ug/Kg 89 65 - 130 1 20
Chloroform 50.0 45.5 ug/Kg 91 77 - 127 2 20
Chloromethane 50.0 42.2 ug/Kg 84 55 - 140 2 20
2-Chlorotoluene 50.0 50.7 ug/Kg 101 70 - 138 2 20
4-Chlorotoluene 50.0 51.0 ug/Kg 102 70 - 136 0 20
Chlorodibromomethane 50.0 49.7 ug/Kg 99 70 - 146 4 20
1,2-Dichlorobenzene 50.0 51.1 ug/Kg 102 70 - 130 0 20
TestAmerica Pleasanton

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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,4-Dichlorobenzene 50.0 50.9 ug/Kg 102 70 - 130 0 20
1,3-Dichloropropane 50.0 47.6 ug/Kg 95 70 - 140 2 20
1,1-Dichloropropene 50.0 48.7 ug/Kg 97 70 - 130 0 20
1,2-Dibromo-3-Chloropropane 50.0 44.0 ug/Kg 88 60 - 145 4 20 Ethylene Dibromide 50.0 50.2 ug/Kg 100 70 - 140 1 20
Dibromomethane 50.0 49.4 ug/Kg 99 70 - 139 2 20
Dichlorodifluoromethane 50.0 49.8 ug/Kg 100 37 - 158 5 20 1,1-Dichloroethane 50.0 48.6 ug/Kg 97 70 - 130 1 20
1,2-Dichloroethane 50.0 49.4 ug/Kg 99 70 - 130 4 20
1,1-Dichloroethene 50.0 41.8 ug/Kg 84 74 - 122 1 20
cis-1,2-Dichloroethene 50.0 48.5 ug/Kg 97 70 - 138 0 20 trans-1,2-Dichloroethene 50.0 48.8 ug/Kg 98 67 - 130 2 20 1,2-Dichloropropane 50.0 52.2 ug/Kg 104 73 - 127 2 20
cis-1,3-Dichloropropene 50.0 55.6 ug/Kg 111 68 - 147 0 20 trans-1,3-Dichloropropene 50.0 56.6 ug/Kg 113 70 - 155 2 20 Ethylbenzene 50.0 49.7 ug/Kg 99 80 - 137 1 20
Hexachlorobutadiene 50.0 50.8 ug/Kg 102 70 - 132 0 20
2-Hexanone 200 209 ug/Kg 105 44 - 133 4 20
Isopropylbenzene 50.0 47.1 ug/Kg 94 70 - 130 1 20
4-Isopropyltoluene 50.0 48.4 ug/Kg 97 70 - 133 1 20
Methylene Chloride 50.0 45.8 ug/Kg 92 70 - 134 0 20
4-Methyl-2-pentanone (MIBK) 200 236 ug/Kg 118 60 - 160 3 20 Naphthalene 50.0 49.0 ug/Kg 98 60 - 147 1 20
N-Propylbenzene 50.0 48.7 ug/Kg 97 70 - 130 1 20
Styrene 50.0 50.5 ug/Kg 101 70 - 130 0 20
1,1,1,2-Tetrachloroethane 50.0 55.2 ug/Kg 110 70 - 130 1 20 1,1,2,2-Tetrachloroethane 50.0 49.2 ug/Kg 98 70 - 146 1 20 Tetrachloroethene 50.0 49.6 ug/Kg 99 70 - 132 0 20
Toluene 50.0 50.7 ug/Kg 101 75 - 120 2 20
1,2,3-Trichlorobenzene 50.0 53.8 ug/Kg 108 60 - 140 0 20 1,2,4-Trichlorobenzene 50.0 56.9 ug/Kg 114 60 - 140 1 20 1,1,1-Trichloroethane 50.0 46.4 ug/Kg 93 70 - 130 4 20
1,1,2-Trichloroethane 50.0 52.4 ug/Kg 105 70 - 130 1 20 Trichloroethene 50.0 50.7 ug/Kg 101 70 - 133 1 20
Trichlorofluoromethane 50.0 45.4 ug/Kg 91 60 - 140 6 20 1,2,3-Trichloropropane 50.0 47.3 ug/Kg 95 70 - 146 3 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 43.0 ug/Kg 86 60 - 140 1 20
1,2,4-Trimethylbenzene 50.0 50.9 ug/Kg 102 70 - 130 1 20 1,3,5-Trimethylbenzene 50.0 50.8 ug/Kg 102 70 - 131 1 20 Vinyl acetate 50.0 45.5 ug/Kg 91 38 - 176 1 20
Vinyl chloride 50.0 45.8 ug/Kg 92 58 - 125 0 20
m-Xylene & p-Xylene 50.0 51.0 ug/Kg 102 70 - 146 1 20
o-Xylene 50.0 48.3 ug/Kg 97 70 - 140 1 20
2,2-Dichloropropane 50.0 47.4 ug/Kg 95 70 - 162 5 20
TestAmerica Pleasanton

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LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 96 60 - 140
Toluene-d8 (Surr) 111 58 - 140
Lab Sample ID: LCSD 720-196326/8 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196326
Gasoline Range Organics (GRO)
-C5-C12
1000 1150 ug/Kg 115 61 - 128 3 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 45 - 131
Surrogate
108

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 100 60 - 140
Toluene-d8 (Surr) 111 58 - 140
Lab Sample ID: MB 720-196408/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408
RL MDL
Methyl tert-butyl ether ND 5.0 ug/Kg 01/28/16 09:07 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/Kg 01/28/16 09:07 1
Benzene ND 5.0 ug/Kg 01/28/16 09:07 1
Dichlorobromomethane ND 5.0 ug/Kg 01/28/16 09:07 1
Bromobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
Chlorobromomethane ND 20 ug/Kg 01/28/16 09:07 1
Bromoform ND 5.0 ug/Kg 01/28/16 09:07 1
Bromomethane ND 10 ug/Kg 01/28/16 09:07 1
2-Butanone (MEK) ND 50 ug/Kg 01/28/16 09:07 1
n-Butylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
sec-Butylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
tert-Butylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
Carbon disulfide ND 5.0 ug/Kg 01/28/16 09:07 1
Carbon tetrachloride ND 5.0 ug/Kg 01/28/16 09:07 1
Chlorobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
Chloroethane ND 10 ug/Kg 01/28/16 09:07 1
Chloroform ND 5.0 ug/Kg 01/28/16 09:07 1
Chloromethane ND 10 ug/Kg 01/28/16 09:07 1
2-Chlorotoluene ND 5.0 ug/Kg 01/28/16 09:07 1
4-Chlorotoluene ND 5.0 ug/Kg 01/28/16 09:07 1
Chlorodibromomethane ND 5.0 ug/Kg 01/28/16 09:07 1
1,2-Dichlorobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
1,3-Dichlorobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
1,4-Dichlorobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
1,3-Dichloropropane ND 5.0 ug/Kg 01/28/16 09:07 1
1,1-Dichloropropene ND 5.0 ug/Kg 01/28/16 09:07 1
TestAmerica Pleasanton

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1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 720-196408/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408
RL MDL
1,2-Dibromo-3-Chloropropane ND 10 ug/Kg 01/28/16 09:07 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Ethylene Dibromide ND 5.0 ug/Kg 01/28/16 09:07 1
Dibromomethane ND 10 ug/Kg 01/28/16 09:07 1
Dichlorodifluoromethane ND 10 ug/Kg 01/28/16 09:07 1
1,1-Dichloroethane ND 5.0 ug/Kg 01/28/16 09:07 1
1,2-Dichloroethane ND 5.0 ug/Kg 01/28/16 09:07 1
1,1-Dichloroethene ND 5.0 ug/Kg 01/28/16 09:07 1
cis-1,2-Dichloroethene ND 5.0 ug/Kg 01/28/16 09:07 1
trans-1,2-Dichloroethene ND 5.0 ug/Kg 01/28/16 09:07 1
1,2-Dichloropropane ND 5.0 ug/Kg 01/28/16 09:07 1
cis-1,3-Dichloropropene ND 5.0 ug/Kg 01/28/16 09:07 1
trans-1,3-Dichloropropene ND 5.0 ug/Kg 01/28/16 09:07 1 Ethylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
Hexachlorobutadiene ND 5.0 ug/Kg 01/28/16 09:07 1
2-Hexanone ND 50 ug/Kg 01/28/16 09:07 1
Isopropylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
4-Isopropyltoluene ND 5.0 ug/Kg 01/28/16 09:07 1
Methylene Chloride ND 10 ug/Kg 01/28/16 09:07 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/Kg 01/28/16 09:07 1 Naphthalene ND 10 ug/Kg 01/28/16 09:07 1
N-Propylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
Styrene ND 5.0 ug/Kg 01/28/16 09:07 1
1,1,1,2-Tetrachloroethane ND 5.0 ug/Kg 01/28/16 09:07 1 1,1,2,2-Tetrachloroethane ND 5.0 ug/Kg 01/28/16 09:07 1 Tetrachloroethene ND 5.0 ug/Kg 01/28/16 09:07 1
Toluene ND 5.0 ug/Kg 01/28/16 09:07 1
1,2,3-Trichlorobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
1,2,4-Trichlorobenzene ND 5.0 ug/Kg 01/28/16 09:07 1
1,1,1-Trichloroethane ND 5.0 ug/Kg 01/28/16 09:07 1
1,1,2-Trichloroethane ND 5.0 ug/Kg 01/28/16 09:07 1
Trichloroethene ND 5.0 ug/Kg 01/28/16 09:07 1
Trichlorofluoromethane ND 5.0 ug/Kg 01/28/16 09:07 1
1,2,3-Trichloropropane ND 5.0 ug/Kg 01/28/16 09:07 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.0 ug/Kg 01/28/16 09:07 1 1,2,4-Trimethylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
1,3,5-Trimethylbenzene ND 5.0 ug/Kg 01/28/16 09:07 1
Vinyl acetate ND 20 ug/Kg 01/28/16 09:07 1
Vinyl chloride ND 5.0 ug/Kg 01/28/16 09:07 1
Xylenes, Total ND 10 ug/Kg 01/28/16 09:07 1
2,2-Dichloropropane ND 5.0 ug/Kg 01/28/16 09:07 1
Gasoline Range Organics (GRO) ND 250 ug/Kg 01/28/16 09:07 1 -C5-C12
4-Bromofluorobenzene 96 45 - 131 01/28/16 09:07 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 97 60 - 140 01/28/16 09:07 1 Toluene-d8 (Surr) 99 58 - 140 01/28/16 09:07 1
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 200 315 ug/Kg 157 30 - 162
Benzene 50.0 51.8 ug/Kg 104 70 - 130
Dichlorobromomethane 50.0 47.8 ug/Kg 96 70 - 140
Bromobenzene 50.0 48.2 ug/Kg 96 70 - 130
Chlorobromomethane 50.0 49.4 ug/Kg 99 70 - 130
Bromoform 50.0 55.8 ug/Kg 112 59 - 158
Bromomethane 50.0 44.9 ug/Kg 90 59 - 132
2-Butanone (MEK) 200 251 ug/Kg 125 53 - 133
n-Butylbenzene 50.0 47.3 ug/Kg 95 70 - 142
sec-Butylbenzene 50.0 47.8 ug/Kg 96 70 - 136
tert-Butylbenzene 50.0 50.2 ug/Kg 100 70 - 130
Carbon disulfide 50.0 48.4 ug/Kg 97 60 - 140
Carbon tetrachloride 50.0 48.0 ug/Kg 96 70 - 142
Chlorobenzene 50.0 51.4 ug/Kg 103 70 - 130
Chloroethane 50.0 44.4 ug/Kg 89 65 - 130
Chloroform 50.0 46.5 ug/Kg 93 77 - 127
Chloromethane 50.0 45.4 ug/Kg 91 55 - 140
2-Chlorotoluene 50.0 47.0 ug/Kg 94 70 - 138
4-Chlorotoluene 50.0 46.9 ug/Kg 94 70 - 136
Chlorodibromomethane 50.0 49.4 ug/Kg 99 70 - 146
1,2-Dichlorobenzene 50.0 47.3 ug/Kg 95 70 - 130
1,3-Dichlorobenzene 50.0 47.2 ug/Kg 94 70 - 131
1,4-Dichlorobenzene 50.0 47.8 ug/Kg 96 70 - 130
1,3-Dichloropropane 50.0 49.8 ug/Kg 100 70 - 140
1,1-Dichloropropene 50.0 48.4 ug/Kg 97 70 - 130
1,2-Dibromo-3-Chloropropane 50.0 50.2 ug/Kg 100 60 - 145 Ethylene Dibromide 50.0 51.2 ug/Kg 102 70 - 140
Dibromomethane 50.0 45.9 ug/Kg 92 70 - 139
Dichlorodifluoromethane 50.0 42.2 ug/Kg 84 37 - 158
1,1-Dichloroethane 50.0 50.2 ug/Kg 100 70 - 130
1,2-Dichloroethane 50.0 50.0 ug/Kg 100 70 - 130
1,1-Dichloroethene 50.0 46.4 ug/Kg 93 74 - 122
cis-1,2-Dichloroethene 50.0 46.6 ug/Kg 93 70 - 138
trans-1,2-Dichloroethene 50.0 50.8 ug/Kg 102 67 - 130
1,2-Dichloropropane 50.0 49.2 ug/Kg 98 73 - 127
cis-1,3-Dichloropropene 50.0 49.7 ug/Kg 99 68 - 147
trans-1,3-Dichloropropene 50.0 53.2 ug/Kg 106 70 - 155
Ethylbenzene 50.0 46.5 ug/Kg 93 80 - 137
Hexachlorobutadiene 50.0 48.6 ug/Kg 97 70 - 132
2-Hexanone 200 223 ug/Kg 111 44 - 133
Isopropylbenzene 50.0 48.2 ug/Kg 96 70 - 130
4-Isopropyltoluene 50.0 47.3 ug/Kg 95 70 - 133
Methylene Chloride 50.0 51.9 ug/Kg 104 70 - 134
4-Methyl-2-pentanone (MIBK) 200 237 ug/Kg 119 60 - 160
Naphthalene 50.0 49.5 ug/Kg 99 60 - 147
N-Propylbenzene 50.0 48.5 ug/Kg 97 70 - 130
Styrene 50.0 48.8 ug/Kg 98 70 - 130
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,2,2-Tetrachloroethane 50.0 47.2 ug/Kg 94 70 - 146
Tetrachloroethene 50.0 50.0 ug/Kg 100 70 - 132
Toluene 50.0 49.2 ug/Kg 98 75 - 120
1,2,3-Trichlorobenzene 50.0 46.3 ug/Kg 93 60 - 140
1,2,4-Trichlorobenzene 50.0 49.6 ug/Kg 99 60 - 140
1,1,1-Trichloroethane 50.0 46.5 ug/Kg 93 70 - 130
1,1,2-Trichloroethane 50.0 51.5 ug/Kg 103 70 - 130
Trichloroethene 50.0 50.3 ug/Kg 101 70 - 133
Trichlorofluoromethane 50.0 49.9 ug/Kg 100 60 - 140
1,2,3-Trichloropropane 50.0 52.1 ug/Kg 104 70 - 146
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 47.8 ug/Kg 96 60 - 140
1,2,4-Trimethylbenzene 50.0 46.3 ug/Kg 93 70 - 130
1,3,5-Trimethylbenzene 50.0 46.6 ug/Kg 93 70 - 131
Vinyl acetate 50.0 51.1 ug/Kg 102 38 - 176
Vinyl chloride 50.0 40.9 ug/Kg 82 58 - 125
m-Xylene & p-Xylene 50.0 49.1 ug/Kg 98 70 - 146
o-Xylene 50.0 46.3 ug/Kg 93 70 - 140
2,2-Dichloropropane 50.0 49.0 ug/Kg 98 70 - 162
4-Bromofluorobenzene 45 - 131
Surrogate
104

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 97 60 - 140
Toluene-d8 (Surr) 102 58 - 140
Lab Sample ID: LCS 720-196408/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408
Gasoline Range Organics (GRO)
-C5-C12
1000 1140 ug/Kg 114 61 - 128
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 45 - 131
Surrogate
102

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 103 60 - 140
Toluene-d8 (Surr) 102 58 - 140
Lab Sample ID: LCSD 720-196408/6 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408
Methyl tert-butyl ether 50.0 49.6 ug/Kg 99 70 - 144 6 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 200 281 ug/Kg 141 30 - 162 11 30
Benzene 50.0 51.3 ug/Kg 103 70 - 130 1 20
Dichlorobromomethane 50.0 47.1 ug/Kg 94 70 - 140 1 20
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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Chlorobromomethane 50.0 48.4 ug/Kg 97 70 - 130 2 20
Bromoform 50.0 53.5 ug/Kg 107 59 - 158 4 20
Bromomethane 50.0 45.0 ug/Kg 90 59 - 132 0 20
2-Butanone (MEK) 200 225 ug/Kg 112 53 - 133 11 20
n-Butylbenzene 50.0 47.7 ug/Kg 95 70 - 142 1 20
sec-Butylbenzene 50.0 48.4 ug/Kg 97 70 - 136 1 20
tert-Butylbenzene 50.0 51.0 ug/Kg 102 70 - 130 2 20
Carbon disulfide 50.0 47.3 ug/Kg 95 60 - 140 2 20
Carbon tetrachloride 50.0 47.6 ug/Kg 95 70 - 142 1 20
Chlorobenzene 50.0 51.2 ug/Kg 102 70 - 130 0 20
Chloroethane 50.0 45.4 ug/Kg 91 65 - 130 2 20
Chloroform 50.0 45.9 ug/Kg 92 77 - 127 1 20
Chloromethane 50.0 44.4 ug/Kg 89 55 - 140 2 20
2-Chlorotoluene 50.0 47.8 ug/Kg 96 70 - 138 2 20
4-Chlorotoluene 50.0 47.6 ug/Kg 95 70 - 136 2 20
Chlorodibromomethane 50.0 47.7 ug/Kg 95 70 - 146 3 20
1,2-Dichlorobenzene 50.0 47.1 ug/Kg 94 70 - 130 0 20
1,3-Dichlorobenzene 50.0 47.6 ug/Kg 95 70 - 131 1 20
1,4-Dichlorobenzene 50.0 47.9 ug/Kg 96 70 - 130 0 20
1,3-Dichloropropane 50.0 47.9 ug/Kg 96 70 - 140 4 20
1,1-Dichloropropene 50.0 47.3 ug/Kg 95 70 - 130 2 20
1,2-Dibromo-3-Chloropropane 50.0 47.8 ug/Kg 96 60 - 145 5 20 Ethylene Dibromide 50.0 48.8 ug/Kg 98 70 - 140 5 20
Dibromomethane 50.0 44.2 ug/Kg 88 70 - 139 4 20
Dichlorodifluoromethane 50.0 42.1 ug/Kg 84 37 - 158 0 20 1,1-Dichloroethane 50.0 49.0 ug/Kg 98 70 - 130 2 20
1,2-Dichloroethane 50.0 48.9 ug/Kg 98 70 - 130 2 20
1,1-Dichloroethene 50.0 46.7 ug/Kg 93 74 - 122 0 20
cis-1,2-Dichloroethene 50.0 46.1 ug/Kg 92 70 - 138 1 20 trans-1,2-Dichloroethene 50.0 50.6 ug/Kg 101 67 - 130 0 20 1,2-Dichloropropane 50.0 49.3 ug/Kg 99 73 - 127 0 20
cis-1,3-Dichloropropene 50.0 49.0 ug/Kg 98 68 - 147 2 20 trans-1,3-Dichloropropene 50.0 51.9 ug/Kg 104 70 - 155 2 20 Ethylbenzene 50.0 46.7 ug/Kg 93 80 - 137 0 20
Hexachlorobutadiene 50.0 48.3 ug/Kg 97 70 - 132 1 20
2-Hexanone 200 202 ug/Kg 101 44 - 133 10 20
Isopropylbenzene 50.0 47.9 ug/Kg 96 70 - 130 1 20
4-Isopropyltoluene 50.0 47.8 ug/Kg 96 70 - 133 1 20
Methylene Chloride 50.0 50.7 ug/Kg 101 70 - 134 2 20
4-Methyl-2-pentanone (MIBK) 200 217 ug/Kg 109 60 - 160 9 20 Naphthalene 50.0 49.1 ug/Kg 98 60 - 147 1 20
N-Propylbenzene 50.0 49.3 ug/Kg 99 70 - 130 2 20
Styrene 50.0 48.5 ug/Kg 97 70 - 130 1 20
1,1,1,2-Tetrachloroethane 50.0 49.2 ug/Kg 98 70 - 130 0 20 1,1,2,2-Tetrachloroethane 50.0 45.9 ug/Kg 92 70 - 146 3 20 Tetrachloroethene 50.0 50.0 ug/Kg 100 70 - 132 0 20
Toluene 50.0 49.6 ug/Kg 99 75 - 120 1 20
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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,2,4-Trichlorobenzene 50.0 49.1 ug/Kg 98 60 - 140 1 20 1,1,1-Trichloroethane 50.0 46.2 ug/Kg 92 70 - 130 1 20
1,1,2-Trichloroethane 50.0 49.6 ug/Kg 99 70 - 130 4 20
Trichloroethene 50.0 50.7 ug/Kg 101 70 - 133 1 20
Trichlorofluoromethane 50.0 49.8 ug/Kg 100 60 - 140 0 20 1,2,3-Trichloropropane 50.0 49.8 ug/Kg 100 70 - 146 4 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 47.7 ug/Kg 95 60 - 140 0 20
1,2,4-Trimethylbenzene 50.0 46.7 ug/Kg 93 70 - 130 1 20 1,3,5-Trimethylbenzene 50.0 47.1 ug/Kg 94 70 - 131 1 20 Vinyl acetate 50.0 48.5 ug/Kg 97 38 - 176 5 20
Vinyl chloride 50.0 41.1 ug/Kg 82 58 - 125 1 20
m-Xylene & p-Xylene 50.0 48.8 ug/Kg 98 70 - 146 1 20
o-Xylene 50.0 46.5 ug/Kg 93 70 - 140 0 20
2,2-Dichloropropane 50.0 49.2 ug/Kg 98 70 - 162 0 20
4-Bromofluorobenzene 45 - 131
Surrogate
102

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 95 60 - 140
Toluene-d8 (Surr) 103 58 - 140
Lab Sample ID: LCSD 720-196408/8 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196408
Gasoline Range Organics (GRO)
-C5-C12
1000 1100 ug/Kg 110 61 - 128 3 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 45 - 131
Surrogate
103

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 100 60 - 140
Toluene-d8 (Surr) 102 58 - 140
Lab Sample ID: MB 720-196468/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196468
RL MDL
Methyl tert-butyl ether ND 5.0 ug/Kg 01/28/16 19:00 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/Kg 01/28/16 19:00 1
Benzene ND 5.0 ug/Kg 01/28/16 19:00 1
Dichlorobromomethane ND 5.0 ug/Kg 01/28/16 19:00 1
Bromobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
Chlorobromomethane ND 20 ug/Kg 01/28/16 19:00 1
Bromoform ND 5.0 ug/Kg 01/28/16 19:00 1
Bromomethane ND 10 ug/Kg 01/28/16 19:00 1
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 720-196468/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196468
RL MDL
2-Butanone (MEK) ND 50 ug/Kg 01/28/16 19:00 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac n-Butylbenzene ND 5.0 ug/Kg 01/28/16 19:00 1
sec-Butylbenzene ND 5.0 ug/Kg 01/28/16 19:00 1
tert-Butylbenzene ND 5.0 ug/Kg 01/28/16 19:00 1
Carbon disulfide ND 5.0 ug/Kg 01/28/16 19:00 1
Carbon tetrachloride ND 5.0 ug/Kg 01/28/16 19:00 1
Chlorobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
Chloroethane ND 10 ug/Kg 01/28/16 19:00 1
Chloroform ND 5.0 ug/Kg 01/28/16 19:00 1
Chloromethane ND 10 ug/Kg 01/28/16 19:00 1
2-Chlorotoluene ND 5.0 ug/Kg 01/28/16 19:00 1
4-Chlorotoluene ND 5.0 ug/Kg 01/28/16 19:00 1
Chlorodibromomethane ND 5.0 ug/Kg 01/28/16 19:00 1
1,2-Dichlorobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
1,3-Dichlorobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
1,4-Dichlorobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
1,3-Dichloropropane ND 5.0 ug/Kg 01/28/16 19:00 1
1,1-Dichloropropene ND 5.0 ug/Kg 01/28/16 19:00 1
1,2-Dibromo-3-Chloropropane ND 10 ug/Kg 01/28/16 19:00 1 Ethylene Dibromide ND 5.0 ug/Kg 01/28/16 19:00 1
Dibromomethane ND 10 ug/Kg 01/28/16 19:00 1
Dichlorodifluoromethane ND 10 ug/Kg 01/28/16 19:00 1
1,1-Dichloroethane ND 5.0 ug/Kg 01/28/16 19:00 1
1,2-Dichloroethane ND 5.0 ug/Kg 01/28/16 19:00 1
1,1-Dichloroethene ND 5.0 ug/Kg 01/28/16 19:00 1
cis-1,2-Dichloroethene ND 5.0 ug/Kg 01/28/16 19:00 1
trans-1,2-Dichloroethene ND 5.0 ug/Kg 01/28/16 19:00 1
1,2-Dichloropropane ND 5.0 ug/Kg 01/28/16 19:00 1
cis-1,3-Dichloropropene ND 5.0 ug/Kg 01/28/16 19:00 1
trans-1,3-Dichloropropene ND 5.0 ug/Kg 01/28/16 19:00 1 Ethylbenzene ND 5.0 ug/Kg 01/28/16 19:00 1
Hexachlorobutadiene ND 5.0 ug/Kg 01/28/16 19:00 1
2-Hexanone ND 50 ug/Kg 01/28/16 19:00 1
Isopropylbenzene ND 5.0 ug/Kg 01/28/16 19:00 1
4-Isopropyltoluene ND 5.0 ug/Kg 01/28/16 19:00 1
Methylene Chloride ND 10 ug/Kg 01/28/16 19:00 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/Kg 01/28/16 19:00 1 Naphthalene ND 10 ug/Kg 01/28/16 19:00 1
N-Propylbenzene ND 5.0 ug/Kg 01/28/16 19:00 1
Styrene ND 5.0 ug/Kg 01/28/16 19:00 1
1,1,1,2-Tetrachloroethane ND 5.0 ug/Kg 01/28/16 19:00 1 1,1,2,2-Tetrachloroethane ND 5.0 ug/Kg 01/28/16 19:00 1 Tetrachloroethene ND 5.0 ug/Kg 01/28/16 19:00 1
Toluene ND 5.0 ug/Kg 01/28/16 19:00 1
1,2,3-Trichlorobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
1,2,4-Trichlorobenzene ND 5.0 ug/Kg 01/28/16 19:00 1
1,1,1-Trichloroethane ND 5.0 ug/Kg 01/28/16 19:00 1
1,1,2-Trichloroethane ND 5.0 ug/Kg 01/28/16 19:00 1
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 200 214 ug/Kg 107 30 - 162
Benzene 50.0 55.5 ug/Kg 111 70 - 130
Dichlorobromomethane 50.0 55.2 ug/Kg 110 70 - 140
Bromobenzene 50.0 56.2 ug/Kg 112 70 - 130
Chlorobromomethane 50.0 55.8 ug/Kg 112 70 - 130
Bromoform 50.0 57.9 ug/Kg 116 59 - 158
Bromomethane 50.0 46.4 ug/Kg 93 59 - 132
2-Butanone (MEK) 200 228 ug/Kg 114 53 - 133
n-Butylbenzene 50.0 51.2 ug/Kg 102 70 - 142
sec-Butylbenzene 50.0 50.2 ug/Kg 100 70 - 136
tert-Butylbenzene 50.0 50.4 ug/Kg 101 70 - 130
Carbon disulfide 50.0 44.8 ug/Kg 90 60 - 140
Carbon tetrachloride 50.0 49.7 ug/Kg 99 70 - 142
Chlorobenzene 50.0 53.8 ug/Kg 108 70 - 130
Chloroethane 50.0 45.1 ug/Kg 90 65 - 130
Chloroform 50.0 49.1 ug/Kg 98 77 - 127
Chloromethane 50.0 40.8 ug/Kg 82 55 - 140
2-Chlorotoluene 50.0 53.7 ug/Kg 107 70 - 138
4-Chlorotoluene 50.0 53.5 ug/Kg 107 70 - 136
Chlorodibromomethane 50.0 55.2 ug/Kg 110 70 - 146
1,2-Dichlorobenzene 50.0 55.1 ug/Kg 110 70 - 130
1,3-Dichlorobenzene 50.0 53.1 ug/Kg 106 70 - 131
1,4-Dichlorobenzene 50.0 54.1 ug/Kg 108 70 - 130
1,3-Dichloropropane 50.0 52.7 ug/Kg 105 70 - 140
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,2-Dibromo-3-Chloropropane 50.0 49.3 ug/Kg 99 60 - 145 Ethylene Dibromide 50.0 55.2 ug/Kg 110 70 - 140
Dibromomethane 50.0 54.3 ug/Kg 109 70 - 139
Dichlorodifluoromethane 50.0 40.5 ug/Kg 81 37 - 158
1,1-Dichloroethane 50.0 51.4 ug/Kg 103 70 - 130
1,2-Dichloroethane 50.0 54.4 ug/Kg 109 70 - 130
1,1-Dichloroethene 50.0 43.8 ug/Kg 88 74 - 122
cis-1,2-Dichloroethene 50.0 52.4 ug/Kg 105 70 - 138
trans-1,2-Dichloroethene 50.0 51.1 ug/Kg 102 67 - 130
1,2-Dichloropropane 50.0 55.5 ug/Kg 111 73 - 127
cis-1,3-Dichloropropene 50.0 59.9 ug/Kg 120 68 - 147
trans-1,3-Dichloropropene 50.0 61.9 ug/Kg 124 70 - 155
Ethylbenzene 50.0 52.5 ug/Kg 105 80 - 137
Hexachlorobutadiene 50.0 51.5 ug/Kg 103 70 - 132
2-Hexanone 200 236 ug/Kg 118 44 - 133
Isopropylbenzene 50.0 49.6 ug/Kg 99 70 - 130
4-Isopropyltoluene 50.0 49.9 ug/Kg 100 70 - 133
Methylene Chloride 50.0 52.6 ug/Kg 105 70 - 134
4-Methyl-2-pentanone (MIBK) 200 265 ug/Kg 133 60 - 160
Naphthalene 50.0 52.8 ug/Kg 106 60 - 147
N-Propylbenzene 50.0 50.9 ug/Kg 102 70 - 130
Styrene 50.0 53.3 ug/Kg 107 70 - 130
1,1,1,2-Tetrachloroethane 50.0 59.5 ug/Kg 119 70 - 130
1,1,2,2-Tetrachloroethane 50.0 55.6 ug/Kg 111 70 - 146
Tetrachloroethene 50.0 51.8 ug/Kg 104 70 - 132
Toluene 50.0 53.1 ug/Kg 106 75 - 120
1,2,3-Trichlorobenzene 50.0 55.8 ug/Kg 112 60 - 140
1,2,4-Trichlorobenzene 50.0 57.0 ug/Kg 114 60 - 140
1,1,1-Trichloroethane 50.0 49.5 ug/Kg 99 70 - 130
1,1,2-Trichloroethane 50.0 57.3 ug/Kg 115 70 - 130
Trichloroethene 50.0 53.7 ug/Kg 107 70 - 133
Trichlorofluoromethane 50.0 45.0 ug/Kg 90 60 - 140
1,2,3-Trichloropropane 50.0 53.4 ug/Kg 107 70 - 146
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 44.7 ug/Kg 89 60 - 140
1,2,4-Trimethylbenzene 50.0 53.1 ug/Kg 106 70 - 130
1,3,5-Trimethylbenzene 50.0 53.1 ug/Kg 106 70 - 131
Vinyl acetate 50.0 47.5 ug/Kg 95 38 - 176
Vinyl chloride 50.0 43.5 ug/Kg 87 58 - 125
m-Xylene & p-Xylene 50.0 53.4 ug/Kg 107 70 - 146
o-Xylene 50.0 51.1 ug/Kg 102 70 - 140
2,2-Dichloropropane 50.0 51.4 ug/Kg 103 70 - 162
4-Bromofluorobenzene 45 - 131
Surrogate
108

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 98 60 - 140
Toluene-d8 (Surr) 111 58 - 140
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Lab Sample ID: LCS 720-196468/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196468
Gasoline Range Organics (GRO)
-C5-C12
1000 1240 ug/Kg 124 61 - 128
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 45 - 131
Surrogate
107

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 102 60 - 140
Toluene-d8 (Surr) 111 58 - 140
Lab Sample ID: LCSD 720-196468/6 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196468
Methyl tert-butyl ether 50.0 56.7 ug/Kg 113 70 - 144 0 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 200 221 ug/Kg 110 30 - 162 3 30
Benzene 50.0 55.4 ug/Kg 111 70 - 130 0 20
Dichlorobromomethane 50.0 54.4 ug/Kg 109 70 - 140 1 20
Bromobenzene 50.0 55.6 ug/Kg 111 70 - 130 1 20
Chlorobromomethane 50.0 55.2 ug/Kg 110 70 - 130 1 20
Bromoform 50.0 57.5 ug/Kg 115 59 - 158 1 20
Bromomethane 50.0 47.3 ug/Kg 95 59 - 132 2 20
2-Butanone (MEK) 200 229 ug/Kg 114 53 - 133 0 20
n-Butylbenzene 50.0 51.1 ug/Kg 102 70 - 142 0 20
sec-Butylbenzene 50.0 49.6 ug/Kg 99 70 - 136 1 20
tert-Butylbenzene 50.0 49.9 ug/Kg 100 70 - 130 1 20
Carbon disulfide 50.0 45.2 ug/Kg 90 60 - 140 1 20
Carbon tetrachloride 50.0 48.6 ug/Kg 97 70 - 142 2 20
Chlorobenzene 50.0 54.1 ug/Kg 108 70 - 130 0 20
Chloroethane 50.0 45.9 ug/Kg 92 65 - 130 2 20
Chloroform 50.0 48.2 ug/Kg 96 77 - 127 2 20
Chloromethane 50.0 42.2 ug/Kg 84 55 - 140 3 20
2-Chlorotoluene 50.0 53.0 ug/Kg 106 70 - 138 1 20
4-Chlorotoluene 50.0 53.3 ug/Kg 107 70 - 136 0 20
Chlorodibromomethane 50.0 53.7 ug/Kg 107 70 - 146 3 20
1,2-Dichlorobenzene 50.0 54.7 ug/Kg 109 70 - 130 1 20
1,3-Dichlorobenzene 50.0 53.4 ug/Kg 107 70 - 131 1 20
1,4-Dichlorobenzene 50.0 53.5 ug/Kg 107 70 - 130 1 20
1,3-Dichloropropane 50.0 51.6 ug/Kg 103 70 - 140 2 20
1,1-Dichloropropene 50.0 50.7 ug/Kg 101 70 - 130 1 20
1,2-Dibromo-3-Chloropropane 50.0 48.1 ug/Kg 96 60 - 145 2 20 Ethylene Dibromide 50.0 53.4 ug/Kg 107 70 - 140 3 20
Dibromomethane 50.0 53.0 ug/Kg 106 70 - 139 2 20
Dichlorodifluoromethane 50.0 40.7 ug/Kg 81 37 - 158 0 20 1,1-Dichloroethane 50.0 51.0 ug/Kg 102 70 - 130 1 20
1,2-Dichloroethane 50.0 52.7 ug/Kg 105 70 - 130 3 20
1,1-Dichloroethene 50.0 43.7 ug/Kg 87 74 - 122 0 20
cis-1,2-Dichloroethene 50.0 51.3 ug/Kg 103 70 - 138 2 20 trans-1,2-Dichloroethene 50.0 51.1 ug/Kg 102 67 - 130 0 20 1,2-Dichloropropane 50.0 55.8 ug/Kg 112 73 - 127 1 20
cis-1,3-Dichloropropene 50.0 59.4 ug/Kg 119 68 - 147 1 20 TestAmerica Pleasanton

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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Ethylbenzene 50.0 52.3 ug/Kg 105 80 - 137 0 20
Hexachlorobutadiene 50.0 51.2 ug/Kg 102 70 - 132 1 20
2-Hexanone 200 233 ug/Kg 117 44 - 133 1 20
Isopropylbenzene 50.0 49.4 ug/Kg 99 70 - 130 1 20
4-Isopropyltoluene 50.0 49.6 ug/Kg 99 70 - 133 1 20
Methylene Chloride 50.0 52.2 ug/Kg 104 70 - 134 1 20
4-Methyl-2-pentanone (MIBK) 200 261 ug/Kg 131 60 - 160 2 20 Naphthalene 50.0 53.1 ug/Kg 106 60 - 147 1 20
N-Propylbenzene 50.0 50.8 ug/Kg 102 70 - 130 0 20
Styrene 50.0 53.8 ug/Kg 108 70 - 130 1 20
1,1,1,2-Tetrachloroethane 50.0 59.0 ug/Kg 118 70 - 130 1 20 1,1,2,2-Tetrachloroethane 50.0 54.1 ug/Kg 108 70 - 146 3 20 Tetrachloroethene 50.0 52.5 ug/Kg 105 70 - 132 1 20
Toluene 50.0 53.7 ug/Kg 107 75 - 120 1 20
1,2,3-Trichlorobenzene 50.0 56.7 ug/Kg 113 60 - 140 1 20 1,2,4-Trichlorobenzene 50.0 58.5 ug/Kg 117 60 - 140 3 20 1,1,1-Trichloroethane 50.0 48.5 ug/Kg 97 70 - 130 2 20
1,1,2-Trichloroethane 50.0 56.7 ug/Kg 113 70 - 130 1 20 Trichloroethene 50.0 53.9 ug/Kg 108 70 - 133 0 20
Trichlorofluoromethane 50.0 45.1 ug/Kg 90 60 - 140 0 20 1,2,3-Trichloropropane 50.0 51.8 ug/Kg 104 70 - 146 3 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 44.9 ug/Kg 90 60 - 140 0 20
1,2,4-Trimethylbenzene 50.0 53.0 ug/Kg 106 70 - 130 0 20 1,3,5-Trimethylbenzene 50.0 52.6 ug/Kg 105 70 - 131 1 20 Vinyl acetate 50.0 48.1 ug/Kg 96 38 - 176 1 20
Vinyl chloride 50.0 44.5 ug/Kg 89 58 - 125 2 20
m-Xylene & p-Xylene 50.0 53.3 ug/Kg 107 70 - 146 0 20
o-Xylene 50.0 51.2 ug/Kg 102 70 - 140 0 20
2,2-Dichloropropane 50.0 49.0 ug/Kg 98 70 - 162 5 20
4-Bromofluorobenzene 45 - 131
Surrogate
107

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 95 60 - 140
Toluene-d8 (Surr) 111 58 - 140
Lab Sample ID: LCSD 720-196468/8 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196468
Gasoline Range Organics (GRO)
-C5-C12
1000 1240 ug/Kg 124 61 - 128 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 45 - 131
Surrogate
108

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 98 60 - 140
TestAmerica Pleasanton

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LCSD LCSD
%Recovery Qualifier Limits
Lab Sample ID: MB 720-196552/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552
RL MDL
Methyl tert-butyl ether ND 5.0 ug/Kg 01/29/16 19:03 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/Kg 01/29/16 19:03 1
Benzene ND 5.0 ug/Kg 01/29/16 19:03 1
Dichlorobromomethane ND 5.0 ug/Kg 01/29/16 19:03 1
Bromobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
Chlorobromomethane ND 20 ug/Kg 01/29/16 19:03 1
Bromoform ND 5.0 ug/Kg 01/29/16 19:03 1
Bromomethane ND 10 ug/Kg 01/29/16 19:03 1
2-Butanone (MEK) ND 50 ug/Kg 01/29/16 19:03 1
n-Butylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
sec-Butylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
tert-Butylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
Carbon disulfide ND 5.0 ug/Kg 01/29/16 19:03 1
Carbon tetrachloride ND 5.0 ug/Kg 01/29/16 19:03 1
Chlorobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
Chloroethane ND 10 ug/Kg 01/29/16 19:03 1
Chloroform ND 5.0 ug/Kg 01/29/16 19:03 1
Chloromethane ND 10 ug/Kg 01/29/16 19:03 1
2-Chlorotoluene ND 5.0 ug/Kg 01/29/16 19:03 1
4-Chlorotoluene ND 5.0 ug/Kg 01/29/16 19:03 1
Chlorodibromomethane ND 5.0 ug/Kg 01/29/16 19:03 1
1,2-Dichlorobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
1,3-Dichlorobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
1,4-Dichlorobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
1,3-Dichloropropane ND 5.0 ug/Kg 01/29/16 19:03 1
1,1-Dichloropropene ND 5.0 ug/Kg 01/29/16 19:03 1
1,2-Dibromo-3-Chloropropane ND 10 ug/Kg 01/29/16 19:03 1 Ethylene Dibromide ND 5.0 ug/Kg 01/29/16 19:03 1
Dibromomethane ND 10 ug/Kg 01/29/16 19:03 1
Dichlorodifluoromethane ND 10 ug/Kg 01/29/16 19:03 1
1,1-Dichloroethane ND 5.0 ug/Kg 01/29/16 19:03 1
1,2-Dichloroethane ND 5.0 ug/Kg 01/29/16 19:03 1
1,1-Dichloroethene ND 5.0 ug/Kg 01/29/16 19:03 1
cis-1,2-Dichloroethene ND 5.0 ug/Kg 01/29/16 19:03 1
trans-1,2-Dichloroethene ND 5.0 ug/Kg 01/29/16 19:03 1
1,2-Dichloropropane ND 5.0 ug/Kg 01/29/16 19:03 1
cis-1,3-Dichloropropene ND 5.0 ug/Kg 01/29/16 19:03 1
trans-1,3-Dichloropropene ND 5.0 ug/Kg 01/29/16 19:03 1 Ethylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
Hexachlorobutadiene ND 5.0 ug/Kg 01/29/16 19:03 1
2-Hexanone ND 50 ug/Kg 01/29/16 19:03 1
TestAmerica Pleasanton

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1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 720-196552/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552
RL MDL
Isopropylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac 4-Isopropyltoluene ND 5.0 ug/Kg 01/29/16 19:03 1
Methylene Chloride ND 10 ug/Kg 01/29/16 19:03 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/Kg 01/29/16 19:03 1 Naphthalene ND 10 ug/Kg 01/29/16 19:03 1
N-Propylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
Styrene ND 5.0 ug/Kg 01/29/16 19:03 1
1,1,1,2-Tetrachloroethane ND 5.0 ug/Kg 01/29/16 19:03 1 1,1,2,2-Tetrachloroethane ND 5.0 ug/Kg 01/29/16 19:03 1 Tetrachloroethene ND 5.0 ug/Kg 01/29/16 19:03 1
Toluene ND 5.0 ug/Kg 01/29/16 19:03 1
1,2,3-Trichlorobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
1,2,4-Trichlorobenzene ND 5.0 ug/Kg 01/29/16 19:03 1
1,1,1-Trichloroethane ND 5.0 ug/Kg 01/29/16 19:03 1
1,1,2-Trichloroethane ND 5.0 ug/Kg 01/29/16 19:03 1
Trichloroethene ND 5.0 ug/Kg 01/29/16 19:03 1
Trichlorofluoromethane ND 5.0 ug/Kg 01/29/16 19:03 1
1,2,3-Trichloropropane ND 5.0 ug/Kg 01/29/16 19:03 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 5.0 ug/Kg 01/29/16 19:03 1 1,2,4-Trimethylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
1,3,5-Trimethylbenzene ND 5.0 ug/Kg 01/29/16 19:03 1
Vinyl acetate ND 20 ug/Kg 01/29/16 19:03 1
Vinyl chloride ND 5.0 ug/Kg 01/29/16 19:03 1
Xylenes, Total ND 10 ug/Kg 01/29/16 19:03 1
2,2-Dichloropropane ND 5.0 ug/Kg 01/29/16 19:03 1
Gasoline Range Organics (GRO) ND 250 ug/Kg 01/29/16 19:03 1 -C5-C12
4-Bromofluorobenzene 97 45 - 131 01/29/16 19:03 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 113 60 - 140 01/29/16 19:03 1 Toluene-d8 (Surr) 101 58 - 140 01/29/16 19:03 1
Lab Sample ID: LCS 720-196552/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552
Methyl tert-butyl ether 50.0 53.2 ug/Kg 106 70 - 144
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 200 209 ug/Kg 105 30 - 162
Benzene 50.0 51.9 ug/Kg 104 70 - 130
Dichlorobromomethane 50.0 54.1 ug/Kg 108 70 - 140
Bromobenzene 50.0 52.3 ug/Kg 105 70 - 130
Chlorobromomethane 50.0 52.0 ug/Kg 104 70 - 130
Bromoform 50.0 55.2 ug/Kg 110 59 - 158
Bromomethane 50.0 49.0 ug/Kg 98 59 - 132
2-Butanone (MEK) 200 216 ug/Kg 108 53 - 133
n-Butylbenzene 50.0 49.3 ug/Kg 99 70 - 142
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
tert-Butylbenzene 50.0 47.1 ug/Kg 94 70 - 130
Carbon disulfide 50.0 40.5 ug/Kg 81 60 - 140
Carbon tetrachloride 50.0 48.7 ug/Kg 97 70 - 142
Chlorobenzene 50.0 50.9 ug/Kg 102 70 - 130
Chloroethane 50.0 46.9 ug/Kg 94 65 - 130
Chloroform 50.0 47.4 ug/Kg 95 77 - 127
Chloromethane 50.0 47.0 ug/Kg 94 55 - 140
2-Chlorotoluene 50.0 50.9 ug/Kg 102 70 - 138
4-Chlorotoluene 50.0 51.3 ug/Kg 103 70 - 136
Chlorodibromomethane 50.0 53.2 ug/Kg 106 70 - 146
1,2-Dichlorobenzene 50.0 51.8 ug/Kg 104 70 - 130
1,3-Dichlorobenzene 50.0 50.2 ug/Kg 100 70 - 131
1,4-Dichlorobenzene 50.0 50.6 ug/Kg 101 70 - 130
1,3-Dichloropropane 50.0 49.9 ug/Kg 100 70 - 140
1,1-Dichloropropene 50.0 48.7 ug/Kg 97 70 - 130
1,2-Dibromo-3-Chloropropane 50.0 44.5 ug/Kg 89 60 - 145 Ethylene Dibromide 50.0 52.0 ug/Kg 104 70 - 140
Dibromomethane 50.0 52.1 ug/Kg 104 70 - 139
Dichlorodifluoromethane 50.0 57.1 ug/Kg 114 37 - 158
1,1-Dichloroethane 50.0 48.6 ug/Kg 97 70 - 130
1,2-Dichloroethane 50.0 53.8 ug/Kg 108 70 - 130
1,1-Dichloroethene 50.0 39.3 ug/Kg 79 74 - 122
cis-1,2-Dichloroethene 50.0 50.7 ug/Kg 101 70 - 138
trans-1,2-Dichloroethene 50.0 46.5 ug/Kg 93 67 - 130
1,2-Dichloropropane 50.0 52.8 ug/Kg 106 73 - 127
cis-1,3-Dichloropropene 50.0 56.7 ug/Kg 113 68 - 147
trans-1,3-Dichloropropene 50.0 59.5 ug/Kg 119 70 - 155
Ethylbenzene 50.0 50.3 ug/Kg 101 80 - 137
Hexachlorobutadiene 50.0 48.7 ug/Kg 97 70 - 132
2-Hexanone 200 235 ug/Kg 118 44 - 133
Isopropylbenzene 50.0 47.3 ug/Kg 95 70 - 130
4-Isopropyltoluene 50.0 47.2 ug/Kg 94 70 - 133
Methylene Chloride 50.0 46.0 ug/Kg 92 70 - 134
4-Methyl-2-pentanone (MIBK) 200 263 ug/Kg 131 60 - 160
Naphthalene 50.0 48.8 ug/Kg 98 60 - 147
N-Propylbenzene 50.0 48.2 ug/Kg 96 70 - 130
Styrene 50.0 50.5 ug/Kg 101 70 - 130
1,1,1,2-Tetrachloroethane 50.0 56.9 ug/Kg 114 70 - 130
1,1,2,2-Tetrachloroethane 50.0 50.9 ug/Kg 102 70 - 146
Tetrachloroethene 50.0 49.3 ug/Kg 99 70 - 132
Toluene 50.0 50.2 ug/Kg 100 75 - 120
1,2,3-Trichlorobenzene 50.0 52.8 ug/Kg 106 60 - 140
1,2,4-Trichlorobenzene 50.0 54.7 ug/Kg 109 60 - 140
1,1,1-Trichloroethane 50.0 48.0 ug/Kg 96 70 - 130
1,1,2-Trichloroethane 50.0 54.3 ug/Kg 109 70 - 130
Trichloroethene 50.0 50.5 ug/Kg 101 70 - 133
Trichlorofluoromethane 50.0 48.3 ug/Kg 97 60 - 140
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 41.7 ug/Kg 83 60 - 140
1,2,4-Trimethylbenzene 50.0 50.7 ug/Kg 101 70 - 130
1,3,5-Trimethylbenzene 50.0 50.3 ug/Kg 101 70 - 131
Vinyl acetate 50.0 48.1 ug/Kg 96 38 - 176
Vinyl chloride 50.0 49.8 ug/Kg 100 58 - 125
m-Xylene & p-Xylene 50.0 51.6 ug/Kg 103 70 - 146
o-Xylene 50.0 49.6 ug/Kg 99 70 - 140
2,2-Dichloropropane 50.0 48.1 ug/Kg 96 70 - 162
4-Bromofluorobenzene 45 - 131
Surrogate
111

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 103 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCS 720-196552/7 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552
Gasoline Range Organics (GRO)
-C5-C12
1000 1190 ug/Kg 119 61 - 128
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 45 - 131
Surrogate
108

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 104 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCSD 720-196552/6 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552
Methyl tert-butyl ether 50.0 54.3 ug/Kg 109 70 - 144 2 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 200 200 ug/Kg 100 30 - 162 4 30
Benzene 50.0 52.0 ug/Kg 104 70 - 130 0 20
Dichlorobromomethane 50.0 53.0 ug/Kg 106 70 - 140 2 20
Bromobenzene 50.0 52.6 ug/Kg 105 70 - 130 1 20
Chlorobromomethane 50.0 51.6 ug/Kg 103 70 - 130 1 20
Bromoform 50.0 54.2 ug/Kg 108 59 - 158 2 20
Bromomethane 50.0 49.0 ug/Kg 98 59 - 132 0 20
2-Butanone (MEK) 200 216 ug/Kg 108 53 - 133 0 20
n-Butylbenzene 50.0 49.8 ug/Kg 100 70 - 142 1 20
sec-Butylbenzene 50.0 47.4 ug/Kg 95 70 - 136 1 20
tert-Butylbenzene 50.0 47.4 ug/Kg 95 70 - 130 1 20
Carbon disulfide 50.0 41.2 ug/Kg 82 60 - 140 2 20
Carbon tetrachloride 50.0 47.4 ug/Kg 95 70 - 142 3 20
TestAmerica Pleasanton

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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Chloroethane 50.0 47.2 ug/Kg 94 65 - 130 1 20
Chloroform 50.0 46.9 ug/Kg 94 77 - 127 1 20
Chloromethane 50.0 48.3 ug/Kg 97 55 - 140 3 20
2-Chlorotoluene 50.0 50.9 ug/Kg 102 70 - 138 0 20
4-Chlorotoluene 50.0 51.1 ug/Kg 102 70 - 136 0 20
Chlorodibromomethane 50.0 52.1 ug/Kg 104 70 - 146 2 20
1,2-Dichlorobenzene 50.0 52.0 ug/Kg 104 70 - 130 0 20
1,3-Dichlorobenzene 50.0 50.4 ug/Kg 101 70 - 131 0 20
1,4-Dichlorobenzene 50.0 50.6 ug/Kg 101 70 - 130 0 20
1,3-Dichloropropane 50.0 49.4 ug/Kg 99 70 - 140 1 20
1,1-Dichloropropene 50.0 48.2 ug/Kg 96 70 - 130 1 20
1,2-Dibromo-3-Chloropropane 50.0 45.3 ug/Kg 91 60 - 145 2 20 Ethylene Dibromide 50.0 51.7 ug/Kg 103 70 - 140 1 20
Dibromomethane 50.0 51.3 ug/Kg 103 70 - 139 2 20
Dichlorodifluoromethane 50.0 57.2 ug/Kg 114 37 - 158 0 20 1,1-Dichloroethane 50.0 48.6 ug/Kg 97 70 - 130 0 20
1,2-Dichloroethane 50.0 52.7 ug/Kg 105 70 - 130 2 20
1,1-Dichloroethene 50.0 39.6 ug/Kg 79 74 - 122 1 20
cis-1,2-Dichloroethene 50.0 49.7 ug/Kg 99 70 - 138 2 20 trans-1,2-Dichloroethene 50.0 46.4 ug/Kg 93 67 - 130 0 20 1,2-Dichloropropane 50.0 53.1 ug/Kg 106 73 - 127 1 20
cis-1,3-Dichloropropene 50.0 57.2 ug/Kg 114 68 - 147 1 20 trans-1,3-Dichloropropene 50.0 58.6 ug/Kg 117 70 - 155 2 20 Ethylbenzene 50.0 50.3 ug/Kg 101 80 - 137 0 20
Hexachlorobutadiene 50.0 48.3 ug/Kg 97 70 - 132 1 20
2-Hexanone 200 232 ug/Kg 116 44 - 133 1 20
Isopropylbenzene 50.0 47.1 ug/Kg 94 70 - 130 0 20
4-Isopropyltoluene 50.0 47.6 ug/Kg 95 70 - 133 1 20
Methylene Chloride 50.0 46.3 ug/Kg 93 70 - 134 1 20
4-Methyl-2-pentanone (MIBK) 200 262 ug/Kg 131 60 - 160 0 20 Naphthalene 50.0 50.7 ug/Kg 101 60 - 147 4 20
N-Propylbenzene 50.0 48.1 ug/Kg 96 70 - 130 0 20
Styrene 50.0 50.8 ug/Kg 102 70 - 130 0 20
1,1,1,2-Tetrachloroethane 50.0 56.1 ug/Kg 112 70 - 130 1 20 1,1,2,2-Tetrachloroethane 50.0 52.1 ug/Kg 104 70 - 146 2 20 Tetrachloroethene 50.0 48.5 ug/Kg 97 70 - 132 2 20
Toluene 50.0 50.2 ug/Kg 100 75 - 120 0 20
1,2,3-Trichlorobenzene 50.0 54.4 ug/Kg 109 60 - 140 3 20 1,2,4-Trichlorobenzene 50.0 55.7 ug/Kg 111 60 - 140 2 20 1,1,1-Trichloroethane 50.0 47.3 ug/Kg 95 70 - 130 2 20
1,1,2-Trichloroethane 50.0 53.9 ug/Kg 108 70 - 130 1 20 Trichloroethene 50.0 49.5 ug/Kg 99 70 - 133 2 20
Trichlorofluoromethane 50.0 47.1 ug/Kg 94 60 - 140 3 20 1,2,3-Trichloropropane 50.0 49.5 ug/Kg 99 70 - 146 0 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne

50.0 40.8 ug/Kg 82 60 - 140 2 20
1,2,4-Trimethylbenzene 50.0 50.8 ug/Kg 102 70 - 130 0 20 TestAmerica Pleasanton

Page 145 of 210 ends

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Vinyl acetate 50.0 50.3 ug/Kg 101 38 - 176 4 20
Vinyl chloride 50.0 49.6 ug/Kg 99 58 - 125 0 20
m-Xylene & p-Xylene 50.0 51.2 ug/Kg 102 70 - 146 1 20
o-Xylene 50.0 49.7 ug/Kg 99 70 - 140 0 20
2,2-Dichloropropane 50.0 48.3 ug/Kg 97 70 - 162 0 20
4-Bromofluorobenzene 45 - 131
Surrogate
109

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 103 60 - 140
Toluene-d8 (Surr) 110 58 - 140
Lab Sample ID: LCSD 720-196552/8 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552
Gasoline Range Organics (GRO)
-C5-C12
1000 1200 ug/Kg 120 61 - 128 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 45 - 131
Surrogate
110

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 60 - 140
Toluene-d8 (Surr) 111 58 - 140
Lab Sample ID: 720-69933-36 MS Client Sample ID: GP-8-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552 Prep Batch: 196561
Methyl tert-butyl ether ND 58.5 66.9 ug/Kg ☼ 114 69 - 130 Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Acetone ND 234 316 ug/Kg ☼ 135 37 - 150
Benzene ND 58.5 64.6 ug/Kg ☼ 111 70 - 130
Dichlorobromomethane ND 58.5 63.4 ug/Kg ☼ 108 64 - 135
Bromobenzene ND 58.5 66.8 ug/Kg ☼ 114 70 - 130
Chlorobromomethane ND 58.5 62.7 ug/Kg ☼ 107 65 - 130
Bromoform ND 58.5 68.5 ug/Kg ☼ 117 58 - 132
Bromomethane ND 58.5 56.8 ug/Kg ☼ 97 56 - 130
2-Butanone (MEK) ND 234 320 ug/Kg ☼ 137 41 - 150
n-Butylbenzene ND 58.5 62.1 ug/Kg ☼ 106 60 - 145
sec-Butylbenzene ND 58.5 62.1 ug/Kg ☼ 106 64 - 137
tert-Butylbenzene ND 58.5 62.8 ug/Kg ☼ 107 63 - 134
Carbon disulfide ND 58.5 51.5 ug/Kg ☼ 88 10 - 150
Carbon tetrachloride ND 58.5 59.2 ug/Kg ☼ 101 54 - 130
Chlorobenzene ND 58.5 62.1 ug/Kg ☼ 106 70 - 130
Chloroethane ND 58.5 55.5 ug/Kg ☼ 95 61 - 130
Chloroform ND 58.5 56.8 ug/Kg ☼ 97 67 - 130
Chloromethane ND 58.5 55.7 ug/Kg ☼ 95 50 - 131
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Limits
4-Chlorotoluene ND 58.5 65.3 ug/Kg ☼ 112 70 - 130
Chlorodibromomethane ND 58.5 61.9 ug/Kg ☼ 106 60 - 141
1,2-Dichlorobenzene ND 58.5 62.5 ug/Kg ☼ 107 70 - 130
1,3-Dichlorobenzene ND 58.5 61.8 ug/Kg ☼ 106 70 - 130
1,4-Dichlorobenzene ND 58.5 62.3 ug/Kg ☼ 107 70 - 130
1,3-Dichloropropane ND 58.5 60.6 ug/Kg ☼ 104 70 - 130
1,1-Dichloropropene ND 58.5 61.3 ug/Kg ☼ 105 67 - 130
1,2-Dibromo-3-Chloropropane ND 58.5 64.9 ug/Kg ☼ 111 57 - 130 Ethylene Dibromide ND 58.5 64.1 ug/Kg ☼ 110 66 - 135
Dibromomethane ND 58.5 62.5 ug/Kg ☼ 107 65 - 131
Dichlorodifluoromethane ND 58.5 67.3 ug/Kg ☼ 115 38 - 130 1,1-Dichloroethane ND 58.5 60.0 ug/Kg ☼ 103 67 - 130
1,2-Dichloroethane ND 58.5 63.7 ug/Kg ☼ 109 70 - 130
1,1-Dichloroethene ND 58.5 52.4 ug/Kg ☼ 90 64 - 130
cis-1,2-Dichloroethene ND 58.5 60.5 ug/Kg ☼ 103 68 - 131 trans-1,2-Dichloroethene ND 58.5 59.1 ug/Kg ☼ 101 70 - 130 1,2-Dichloropropane ND 58.5 64.5 ug/Kg ☼ 110 65 - 133
cis-1,3-Dichloropropene ND 58.5 67.5 ug/Kg ☼ 116 46 - 139 trans-1,3-Dichloropropene ND 58.5 69.2 ug/Kg ☼ 118 55 - 131 Ethylbenzene ND 58.5 63.6 ug/Kg ☼ 109 65 - 130
Hexachlorobutadiene ND 58.5 53.7 ug/Kg ☼ 92 58 - 132
2-Hexanone ND 234 331 ug/Kg ☼ 142 44 - 150
Isopropylbenzene ND 58.5 59.6 ug/Kg ☼ 102 65 - 130
4-Isopropyltoluene ND 58.5 61.9 ug/Kg ☼ 106 69 - 134
Methylene Chloride ND 58.5 56.7 ug/Kg ☼ 97 63 - 130
4-Methyl-2-pentanone (MIBK) ND F1 234 365 F1 ug/Kg ☼ 156 51 - 140 Naphthalene ND 58.5 59.0 ug/Kg ☼ 101 45 - 146
N-Propylbenzene ND 58.5 64.4 ug/Kg ☼ 110 70 - 130
Styrene ND 58.5 61.1 ug/Kg ☼ 105 58 - 135
1,1,1,2-Tetrachloroethane ND 58.5 68.7 ug/Kg ☼ 117 64 - 133 1,1,2,2-Tetrachloroethane ND 58.5 64.9 ug/Kg ☼ 111 70 - 131 Tetrachloroethene ND 58.5 60.7 ug/Kg ☼ 104 67 - 130
Toluene ND 58.5 64.2 ug/Kg ☼ 110 70 - 130
1,2,3-Trichlorobenzene ND 58.5 57.1 ug/Kg ☼ 98 58 - 138 1,2,4-Trichlorobenzene ND 58.5 58.8 ug/Kg ☼ 101 49 - 144 1,1,1-Trichloroethane ND 58.5 58.2 ug/Kg ☼ 100 57 - 133 1,1,2-Trichloroethane ND 58.5 66.6 ug/Kg ☼ 114 68 - 132 Trichloroethene ND 58.5 67.6 ug/Kg ☼ 116 66 - 130
Trichlorofluoromethane ND 58.5 55.7 ug/Kg ☼ 95 61 - 130 1,2,3-Trichloropropane ND 58.5 72.0 ug/Kg ☼ 123 62 - 150 1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 58.5 52.6 ug/Kg ☼ 90 52 - 130
1,2,4-Trimethylbenzene ND 58.5 65.6 ug/Kg ☼ 112 64 - 140 1,3,5-Trimethylbenzene ND 58.5 66.4 ug/Kg ☼ 114 67 - 134 Vinyl acetate ND F1 F2 58.5 ND F1 ug/Kg ☼ 33 52 - 150
Vinyl chloride ND 58.5 58.1 ug/Kg ☼ 99 62 - 130
m-Xylene & p-Xylene ND 58.5 63.8 ug/Kg ☼ 109 70 - 130
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Limits
2,2-Dichloropropane ND 58.5 54.9 ug/Kg ☼ 94 63 - 130
4-Bromofluorobenzene 45 - 131
Surrogate
105
MS MS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 103 60 - 140
Toluene-d8 (Surr) 109 58 - 140
Lab Sample ID: 720-69933-36 MSD Client Sample ID: GP-8-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196552 Prep Batch: 196561
Methyl tert-butyl ether ND 57.1 61.9 ug/Kg ☼ 109 69 - 130 8 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Acetone ND 228 281 ug/Kg ☼ 123 37 - 150 12 20
Benzene ND 57.1 59.7 ug/Kg ☼ 105 70 - 130 8 20
Dichlorobromomethane ND 57.1 57.7 ug/Kg ☼ 101 64 - 135 9 20 Bromobenzene ND 57.1 64.2 ug/Kg ☼ 112 70 - 130 4 20
Chlorobromomethane ND 57.1 57.9 ug/Kg ☼ 101 65 - 130 8 20 Bromoform ND 57.1 64.6 ug/Kg ☼ 113 58 - 132 6 20
Bromomethane ND 57.1 49.5 ug/Kg ☼ 87 56 - 130 14 20
2-Butanone (MEK) ND 228 277 ug/Kg ☼ 121 41 - 150 14 20
n-Butylbenzene ND 57.1 58.5 ug/Kg ☼ 103 60 - 145 6 20
sec-Butylbenzene ND 57.1 59.2 ug/Kg ☼ 104 64 - 137 5 20 tert-Butylbenzene ND 57.1 60.2 ug/Kg ☼ 105 63 - 134 4 20 Carbon disulfide ND 57.1 47.7 ug/Kg ☼ 84 10 - 150 8 20
Carbon tetrachloride ND 57.1 53.9 ug/Kg ☼ 94 54 - 130 9 20 Chlorobenzene ND 57.1 58.7 ug/Kg ☼ 103 70 - 130 6 20
Chloroethane ND 57.1 49.0 ug/Kg ☼ 86 61 - 130 13 20
Chloroform ND 57.1 52.1 ug/Kg ☼ 91 67 - 130 9 20
Chloromethane ND 57.1 49.7 ug/Kg ☼ 87 50 - 131 11 20
2-Chlorotoluene ND 57.1 63.6 ug/Kg ☼ 111 70 - 130 3 20
4-Chlorotoluene ND 57.1 62.4 ug/Kg ☼ 109 70 - 130 5 20
Chlorodibromomethane ND 57.1 56.9 ug/Kg ☼ 100 60 - 141 8 20 1,2-Dichlorobenzene ND 57.1 58.8 ug/Kg ☼ 103 70 - 130 6 20 1,3-Dichlorobenzene ND 57.1 58.6 ug/Kg ☼ 103 70 - 130 5 20 1,4-Dichlorobenzene ND 57.1 58.8 ug/Kg ☼ 103 70 - 130 6 20 1,3-Dichloropropane ND 57.1 55.7 ug/Kg ☼ 98 70 - 130 9 20 1,1-Dichloropropene ND 57.1 56.0 ug/Kg ☼ 98 67 - 130 9 20 1,2-Dibromo-3-Chloropropane ND 57.1 59.4 ug/Kg ☼ 104 57 - 130 9 20 Ethylene Dibromide ND 57.1 58.1 ug/Kg ☼ 102 66 - 135 10 20 Dibromomethane ND 57.1 57.6 ug/Kg ☼ 101 65 - 131 8 20
Dichlorodifluoromethane ND 57.1 57.0 ug/Kg ☼ 100 38 - 130 17 20 1,1-Dichloroethane ND 57.1 55.9 ug/Kg ☼ 98 67 - 130 7 20 1,2-Dichloroethane ND 57.1 58.3 ug/Kg ☼ 102 70 - 130 9 20 1,1-Dichloroethene ND 57.1 47.8 ug/Kg ☼ 84 64 - 130 9 20 cis-1,2-Dichloroethene ND 57.1 55.8 ug/Kg ☼ 98 68 - 131 8 20 trans-1,2-Dichloroethene ND 57.1 55.4 ug/Kg ☼ 97 70 - 130 6 20 TestAmerica Pleasanton

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MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
cis-1,3-Dichloropropene ND 57.1 62.6 ug/Kg ☼ 110 46 - 139 8 20 trans-1,3-Dichloropropene ND 57.1 63.9 ug/Kg ☼ 112 55 - 131 8 20 Ethylbenzene ND 57.1 60.0 ug/Kg ☼ 105 65 - 130 6 20
Hexachlorobutadiene ND 57.1 50.3 ug/Kg ☼ 88 58 - 132 7 20 2-Hexanone ND 228 292 ug/Kg ☼ 128 44 - 150 13 20
Isopropylbenzene ND 57.1 55.8 ug/Kg ☼ 98 65 - 130 7 20
4-Isopropyltoluene ND 57.1 58.7 ug/Kg ☼ 103 69 - 134 5 20 Methylene Chloride ND 57.1 52.9 ug/Kg ☼ 93 63 - 130 7 20 4-Methyl-2-pentanone (MIBK) ND F1 228 322 F1 ug/Kg ☼ 141 51 - 140 13 20 Naphthalene ND 57.1 54.7 ug/Kg ☼ 96 45 - 146 7 20
N-Propylbenzene ND 57.1 62.7 ug/Kg ☼ 110 70 - 130 3 20
Styrene ND 57.1 57.0 ug/Kg ☼ 100 58 - 135 7 20
1,1,1,2-Tetrachloroethane ND 57.1 65.2 ug/Kg ☼ 114 64 - 133 5 20 1,1,2,2-Tetrachloroethane ND 57.1 60.0 ug/Kg ☼ 105 70 - 131 8 20 Tetrachloroethene ND 57.1 54.8 ug/Kg ☼ 96 67 - 130 10 20 Toluene ND 57.1 60.9 ug/Kg ☼ 107 70 - 130 5 20
1,2,3-Trichlorobenzene ND 57.1 52.9 ug/Kg ☼ 93 58 - 138 8 20 1,2,4-Trichlorobenzene ND 57.1 54.2 ug/Kg ☼ 95 49 - 144 8 20 1,1,1-Trichloroethane ND 57.1 53.6 ug/Kg ☼ 94 57 - 133 8 20 1,1,2-Trichloroethane ND 57.1 61.0 ug/Kg ☼ 107 68 - 132 9 20 Trichloroethene ND 57.1 63.2 ug/Kg ☼ 111 66 - 130 7 20
Trichlorofluoromethane ND 57.1 47.4 ug/Kg ☼ 83 61 - 130 16 20 1,2,3-Trichloropropane ND 57.1 68.5 ug/Kg ☼ 120 62 - 150 5 20 1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 57.1 48.1 ug/Kg ☼ 84 52 - 130 9 20
1,2,4-Trimethylbenzene ND 57.1 62.5 ug/Kg ☼ 110 64 - 140 5 20 1,3,5-Trimethylbenzene ND 57.1 63.2 ug/Kg ☼ 111 67 - 134 5 20 Vinyl acetate ND F1 F2 57.1 ND F1 F2 ug/Kg ☼ 20 52 - 150 48 20 Vinyl chloride ND 57.1 51.3 ug/Kg ☼ 90 62 - 130 12 20
m-Xylene & p-Xylene ND 57.1 60.4 ug/Kg ☼ 106 70 - 130 5 20 o-Xylene ND 57.1 57.4 ug/Kg ☼ 101 68 - 130 6 20
2,2-Dichloropropane ND 57.1 52.6 ug/Kg ☼ 92 63 - 130 4 20 4-Bromofluorobenzene 45 - 131
Surrogate
105

MSD MSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 60 - 140
Toluene-d8 (Surr) 107 58 - 140
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS
Lab Sample ID: MB 720-196234/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 196234
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 08:51 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 08:51 1
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1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) Lab Sample ID: MB 720-196234/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 196234
RL MDL
Benzene ND 0.50 ug/L 01/26/16 08:51 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dichlorobromomethane ND 0.50 ug/L 01/26/16 08:51 1
Bromobenzene ND 1.0 ug/L 01/26/16 08:51 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 08:51 1
Bromoform ND 1.0 ug/L 01/26/16 08:51 1
Bromomethane ND 1.0 ug/L 01/26/16 08:51 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 08:51 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 08:51 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 08:51 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 08:51 1
Carbon disulfide ND 5.0 ug/L 01/26/16 08:51 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 08:51 1
Chlorobenzene ND 0.50 ug/L 01/26/16 08:51 1
Chloroethane ND 1.0 ug/L 01/26/16 08:51 1
Chloroform ND 1.0 ug/L 01/26/16 08:51 1
Chloromethane ND 1.0 ug/L 01/26/16 08:51 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 08:51 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 08:51 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 08:51 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 08:51 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 08:51 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 08:51 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 08:51 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 08:51 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 08:51 1 Ethylene Dibromide ND 0.50 ug/L 01/26/16 08:51 1
Dibromomethane ND 0.50 ug/L 01/26/16 08:51 1
Dichlorodifluoromethane ND 0.50 ug/L 01/26/16 08:51 1
1,1-Dichloroethane ND 0.50 ug/L 01/26/16 08:51 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 08:51 1
1,1-Dichloroethene ND 0.50 ug/L 01/26/16 08:51 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 08:51 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 08:51 1
1,2-Dichloropropane ND 0.50 ug/L 01/26/16 08:51 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 08:51 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 08:51 1 Ethylbenzene ND 0.50 ug/L 01/26/16 08:51 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 08:51 1
2-Hexanone ND 50 ug/L 01/26/16 08:51 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 08:51 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 08:51 1
Methylene Chloride ND 5.0 ug/L 01/26/16 08:51 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 08:51 1 Naphthalene ND 1.0 ug/L 01/26/16 08:51 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 08:51 1
Styrene ND 0.50 ug/L 01/26/16 08:51 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 08:51 1 1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 08:51 1 TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 67 - 130
Surrogate
99 LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 72 - 130
Toluene-d8 (Surr) 103 70 - 130
Lab Sample ID: LCS 720-196234/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 196234
Methyl tert-butyl ether 25.0 25.1 ug/L 100 62 - 130
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 100 97.3 ug/L 97 26 - 180
Benzene 25.0 25.7 ug/L 103 79 - 130
Dichlorobromomethane 25.0 27.1 ug/L 109 70 - 130
Bromobenzene 25.0 26.5 ug/L 106 70 - 130
Chlorobromomethane 25.0 26.8 ug/L 107 70 - 130
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Bromomethane 25.0 28.2 ug/L 113 43 - 151
2-Butanone (MEK) 100 102 ug/L 102 54 - 130
n-Butylbenzene 25.0 27.3 ug/L 109 70 - 142
sec-Butylbenzene 25.0 26.8 ug/L 107 70 - 134
tert-Butylbenzene 25.0 26.8 ug/L 107 70 - 135
Carbon disulfide 25.0 22.4 ug/L 90 58 - 130
Carbon tetrachloride 25.0 26.2 ug/L 105 70 - 146
Chlorobenzene 25.0 26.6 ug/L 106 70 - 130
Chloroethane 25.0 24.9 ug/L 100 62 - 138
Chloroform 25.0 26.5 ug/L 106 70 - 130
Chloromethane 25.0 26.4 ug/L 106 52 - 175
2-Chlorotoluene 25.0 26.2 ug/L 105 70 - 130
4-Chlorotoluene 25.0 27.0 ug/L 108 70 - 130
Chlorodibromomethane 25.0 27.3 ug/L 109 70 - 145
1,2-Dichlorobenzene 25.0 26.2 ug/L 105 70 - 130
1,3-Dichlorobenzene 25.0 25.8 ug/L 103 70 - 130
1,4-Dichlorobenzene 25.0 26.4 ug/L 106 70 - 130
1,3-Dichloropropane 25.0 25.6 ug/L 102 70 - 130
1,1-Dichloropropene 25.0 26.8 ug/L 107 70 - 130
1,2-Dibromo-3-Chloropropane 25.0 25.7 ug/L 103 70 - 136 Ethylene Dibromide 25.0 27.7 ug/L 111 70 - 130
Dibromomethane 25.0 26.5 ug/L 106 70 - 130
Dichlorodifluoromethane 25.0 29.1 ug/L 116 34 - 132
1,1-Dichloroethane 25.0 25.9 ug/L 103 70 - 130
1,2-Dichloroethane 25.0 25.2 ug/L 101 61 - 132
1,1-Dichloroethene 25.0 23.7 ug/L 95 64 - 128
cis-1,2-Dichloroethene 25.0 26.4 ug/L 106 70 - 130
trans-1,2-Dichloroethene 25.0 25.4 ug/L 102 68 - 130
1,2-Dichloropropane 25.0 26.6 ug/L 106 70 - 130
cis-1,3-Dichloropropene 25.0 28.2 ug/L 113 70 - 130
trans-1,3-Dichloropropene 25.0 28.5 ug/L 114 70 - 140
Ethylbenzene 25.0 27.1 ug/L 108 80 - 120
Hexachlorobutadiene 25.0 26.4 ug/L 106 70 - 130
2-Hexanone 100 101 ug/L 101 60 - 164
Isopropylbenzene 25.0 28.2 ug/L 113 70 - 130
4-Isopropyltoluene 25.0 26.5 ug/L 106 70 - 130
Methylene Chloride 25.0 24.1 ug/L 96 70 - 147
4-Methyl-2-pentanone (MIBK) 100 108 ug/L 108 58 - 130
Naphthalene 25.0 24.6 ug/L 99 70 - 130
N-Propylbenzene 25.0 27.3 ug/L 109 70 - 130
Styrene 25.0 27.3 ug/L 109 70 - 130
1,1,1,2-Tetrachloroethane 25.0 26.9 ug/L 107 70 - 130
1,1,2,2-Tetrachloroethane 25.0 25.9 ug/L 103 70 - 130
Tetrachloroethene 25.0 26.8 ug/L 107 70 - 130
Toluene 25.0 27.4 ug/L 110 78 - 120
1,2,3-Trichlorobenzene 25.0 25.6 ug/L 103 70 - 130
1,2,4-Trichlorobenzene 25.0 26.6 ug/L 106 70 - 130
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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,2-Trichloroethane 25.0 26.8 ug/L 107 70 - 130
Trichloroethene 25.0 27.3 ug/L 109 70 - 130
Trichlorofluoromethane 25.0 26.5 ug/L 106 66 - 132
1,2,3-Trichloropropane 25.0 25.7 ug/L 103 70 - 130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

25.0 24.1 ug/L 96 42 - 162
1,2,4-Trimethylbenzene 25.0 26.7 ug/L 107 70 - 132
1,3,5-Trimethylbenzene 25.0 27.1 ug/L 109 70 - 130
Vinyl acetate 25.0 24.9 ug/L 99 43 - 163
Vinyl chloride 25.0 27.6 ug/L 111 54 - 135
m-Xylene & p-Xylene 25.0 26.8 ug/L 107 70 - 142
o-Xylene 25.0 26.8 ug/L 107 70 - 130
2,2-Dichloropropane 25.0 26.3 ug/L 105 70 - 140
4-Bromofluorobenzene 67 - 130
Surrogate
104

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 89 72 - 130
Toluene-d8 (Surr) 102 70 - 130
Lab Sample ID: LCSD 720-196234/15 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 196234
Gasoline Range Organics (GRO)
-C5-C12
500 500 ug/L 100 62 - 120 0 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 67 - 130
Surrogate
104

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 72 - 130
Toluene-d8 (Surr) 106 70 - 130
Lab Sample ID: LCSD 720-196234/6 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 196234
Methyl tert-butyl ether 25.0 26.4 ug/L 106 62 - 130 5 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 100 106 ug/L 106 26 - 180 8 30
Benzene 25.0 26.2 ug/L 105 79 - 130 2 20
Dichlorobromomethane 25.0 27.7 ug/L 111 70 - 130 2 20
Bromobenzene 25.0 26.0 ug/L 104 70 - 130 2 20
Chlorobromomethane 25.0 27.8 ug/L 111 70 - 130 4 20
Bromoform 25.0 29.8 ug/L 119 68 - 136 3 20
Bromomethane 25.0 29.2 ug/L 117 43 - 151 4 20
2-Butanone (MEK) 100 111 ug/L 111 54 - 130 8 20
n-Butylbenzene 25.0 26.7 ug/L 107 70 - 142 2 20
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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
tert-Butylbenzene 25.0 26.4 ug/L 106 70 - 135 2 20
Carbon disulfide 25.0 22.5 ug/L 90 58 - 130 1 20
Carbon tetrachloride 25.0 26.8 ug/L 107 70 - 146 2 20
Chlorobenzene 25.0 27.0 ug/L 108 70 - 130 2 20
Chloroethane 25.0 24.0 ug/L 96 62 - 138 4 20
Chloroform 25.0 26.7 ug/L 107 70 - 130 1 20
Chloromethane 25.0 27.8 ug/L 111 52 - 175 5 20
2-Chlorotoluene 25.0 25.6 ug/L 103 70 - 130 2 20
4-Chlorotoluene 25.0 26.2 ug/L 105 70 - 130 3 20
Chlorodibromomethane 25.0 27.8 ug/L 111 70 - 145 2 20
1,2-Dichlorobenzene 25.0 26.1 ug/L 105 70 - 130 0 20
1,3-Dichlorobenzene 25.0 25.7 ug/L 103 70 - 130 0 20
1,4-Dichlorobenzene 25.0 26.1 ug/L 104 70 - 130 1 20
1,3-Dichloropropane 25.0 27.5 ug/L 110 70 - 130 7 20
1,1-Dichloropropene 25.0 27.3 ug/L 109 70 - 130 2 20
1,2-Dibromo-3-Chloropropane 25.0 27.0 ug/L 108 70 - 136 5 20 Ethylene Dibromide 25.0 28.9 ug/L 115 70 - 130 4 20
Dibromomethane 25.0 27.3 ug/L 109 70 - 130 3 20
Dichlorodifluoromethane 25.0 30.4 ug/L 122 34 - 132 5 20 1,1-Dichloroethane 25.0 26.6 ug/L 106 70 - 130 3 20
1,2-Dichloroethane 25.0 26.1 ug/L 104 61 - 132 3 20
1,1-Dichloroethene 25.0 24.0 ug/L 96 64 - 128 1 20
cis-1,2-Dichloroethene 25.0 27.2 ug/L 109 70 - 130 3 20 trans-1,2-Dichloroethene 25.0 25.9 ug/L 104 68 - 130 2 20 1,2-Dichloropropane 25.0 27.9 ug/L 111 70 - 130 5 20
cis-1,3-Dichloropropene 25.0 29.1 ug/L 116 70 - 130 3 20 trans-1,3-Dichloropropene 25.0 29.7 ug/L 119 70 - 140 4 20 Ethylbenzene 25.0 27.6 ug/L 110 80 - 120 2 20
Hexachlorobutadiene 25.0 25.5 ug/L 102 70 - 130 3 20
2-Hexanone 100 111 ug/L 111 60 - 164 10 20
Isopropylbenzene 25.0 28.6 ug/L 115 70 - 130 2 20
4-Isopropyltoluene 25.0 25.7 ug/L 103 70 - 130 3 20
Methylene Chloride 25.0 24.5 ug/L 98 70 - 147 2 20
4-Methyl-2-pentanone (MIBK) 100 116 ug/L 116 58 - 130 7 20 Naphthalene 25.0 25.6 ug/L 102 70 - 130 4 20
N-Propylbenzene 25.0 26.4 ug/L 106 70 - 130 3 20
Styrene 25.0 27.6 ug/L 110 70 - 130 1 20
1,1,1,2-Tetrachloroethane 25.0 27.3 ug/L 109 70 - 130 2 20 1,1,2,2-Tetrachloroethane 25.0 26.3 ug/L 105 70 - 130 2 20 Tetrachloroethene 25.0 27.1 ug/L 109 70 - 130 1 20
Toluene 25.0 27.6 ug/L 110 78 - 120 1 20
1,2,3-Trichlorobenzene 25.0 25.8 ug/L 103 70 - 130 1 20 1,2,4-Trichlorobenzene 25.0 26.5 ug/L 106 70 - 130 1 20 1,1,1-Trichloroethane 25.0 25.9 ug/L 103 70 - 130 1 20
1,1,2-Trichloroethane 25.0 27.8 ug/L 111 70 - 130 4 20
Trichloroethene 25.0 27.6 ug/L 111 70 - 130 1 20
Trichlorofluoromethane 25.0 27.0 ug/L 108 66 - 132 2 20 TestAmerica Pleasanton

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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

25.0 24.5 ug/L 98 42 - 162 2 20
1,2,4-Trimethylbenzene 25.0 26.4 ug/L 106 70 - 132 1 20 1,3,5-Trimethylbenzene 25.0 26.7 ug/L 107 70 - 130 2 20 Vinyl acetate 25.0 26.1 ug/L 104 43 - 163 5 20
Vinyl chloride 25.0 28.4 ug/L 114 54 - 135 3 20
m-Xylene & p-Xylene 25.0 27.2 ug/L 109 70 - 142 1 20
o-Xylene 25.0 27.3 ug/L 109 70 - 130 2 20
2,2-Dichloropropane 25.0 26.4 ug/L 105 70 - 140 0 20
4-Bromofluorobenzene 67 - 130
Surrogate
106

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 92 72 - 130
Toluene-d8 (Surr) 106 70 - 130
Lab Sample ID: MB 720-196293/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 196293
RL MDL
Methyl tert-butyl ether ND 0.50 ug/L 01/26/16 19:22 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Acetone ND 50 ug/L 01/26/16 19:22 1
Benzene ND 0.50 ug/L 01/26/16 19:22 1
Dichlorobromomethane ND 0.50 ug/L 01/26/16 19:22 1
Bromobenzene ND 1.0 ug/L 01/26/16 19:22 1
Chlorobromomethane ND 1.0 ug/L 01/26/16 19:22 1
Bromoform ND 1.0 ug/L 01/26/16 19:22 1
Bromomethane ND 1.0 ug/L 01/26/16 19:22 1
2-Butanone (MEK) ND 50 ug/L 01/26/16 19:22 1
n-Butylbenzene ND 1.0 ug/L 01/26/16 19:22 1
sec-Butylbenzene ND 1.0 ug/L 01/26/16 19:22 1
tert-Butylbenzene ND 1.0 ug/L 01/26/16 19:22 1
Carbon disulfide ND 5.0 ug/L 01/26/16 19:22 1
Carbon tetrachloride ND 0.50 ug/L 01/26/16 19:22 1
Chlorobenzene ND 0.50 ug/L 01/26/16 19:22 1
Chloroethane ND 1.0 ug/L 01/26/16 19:22 1
Chloroform ND 1.0 ug/L 01/26/16 19:22 1
Chloromethane ND 1.0 ug/L 01/26/16 19:22 1
2-Chlorotoluene ND 0.50 ug/L 01/26/16 19:22 1
4-Chlorotoluene ND 0.50 ug/L 01/26/16 19:22 1
Chlorodibromomethane ND 0.50 ug/L 01/26/16 19:22 1
1,2-Dichlorobenzene ND 0.50 ug/L 01/26/16 19:22 1
1,3-Dichlorobenzene ND 0.50 ug/L 01/26/16 19:22 1
1,4-Dichlorobenzene ND 0.50 ug/L 01/26/16 19:22 1
1,3-Dichloropropane ND 1.0 ug/L 01/26/16 19:22 1
1,1-Dichloropropene ND 0.50 ug/L 01/26/16 19:22 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 01/26/16 19:22 1 TestAmerica Pleasanton

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1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8260B/CA_LUFTMS - 8260B / CA LUFT MS (Continued) Lab Sample ID: MB 720-196293/4 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 196293
RL MDL
Ethylene Dibromide ND 0.50 ug/L 01/26/16 19:22 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dibromomethane ND 0.50 ug/L 01/26/16 19:22 1
Dichlorodifluoromethane ND 0.50 ug/L 01/26/16 19:22 1
1,1-Dichloroethane ND 0.50 ug/L 01/26/16 19:22 1
1,2-Dichloroethane ND 0.50 ug/L 01/26/16 19:22 1
1,1-Dichloroethene ND 0.50 ug/L 01/26/16 19:22 1
cis-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 19:22 1
trans-1,2-Dichloroethene ND 0.50 ug/L 01/26/16 19:22 1
1,2-Dichloropropane ND 0.50 ug/L 01/26/16 19:22 1
cis-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 19:22 1
trans-1,3-Dichloropropene ND 0.50 ug/L 01/26/16 19:22 1 Ethylbenzene ND 0.50 ug/L 01/26/16 19:22 1
Hexachlorobutadiene ND 1.0 ug/L 01/26/16 19:22 1
2-Hexanone ND 50 ug/L 01/26/16 19:22 1
Isopropylbenzene ND 0.50 ug/L 01/26/16 19:22 1
4-Isopropyltoluene ND 1.0 ug/L 01/26/16 19:22 1
Methylene Chloride ND 5.0 ug/L 01/26/16 19:22 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 01/26/16 19:22 1 Naphthalene ND 1.0 ug/L 01/26/16 19:22 1
N-Propylbenzene ND 1.0 ug/L 01/26/16 19:22 1
Styrene ND 0.50 ug/L 01/26/16 19:22 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 19:22 1 1,1,2,2-Tetrachloroethane ND 0.50 ug/L 01/26/16 19:22 1 Tetrachloroethene ND 0.50 ug/L 01/26/16 19:22 1
Toluene ND 0.50 ug/L 01/26/16 19:22 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 01/26/16 19:22 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 01/26/16 19:22 1
1,1,1-Trichloroethane ND 0.50 ug/L 01/26/16 19:22 1
1,1,2-Trichloroethane ND 0.50 ug/L 01/26/16 19:22 1
Trichloroethene ND 0.50 ug/L 01/26/16 19:22 1
Trichlorofluoromethane ND 1.0 ug/L 01/26/16 19:22 1
1,2,3-Trichloropropane ND 0.50 ug/L 01/26/16 19:22 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 01/26/16 19:22 1 1,2,4-Trimethylbenzene ND 0.50 ug/L 01/26/16 19:22 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 01/26/16 19:22 1
Vinyl acetate ND 10 ug/L 01/26/16 19:22 1
Vinyl chloride ND 0.50 ug/L 01/26/16 19:22 1
Xylenes, Total ND 1.0 ug/L 01/26/16 19:22 1
2,2-Dichloropropane ND 0.50 ug/L 01/26/16 19:22 1
Gasoline Range Organics (GRO) ND 50 ug/L 01/26/16 19:22 1 -C5-C12
4-Bromofluorobenzene 99 67 - 130 01/26/16 19:22 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 118 72 - 130 01/26/16 19:22 1 Toluene-d8 (Surr) 98 70 - 130 01/26/16 19:22 1
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Acetone 125 117 ug/L 93 26 - 180
Benzene 25.0 23.7 ug/L 95 79 - 130
Dichlorobromomethane 25.0 27.8 ug/L 111 70 - 130
Bromobenzene 25.0 25.5 ug/L 102 70 - 130
Chlorobromomethane 25.0 28.1 ug/L 112 70 - 130
Bromoform 25.0 27.5 ug/L 110 68 - 136
Bromomethane 25.0 30.2 ug/L 121 43 - 151
2-Butanone (MEK) 125 131 ug/L 105 54 - 130
n-Butylbenzene 25.0 21.4 ug/L 86 70 - 142
sec-Butylbenzene 25.0 22.8 ug/L 91 70 - 134
tert-Butylbenzene 25.0 24.2 ug/L 97 70 - 135
Carbon disulfide 25.0 28.6 ug/L 115 58 - 130
Carbon tetrachloride 25.0 31.6 ug/L 126 70 - 146
Chlorobenzene 25.0 25.2 ug/L 101 70 - 130
Chloroethane 25.0 25.5 ug/L 102 62 - 138
Chloroform 25.0 26.9 ug/L 108 70 - 130
Chloromethane 25.0 23.3 ug/L 93 52 - 175
2-Chlorotoluene 25.0 24.5 ug/L 98 70 - 130
4-Chlorotoluene 25.0 23.5 ug/L 94 70 - 130
Chlorodibromomethane 25.0 29.2 ug/L 117 70 - 145
1,2-Dichlorobenzene 25.0 24.4 ug/L 98 70 - 130
1,3-Dichlorobenzene 25.0 24.7 ug/L 99 70 - 130
1,4-Dichlorobenzene 25.0 24.6 ug/L 98 70 - 130
1,3-Dichloropropane 25.0 24.3 ug/L 97 70 - 130
1,1-Dichloropropene 25.0 25.9 ug/L 103 70 - 130
1,2-Dibromo-3-Chloropropane 25.0 23.2 ug/L 93 70 - 136
Ethylene Dibromide 25.0 25.7 ug/L 103 70 - 130
Dibromomethane 25.0 26.4 ug/L 106 70 - 130
Dichlorodifluoromethane 25.0 35.4 * ug/L 141 34 - 132
1,1-Dichloroethane 25.0 24.0 ug/L 96 70 - 130
1,2-Dichloroethane 25.0 29.0 ug/L 116 61 - 132
1,1-Dichloroethene 25.0 26.8 ug/L 107 64 - 128
cis-1,2-Dichloroethene 25.0 25.2 ug/L 101 70 - 130
trans-1,2-Dichloroethene 25.0 25.6 ug/L 102 68 - 130
1,2-Dichloropropane 25.0 21.9 ug/L 88 70 - 130
cis-1,3-Dichloropropene 25.0 26.0 ug/L 104 70 - 130
trans-1,3-Dichloropropene 25.0 27.4 ug/L 110 70 - 140
Ethylbenzene 25.0 22.2 ug/L 89 80 - 120
Hexachlorobutadiene 25.0 26.3 ug/L 105 70 - 130
2-Hexanone 125 118 ug/L 94 60 - 164
Isopropylbenzene 25.0 23.6 ug/L 94 70 - 130
4-Isopropyltoluene 25.0 23.6 ug/L 95 70 - 130
Methylene Chloride 25.0 26.6 ug/L 106 70 - 147
4-Methyl-2-pentanone (MIBK) 125 113 ug/L 91 58 - 130
Naphthalene 25.0 21.5 ug/L 86 70 - 130
N-Propylbenzene 25.0 23.8 ug/L 95 70 - 130
Styrene 25.0 23.3 ug/L 93 70 - 130
TestAmerica Pleasanton

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LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
1,1,2,2-Tetrachloroethane 25.0 20.5 ug/L 82 70 - 130
Tetrachloroethene 25.0 26.7 ug/L 107 70 - 130
Toluene 25.0 22.1 ug/L 88 78 - 120
1,2,3-Trichlorobenzene 25.0 24.7 ug/L 99 70 - 130
1,2,4-Trichlorobenzene 25.0 25.0 ug/L 100 70 - 130
1,1,1-Trichloroethane 25.0 30.1 ug/L 120 70 - 130
1,1,2-Trichloroethane 25.0 23.8 ug/L 95 70 - 130
Trichloroethene 25.0 27.4 ug/L 110 70 - 130
Trichlorofluoromethane 25.0 33.1 * ug/L 133 66 - 132
1,2,3-Trichloropropane 25.0 23.4 ug/L 94 70 - 130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

25.0 33.0 ug/L 132 42 - 162
1,2,4-Trimethylbenzene 25.0 24.8 ug/L 99 70 - 132
1,3,5-Trimethylbenzene 25.0 23.0 ug/L 92 70 - 130
Vinyl acetate 25.0 23.2 ug/L 93 43 - 163
Vinyl chloride 25.0 26.7 ug/L 107 54 - 135
m-Xylene & p-Xylene 25.0 24.9 ug/L 100 70 - 142
o-Xylene 25.0 25.8 ug/L 103 70 - 130
2,2-Dichloropropane 25.0 29.4 ug/L 117 70 - 140
4-Bromofluorobenzene 67 - 130
Surrogate
101

LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 112 72 - 130
Toluene-d8 (Surr) 101 70 - 130
Lab Sample ID: LCS 720-196293/7 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 196293
Gasoline Range Organics (GRO)
-C5-C12
500 523 ug/L 105 62 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
4-Bromofluorobenzene 67 - 130
Surrogate
97 LCS LCS
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 110 72 - 130
Toluene-d8 (Surr) 100 70 - 130
Lab Sample ID: LCSD 720-196293/6 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 196293
Methyl tert-butyl ether 25.0 26.8 ug/L 107 62 - 130 2 20 Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Acetone 125 117 ug/L 94 26 - 180 0 30
Benzene 25.0 23.5 ug/L 94 79 - 130 1 20
Dichlorobromomethane 25.0 27.4 ug/L 109 70 - 130 2 20
TestAmerica Pleasanton

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LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Chlorobromomethane 25.0 27.2 ug/L 109 70 - 130 3 20
Bromoform 25.0 27.5 ug/L 110 68 - 136 0 20
Bromomethane 25.0 29.5 ug/L 118 43 - 151 2 20
2-Butanone (MEK) 125 122 ug/L 97 54 - 130 7 20
n-Butylbenzene 25.0 21.4 ug/L 85 70 - 142 0 20
sec-Butylbenzene 25.0 23.1 ug/L 92 70 - 134 1 20
tert-Butylbenzene 25.0 24.2 ug/L 97 70 - 135 0 20
Carbon disulfide 25.0 28.0 ug/L 112 58 - 130 2 20
Carbon tetrachloride 25.0 30.9 ug/L 124 70 - 146 2 20
Chlorobenzene 25.0 25.4 ug/L 102 70 - 130 1 20
Chloroethane 25.0 25.0 ug/L 100 62 - 138 2 20
Chloroform 25.0 26.7 ug/L 107 70 - 130 1 20
Chloromethane 25.0 23.3 ug/L 93 52 - 175 0 20
2-Chlorotoluene 25.0 24.2 ug/L 97 70 - 130 1 20
4-Chlorotoluene 25.0 23.5 ug/L 94 70 - 130 0 20
Chlorodibromomethane 25.0 28.0 ug/L 112 70 - 145 4 20
1,2-Dichlorobenzene 25.0 24.6 ug/L 98 70 - 130 1 20
1,3-Dichlorobenzene 25.0 24.8 ug/L 99 70 - 130 0 20
1,4-Dichlorobenzene 25.0 24.7 ug/L 99 70 - 130 0 20
1,3-Dichloropropane 25.0 23.5 ug/L 94 70 - 130 3 20
1,1-Dichloropropene 25.0 25.4 ug/L 102 70 - 130 2 20
1,2-Dibromo-3-Chloropropane 25.0 23.2 ug/L 93 70 - 136 0 20 Ethylene Dibromide 25.0 25.2 ug/L 101 70 - 130 2 20
Dibromomethane 25.0 25.8 ug/L 103 70 - 130 2 20
Dichlorodifluoromethane 25.0 34.4 * ug/L 138 34 - 132 3 20 1,1-Dichloroethane 25.0 23.7 ug/L 95 70 - 130 1 20
1,2-Dichloroethane 25.0 28.0 ug/L 112 61 - 132 3 20
1,1-Dichloroethene 25.0 26.0 ug/L 104 64 - 128 3 20
cis-1,2-Dichloroethene 25.0 24.9 ug/L 99 70 - 130 2 20
trans-1,2-Dichloroethene 25.0 25.1 ug/L 100 68 - 130 2 20 1,2-Dichloropropane 25.0 21.7 ug/L 87 70 - 130 1 20
cis-1,3-Dichloropropene 25.0 25.5 ug/L 102 70 - 130 2 20 trans-1,3-Dichloropropene 25.0 26.6 ug/L 106 70 - 140 3 20 Ethylbenzene 25.0 22.5 ug/L 90 80 - 120 1 20
Hexachlorobutadiene 25.0 25.9 ug/L 104 70 - 130 2 20
2-Hexanone 125 111 ug/L 89 60 - 164 6 20
Isopropylbenzene 25.0 23.9 ug/L 95 70 - 130 1 20
4-Isopropyltoluene 25.0 23.7 ug/L 95 70 - 130 0 20
Methylene Chloride 25.0 26.5 ug/L 106 70 - 147 0 20
4-Methyl-2-pentanone (MIBK) 125 108 ug/L 86 58 - 130 5 20 Naphthalene 25.0 21.2 ug/L 85 70 - 130 1 20
N-Propylbenzene 25.0 23.9 ug/L 96 70 - 130 1 20
Styrene 25.0 23.5 ug/L 94 70 - 130 1 20
1,1,1,2-Tetrachloroethane 25.0 26.6 ug/L 106 70 - 130 1 20 1,1,2,2-Tetrachloroethane 25.0 20.2 ug/L 81 70 - 130 1 20 Tetrachloroethene 25.0 26.3 ug/L 105 70 - 130 2 20
Toluene 25.0 22.8 ug/L 91 78 - 120 3 20
TestAmerica Pleasanton

Page 159 of 210 ends

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
1,2,4-Trichlorobenzene 25.0 24.5 ug/L 98 70 - 130 2 20
1,1,1-Trichloroethane 25.0 29.9 ug/L 120 70 - 130 1 20
1,1,2-Trichloroethane 25.0 22.6 ug/L 90 70 - 130 5 20
Trichloroethene 25.0 27.2 ug/L 109 70 - 130 1 20
Trichlorofluoromethane 25.0 31.8 ug/L 127 66 - 132 4 20 1,2,3-Trichloropropane 25.0 23.6 ug/L 94 70 - 130 1 20
1,1,2-Trichloro-1,2,2-trifluoroetha
ne

25.0 31.8 ug/L 127 42 - 162 4 20
1,2,4-Trimethylbenzene 25.0 24.7 ug/L 99 70 - 132 0 20
1,3,5-Trimethylbenzene 25.0 23.4 ug/L 94 70 - 130 2 20
Vinyl acetate 25.0 22.0 ug/L 88 43 - 163 5 20
Vinyl chloride 25.0 26.8 ug/L 107 54 - 135 0 20
m-Xylene & p-Xylene 25.0 25.3 ug/L 101 70 - 142 1 20
o-Xylene 25.0 25.9 ug/L 104 70 - 130 1 20
2,2-Dichloropropane 25.0 28.1 ug/L 112 70 - 140 4 20
4-Bromofluorobenzene 67 - 130
Surrogate
101

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 109 72 - 130
Toluene-d8 (Surr) 101 70 - 130
Lab Sample ID: LCSD 720-196293/8 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 196293
Gasoline Range Organics (GRO)
-C5-C12
500 557 ug/L 111 62 - 120 6 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
4-Bromofluorobenzene 67 - 130
Surrogate
101

LCSD LCSD
%Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 107 72 - 130
Toluene-d8 (Surr) 100 70 - 130
Method: 8015B - Diesel Range Organics (DRO) (GC)
Lab Sample ID: MB 720-196382/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 196414 Prep Batch: 196382
RL MDL
Diesel Range Organics [C10-C28] ND 50 ug/L 01/27/16 16:40 01/28/16 12:26 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 99 ug/L 01/27/16 16:40 01/28/16 12:26 1 Capric Acid (Surr) 0.008 0 - 5 01/28/16 12:26 1
MB MB
Surrogate
01/27/16 16:40
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
TestAmerica Pleasanton

Page 160 of 210 ends

1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued) Lab Sample ID: MB 720-196382/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 196414 Prep Batch: 196382
p-Terphenyl 105 31 - 150 01/28/16 12:26 1
MB MB
Surrogate
01/27/16 16:40
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
Lab Sample ID: LCS 720-196382/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 196414 Prep Batch: 196382
Diesel Range Organics
[C10-C28]
2500 1610 ug/L 64 32 - 119
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
p-Terphenyl 31 - 150
Surrogate
99 LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: LCSD 720-196382/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Silica Gel Cleanup
Analysis Batch: 196414 Prep Batch: 196382
Diesel Range Organics
[C10-C28]
2500 1970 ug/L 79 32 - 119 20 35
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
p-Terphenyl 31 - 150
Surrogate
88 LCSD LCSD
%Recovery Qualifier Limits
Lab Sample ID: MB 720-196403/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 196415 Prep Batch: 196403
RL MDL
Diesel Range Organics [C10-C28] ND 1.0 mg/Kg 01/27/16 20:37 01/29/16 00:34 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 50 mg/Kg 01/27/16 20:37 01/29/16 00:34 1 Capric Acid (Surr) 0 0 - 1 01/29/16 00:34 1
MB MB
Surrogate
01/27/16 20:37
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
p-Terphenyl 123 38 - 148 01/27/16 20:37 01/29/16 00:34 1 Lab Sample ID: LCS 720-196403/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 196415 Prep Batch: 196403
Diesel Range Organics
[C10-C28]

83.3 56.2 mg/Kg 67 36 - 112
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
p-Terphenyl 38 - 148
Surrogate
107

LCS LCS
%Recovery Qualifier Limits
TestAmerica Pleasanton

Page 161 of 210 ends

1 2
3 4
5 6
7 8
9 10
11 12
13 14
QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued) Lab Sample ID: MB 720-196404/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 196415 Prep Batch: 196404
RL MDL
Diesel Range Organics [C10-C28] ND 1.0 mg/Kg 01/27/16 21:05 01/29/16 03:47 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Motor Oil Range Organics [C24-C36] ND 50 mg/Kg 01/27/16 21:05 01/29/16 03:47 1 Capric Acid (Surr) 0.002 0 - 1 01/29/16 03:47 1
MB MB
Surrogate
01/27/16 21:05
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
p-Terphenyl 94 38 - 148 01/27/16 21:05 01/29/16 03:47 1 Lab Sample ID: LCS 720-196404/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 196415 Prep Batch: 196404
Diesel Range Organics
[C10-C28]

83.3 52.6 mg/Kg 63 36 - 112
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
p-Terphenyl 38 - 148
Surrogate
102

LCS LCS
%Recovery Qualifier Limits
Lab Sample ID: 720-69933-43 MS Client Sample ID: GP-10-3.5-4' Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 196414 Prep Batch: 196404
Diesel Range Organics
[C10-C28]
400 95.2 390 4 mg/Kg ☼ -5 50 - 150
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
p-Terphenyl X D 38 - 148
Surrogate
0 MS MS
%Recovery Qualifier Limits
Lab Sample ID: 720-69933-43 MSD Client Sample ID: GP-10-3.5-4' Matrix: Solid Prep Type: Silica Gel Cleanup
Analysis Batch: 196414 Prep Batch: 196404
Diesel Range Organics
[C10-C28]
400 95.2 407 4 mg/Kg ☼ 12 50 - 150 4 30
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
p-Terphenyl X D 38 - 148
Surrogate
0 MSD MSD
%Recovery Qualifier Limits
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8081A - Organochlorine Pesticides (GC)
Lab Sample ID: MB 720-196366/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196422 Prep Batch: 196366
RL MDL
Aldrin ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Dieldrin ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
Endrin aldehyde ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Endrin ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
Endrin ketone ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Heptachlor ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Heptachlor epoxide ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 4,4'-DDT ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
4,4'-DDE ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
4,4'-DDD ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
Endosulfan I ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Endosulfan II ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 alpha-BHC ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
beta-BHC ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
gamma-BHC (Lindane) ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 delta-BHC ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
Endosulfan sulfate ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Methoxychlor ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Toxaphene ND 40 ug/Kg 01/27/16 15:48 01/28/16 13:41 1
Chlordane (technical) ND 40 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 alpha-Chlordane ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 gamma-Chlordane ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Hexachlorobenzene ND 2.0 ug/Kg 01/27/16 15:48 01/28/16 13:41 1 Tetrachloro-m-xylene 99 57 - 122 01/28/16 13:41 1
MB MB
Surrogate
01/27/16 15:48
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
DCB Decachlorobiphenyl 107 21 - 136 01/27/16 15:48 01/28/16 13:41 1 Lab Sample ID: LCS 720-196366/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196422 Prep Batch: 196366
Aldrin 16.7 17.7 ug/Kg 106 65 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Dieldrin 16.7 17.4 ug/Kg 104 72 - 120
Endrin aldehyde 16.7 18.4 ug/Kg 111 68 - 120
Endrin 16.7 17.9 ug/Kg 107 68 - 120
Endrin ketone 16.7 18.4 ug/Kg 110 84 - 133
Heptachlor 16.7 17.4 ug/Kg 104 69 - 120
Heptachlor epoxide 16.7 18.0 ug/Kg 108 68 - 120
4,4'-DDT 16.7 17.5 ug/Kg 105 63 - 127
4,4'-DDE 16.7 18.2 ug/Kg 109 84 - 126
4,4'-DDD 16.7 17.7 ug/Kg 106 85 - 128
Endosulfan I 16.7 17.6 ug/Kg 105 62 - 120
Endosulfan II 16.7 17.7 ug/Kg 106 65 - 120
alpha-BHC 16.7 17.2 ug/Kg 103 62 - 120
beta-BHC 16.7 18.5 ug/Kg 111 74 - 124
gamma-BHC (Lindane) 16.7 17.6 ug/Kg 105 72 - 120
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8081A - Organochlorine Pesticides (GC) (Continued) Lab Sample ID: LCS 720-196366/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196422 Prep Batch: 196366
delta-BHC 16.7 14.5 ug/Kg 87 43 - 125
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Endosulfan sulfate 16.7 17.7 ug/Kg 106 84 - 126
Methoxychlor 16.7 18.9 ug/Kg 114 71 - 132
alpha-Chlordane 16.7 17.7 ug/Kg 106 70 - 120
gamma-Chlordane 16.7 17.7 ug/Kg 106 68 - 120
Tetrachloro-m-xylene 57 - 122
Surrogate
105

LCS LCS
%Recovery Qualifier Limits
DCB Decachlorobiphenyl 113 21 - 136
Lab Sample ID: 720-69933-27 MS Client Sample ID: GP-6-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196422 Prep Batch: 196366
Aldrin ND 18.8 18.3 ug/Kg ☼ 97 53 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Dieldrin 11 18.8 28.8 ug/Kg ☼ 93 46 - 130
Endrin aldehyde ND 18.8 16.5 ug/Kg ☼ 88 40 - 120
Endrin ND 18.8 24.9 ug/Kg ☼ 132 32 - 143
Endrin ketone ND 18.8 18.9 ug/Kg ☼ 100 40 - 120
Heptachlor ND 18.8 17.9 ug/Kg ☼ 95 52 - 120
Heptachlor epoxide ND 18.8 19.0 ug/Kg ☼ 101 40 - 120
4,4'-DDT 11 18.8 32.5 ug/Kg ☼ 112 17 - 144
4,4'-DDE 18 18.8 39.4 ug/Kg ☼ 115 40 - 120
4,4'-DDD 4.4 18.8 23.1 ug/Kg ☼ 99 40 - 120
Endosulfan I ND 18.8 18.8 ug/Kg ☼ 100 40 - 120
Endosulfan II ND 18.8 21.0 ug/Kg ☼ 112 40 - 120
alpha-BHC ND 18.8 18.9 ug/Kg ☼ 100 40 - 120
beta-BHC ND 18.8 21.7 ug/Kg ☼ 115 40 - 120
gamma-BHC (Lindane) ND 18.8 20.3 ug/Kg ☼ 108 58 - 120
delta-BHC ND 18.8 16.0 ug/Kg ☼ 85 40 - 120
Endosulfan sulfate ND 18.8 18.5 ug/Kg ☼ 98 40 - 120
Methoxychlor ND 18.8 18.4 ug/Kg ☼ 97 40 - 120
alpha-Chlordane ND 18.8 20.7 ug/Kg ☼ 104 40 - 120
gamma-Chlordane ND 18.8 22.6 ug/Kg ☼ 111 40 - 120
Tetrachloro-m-xylene 57 - 122
Surrogate
109
MS MS
%Recovery Qualifier Limits
DCB Decachlorobiphenyl 110 21 - 136
Lab Sample ID: 720-69933-27 MSD Client Sample ID: GP-6-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196422 Prep Batch: 196366
Aldrin ND 19.1 17.2 ug/Kg ☼ 90 53 - 120 6 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Dieldrin 11 19.1 30.7 ug/Kg ☼ 102 46 - 130 6 20
Endrin aldehyde ND 19.1 15.4 ug/Kg ☼ 81 40 - 120 7 20
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8081A - Organochlorine Pesticides (GC) (Continued) Lab Sample ID: 720-69933-27 MSD Client Sample ID: GP-6-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196422 Prep Batch: 196366
Endrin ND 19.1 25.6 ug/Kg ☼ 134 32 - 143 3 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Endrin ketone ND 19.1 16.7 ug/Kg ☼ 87 40 - 120 12 20
Heptachlor ND 19.1 18.1 ug/Kg ☼ 95 52 - 120 1 20
Heptachlor epoxide ND 19.1 17.9 ug/Kg ☼ 93 40 - 120 6 20 4,4'-DDT 11 19.1 35.3 ug/Kg ☼ 126 17 - 144 8 20
4,4'-DDE 18 19.1 43.0 F1 ug/Kg ☼ 132 40 - 120 9 20
4,4'-DDD 4.4 19.1 23.7 ug/Kg ☼ 101 40 - 120 3 20
Endosulfan I ND 19.1 17.6 ug/Kg ☼ 92 40 - 120 7 20
Endosulfan II ND 19.1 19.9 ug/Kg ☼ 104 40 - 120 5 30
alpha-BHC ND 19.1 17.8 ug/Kg ☼ 93 40 - 120 6 20
beta-BHC ND 19.1 20.7 ug/Kg ☼ 109 40 - 120 5 20
gamma-BHC (Lindane) ND 19.1 20.1 ug/Kg ☼ 105 58 - 120 1 20 delta-BHC ND 19.1 15.4 ug/Kg ☼ 81 40 - 120 4 20
Endosulfan sulfate ND 19.1 19.7 ug/Kg ☼ 103 40 - 120 6 20 Methoxychlor ND 19.1 17.5 ug/Kg ☼ 92 40 - 120 5 20
alpha-Chlordane ND 19.1 19.5 ug/Kg ☼ 96 40 - 120 6 20
gamma-Chlordane ND 19.1 21.9 ug/Kg ☼ 106 40 - 120 3 20
Tetrachloro-m-xylene 57 - 122
Surrogate
107

MSD MSD
%Recovery Qualifier Limits
DCB Decachlorobiphenyl 98 21 - 136
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Lab Sample ID: MB 720-196367/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196419 Prep Batch: 196367
RL MDL
PCB-1016 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac PCB-1221 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
PCB-1232 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
PCB-1242 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
PCB-1248 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
PCB-1254 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
PCB-1260 ND 50 ug/Kg 01/27/16 15:59 01/28/16 15:52 1
Tetrachloro-m-xylene 78 45 - 132 01/28/16 15:52 1
MB MB
Surrogate
01/27/16 15:59
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
DCB Decachlorobiphenyl 86 42 - 146 01/27/16 15:59 01/28/16 15:52 1 Lab Sample ID: LCS 720-196367/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196419 Prep Batch: 196367
PCB-1016 133 108 ug/Kg 81 65 - 121
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) Lab Sample ID: LCS 720-196367/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196419 Prep Batch: 196367
PCB-1260 133 114 ug/Kg 85 68 - 127
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Tetrachloro-m-xylene 45 - 132
Surrogate
80 LCS LCS
%Recovery Qualifier Limits
DCB Decachlorobiphenyl 92 42 - 146
Lab Sample ID: 720-69933-9 MS Client Sample ID: GP-1-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196419 Prep Batch: 196367
PCB-1016 ND 151 148 ug/Kg ☼ 98 69 - 120
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
PCB-1260 ND 151 142 ug/Kg ☼ 81 73 - 114
Tetrachloro-m-xylene 45 - 132
Surrogate
98 MS MS
%Recovery Qualifier Limits
DCB Decachlorobiphenyl 85 42 - 146
Lab Sample ID: 720-69933-9 MSD Client Sample ID: GP-1-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196419 Prep Batch: 196367
PCB-1016 ND 154 139 ug/Kg ☼ 90 69 - 120 7 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
PCB-1260 ND 154 132 ug/Kg ☼ 74 73 - 114 7 20
Tetrachloro-m-xylene 45 - 132
Surrogate
92 MSD MSD
%Recovery Qualifier Limits
DCB Decachlorobiphenyl 78 42 - 146
Method: 6010B - Metals (ICP)
Lab Sample ID: MB 720-196275/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
RL MDL
Antimony ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 1.0 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Barium ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Beryllium ND 0.10 mg/Kg 01/26/16 14:13 01/27/16 21:07 1 Cadmium ND 0.13 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Chromium ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Cobalt ND 0.20 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Copper ND 1.5 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Lead ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Molybdenum ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1 TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: MB 720-196275/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
RL MDL
Nickel ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Selenium ND 1.0 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Silver ND 0.25 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Thallium ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Vanadium ND 0.50 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Zinc ND 1.5 mg/Kg 01/26/16 14:13 01/27/16 21:07 1
Lab Sample ID: LCS 720-196275/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
Antimony 50.0 45.7 mg/Kg 91 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 50.0 46.4 mg/Kg 93 80 - 120
Barium 50.0 47.9 mg/Kg 96 80 - 120
Beryllium 50.0 48.6 mg/Kg 97 80 - 120
Cadmium 50.0 47.3 mg/Kg 95 80 - 120
Chromium 50.0 48.6 mg/Kg 97 80 - 120
Cobalt 50.0 48.9 mg/Kg 98 80 - 120
Copper 50.0 48.0 mg/Kg 96 80 - 120
Lead 50.0 47.4 mg/Kg 95 80 - 120
Molybdenum 50.0 47.5 mg/Kg 95 80 - 120
Nickel 50.0 48.4 mg/Kg 97 80 - 120
Selenium 50.0 46.4 mg/Kg 93 80 - 120
Silver 25.0 23.4 mg/Kg 93 80 - 120
Thallium 50.0 47.6 mg/Kg 95 80 - 120
Vanadium 50.0 47.2 mg/Kg 94 80 - 120
Zinc 50.0 47.3 mg/Kg 95 80 - 120
Lab Sample ID: LCSD 720-196275/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
Antimony 50.0 46.1 mg/Kg 92 80 - 120 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Arsenic 50.0 46.1 mg/Kg 92 80 - 120 1 20
Barium 50.0 47.9 mg/Kg 96 80 - 120 0 20
Beryllium 50.0 48.0 mg/Kg 96 80 - 120 1 20
Cadmium 50.0 46.8 mg/Kg 94 80 - 120 1 20
Chromium 50.0 47.7 mg/Kg 95 80 - 120 2 20
Cobalt 50.0 48.6 mg/Kg 97 80 - 120 1 20
Copper 50.0 47.7 mg/Kg 95 80 - 120 1 20
Lead 50.0 47.0 mg/Kg 94 80 - 120 1 20
Molybdenum 50.0 47.1 mg/Kg 94 80 - 120 1 20
Nickel 50.0 48.0 mg/Kg 96 80 - 120 1 20
Selenium 50.0 46.0 mg/Kg 92 80 - 120 1 20
Silver 25.0 23.2 mg/Kg 93 80 - 120 1 20
Thallium 50.0 47.5 mg/Kg 95 80 - 120 0 20
Vanadium 50.0 46.5 mg/Kg 93 80 - 120 2 20
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: LCSD 720-196275/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
Zinc 50.0 46.9 mg/Kg 94 80 - 120 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Lab Sample ID: LCSSRM 720-196275/4-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
Antimony 74.6 36.2 mg/Kg 49 11 - 101
Analyte

LCSSRM LCSSRM
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 45.5 40.3 mg/Kg 89 69 - 119
Barium 579 477 mg/Kg 82 61 - 117
Beryllium 155 141 mg/Kg 91 56 - 102
Cadmium 201 176 mg/Kg 88 67 - 118
Chromium 106 94.9 mg/Kg 90 67 - 121
Cobalt 247 224 mg/Kg 91 64 - 133
Copper 130 118 mg/Kg 91 68 - 126
Lead 302 259 mg/Kg 86 62 - 113
Molybdenum 165 140 mg/Kg 85 62 - 128
Nickel 305 273 mg/Kg 89 65 - 117
Selenium 133 121 mg/Kg 91 63 - 126
Silver 33.5 29.6 mg/Kg 88 51 - 130
Thallium 191 168 mg/Kg 88 64 - 124
Vanadium 214 189 mg/Kg 89 67 - 123
Zinc 388 336 mg/Kg 87 62 - 110
Lab Sample ID: 720-69933-8 MS Client Sample ID: GP-1-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
Antimony 2.5 F1 46.4 13.5 F1 mg/Kg ☼ 24 75 - 125
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic 8.7 46.4 49.8 mg/Kg ☼ 88 75 - 125
Barium 160 F1 F2 46.4 279 F1 mg/Kg ☼ 255 75 - 125
Beryllium 0.54 46.4 44.1 mg/Kg ☼ 94 75 - 125
Cadmium ND 46.4 41.8 mg/Kg ☼ 90 75 - 125
Chromium 73 F1 46.4 117 mg/Kg ☼ 95 75 - 125
Cobalt 17 46.4 58.3 mg/Kg ☼ 89 75 - 125
Copper 36 46.4 80.5 mg/Kg ☼ 96 75 - 125
Lead 14 46.4 60.7 mg/Kg ☼ 101 75 - 125
Molybdenum 2.7 46.4 42.0 mg/Kg ☼ 85 75 - 125
Nickel 94 F1 46.4 161 F1 mg/Kg ☼ 144 75 - 125
Selenium ND 46.4 41.2 mg/Kg ☼ 89 75 - 125
Silver ND 23.2 21.5 mg/Kg ☼ 93 75 - 125
Thallium 2.1 46.4 42.7 mg/Kg ☼ 87 75 - 125
Vanadium 41 46.4 87.9 mg/Kg ☼ 101 75 - 125
Zinc 58 46.4 95.7 mg/Kg ☼ 81 75 - 125
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: 720-69933-8 MSD Client Sample ID: GP-1-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196432 Prep Batch: 196275
Antimony 2.5 F1 46.4 11.5 F1 mg/Kg ☼ 19 75 - 125 16 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic 8.7 46.4 49.2 mg/Kg ☼ 87 75 - 125 1 20
Barium 160 F1 F2 46.4 225 F1 F2 mg/Kg ☼ 138 75 - 125 21 20 Beryllium 0.54 46.4 44.4 mg/Kg ☼ 95 75 - 125 1 20
Cadmium ND 46.4 42.4 mg/Kg ☼ 91 75 - 125 1 20
Chromium 73 F1 46.4 134 F1 mg/Kg ☼ 131 75 - 125 13 20
Cobalt 17 46.4 57.1 mg/Kg ☼ 86 75 - 125 2 20
Copper 36 46.4 79.0 mg/Kg ☼ 93 75 - 125 2 20
Lead 14 46.4 59.4 mg/Kg ☼ 99 75 - 125 2 20
Molybdenum 2.7 46.4 41.9 mg/Kg ☼ 85 75 - 125 0 20
Nickel 94 F1 46.4 169 F1 mg/Kg ☼ 162 75 - 125 5 20
Selenium ND 46.4 41.4 mg/Kg ☼ 89 75 - 125 0 20
Silver ND 23.2 22.0 mg/Kg ☼ 95 75 - 125 2 20
Thallium 2.1 46.4 42.8 mg/Kg ☼ 88 75 - 125 0 20
Vanadium 41 46.4 90.0 mg/Kg ☼ 105 75 - 125 2 20
Zinc 58 46.4 100 mg/Kg ☼ 90 75 - 125 5 20
Lab Sample ID: MB 720-196285/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
RL MDL
Antimony ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 1.0 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Barium ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Beryllium ND 0.10 mg/Kg 01/26/16 14:58 01/28/16 18:08 1 Cadmium ND 0.13 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Chromium ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Cobalt ND 0.20 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Copper ND 1.5 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Lead ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Molybdenum ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1 Nickel ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Selenium ND 1.0 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Silver ND 0.25 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Thallium ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Vanadium ND 0.50 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Zinc ND 1.5 mg/Kg 01/26/16 14:58 01/28/16 18:08 1
Lab Sample ID: LCS 720-196285/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Antimony 50.0 47.7 mg/Kg 95 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 50.0 48.0 mg/Kg 96 80 - 120
Barium 50.0 49.2 mg/Kg 98 80 - 120
Beryllium 50.0 47.9 mg/Kg 96 80 - 120
TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: LCS 720-196285/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Cadmium 50.0 47.7 mg/Kg 95 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Chromium 50.0 49.1 mg/Kg 98 80 - 120
Cobalt 50.0 49.9 mg/Kg 100 80 - 120
Copper 50.0 49.2 mg/Kg 98 80 - 120
Lead 50.0 49.1 mg/Kg 98 80 - 120
Molybdenum 50.0 49.3 mg/Kg 99 80 - 120
Nickel 50.0 48.9 mg/Kg 98 80 - 120
Selenium 50.0 46.8 mg/Kg 94 80 - 120
Silver 25.0 23.9 mg/Kg 95 80 - 120
Thallium 50.0 49.8 mg/Kg 100 80 - 120
Vanadium 50.0 48.2 mg/Kg 96 80 - 120
Zinc 50.0 47.8 mg/Kg 96 80 - 120
Lab Sample ID: LCSD 720-196285/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Antimony 50.0 47.3 mg/Kg 95 80 - 120 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Arsenic 50.0 47.4 mg/Kg 95 80 - 120 1 20
Barium 50.0 48.7 mg/Kg 97 80 - 120 1 20
Beryllium 50.0 47.5 mg/Kg 95 80 - 120 1 20
Cadmium 50.0 47.1 mg/Kg 94 80 - 120 1 20
Chromium 50.0 48.6 mg/Kg 97 80 - 120 1 20
Cobalt 50.0 49.5 mg/Kg 99 80 - 120 1 20
Copper 50.0 48.7 mg/Kg 97 80 - 120 1 20
Lead 50.0 48.7 mg/Kg 97 80 - 120 1 20
Molybdenum 50.0 48.9 mg/Kg 98 80 - 120 1 20
Nickel 50.0 48.4 mg/Kg 97 80 - 120 1 20
Selenium 50.0 46.4 mg/Kg 93 80 - 120 1 20
Silver 25.0 23.6 mg/Kg 95 80 - 120 1 20
Thallium 50.0 49.1 mg/Kg 98 80 - 120 1 20
Vanadium 50.0 47.6 mg/Kg 95 80 - 120 1 20
Zinc 50.0 47.2 mg/Kg 94 80 - 120 1 20
Lab Sample ID: LCSSRM 720-196285/4-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Antimony 74.6 39.7 mg/Kg 53 11 - 101
Analyte

LCSSRM LCSSRM
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 45.5 42.5 mg/Kg 93 69 - 119
Barium 579 509 mg/Kg 88 61 - 117
Beryllium 155 135 mg/Kg 87 56 - 102
Cadmium 201 181 mg/Kg 90 67 - 118
Chromium 106 95.7 mg/Kg 90 67 - 121
Cobalt 247 228 mg/Kg 92 64 - 133
Copper 130 119 mg/Kg 92 68 - 126
Lead 302 265 mg/Kg 88 62 - 113
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: LCSSRM 720-196285/4-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Molybdenum 165 146 mg/Kg 89 62 - 128
Analyte

LCSSRM LCSSRM
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Nickel 305 276 mg/Kg 91 65 - 117
Selenium 133 125 mg/Kg 94 63 - 126
Silver 33.5 30.8 mg/Kg 92 51 - 130
Thallium 191 171 mg/Kg 89 64 - 124
Vanadium 214 196 mg/Kg 91 67 - 123
Zinc 388 345 mg/Kg 89 62 - 110
Lab Sample ID: 720-69933-47 MS Client Sample ID: GP-11-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Antimony ND F1 F2 57.7 10.4 F1 mg/Kg ☼ 18 75 - 125
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic 7.8 57.7 62.1 mg/Kg ☼ 94 75 - 125
Barium 140 F1 F2 57.7 198 mg/Kg ☼ 104 75 - 125
Beryllium ND 57.7 55.3 mg/Kg ☼ 95 75 - 125
Cadmium ND 57.7 55.7 mg/Kg ☼ 96 75 - 125
Chromium 480 57.7 461 4 mg/Kg ☼ -30 75 - 125
Cobalt 64 57.7 107 mg/Kg ☼ 76 75 - 125
Copper 35 57.7 82.7 mg/Kg ☼ 82 75 - 125
Lead 44 F1 57.7 84.7 F1 mg/Kg ☼ 71 75 - 125
Molybdenum ND 57.7 54.8 mg/Kg ☼ 93 75 - 125
Nickel 1100 57.7 1010 4 mg/Kg ☼ -251 75 - 125
Selenium ND 57.7 56.9 mg/Kg ☼ 97 75 - 125
Silver ND 28.8 28.6 mg/Kg ☼ 99 75 - 125
Thallium ND 57.7 52.5 mg/Kg ☼ 91 75 - 125
Vanadium 39 57.7 90.7 mg/Kg ☼ 89 75 - 125
Zinc 68 F1 57.7 111 F1 mg/Kg ☼ 74 75 - 125
Lab Sample ID: 720-69933-47 MSD Client Sample ID: GP-11-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Antimony ND F1 F2 57.7 7.82 F1 F2 mg/Kg ☼ 14 75 - 125 28 20 Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic 7.8 57.7 63.8 mg/Kg ☼ 97 75 - 125 3 20
Barium 140 F1 F2 57.7 279 F1 F2 mg/Kg ☼ 244 75 - 125 34 20 Beryllium ND 57.7 54.6 mg/Kg ☼ 94 75 - 125 1 20
Cadmium ND 57.7 55.6 mg/Kg ☼ 96 75 - 125 0 20
Chromium 480 57.7 496 4 mg/Kg ☼ 32 75 - 125 7 20
Cobalt 64 57.7 109 mg/Kg ☼ 79 75 - 125 2 20
Copper 35 57.7 88.3 mg/Kg ☼ 92 75 - 125 7 20
Lead 44 F1 57.7 93.9 mg/Kg ☼ 87 75 - 125 10 20
Molybdenum ND 57.7 52.9 mg/Kg ☼ 90 75 - 125 4 20
Nickel 1100 57.7 982 4 mg/Kg ☼ -292 75 - 125 2 20
Selenium ND 57.7 56.1 mg/Kg ☼ 96 75 - 125 1 20
Silver ND 28.8 29.4 mg/Kg ☼ 102 75 - 125 3 20
Thallium ND 57.7 51.7 mg/Kg ☼ 90 75 - 125 1 20
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: 720-69933-47 MSD Client Sample ID: GP-11-3.5-4' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196482 Prep Batch: 196285
Vanadium 39 57.7 93.6 mg/Kg ☼ 94 75 - 125 3 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Zinc 68 F1 57.7 121 mg/Kg ☼ 93 75 - 125 9 20
Lab Sample ID: MB 720-196361/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 196481 Prep Batch: 196361
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1
Barium ND 0.050 mg/L 01/27/16 14:17 01/28/16 17:08 1
Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:08 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:08 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1
Cobalt ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:08 1
Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:08 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:08 1
Molybdenum ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1 Nickel ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1
Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:08 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:08 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1
Vanadium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:08 1
Zinc ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:08 1
Lab Sample ID: LCS 720-196361/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 196481 Prep Batch: 196361
Antimony 1.00 0.935 mg/L 93
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Arsenic 1.00 0.910 mg/L 91
Barium 1.00 0.963 mg/L 96
Beryllium 1.00 0.926 mg/L 93
Cadmium 1.00 0.927 mg/L 93
Chromium 1.00 0.935 mg/L 94
Cobalt 1.00 0.950 mg/L 95
Copper 1.00 0.935 mg/L 93
Lead 1.00 0.922 mg/L 92
Molybdenum 1.00 0.910 mg/L 91
Nickel 1.00 0.952 mg/L 95
Selenium 1.00 0.956 mg/L 96
Silver 0.500 0.461 mg/L 92
Thallium 1.00 0.907 mg/L 91
Vanadium 1.00 0.898 mg/L 90
Zinc 1.00 0.966 mg/L 97
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: LCSD 720-196361/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 196481 Prep Batch: 196361
Antimony 1.00 0.907 mg/L 91 3
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Arsenic 1.00 0.907 mg/L 91 0
Barium 1.00 0.966 mg/L 97 0
Beryllium 1.00 0.928 mg/L 93 0
Cadmium 1.00 0.925 mg/L 93 0
Chromium 1.00 0.942 mg/L 94 1
Cobalt 1.00 0.946 mg/L 95 0
Copper 1.00 0.943 mg/L 94 1
Lead 1.00 0.916 mg/L 92 1
Molybdenum 1.00 0.909 mg/L 91 0
Nickel 1.00 0.952 mg/L 95 0
Selenium 1.00 0.959 mg/L 96 0
Silver 0.500 0.463 mg/L 93 0
Thallium 1.00 0.913 mg/L 91 1
Vanadium 1.00 0.898 mg/L 90 0
Zinc 1.00 0.968 mg/L 97 0
Lab Sample ID: MB 720-196284/1-B Client Sample ID: Method Blank Matrix: Water Prep Type: Dissolved
Analysis Batch: 196481 Prep Batch: 196361
RL MDL
Antimony ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Arsenic ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1
Barium ND 0.050 mg/L 01/27/16 14:17 01/28/16 17:13 1
Beryllium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:13 1 Cadmium ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:13 1
Chromium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1
Cobalt ND 0.0020 mg/L 01/27/16 14:17 01/28/16 17:13 1
Copper ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:13 1
Lead ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:13 1
Molybdenum ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1 Nickel ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1
Selenium ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:13 1
Silver ND 0.0050 mg/L 01/27/16 14:17 01/28/16 17:13 1
Thallium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1
Vanadium ND 0.010 mg/L 01/27/16 14:17 01/28/16 17:13 1
Zinc ND 0.020 mg/L 01/27/16 14:17 01/28/16 17:13 1
Lab Sample ID: 720-69933-1 MS Client Sample ID: GP-1
Matrix: Water Prep Type: Dissolved
Analysis Batch: 196481 Prep Batch: 196361
Antimony ND 1.00 0.949 mg/L 95
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Arsenic ND 1.00 0.980 mg/L 97
Barium ND 1.00 1.00 mg/L 97
Beryllium ND 1.00 0.936 mg/L 94
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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 6010B - Metals (ICP) (Continued)
Lab Sample ID: 720-69933-1 MS Client Sample ID: GP-1
Matrix: Water Prep Type: Dissolved
Analysis Batch: 196481 Prep Batch: 196361
Cadmium ND 1.00 0.926 mg/L 92
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Chromium ND 1.00 0.944 mg/L 94
Cobalt 0.0038 1.00 0.928 mg/L 92
Copper ND 1.00 0.940 mg/L 94
Lead ND 1.00 0.885 mg/L 89
Molybdenum 0.049 1.00 0.972 mg/L 92
Nickel 0.010 1.00 0.934 mg/L 92
Selenium ND 1.00 0.991 mg/L 99
Silver ND 0.500 0.479 mg/L 96
Thallium ND 1.00 0.836 mg/L 83
Vanadium ND 1.00 0.925 mg/L 92
Zinc ND 1.00 0.993 mg/L 99
Lab Sample ID: 720-69933-1 MSD Client Sample ID: GP-1
Matrix: Water Prep Type: Dissolved
Analysis Batch: 196481 Prep Batch: 196361
Antimony ND 1.00 0.957 mg/L 96 1
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Arsenic ND 1.00 0.973 mg/L 97 1
Barium ND 1.00 1.01 mg/L 97 1
Beryllium ND 1.00 0.944 mg/L 94 1
Cadmium ND 1.00 0.924 mg/L 92 0
Chromium ND 1.00 0.939 mg/L 94 1
Cobalt 0.0038 1.00 0.925 mg/L 92 0
Copper ND 1.00 0.937 mg/L 94 0
Lead ND 1.00 0.878 mg/L 88 1
Molybdenum 0.049 1.00 0.969 mg/L 92 0
Nickel 0.010 1.00 0.935 mg/L 92 0
Selenium ND 1.00 0.989 mg/L 99 0
Silver ND 0.500 0.480 mg/L 96 0
Thallium ND 1.00 0.832 mg/L 83 1
Vanadium ND 1.00 0.919 mg/L 91 1
Zinc ND 1.00 0.990 mg/L 99 0
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 720-196443/1-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA
Analysis Batch: 196474 Prep Batch: 196443
RL MDL
Mercury ND 0.00020 mg/L 01/28/16 12:32 01/28/16 17:14 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 7470A - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 720-196443/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA
Analysis Batch: 196474 Prep Batch: 196443
Mercury 0.0100 0.00994 mg/L 99 85 - 115
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: LCSD 720-196443/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA
Analysis Batch: 196474 Prep Batch: 196443
Mercury 0.0100 0.00980 mg/L 98 85 - 115 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Lab Sample ID: MB 720-196284/1-C Client Sample ID: Method Blank Matrix: Water Prep Type: Dissolved
Analysis Batch: 196474 Prep Batch: 196443
RL MDL
Mercury ND 0.00020 mg/L 01/28/16 12:32 01/28/16 17:33 1 MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Method: 7471A - Mercury (CVAA)
Lab Sample ID: MB 720-196308/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196381 Prep Batch: 196308
RL MDL
Mercury ND 0.010 mg/Kg 01/26/16 17:30 01/27/16 16:19 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac Lab Sample ID: LCS 720-196308/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196381 Prep Batch: 196308
Mercury 0.833 0.850 mg/Kg 102 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: LCSD 720-196308/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196381 Prep Batch: 196308
Mercury 0.833 0.842 mg/Kg 101 80 - 120 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Lab Sample ID: MB 720-196312/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196405 Prep Batch: 196312
RL MDL
Mercury ND 0.010 mg/Kg 01/26/16 18:10 01/27/16 19:43 1
MB MB
Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac TestAmerica Pleasanton

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QC Sample Results
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method: 7471A - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 720-196312/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196405 Prep Batch: 196312
Mercury 0.833 0.842 mg/Kg 101 80 - 120
Analyte

LCS LCS
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits
Lab Sample ID: LCSD 720-196312/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196405 Prep Batch: 196312
Mercury 0.833 0.833 mg/Kg 100 80 - 120 1 20
Analyte

LCSD LCSD
Result Qualifier Unit D %Rec
Spike
Added
%Rec.

Limits RPD Limit
RPD
Lab Sample ID: 720-69933-44 MS Client Sample ID: GP-10-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196405 Prep Batch: 196312
Mercury 0.11 F1 1.01 1.38 F1 mg/Kg ☼ 126 75 - 125
Analyte
MS MS
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits
Lab Sample ID: 720-69933-44 MSD Client Sample ID: GP-10-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196405 Prep Batch: 196312
Mercury 0.11 F1 1.05 1.32 mg/Kg ☼ 116 75 - 125 5 20
Analyte

MSD MSD
Result Qualifier Unit D %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.

Limits RPD Limit
RPD
Method: Moisture - Percent Moisture
Lab Sample ID: 720-69933-9 DU Client Sample ID: GP-1-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196337
Percent Moisture 14 12 % 10 20
Analyte
DU DU
Result Qualifier Unit D
Sample
Result
Sample
Qualifier RPD Limit
RPD
Lab Sample ID: 720-69933-48 DU Client Sample ID: GP-11-7.5-8' Matrix: Solid Prep Type: Total/NA
Analysis Batch: 196350
Percent Moisture 21 20 % 1 20
Analyte
DU DU
Result Qualifier Unit D
Sample
Result
Sample
Qualifier RPD Limit
RPD
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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High

GC/MS VOA
Analysis Batch: 196192
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-7 TRIP BLANK Total/NA Water 8260B
LCS 720-196192/5 Lab Control Sample Total/NA Water 8260B LCSD 720-196192/6 Lab Control Sample Dup Total/NA Water 8260B MB 720-196192/4 Method Blank Total/NA Water 8260B
Prep Batch: 196202
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-9 GP-1-7.5-8' Total/NA Solid 5030B
720-69933-12 GP-2-3.5-4' Total/NA Solid 5030B
720-69933-12 MS GP-2-3.5-4' Total/NA Solid 5030B
720-69933-12 MSD GP-2-3.5-4' Total/NA Solid 5030B
720-69933-16 GP-3-7.5-8' Total/NA Solid 5030B
720-69933-19 GP-4-3.5-4' Total/NA Solid 5030B
720-69933-23 GP-5-4.5-5' Total/NA Solid 5030B
720-69933-32 GP-7-7.5-8' Total/NA Solid 5030B
Analysis Batch: 196234
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260B/CA_LUFT
MS
720-69933-1 GP-1 Total/NA
Water 8260B/CA_LUFT
MS
720-69933-2 GP-2 Total/NA
Water 8260B/CA_LUFT
MS
720-69933-3 GP-3 Total/NA
Water 8260B/CA_LUFT
MS
720-69933-4 GP-6 Total/NA
Water 8260B/CA_LUFT
MS
LCS 720-196234/14 Lab Control Sample Total/NA
Water 8260B/CA_LUFT
MS
LCS 720-196234/5 Lab Control Sample Total/NA
Water 8260B/CA_LUFT
MS
LCSD 720-196234/15 Lab Control Sample Dup Total/NA
Water 8260B/CA_LUFT
MS
LCSD 720-196234/6 Lab Control Sample Dup Total/NA
Water 8260B/CA_LUFT
MS
MB 720-196234/4 Method Blank Total/NA
Analysis Batch: 196288
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-9 GP-1-7.5-8' Total/NA Solid 8260B 196202
720-69933-16 GP-3-7.5-8' Total/NA Solid 8260B 196202
LCS 720-196288/5 Lab Control Sample Total/NA Solid 8260B LCS 720-196288/7 Lab Control Sample Total/NA Solid 8260B LCSD 720-196288/6 Lab Control Sample Dup Total/NA Solid 8260B LCSD 720-196288/8 Lab Control Sample Dup Total/NA Solid 8260B MB 720-196288/4 Method Blank Total/NA Solid 8260B
Analysis Batch: 196293
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260B/CA_LUFT
MS
720-69933-5 GP-7 Total/NA
Water 8260B/CA_LUFT
MS
720-69933-6 GP-10 Total/NA
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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
GC/MS VOA (Continued)
Analysis Batch: 196293 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260B/CA_LUFT
MS
LCS 720-196293/5 Lab Control Sample Total/NA
Water 8260B/CA_LUFT
MS
LCS 720-196293/7 Lab Control Sample Total/NA
Water 8260B/CA_LUFT
MS
LCSD 720-196293/6 Lab Control Sample Dup Total/NA
Water 8260B/CA_LUFT
MS
LCSD 720-196293/8 Lab Control Sample Dup Total/NA
Water 8260B/CA_LUFT
MS
MB 720-196293/4 Method Blank Total/NA
Prep Batch: 196295
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 5030B
720-69933-13 GP-2-7.5-8' Total/NA Solid 5030B
720-69933-15 GP-3-3.5-4' Total/NA Solid 5030B
720-69933-24 GP-5-7.5-8' Total/NA Solid 5030B
720-69933-27 GP-6-3.5-4' Total/NA Solid 5030B
720-69933-31 GP-7-3.5-4' Total/NA Solid 5030B
720-69933-35 GP-8-3.5-4' Total/NA Solid 5030B
720-69933-35 MS GP-8-3.5-4' Total/NA Solid 5030B
720-69933-35 MSD GP-8-3.5-4' Total/NA Solid 5030B
720-69933-43 GP-10-3.5-4' Total/NA Solid 5030B
Analysis Batch: 196326
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-12 GP-2-3.5-4' Total/NA Solid 8260B 196202
720-69933-12 MS GP-2-3.5-4' Total/NA Solid 8260B 196202 720-69933-12 MSD GP-2-3.5-4' Total/NA Solid 8260B 196202 720-69933-19 GP-4-3.5-4' Total/NA Solid 8260B 196202
720-69933-23 GP-5-4.5-5' Total/NA Solid 8260B 196202
720-69933-32 GP-7-7.5-8' Total/NA Solid 8260B 196202
LCS 720-196326/5 Lab Control Sample Total/NA Solid 8260B LCS 720-196326/7 Lab Control Sample Total/NA Solid 8260B LCSD 720-196326/6 Lab Control Sample Dup Total/NA Solid 8260B LCSD 720-196326/8 Lab Control Sample Dup Total/NA Solid 8260B MB 720-196326/4 Method Blank Total/NA Solid 8260B
Analysis Batch: 196408
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 8260B 196295
720-69933-13 GP-2-7.5-8' Total/NA Solid 8260B 196295
720-69933-15 GP-3-3.5-4' Total/NA Solid 8260B 196295
720-69933-31 GP-7-3.5-4' Total/NA Solid 8260B 196295
720-69933-35 GP-8-3.5-4' Total/NA Solid 8260B 196295
720-69933-35 MS GP-8-3.5-4' Total/NA Solid 8260B 196295 720-69933-35 MSD GP-8-3.5-4' Total/NA Solid 8260B 196295 LCS 720-196408/5 Lab Control Sample Total/NA Solid 8260B LCS 720-196408/7 Lab Control Sample Total/NA Solid 8260B LCSD 720-196408/6 Lab Control Sample Dup Total/NA Solid 8260B LCSD 720-196408/8 Lab Control Sample Dup Total/NA Solid 8260B MB 720-196408/4 Method Blank Total/NA Solid 8260B
TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Analysis Batch: 196468
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-24 GP-5-7.5-8' Total/NA Solid 8260B 196295
720-69933-27 GP-6-3.5-4' Total/NA Solid 8260B 196295
720-69933-43 GP-10-3.5-4' Total/NA Solid 8260B 196295
LCS 720-196468/5 Lab Control Sample Total/NA Solid 8260B LCS 720-196468/7 Lab Control Sample Total/NA Solid 8260B LCSD 720-196468/6 Lab Control Sample Dup Total/NA Solid 8260B LCSD 720-196468/8 Lab Control Sample Dup Total/NA Solid 8260B MB 720-196468/4 Method Blank Total/NA Solid 8260B
Analysis Batch: 196552
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-28 GP-6-7.5-8' Total/NA Solid 8260B 196561
720-69933-36 GP-8-7.5-8' Total/NA Solid 8260B 196561
720-69933-36 MS GP-8-7.5-8' Total/NA Solid 8260B 196561 720-69933-36 MSD GP-8-7.5-8' Total/NA Solid 8260B 196561 720-69933-39 GP-9-4.5-5' Total/NA Solid 8260B 196561
720-69933-40 GP-9-7.5-8' Total/NA Solid 8260B 196561
720-69933-44 GP-10-7.5-8' Total/NA Solid 8260B 196561
720-69933-47 GP-11-3.5-4' Total/NA Solid 8260B 196561
720-69933-48 GP-11-7.5-8' Total/NA Solid 8260B 196561
LCS 720-196552/5 Lab Control Sample Total/NA Solid 8260B LCS 720-196552/7 Lab Control Sample Total/NA Solid 8260B LCSD 720-196552/6 Lab Control Sample Dup Total/NA Solid 8260B LCSD 720-196552/8 Lab Control Sample Dup Total/NA Solid 8260B MB 720-196552/4 Method Blank Total/NA Solid 8260B
Prep Batch: 196561
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-28 GP-6-7.5-8' Total/NA Solid 5030B
720-69933-36 GP-8-7.5-8' Total/NA Solid 5030B
720-69933-36 MS GP-8-7.5-8' Total/NA Solid 5030B
720-69933-36 MSD GP-8-7.5-8' Total/NA Solid 5030B
720-69933-39 GP-9-4.5-5' Total/NA Solid 5030B
720-69933-40 GP-9-7.5-8' Total/NA Solid 5030B
720-69933-44 GP-10-7.5-8' Total/NA Solid 5030B
720-69933-47 GP-11-3.5-4' Total/NA Solid 5030B
720-69933-48 GP-11-7.5-8' Total/NA Solid 5030B
GC Semi VOA
Prep Batch: 196366
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 3546
720-69933-9 GP-1-7.5-8' Total/NA Solid 3546
720-69933-27 GP-6-3.5-4' Total/NA Solid 3546
720-69933-27 MS GP-6-3.5-4' Total/NA Solid 3546
720-69933-27 MSD GP-6-3.5-4' Total/NA Solid 3546
720-69933-28 GP-6-7.5-8' Total/NA Solid 3546
720-69933-35 GP-8-3.5-4' Total/NA Solid 3546
720-69933-36 GP-8-7.5-8' Total/NA Solid 3546
720-69933-43 GP-10-3.5-4' Total/NA Solid 3546
720-69933-44 GP-10-7.5-8' Total/NA Solid 3546
LCS 720-196366/2-A Lab Control Sample Total/NA Solid 3546 TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
GC Semi VOA (Continued)
Prep Batch: 196366 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch MB 720-196366/1-A Method Blank Total/NA Solid 3546
Prep Batch: 196367
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 3546
720-69933-9 GP-1-7.5-8' Total/NA Solid 3546
720-69933-9 MS GP-1-7.5-8' Total/NA Solid 3546
720-69933-9 MSD GP-1-7.5-8' Total/NA Solid 3546
720-69933-27 GP-6-3.5-4' Total/NA Solid 3546
720-69933-28 GP-6-7.5-8' Total/NA Solid 3546
720-69933-35 GP-8-3.5-4' Total/NA Solid 3546
720-69933-36 GP-8-7.5-8' Total/NA Solid 3546
720-69933-43 GP-10-3.5-4' Total/NA Solid 3546
720-69933-44 GP-10-7.5-8' Total/NA Solid 3546
LCS 720-196367/2-A Lab Control Sample Total/NA Solid 3546 MB 720-196367/1-A Method Blank Total/NA Solid 3546
Prep Batch: 196382
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Silica Gel Cleanup Water 3510C SGC
720-69933-2 GP-2 Silica Gel Cleanup Water 3510C SGC
720-69933-3 GP-3 Silica Gel Cleanup Water 3510C SGC
720-69933-4 GP-6 Silica Gel Cleanup Water 3510C SGC
720-69933-5 GP-7 Silica Gel Cleanup Water 3510C SGC
720-69933-6 GP-10 Silica Gel Cleanup Water 3510C SGC
LCS 720-196382/2-A Lab Control Sample Silica Gel Cleanup Water 3510C SGC LCSD 720-196382/3-A Lab Control Sample Dup Silica Gel Cleanup Water 3510C SGC MB 720-196382/1-A Method Blank Silica Gel Cleanup Water 3510C SGC Prep Batch: 196403
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-9 GP-1-7.5-8' Silica Gel Cleanup Solid 3546
720-69933-13 GP-2-7.5-8' Silica Gel Cleanup Solid 3546
720-69933-15 GP-3-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-27 GP-6-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-28 GP-6-7.5-8' Silica Gel Cleanup Solid 3546
720-69933-31 GP-7-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-35 GP-8-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-36 GP-8-7.5-8' Silica Gel Cleanup Solid 3546
LCS 720-196403/2-A Lab Control Sample Silica Gel Cleanup Solid 3546 MB 720-196403/1-A Method Blank Silica Gel Cleanup Solid 3546 Prep Batch: 196404
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-12 GP-2-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-16 GP-3-7.5-8' Silica Gel Cleanup Solid 3546
720-69933-19 GP-4-3.5-4' Silica Gel Cleanup Solid 3546
720-69933-23 GP-5-4.5-5' Silica Gel Cleanup Solid 3546
720-69933-24 GP-5-7.5-8' Silica Gel Cleanup Solid 3546
720-69933-32 GP-7-7.5-8' Silica Gel Cleanup Solid 3546
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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
GC Semi VOA (Continued)
Prep Batch: 196404 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-39 GP-9-4.5-5' Silica Gel Cleanup Solid 3546
720-69933-40 GP-9-7.5-8' Silica Gel Cleanup Solid 3546
720-69933-43 GP-10-3.5-4' Silica Gel Cleanup Solid 3546 720-69933-43 MS GP-10-3.5-4' Silica Gel Cleanup Solid 3546 720-69933-43 MSD GP-10-3.5-4' Silica Gel Cleanup Solid 3546 720-69933-44 GP-10-7.5-8' Silica Gel Cleanup Solid 3546 720-69933-47 GP-11-3.5-4' Silica Gel Cleanup Solid 3546 720-69933-48 GP-11-7.5-8' Silica Gel Cleanup Solid 3546 LCS 720-196404/2-A Lab Control Sample Silica Gel Cleanup Solid 3546 MB 720-196404/1-A Method Blank Silica Gel Cleanup Solid 3546 Analysis Batch: 196412
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Silica Gel Cleanup Solid 8015B 196403 Analysis Batch: 196413
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-19 GP-4-3.5-4' Silica Gel Cleanup Solid 8015B 196404 720-69933-23 GP-5-4.5-5' Silica Gel Cleanup Solid 8015B 196404 720-69933-24 GP-5-7.5-8' Silica Gel Cleanup Solid 8015B 196404 720-69933-27 GP-6-3.5-4' Silica Gel Cleanup Solid 8015B 196403 720-69933-28 GP-6-7.5-8' Silica Gel Cleanup Solid 8015B 196403 720-69933-31 GP-7-3.5-4' Silica Gel Cleanup Solid 8015B 196403 720-69933-32 GP-7-7.5-8' Silica Gel Cleanup Solid 8015B 196404 720-69933-35 GP-8-3.5-4' Silica Gel Cleanup Solid 8015B 196403 720-69933-36 GP-8-7.5-8' Silica Gel Cleanup Solid 8015B 196403 720-69933-39 GP-9-4.5-5' Silica Gel Cleanup Solid 8015B 196404 720-69933-40 GP-9-7.5-8' Silica Gel Cleanup Solid 8015B 196404 720-69933-44 GP-10-7.5-8' Silica Gel Cleanup Solid 8015B 196404 720-69933-48 GP-11-7.5-8' Silica Gel Cleanup Solid 8015B 196404 Analysis Batch: 196414
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Silica Gel Cleanup Water 8015B 196382
720-69933-2 GP-2 Silica Gel Cleanup Water 8015B 196382
720-69933-3 GP-3 Silica Gel Cleanup Water 8015B 196382
720-69933-4 GP-6 Silica Gel Cleanup Water 8015B 196382
720-69933-5 GP-7 Silica Gel Cleanup Water 8015B 196382
720-69933-6 GP-10 Silica Gel Cleanup Water 8015B 196382 720-69933-12 GP-2-3.5-4' Silica Gel Cleanup Solid 8015B 196404 720-69933-13 GP-2-7.5-8' Silica Gel Cleanup Solid 8015B 196403 720-69933-15 GP-3-3.5-4' Silica Gel Cleanup Solid 8015B 196403 720-69933-43 GP-10-3.5-4' Silica Gel Cleanup Solid 8015B 196404 720-69933-43 MS GP-10-3.5-4' Silica Gel Cleanup Solid 8015B 196404 720-69933-43 MSD GP-10-3.5-4' Silica Gel Cleanup Solid 8015B 196404 LCS 720-196382/2-A Lab Control Sample Silica Gel Cleanup Water 8015B 196382 LCSD 720-196382/3-A Lab Control Sample Dup Silica Gel Cleanup Water 8015B 196382 MB 720-196382/1-A Method Blank Silica Gel Cleanup Water 8015B 196382 TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
GC Semi VOA (Continued)
Analysis Batch: 196415
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-9 GP-1-7.5-8' Silica Gel Cleanup Solid 8015B 196403 720-69933-16 GP-3-7.5-8' Silica Gel Cleanup Solid 8015B 196404 720-69933-47 GP-11-3.5-4' Silica Gel Cleanup Solid 8015B 196404 LCS 720-196403/2-A Lab Control Sample Silica Gel Cleanup Solid 8015B 196403 LCS 720-196404/2-A Lab Control Sample Silica Gel Cleanup Solid 8015B 196404 MB 720-196403/1-A Method Blank Silica Gel Cleanup Solid 8015B 196403 MB 720-196404/1-A Method Blank Silica Gel Cleanup Solid 8015B 196404 Analysis Batch: 196419
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 8082 196367
720-69933-9 GP-1-7.5-8' Total/NA Solid 8082 196367
720-69933-9 MS GP-1-7.5-8' Total/NA Solid 8082 196367
720-69933-9 MSD GP-1-7.5-8' Total/NA Solid 8082 196367
720-69933-27 GP-6-3.5-4' Total/NA Solid 8082 196367
720-69933-28 GP-6-7.5-8' Total/NA Solid 8082 196367
720-69933-35 GP-8-3.5-4' Total/NA Solid 8082 196367
720-69933-36 GP-8-7.5-8' Total/NA Solid 8082 196367
720-69933-43 GP-10-3.5-4' Total/NA Solid 8082 196367
720-69933-44 GP-10-7.5-8' Total/NA Solid 8082 196367
LCS 720-196367/2-A Lab Control Sample Total/NA Solid 8082 196367 MB 720-196367/1-A Method Blank Total/NA Solid 8082 196367 Analysis Batch: 196422
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 8081A 196366
720-69933-9 GP-1-7.5-8' Total/NA Solid 8081A 196366
720-69933-27 GP-6-3.5-4' Total/NA Solid 8081A 196366
720-69933-27 MS GP-6-3.5-4' Total/NA Solid 8081A 196366 720-69933-27 MSD GP-6-3.5-4' Total/NA Solid 8081A 196366 720-69933-28 GP-6-7.5-8' Total/NA Solid 8081A 196366
720-69933-35 GP-8-3.5-4' Total/NA Solid 8081A 196366
720-69933-36 GP-8-7.5-8' Total/NA Solid 8081A 196366
720-69933-43 GP-10-3.5-4' Total/NA Solid 8081A 196366
720-69933-44 GP-10-7.5-8' Total/NA Solid 8081A 196366
LCS 720-196366/2-A Lab Control Sample Total/NA Solid 8081A 196366 MB 720-196366/1-A Method Blank Total/NA Solid 8081A 196366 Metals
Prep Batch: 196275
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 3050B
720-69933-8 MS GP-1-3.5-4' Total/NA Solid 3050B
720-69933-8 MSD GP-1-3.5-4' Total/NA Solid 3050B
720-69933-9 GP-1-7.5-8' Total/NA Solid 3050B
720-69933-12 GP-2-3.5-4' Total/NA Solid 3050B
720-69933-13 GP-2-7.5-8' Total/NA Solid 3050B
720-69933-15 GP-3-3.5-4' Total/NA Solid 3050B
720-69933-16 GP-3-7.5-8' Total/NA Solid 3050B
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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Metals (Continued)
Prep Batch: 196275 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-19 GP-4-3.5-4' Total/NA Solid 3050B
720-69933-23 GP-5-4.5-5' Total/NA Solid 3050B
720-69933-24 GP-5-7.5-8' Total/NA Solid 3050B
720-69933-27 GP-6-3.5-4' Total/NA Solid 3050B
720-69933-28 GP-6-7.5-8' Total/NA Solid 3050B
720-69933-31 GP-7-3.5-4' Total/NA Solid 3050B
720-69933-32 GP-7-7.5-8' Total/NA Solid 3050B
720-69933-35 GP-8-3.5-4' Total/NA Solid 3050B
720-69933-36 GP-8-7.5-8' Total/NA Solid 3050B
720-69933-39 GP-9-4.5-5' Total/NA Solid 3050B
720-69933-40 GP-9-7.5-8' Total/NA Solid 3050B
720-69933-43 GP-10-3.5-4' Total/NA Solid 3050B
720-69933-44 GP-10-7.5-8' Total/NA Solid 3050B
LCS 720-196275/2-A Lab Control Sample Total/NA Solid 3050B LCSD 720-196275/3-A Lab Control Sample Dup Total/NA Solid 3050B LCSSRM 720-196275/4-A Lab Control Sample Total/NA Solid 3050B MB 720-196275/1-A Method Blank Total/NA Solid 3050B
Filtration Batch: 196284
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Dissolved Water FILTRATION
720-69933-1 MS GP-1 Dissolved Water FILTRATION
720-69933-1 MSD GP-1 Dissolved Water FILTRATION
720-69933-2 GP-2 Dissolved Water FILTRATION
720-69933-3 GP-3 Dissolved Water FILTRATION
720-69933-4 GP-6 Dissolved Water FILTRATION
720-69933-5 GP-7 Dissolved Water FILTRATION
720-69933-6 GP-10 Dissolved Water FILTRATION
MB 720-196284/1-B Method Blank Dissolved Water FILTRATION MB 720-196284/1-C Method Blank Dissolved Water FILTRATION Prep Batch: 196285
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-47 GP-11-3.5-4' Total/NA Solid 3050B
720-69933-47 MS GP-11-3.5-4' Total/NA Solid 3050B
720-69933-47 MSD GP-11-3.5-4' Total/NA Solid 3050B
720-69933-48 GP-11-7.5-8' Total/NA Solid 3050B
LCS 720-196285/2-A Lab Control Sample Total/NA Solid 3050B LCSD 720-196285/3-A Lab Control Sample Dup Total/NA Solid 3050B LCSSRM 720-196285/4-A Lab Control Sample Total/NA Solid 3050B MB 720-196285/1-A Method Blank Total/NA Solid 3050B
Prep Batch: 196308
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 7471A
720-69933-9 GP-1-7.5-8' Total/NA Solid 7471A
720-69933-12 GP-2-3.5-4' Total/NA Solid 7471A
720-69933-13 GP-2-7.5-8' Total/NA Solid 7471A
720-69933-15 GP-3-3.5-4' Total/NA Solid 7471A
720-69933-16 GP-3-7.5-8' Total/NA Solid 7471A
720-69933-19 GP-4-3.5-4' Total/NA Solid 7471A
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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Metals (Continued)
Prep Batch: 196308 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-23 GP-5-4.5-5' Total/NA Solid 7471A
720-69933-24 GP-5-7.5-8' Total/NA Solid 7471A
720-69933-27 GP-6-3.5-4' Total/NA Solid 7471A
720-69933-28 GP-6-7.5-8' Total/NA Solid 7471A
720-69933-31 GP-7-3.5-4' Total/NA Solid 7471A
720-69933-32 GP-7-7.5-8' Total/NA Solid 7471A
720-69933-35 GP-8-3.5-4' Total/NA Solid 7471A
720-69933-36 GP-8-7.5-8' Total/NA Solid 7471A
720-69933-39 GP-9-4.5-5' Total/NA Solid 7471A
720-69933-40 GP-9-7.5-8' Total/NA Solid 7471A
720-69933-43 GP-10-3.5-4' Total/NA Solid 7471A
LCS 720-196308/2-A Lab Control Sample Total/NA Solid 7471A LCSD 720-196308/3-A Lab Control Sample Dup Total/NA Solid 7471A MB 720-196308/1-A Method Blank Total/NA Solid 7471A
Prep Batch: 196312
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-44 GP-10-7.5-8' Total/NA Solid 7471A
720-69933-44 MS GP-10-7.5-8' Total/NA Solid 7471A
720-69933-44 MSD GP-10-7.5-8' Total/NA Solid 7471A
720-69933-47 GP-11-3.5-4' Total/NA Solid 7471A
720-69933-48 GP-11-7.5-8' Total/NA Solid 7471A
LCS 720-196312/2-A Lab Control Sample Total/NA Solid 7471A LCSD 720-196312/3-A Lab Control Sample Dup Total/NA Solid 7471A MB 720-196312/1-A Method Blank Total/NA Solid 7471A
Prep Batch: 196361
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Dissolved Water 3005A 196284
720-69933-1 MS GP-1 Dissolved Water 3005A 196284
720-69933-1 MSD GP-1 Dissolved Water 3005A 196284
720-69933-2 GP-2 Dissolved Water 3005A 196284
720-69933-3 GP-3 Dissolved Water 3005A 196284
720-69933-4 GP-6 Dissolved Water 3005A 196284
720-69933-5 GP-7 Dissolved Water 3005A 196284
720-69933-6 GP-10 Dissolved Water 3005A 196284
LCS 720-196361/2-A Lab Control Sample Total Recoverable Water 3005A LCSD 720-196361/3-A Lab Control Sample Dup Total Recoverable Water 3005A MB 720-196284/1-B Method Blank Dissolved Water 3005A 196284 MB 720-196361/1-A Method Blank Total Recoverable Water 3005A Analysis Batch: 196381
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCS 720-196308/2-A Lab Control Sample Total/NA Solid 7471A 196308 LCSD 720-196308/3-A Lab Control Sample Dup Total/NA Solid 7471A 196308 MB 720-196308/1-A Method Blank Total/NA Solid 7471A 196308 Analysis Batch: 196393
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 7471A 196308
720-69933-9 GP-1-7.5-8' Total/NA Solid 7471A 196308
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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Metals (Continued)
Analysis Batch: 196393 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-12 GP-2-3.5-4' Total/NA Solid 7471A 196308
720-69933-13 GP-2-7.5-8' Total/NA Solid 7471A 196308
720-69933-15 GP-3-3.5-4' Total/NA Solid 7471A 196308
720-69933-16 GP-3-7.5-8' Total/NA Solid 7471A 196308
720-69933-19 GP-4-3.5-4' Total/NA Solid 7471A 196308
720-69933-23 GP-5-4.5-5' Total/NA Solid 7471A 196308
720-69933-24 GP-5-7.5-8' Total/NA Solid 7471A 196308
720-69933-27 GP-6-3.5-4' Total/NA Solid 7471A 196308
720-69933-28 GP-6-7.5-8' Total/NA Solid 7471A 196308
720-69933-31 GP-7-3.5-4' Total/NA Solid 7471A 196308
720-69933-32 GP-7-7.5-8' Total/NA Solid 7471A 196308
720-69933-35 GP-8-3.5-4' Total/NA Solid 7471A 196308
720-69933-36 GP-8-7.5-8' Total/NA Solid 7471A 196308
720-69933-39 GP-9-4.5-5' Total/NA Solid 7471A 196308
720-69933-40 GP-9-7.5-8' Total/NA Solid 7471A 196308
720-69933-43 GP-10-3.5-4' Total/NA Solid 7471A 196308
Analysis Batch: 196405
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-44 GP-10-7.5-8' Total/NA Solid 7471A 196312
720-69933-44 MS GP-10-7.5-8' Total/NA Solid 7471A 196312 720-69933-44 MSD GP-10-7.5-8' Total/NA Solid 7471A 196312 720-69933-47 GP-11-3.5-4' Total/NA Solid 7471A 196312
720-69933-48 GP-11-7.5-8' Total/NA Solid 7471A 196312
LCS 720-196312/2-A Lab Control Sample Total/NA Solid 7471A 196312 LCSD 720-196312/3-A Lab Control Sample Dup Total/NA Solid 7471A 196312 MB 720-196312/1-A Method Blank Total/NA Solid 7471A 196312 Analysis Batch: 196432
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid 6010B 196275
720-69933-8 MS GP-1-3.5-4' Total/NA Solid 6010B 196275
720-69933-8 MSD GP-1-3.5-4' Total/NA Solid 6010B 196275 720-69933-9 GP-1-7.5-8' Total/NA Solid 6010B 196275
720-69933-12 GP-2-3.5-4' Total/NA Solid 6010B 196275
720-69933-13 GP-2-7.5-8' Total/NA Solid 6010B 196275
720-69933-15 GP-3-3.5-4' Total/NA Solid 6010B 196275
720-69933-16 GP-3-7.5-8' Total/NA Solid 6010B 196275
720-69933-19 GP-4-3.5-4' Total/NA Solid 6010B 196275
720-69933-23 GP-5-4.5-5' Total/NA Solid 6010B 196275
720-69933-24 GP-5-7.5-8' Total/NA Solid 6010B 196275
720-69933-27 GP-6-3.5-4' Total/NA Solid 6010B 196275
720-69933-28 GP-6-7.5-8' Total/NA Solid 6010B 196275
720-69933-31 GP-7-3.5-4' Total/NA Solid 6010B 196275
720-69933-32 GP-7-7.5-8' Total/NA Solid 6010B 196275
720-69933-35 GP-8-3.5-4' Total/NA Solid 6010B 196275
720-69933-36 GP-8-7.5-8' Total/NA Solid 6010B 196275
720-69933-39 GP-9-4.5-5' Total/NA Solid 6010B 196275
720-69933-40 GP-9-7.5-8' Total/NA Solid 6010B 196275
720-69933-43 GP-10-3.5-4' Total/NA Solid 6010B 196275
720-69933-44 GP-10-7.5-8' Total/NA Solid 6010B 196275
TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Metals (Continued)
Analysis Batch: 196432 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCS 720-196275/2-A Lab Control Sample Total/NA Solid 6010B 196275 LCSD 720-196275/3-A Lab Control Sample Dup Total/NA Solid 6010B 196275 LCSSRM 720-196275/4-A Lab Control Sample Total/NA Solid 6010B 196275 MB 720-196275/1-A Method Blank Total/NA Solid 6010B 196275 Prep Batch: 196443
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Dissolved Water 7470A 196284
720-69933-2 GP-2 Dissolved Water 7470A 196284
720-69933-3 GP-3 Dissolved Water 7470A 196284
720-69933-4 GP-6 Dissolved Water 7470A 196284
720-69933-5 GP-7 Dissolved Water 7470A 196284
720-69933-6 GP-10 Dissolved Water 7470A 196284
LCS 720-196443/2-A Lab Control Sample Total/NA Water 7470A LCSD 720-196443/3-A Lab Control Sample Dup Total/NA Water 7470A MB 720-196284/1-C Method Blank Dissolved Water 7470A 196284 MB 720-196443/1-A Method Blank Total/NA Water 7470A
Analysis Batch: 196472
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-9 GP-1-7.5-8' Total/NA Solid 6010B 196275
720-69933-12 GP-2-3.5-4' Total/NA Solid 6010B 196275
720-69933-19 GP-4-3.5-4' Total/NA Solid 6010B 196275
720-69933-23 GP-5-4.5-5' Total/NA Solid 6010B 196275
720-69933-27 GP-6-3.5-4' Total/NA Solid 6010B 196275
720-69933-43 GP-10-3.5-4' Total/NA Solid 6010B 196275
Analysis Batch: 196474
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Dissolved Water 7470A 196443
720-69933-2 GP-2 Dissolved Water 7470A 196443
720-69933-3 GP-3 Dissolved Water 7470A 196443
720-69933-4 GP-6 Dissolved Water 7470A 196443
720-69933-5 GP-7 Dissolved Water 7470A 196443
720-69933-6 GP-10 Dissolved Water 7470A 196443
LCS 720-196443/2-A Lab Control Sample Total/NA Water 7470A 196443 LCSD 720-196443/3-A Lab Control Sample Dup Total/NA Water 7470A 196443 MB 720-196284/1-C Method Blank Dissolved Water 7470A 196443 MB 720-196443/1-A Method Blank Total/NA Water 7470A 196443 Analysis Batch: 196481
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-1 GP-1 Dissolved Water 6010B 196361
720-69933-1 MS GP-1 Dissolved Water 6010B 196361
720-69933-1 MSD GP-1 Dissolved Water 6010B 196361
720-69933-2 GP-2 Dissolved Water 6010B 196361
720-69933-3 GP-3 Dissolved Water 6010B 196361
720-69933-4 GP-6 Dissolved Water 6010B 196361
720-69933-5 GP-7 Dissolved Water 6010B 196361
720-69933-6 GP-10 Dissolved Water 6010B 196361
LCS 720-196361/2-A Lab Control Sample Total Recoverable Water 6010B 196361 TestAmerica Pleasanton

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QC Association Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Metals (Continued)
Analysis Batch: 196481 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCSD 720-196361/3-A Lab Control Sample Dup Total Recoverable Water 6010B 196361 MB 720-196284/1-B Method Blank Dissolved Water 6010B 196361 MB 720-196361/1-A Method Blank Total Recoverable Water 6010B 196361 Analysis Batch: 196482
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-47 GP-11-3.5-4' Total/NA Solid 6010B 196285
720-69933-47 MS GP-11-3.5-4' Total/NA Solid 6010B 196285 720-69933-47 MSD GP-11-3.5-4' Total/NA Solid 6010B 196285 720-69933-48 GP-11-7.5-8' Total/NA Solid 6010B 196285
LCS 720-196285/2-A Lab Control Sample Total/NA Solid 6010B 196285 LCSD 720-196285/3-A Lab Control Sample Dup Total/NA Solid 6010B 196285 LCSSRM 720-196285/4-A Lab Control Sample Total/NA Solid 6010B 196285 MB 720-196285/1-A Method Blank Total/NA Solid 6010B 196285 General Chemistry
Analysis Batch: 196337
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-8 GP-1-3.5-4' Total/NA Solid Moisture
720-69933-9 GP-1-7.5-8' Total/NA Solid Moisture
720-69933-9 DU GP-1-7.5-8' Total/NA Solid Moisture
720-69933-12 GP-2-3.5-4' Total/NA Solid Moisture
720-69933-13 GP-2-7.5-8' Total/NA Solid Moisture
720-69933-15 GP-3-3.5-4' Total/NA Solid Moisture
720-69933-16 GP-3-7.5-8' Total/NA Solid Moisture
720-69933-19 GP-4-3.5-4' Total/NA Solid Moisture
720-69933-23 GP-5-4.5-5' Total/NA Solid Moisture
720-69933-24 GP-5-7.5-8' Total/NA Solid Moisture
720-69933-27 GP-6-3.5-4' Total/NA Solid Moisture
720-69933-28 GP-6-7.5-8' Total/NA Solid Moisture
720-69933-31 GP-7-3.5-4' Total/NA Solid Moisture
720-69933-32 GP-7-7.5-8' Total/NA Solid Moisture
720-69933-35 GP-8-3.5-4' Total/NA Solid Moisture
720-69933-36 GP-8-7.5-8' Total/NA Solid Moisture
720-69933-39 GP-9-4.5-5' Total/NA Solid Moisture
720-69933-40 GP-9-7.5-8' Total/NA Solid Moisture
720-69933-43 GP-10-3.5-4' Total/NA Solid Moisture
720-69933-44 GP-10-7.5-8' Total/NA Solid Moisture
720-69933-47 GP-11-3.5-4' Total/NA Solid Moisture
Analysis Batch: 196350
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 720-69933-48 GP-11-7.5-8' Total/NA Solid Moisture
720-69933-48 DU GP-11-7.5-8' Total/NA Solid Moisture
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-1 Lab Sample ID: 720-69933-1
Date Collected: 01/21/16 15:00 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B/CA_LUFTMS 1 196234 01/26/16 15:19 LPL TAL PLS Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3510C SGC 196382 01/27/16 16:40 BSY TAL PLS Silica Gel Cleanup Analysis 8015B 1 196414 01/28/16 14:53 JXL TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 3005A 196361 01/27/16 14:17 ASB TAL PLS
Dissolved Analysis 6010B 1 196481 01/28/16 17:44 CAM TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 7470A 196443 01/28/16 12:32 ASB TAL PLS
Dissolved Analysis 7470A 1 196474 01/28/16 17:36 SLK TAL PLS Client Sample ID: GP-2 Lab Sample ID: 720-69933-2
Date Collected: 01/21/16 12:00 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B/CA_LUFTMS 1 196234 01/26/16 15:47 LPL TAL PLS Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3510C SGC 196382 01/27/16 16:40 BSY TAL PLS Silica Gel Cleanup Analysis 8015B 5 196414 01/28/16 16:55 JXL TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 3005A 196361 01/27/16 14:17 ASB TAL PLS
Dissolved Analysis 6010B 1 196481 01/28/16 17:49 CAM TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 7470A 196443 01/28/16 12:32 ASB TAL PLS
Dissolved Analysis 7470A 1 196474 01/28/16 17:43 SLK TAL PLS Client Sample ID: GP-3 Lab Sample ID: 720-69933-3
Date Collected: 01/21/16 14:10 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B/CA_LUFTMS 1 196234 01/26/16 16:14 LPL TAL PLS Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3510C SGC 196382 01/27/16 16:40 BSY TAL PLS Silica Gel Cleanup Analysis 8015B 1 196414 01/28/16 15:42 JXL TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 3005A 196361 01/27/16 14:17 ASB TAL PLS
Dissolved Analysis 6010B 1 196481 01/28/16 17:54 CAM TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 7470A 196443 01/28/16 12:32 ASB TAL PLS
Dissolved Analysis 7470A 1 196474 01/28/16 17:45 SLK TAL PLS TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-6 Lab Sample ID: 720-69933-4
Date Collected: 01/21/16 16:55 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B/CA_LUFTMS 1 196234 01/26/16 16:42 LPL TAL PLS Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3510C SGC 196382 01/27/16 16:40 BSY TAL PLS Silica Gel Cleanup Analysis 8015B 1 196414 01/28/16 16:06 JXL TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 3005A 196361 01/27/16 14:17 ASB TAL PLS
Dissolved Analysis 6010B 1 196481 01/28/16 18:10 CAM TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 7470A 196443 01/28/16 12:32 ASB TAL PLS
Dissolved Analysis 7470A 1 196474 01/28/16 17:48 SLK TAL PLS Client Sample ID: GP-7 Lab Sample ID: 720-69933-5
Date Collected: 01/22/16 09:10 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B/CA_LUFTMS 1 196293 01/27/16 04:14 JRM TAL PLS Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3510C SGC 196382 01/27/16 16:40 BSY TAL PLS Silica Gel Cleanup Analysis 8015B 1 196414 01/28/16 16:30 JXL TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 3005A 196361 01/27/16 14:17 ASB TAL PLS
Dissolved Analysis 6010B 1 196481 01/28/16 18:15 CAM TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 7470A 196443 01/28/16 12:32 ASB TAL PLS
Dissolved Analysis 7470A 1 196474 01/28/16 17:50 SLK TAL PLS Client Sample ID: GP-10 Lab Sample ID: 720-69933-6
Date Collected: 01/22/16 11:50 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B/CA_LUFTMS 1 196293 01/27/16 04:42 JRM TAL PLS Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3510C SGC 196382 01/27/16 16:40 BSY TAL PLS Silica Gel Cleanup Analysis 8015B 1 196414 01/28/16 15:18 JXL TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 3005A 196361 01/27/16 14:17 ASB TAL PLS
Dissolved Analysis 6010B 1 196481 01/28/16 18:20 CAM TAL PLS Dissolved Filtration FILTRATION 196284 01/26/16 09:40 ASB TAL PLS Dissolved Prep 7470A 196443 01/28/16 12:32 ASB TAL PLS
Dissolved Analysis 7470A 1 196474 01/28/16 17:52 SLK TAL PLS TestAmerica Pleasanton

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Lab Chronicle
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: TRIP BLANK Lab Sample ID: 720-69933-7 Date Collected: 01/22/16 12:30 Matrix: Water
Date Received: 01/22/16 17:10
Analysis 8260B 1 196192 01/26/16 01:36 YB1 TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-1-3.5-4' Lab Sample ID: 720-69933-8 Date Collected: 01/21/16 10:25 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-1-3.5-4' Lab Sample ID: 720-69933-8 Date Collected: 01/21/16 10:25 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.9
Prep 5030B 196295 01/27/16 18:59 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196408 01/28/16 14:59 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196412 01/29/16 02:34 JXL TAL PLS Total/NA Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Total/NA Analysis 8081A 1 196422 01/28/16 16:29 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 17:15 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 21:42 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:00 SLK TAL PLS Client Sample ID: GP-1-7.5-8' Lab Sample ID: 720-69933-9 Date Collected: 01/21/16 10:26 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-1-7.5-8' Lab Sample ID: 720-69933-9 Date Collected: 01/21/16 10:26 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.3
Prep 5030B 196202 01/25/16 19:58 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196288 01/27/16 04:39 PRD TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 10 196415 01/28/16 22:58 JXL TAL PLS TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8081A 2 196422 01/28/16 18:44 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 16:58 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 21:47 SLK TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 1 196472 01/28/16 16:02 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:02 SLK TAL PLS Client Sample ID: GP-2-3.5-4' Lab Sample ID: 720-69933-12 Date Collected: 01/21/16 11:40 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-3.5-4' Lab Sample ID: 720-69933-12 Date Collected: 01/21/16 11:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.7
Prep 5030B 196202 01/25/16 19:58 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196326 01/27/16 12:37 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196414 01/29/16 02:10 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 21:52 SLK TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 1 196472 01/28/16 16:07 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:04 SLK TAL PLS Client Sample ID: GP-2-7.5-8' Lab Sample ID: 720-69933-13 Date Collected: 01/21/16 11:42 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-2-7.5-8' Lab Sample ID: 720-69933-13 Date Collected: 01/21/16 11:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 76.9
Prep 5030B 196295 01/27/16 18:59 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-2-7.5-8' Lab Sample ID: 720-69933-13 Date Collected: 01/21/16 11:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 76.9
Analysis 8260B 1 196408 01/28/16 15:28 YB1 TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 20 196414 01/28/16 23:22 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:07 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:07 SLK TAL PLS Client Sample ID: GP-3-3.5-4' Lab Sample ID: 720-69933-15 Date Collected: 01/21/16 13:45 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-3-3.5-4' Lab Sample ID: 720-69933-15 Date Collected: 01/21/16 13:45 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 89.7
Prep 5030B 196295 01/27/16 18:59 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196408 01/28/16 15:57 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 10 196414 01/28/16 23:46 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:12 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:09 SLK TAL PLS Client Sample ID: GP-3-7.5-8' Lab Sample ID: 720-69933-16 Date Collected: 01/21/16 13:46 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-3-7.5-8' Lab Sample ID: 720-69933-16 Date Collected: 01/21/16 13:46 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 83.0
Prep 5030B 196202 01/25/16 19:58 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196288 01/27/16 06:11 PRD TAL PLS TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Prep 3546 196404 01/27/16 21:05 AFM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Silica Gel Cleanup
Silica Gel Cleanup Analysis 8015B 1 196415 01/29/16 02:10 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:17 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:11 SLK TAL PLS Client Sample ID: GP-4-3.5-4' Lab Sample ID: 720-69933-19 Date Collected: 01/21/16 15:35 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-4-3.5-4' Lab Sample ID: 720-69933-19 Date Collected: 01/21/16 15:35 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 69.1
Prep 5030B 196202 01/25/16 19:58 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196326 01/27/16 13:07 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 00:37 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:22 SLK TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 1 196472 01/28/16 16:12 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:14 SLK TAL PLS Client Sample ID: GP-5-4.5-5' Lab Sample ID: 720-69933-23 Date Collected: 01/21/16 16:06 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-5-4.5-5' Lab Sample ID: 720-69933-23 Date Collected: 01/21/16 16:06 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.9
Prep 5030B 196202 01/25/16 19:58 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196326 01/27/16 13:38 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 03:32 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-5-4.5-5' Lab Sample ID: 720-69933-23 Date Collected: 01/21/16 16:06 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.9
Analysis 6010B 4 196432 01/27/16 22:27 SLK TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196472 01/28/16 16:17 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:16 SLK TAL PLS Client Sample ID: GP-5-7.5-8' Lab Sample ID: 720-69933-24 Date Collected: 01/21/16 16:05 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-5-7.5-8' Lab Sample ID: 720-69933-24 Date Collected: 01/21/16 16:05 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.0
Prep 5030B 196295 01/28/16 18:30 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196468 01/29/16 00:36 LPL TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 04:02 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:31 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:19 SLK TAL PLS Client Sample ID: GP-6-3.5-4' Lab Sample ID: 720-69933-27 Date Collected: 01/21/16 16:30 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-6-3.5-4' Lab Sample ID: 720-69933-27 Date Collected: 01/21/16 16:30 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 86.8
Prep 5030B 196295 01/28/16 18:30 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196468 01/29/16 01:07 LPL TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 02:34 JXL TAL PLS TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8081A 1 196422 01/28/16 16:12 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 17:32 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:36 SLK TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 1 196472 01/28/16 16:22 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:21 SLK TAL PLS Client Sample ID: GP-6-7.5-8' Lab Sample ID: 720-69933-28 Date Collected: 01/21/16 16:32 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-6-7.5-8' Lab Sample ID: 720-69933-28 Date Collected: 01/21/16 16:32 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.4
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/29/16 21:35 JRM TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/28/16 23:39 JXL TAL PLS Total/NA Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Total/NA Analysis 8081A 1 196422 01/28/16 16:46 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 20:51 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:41 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:28 SLK TAL PLS Client Sample ID: GP-7-3.5-4' Lab Sample ID: 720-69933-31 Date Collected: 01/22/16 08:40 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-7-3.5-4' Lab Sample ID: 720-69933-31 Date Collected: 01/22/16 08:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 82.1
Prep 5030B 196295 01/27/16 19:40 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196408 01/28/16 16:56 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 01:36 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:46 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:31 SLK TAL PLS Client Sample ID: GP-7-7.5-8' Lab Sample ID: 720-69933-32 Date Collected: 01/22/16 08:45 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-7-7.5-8' Lab Sample ID: 720-69933-32 Date Collected: 01/22/16 08:45 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.2
Prep 5030B 196202 01/27/16 09:20 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196326 01/27/16 15:09 YB1 TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/28/16 22:40 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 22:51 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:33 SLK TAL PLS Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Date Collected: 01/22/16 09:40 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Date Collected: 01/22/16 09:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.0
Prep 5030B 196295 01/27/16 19:40 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-8-3.5-4' Lab Sample ID: 720-69933-35 Date Collected: 01/22/16 09:40 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.0
Analysis 8260B 1 196408 01/28/16 14:29 YB1 TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 02:05 JXL TAL PLS Total/NA Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Total/NA Analysis 8081A 1 196422 01/28/16 17:03 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 18:05 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 23:06 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 10 196393 01/27/16 17:59 SLK TAL PLS Client Sample ID: GP-8-7.5-8' Lab Sample ID: 720-69933-36 Date Collected: 01/22/16 09:42 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-8-7.5-8' Lab Sample ID: 720-69933-36 Date Collected: 01/22/16 09:42 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 81.3
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/29/16 23:07 JRM TAL PLS Silica Gel Cleanup Prep 3546 196403 01/27/16 20:37 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/28/16 22:11 JXL TAL PLS Total/NA Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Total/NA Analysis 8081A 1 196422 01/28/16 17:19 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 18:22 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 23:11 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:38 SLK TAL PLS Client Sample ID: GP-9-4.5-5' Lab Sample ID: 720-69933-39 Date Collected: 01/22/16 10:22 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-9-4.5-5' Lab Sample ID: 720-69933-39 Date Collected: 01/22/16 10:22 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 78.2
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/29/16 23:37 JRM TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 01:06 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 23:16 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 10 196393 01/27/16 18:01 SLK TAL PLS Client Sample ID: GP-9-7.5-8' Lab Sample ID: 720-69933-40 Date Collected: 01/22/16 10:24 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-9-7.5-8' Lab Sample ID: 720-69933-40 Date Collected: 01/22/16 10:24 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 77.4
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/30/16 00:08 JRM TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 03:03 JXL TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 23:21 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:42 SLK TAL PLS Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Date Collected: 01/22/16 11:10 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Date Collected: 01/22/16 11:10 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 87.1
Prep 5030B 196295 01/27/16 19:40 JRM TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-10-3.5-4' Lab Sample ID: 720-69933-43 Date Collected: 01/22/16 11:10 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 87.1
Analysis 8260B 1 196468 01/29/16 03:40 LPL TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 20 196414 01/29/16 02:35 JXL TAL PLS Total/NA Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Total/NA Analysis 8081A 2 196422 01/28/16 19:00 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 18:38 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 23:26 SLK TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 1 196472 01/28/16 16:27 SLK TAL PLS Total/NA Prep 7471A 196308 01/26/16 17:30 ASB TAL PLS
Total/NA Analysis 7471A 1 196393 01/27/16 17:45 SLK TAL PLS Client Sample ID: GP-10-7.5-8' Lab Sample ID: 720-69933-44 Date Collected: 01/22/16 11:12 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-10-7.5-8' Lab Sample ID: 720-69933-44 Date Collected: 01/22/16 11:12 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 73.6
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/30/16 00:38 JRM TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/28/16 23:10 JXL TAL PLS Total/NA Prep 3546 196366 01/27/16 15:48 KMK TAL PLS
Total/NA Analysis 8081A 1 196422 01/28/16 17:36 JZT TAL PLS Total/NA Prep 3546 196367 01/27/16 15:59 KMK TAL PLS
Total/NA Analysis 8082 1 196419 01/28/16 18:55 DCH TAL PLS Total/NA Prep 3050B 196275 01/26/16 14:13 MJD TAL PLS
Total/NA Analysis 6010B 4 196432 01/27/16 23:31 SLK TAL PLS Total/NA Prep 7471A 196312 01/26/16 18:10 ASB TAL PLS
Total/NA Analysis 7471A 1 196405 01/27/16 19:55 SLK TAL PLS TestAmerica Pleasanton

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Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Client Sample ID: GP-11-3.5-4' Lab Sample ID: 720-69933-47 Date Collected: 01/22/16 12:00 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196337 01/27/16 09:39 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-11-3.5-4' Lab Sample ID: 720-69933-47 Date Collected: 01/22/16 12:00 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 79.5
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/30/16 01:08 JRM TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 3 196415 01/29/16 02:35 JXL TAL PLS Total/NA Prep 3050B 196285 01/26/16 14:58 MJD TAL PLS
Total/NA Analysis 6010B 4 196482 01/28/16 18:42 SLK TAL PLS Total/NA Prep 7471A 196312 01/26/16 18:10 ASB TAL PLS
Total/NA Analysis 7471A 1 196405 01/27/16 19:57 SLK TAL PLS Client Sample ID: GP-11-7.5-8' Lab Sample ID: 720-69933-48 Date Collected: 01/22/16 12:02 Matrix: Solid
Date Received: 01/22/16 17:10
Analysis Moisture 1 196350 01/27/16 12:04 NVP TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: GP-11-7.5-8' Lab Sample ID: 720-69933-48 Date Collected: 01/22/16 12:02 Matrix: Solid
Date Received: 01/22/16 17:10 Percent Solids: 79.5
Prep 5030B 196561 01/29/16 19:09 CTD TAL PLS
Type
Batch Batch
Prep Type Method Run Analyst Lab
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Total/NA Analysis 8260B 1 196552 01/30/16 01:39 JRM TAL PLS Silica Gel Cleanup Prep 3546 196404 01/27/16 21:05 AFM TAL PLS Silica Gel Cleanup Analysis 8015B 1 196413 01/29/16 00:08 JXL TAL PLS Total/NA Prep 3050B 196285 01/26/16 14:58 MJD TAL PLS
Total/NA Analysis 6010B 4 196482 01/28/16 18:46 SLK TAL PLS Total/NA Prep 7471A 196312 01/26/16 18:10 ASB TAL PLS
Total/NA Analysis 7471A 1 196405 01/27/16 20:00 SLK TAL PLS Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 TestAmerica Pleasanton

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Certification Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Laboratory: TestAmerica Pleasanton
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.

Authority Program EPA Region Certification ID Expiration Date California State Program 9 2496 01-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:

Moisture Solid Percent Moisture
TestAmerica Pleasanton

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Method Summary
Client: Geologica Inc TestAmerica Job ID: 720-69933-1
Project/Site: Pin High
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL PLS
8260B/CA_LUFTM SW846
S
8260B / CA LUFT MS TAL PLS
8015B Diesel Range Organics (DRO) (GC) SW846 TAL PLS
8081A Organochlorine Pesticides (GC) SW846 TAL PLS
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL PLS 6010B Metals (ICP) SW846 TAL PLS
7470A Mercury (CVAA) SW846 TAL PLS
7471A Mercury (CVAA) SW846 TAL PLS
Moisture Percent Moisture EPA TAL PLS
Protocol References:

EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 TestAmerica Pleasanton

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San Jose City CouncilAugust 9, 2022

San Jose City Council
August 9, 2022